CN103355651A - Preparation method of bamboo fungus and sparassis crispa freeze-drying ultrafine powder capsules - Google Patents
Preparation method of bamboo fungus and sparassis crispa freeze-drying ultrafine powder capsules Download PDFInfo
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Abstract
The invention provides a preparation method of bamboo fungus and sparassis crispa freeze-drying ultrafine powder capsules. The preparation method of bamboo fungus and sparassis crispa freeze-drying ultrafine powder capsules comprises the following steps of: taking sorted and pedicle-removed sparassis crispa and bamboo fungus according to the weight ratio of 5:1, cleaning, and crushing; inputting into a pulping machine and pulping; milling mixed pulp obtained through pulping by a colloid mill; placing the mixed pulp after milling pulp into a vacuum freezing and drying machine, freezing, and vacuumizing; then drying so as to enable water in the mixed pulp to be sublimated into steam, and capturing the steam by a cold trap of the vacuum freezing and drying machine, and freezing and drying the mixed pulp; crushing the frozen and dried mixed pulp by an ultrafine crusher, and sieving by a 200-mesh mesh screen so as to obtain frozen and dried powder; packaging the frozen and dried powder into capsule shells, and packaging under an aseptic condition, thereby obtaining bamboo fungus and sparassis crispa freeze-drying ultrafine powder capsule finished products. Through the preparation method provided by the invention, not only can the effective ingredients, active substances and nutritional substances of bamboo fungus and sparassis crispa be stored maximally, but also because of the adding of bamboo fungus, natural preservatives are also provided, the nutritional ingredients of capsules are enriched, so that the capsules are difficult to deteriorate.
Description
[technical field]
The present invention relates to a kind of preparation method of health food, relate in particular to a kind of dictyophora phalloidea Sparassis crispa freeze dried superfines capsule preparation method thereof.
[background technology]
Sparassis crispa is non-pleat pore fungi order, silk ball Cordycepps, a kind of very rare immunological regulation edible and medical fungi of silk ball Pseudomonas, and its protein content is about 12.9%, far above general vegetables, fruit; Sparassis crispa contains 7 kinds of amino acid/11s, is about 9.3%, A wide selection of colours and designs, and wherein 8 seed amino acids of needed by human account for 33.9% of total amount; Contain a large amount of beta glucans, silk ball mykol (Sparasso1) and close glycoprotein (claiming again immune modulator), and except being rich in a large amount of beta glucans, Sparassis crispa also contains a large amount of vitamin, mineral matter and polyphenoils.According to surveying and determination, the content of hepatocuprein (SOD) occupies first of the various edible mushrooms in the Sparassis crispa; Modern study confirm Sparassis crispa have antitumor action, immunoloregulation function, promotion wound healing effect, promote hematopoiesis function, hypoglycemic, regulate blood pressure, blood fat, reduce that cholesterol, antiallergy, promotion collagen produce, the effect such as anti-oxidant.Although the protein of Sparassis crispa, amino acid, vitamin, micro elements needed by human content are all higher, its main functional components is the fungi activity polysaccharide.
Dictyophora phalloidea is a kind of famous edible mushroom during Phallales Phallaceae dictyophora phalloidea belongs to, and classifies in history " imperial palace tribute " as, and also be dietotherapy good merchantable brand simultaneously as the state banquet famous dish modern age; It is nutritious, contains according to surveying and determination protein 19.4%, fat 2.6% in the dried dictyophora phalloidea, carbohydrate total amount 60.4%, wherein bacterium sugar 4.2%, crude fibre 8.4%, ash content 9.3%.The contained polysaccharide of dictyophora phalloidea also contains multiple composition to the human body beneficial such as carrotene, thiamine, ascorbic acid, niacin etc. simultaneously take different polysaccharide such as glucose, mannose, wood sugar and galactolipins as main.The traditional Chinese medical science thinks, dictyophora phalloidea has very large benifit for strengthening digestive function of spleen and stomach, also has the greasy digestant effect of separating, and often ediblely can eliminate the unnecessary fat of stomach wall, has obvious fat-reducing effect.Medical research shows, dictyophora phalloidea belongs to physiological alkalinity food, and long-term taking can be regulated aliphatic acid and the hematic acid content in person in middle and old age's human body, and the effect that reduces hypertension and body inner cholesterol is arranged.Polysaccharide in the dictyophora phalloidea all has certain curative effect at antitumor, anti-inflammatory, anticoagulation, immune stimulatory, reduction blood sugar and enhancing immunology, and AIDS is also had inhibitory action.In addition, dictyophora phalloidea can be brought into play bacteriostasis in neutrality to alkali condition, and antibacterial substance is stable to high temperature, condition of high voltage, can be used as a kind of natural food preservative.
Vacuum Freezing ﹠ Drying Technology is to be frozen into wet stock or solution solid-state under lower temperature (one 10 ℃ 30 ℃ one by one), then (make moisture wherein be directly sublimed into gaseous state without liquid state under (1.3-13 handkerchief), finally make the dry technology of material dewatering in vacuum.China is production of raw medicine big country, so the application prospect of Vacuum Freezing ﹠ Drying Technology is very wide.Vacuum Freezing ﹠ Drying Technology is promoted very fastly in China in recent years, but uses Lyophilisation technique for making fewer at plant, mushroom, the especially application on Sparassis crispa.Because bright Sparassis crispa water content greater than 90%, is not easy to deep processing and storage, necessary stored dry; General drying means all is high temperature drying or microwave drying, but the active ingredient in the bright Sparassis crispa will be destroyed when temperature surpasses 45 ℃, and polyoses content can drop to below 10% in the Sparassis crispa, and health-care effect is reduced greatly.
Therefore, can work out and a kind ofly can guarantee Sparassis crispa and dictyophora phalloidea active constituent content, at utmost reduce polysaccharide loss, the health products preparation method that can extend the shelf life again simultaneously is practitioner's letter major issue to be solved.
[summary of the invention]
Technical problem to be solved by this invention is to provide a kind of dictyophora phalloidea Sparassis crispa freeze dried superfines capsule preparation method thereof.
The present invention solves the problems of the technologies described above by the following technical programs: a kind of dictyophora phalloidea Sparassis crispa freeze dried superfines capsule preparation method thereof specifically comprises following operation:
(1) plucks respectively Sparassis crispa, dictyophora phalloidea and sorting and remove the base of a fruit, get Sparassis crispa and dictyophora phalloidea after the base of a fruit is removed in sorting by the weight ratio of 5:1 afterwards, and clean and broken; Then the Sparassis crispa after the fragmentation and dictyophora phalloidea are dropped in the beater, and the pure water of the weight such as adding and dictyophora phalloidea is pulled an oar; Then the mixing slurry colloid mill defibrination of the Sparassis crispa dictyophora phalloidea that will obtain after will pulling an oar;
(2) slurry of the mixing behind the defibrination is placed in the vacuum freeze drier, by 8～12kg/m
2Stone, and in 2 hours～4 hours, will mix the temperature of starching and be down to-15 ℃～-27 ℃, make to mix to starch and freeze; Then in 30 minutes～1 hour, the condenser temperature of vacuum freeze drier is down to-30 ℃～-35 ℃; Again vacuum freeze drier is evacuated to 0.6mmhg～1.0mmhg; Dry afterwards and make the water sublimate that mixes in the slurry become steam and by the cold trap trapping of vacuum freeze drier, make and mix the slurry freeze-drying;
Wherein, the temperature and time of oven dry is specially: the oven dry initial temperature is 120 ℃, keeps temperature 3 hours; In 1 hour, be down to 100 ℃ from 120 ℃, and located to keep temperature 1 hour at 100 ℃; In 1 hour, drop to 80 ℃ from 100 ℃; In 0.5 hour, drop to 60 ℃ from 80 ℃, and located to keep temperature 5.5 hours at 60 ℃;
(3) mixing after freeze-drying slurry is adopted the ultramicro grinding crusher machine, crosses 200 order mesh screens to obtain freeze-dried powder, afterwards freeze-dried powder is incapsulated and under aseptic condition packing namely get described dictyophora phalloidea Sparassis crispa freeze dried superfines capsule finished product.
Further, this preparation method also comprises following operation: the dictyophora phalloidea Sparassis crispa freeze dried superfines capsule finished product of gained adopts co-60 radiation after will packing.
Further, described capsule shells is No. 1 capsule shells, and the described freeze-dried powder of 290mg of packing in every seed lac softgel shell.
The beneficial effect of a kind of dictyophora phalloidea Sparassis crispa of the present invention freeze dried superfines capsule preparation method thereof is: the health products that obtain by this preparation method are that dictyophora phalloidea Sparassis crispa freeze dried superfines capsule not only can larger limit have been preserved active ingredient, active material and the nutriment of dictyophora phalloidea and Sparassis crispa, and kept the contained polysaccharide of Sparassis crispa largely, also because of the adding of dictyophora phalloidea, natural antiseptic agent also is provided when having enriched nutritional labeling, make capsule not perishable, can carry, edible at any time, convenient feasible.
[specific embodiment]
A kind of dictyophora phalloidea Sparassis crispa of the present invention freeze dried superfines capsule preparation method thereof, specifically comprise following operation: (1) is plucked respectively Sparassis crispa, dictyophora phalloidea and sorting and is removed the base of a fruit, gets Sparassis crispa and dictyophora phalloidea after the base of a fruit is removed in sorting by the weight ratio of 5:1 afterwards, and cleans and broken; Then the Sparassis crispa after the fragmentation and dictyophora phalloidea are dropped in the beater, and the pure water of the weight such as adding and dictyophora phalloidea is pulled an oar; Then the mixing slurry colloid mill defibrination of the Sparassis crispa dictyophora phalloidea that will obtain after will pulling an oar; (2) slurry of the mixing behind the defibrination is placed in the vacuum freeze drier, by 8～12kg/m
2Stone, and in 2 hours～4 hours, will mix the temperature of starching and be down to-15 ℃～-27 ℃, make to mix to starch and freeze; Then in 30 minutes～1 hour, the condenser temperature of vacuum freeze drier is down to-30 ℃～-35 ℃; Again vacuum freeze drier is evacuated to 0.6mmhg～1.0mmhg; Dry afterwards and make the water sublimate that mixes in the slurry become steam and by the cold trap trapping of vacuum freeze drier, make and mix the slurry freeze-drying; Wherein, the temperature and time of oven dry is specially: the oven dry initial temperature is 120 ℃, keeps temperature 3 hours; In 1 hour, be down to 100 ℃ from 120 ℃, and located to keep temperature 1 hour at 100 ℃; In 1 hour, drop to 80 ℃ from 100 ℃; In 0.5 hour, drop to 60 ℃ from 80 ℃, and located to keep temperature 5.5 hours at 60 ℃; (3) mixing after freeze-drying slurry is adopted the ultramicro grinding crusher machine, crosses 200 order mesh screens to obtain freeze-dried powder, afterwards freeze-dried powder is incapsulated shell and under aseptic condition packing namely get described dictyophora phalloidea Sparassis crispa freeze dried superfines capsule finished product.
In addition, in order to prolong the shelf-life of the capsule finished product that the present invention prepares, can packing after the dictyophora phalloidea Sparassis crispa freeze dried superfines capsule finished product of gained adopt co-60 radiation; Described capsule shells is No. 1 capsule shells, and the described freeze-dried powder of 290mg of packing in every seed lac softgel shell.
In order better method of the present invention to be set forth explanation, the present invention has exemplified following embodiment.
Embodiment 1
Pluck fresh bamboo fungi and Sparassis crispa, and sorting goes the base of a fruit to remove root, for subsequent use; To remove root 20 kilograms of fresh bamboo fungis, and 100 kilograms of Sparassis crispas clean up with running water and broken; Then the Sparassis crispa after the fragmentation and dictyophora phalloidea are put in the beater, added 20 kilograms of pure water making beating; Mixing slurry colloid mill defibrination with 140 kilograms of dictyophora phalloidea Sparassis crispas after the making beating; Mixing behind defibrination slurry is placed in the vacuum freeze drier (Lima, Xiamen freezing equipment Co., Ltd, UFD-180 model), press 12kg/m
2Pave; To mix the temperature of slurry with 4 hours and be down to one 15 ℃, and make to mix and starch freezing freezing; Then in 30 minutes just the condenser temperature of vacuum freeze drier be down to one 30 ℃, open vacuum equipment, vacuum freeze drier vacuumized reach 0.8mmhg; Dry afterwards and make the water sublimate that mixes in the slurry become steam and by the cold trap trapping of vacuum freeze drier, make and mix the slurry freeze-drying; Mixing after freeze-drying slurry is adopted the ultramicro grinding crusher machine, crosses 200 order mesh screens to obtain freeze-dried powder, afterwards freeze-dried powder is incapsulated shell and under aseptic condition packing namely get described dictyophora phalloidea Sparassis crispa freeze dried superfines capsule finished product.
Embodiment 2
Pluck fresh bamboo fungi and Sparassis crispa, and sorting goes the base of a fruit to remove root, for subsequent use; To remove root 20 kilograms of fresh bamboo fungis, and 100 kilograms of Sparassis crispas clean up with running water and broken; Then the Sparassis crispa after the fragmentation and dictyophora phalloidea are put in the beater, added 20 kilograms of pure water making beating; Mixing slurry colloid mill defibrination with 140 kilograms of dictyophora phalloidea Sparassis crispas after the making beating; Mixing behind defibrination slurry is placed in the vacuum freeze drier (Lima, Xiamen freezing equipment Co., Ltd, UFD-180 model), press 10kg/m
2Pave; To mix the temperature of slurry with 3 hours and be down to one 27 ℃, and make to mix and starch freezing freezing; Then in 45 minutes just the condenser temperature of vacuum freeze drier be down to one 33 ℃, open vacuum equipment, vacuum freeze drier vacuumized reach 0.6mmhg; Dry afterwards and make the water sublimate that mixes in the slurry become steam and by the cold trap trapping of vacuum freeze drier, make and mix the slurry freeze-drying; Mixing after freeze-drying slurry is adopted the ultramicro grinding crusher machine, crosses 200 order mesh screens to obtain freeze-dried powder, afterwards freeze-dried powder is incapsulated shell and under aseptic condition packing namely get described dictyophora phalloidea Sparassis crispa freeze dried superfines capsule finished product.
Embodiment 3
Pluck fresh bamboo fungi and Sparassis crispa, and sorting goes the base of a fruit to remove root, for subsequent use; To remove root 7 kilograms of fresh bamboo fungis, and 35 kilograms of Sparassis crispas clean up with running water and broken; Then the Sparassis crispa after the fragmentation and dictyophora phalloidea are put in the beater, added 7 kilograms of pure water making beating; Mixing slurry colloid mill defibrination with 49 kilograms of dictyophora phalloidea Sparassis crispas after the making beating; Mixing behind defibrination slurry is placed in the vacuum freeze drier (Lima, Xiamen freezing equipment Co., Ltd, UFD-180 model), press 8kg/m
2Pave; To mix the temperature of slurry with 2 hours and be down to one 20 ℃, and make to mix and starch freezing freezing; Then in 1 hour just the condenser temperature of vacuum freeze drier be down to one 35 ℃, open vacuum equipment, vacuum freeze drier vacuumized reach 1.0mmhg; Dry afterwards and make the water sublimate that mixes in the slurry become steam and by the cold trap trapping of vacuum freeze drier, make and mix the slurry freeze-drying; Mixing after freeze-drying slurry is adopted the ultramicro grinding crusher machine, crosses 200 order mesh screens to obtain freeze-dried powder, afterwards freeze-dried powder is incapsulated shell and under aseptic condition packing namely get described dictyophora phalloidea Sparassis crispa freeze dried superfines capsule finished product.
Need to prove, actual temp and the time of drying in the various embodiments described above are: the oven dry initial temperature is 120 ℃, keeps temperature 3 hours; In 1 hour, be down to 100 ℃ from 120 ℃, and located to keep temperature 1 hour at 100 ℃; In 1 hour, drop to 80 ℃ from 100 ℃; In 0.5 hour, drop to 60 ℃ from 80 ℃, and located to keep temperature 5.5 hours at 60 ℃.
To sum up, the health products that obtain by preparation method of the present invention are that dictyophora phalloidea Sparassis crispa freeze dried superfines capsule not only can larger limit have been preserved active ingredient, active material and the nutriment of dictyophora phalloidea and Sparassis crispa, and kept the contained polysaccharide of Sparassis crispa largely, also because of the adding of dictyophora phalloidea, natural antiseptic agent also is provided when having enriched nutritional labeling, has made capsule not perishable, can carry, edible at any time, convenient feasible.
Claims (3)
1. dictyophora phalloidea Sparassis crispa freeze dried superfines capsule preparation method thereof is characterized in that: specifically comprise following operation:
(1) plucks respectively Sparassis crispa, dictyophora phalloidea and sorting and remove the base of a fruit, get Sparassis crispa and dictyophora phalloidea after the base of a fruit is removed in sorting by the weight ratio of 5:1 afterwards, and clean and broken; Then the Sparassis crispa after the fragmentation and dictyophora phalloidea are dropped in the beater, and the pure water of the weight such as adding and dictyophora phalloidea is pulled an oar; Then the mixing slurry colloid mill defibrination of the Sparassis crispa dictyophora phalloidea that will obtain after will pulling an oar;
(2) slurry of the mixing behind the defibrination is placed in the vacuum freeze drier, by 8～12kg/m
2Stone, and in 2 hours～4 hours, will mix the temperature of starching and be down to-15 ℃～-27 ℃, make to mix to starch and freeze; Then in 30 minutes～1 hour, the condenser temperature of vacuum freeze drier is down to-30 ℃～-35 ℃; Again vacuum freeze drier is evacuated to 0.6mmhg～1.0mmhg; Dry afterwards and make the water sublimate that mixes in the slurry become steam and by the cold trap trapping of vacuum freeze drier, make and mix the slurry freeze-drying;
Wherein, the temperature and time of oven dry is specially: the oven dry initial temperature is 120 ℃, keeps temperature 3 hours; In 1 hour, be down to 100 ℃ from 120 ℃, and located to keep temperature 1 hour at 100 ℃; In 1 hour, drop to 80 ℃ from 100 ℃; In 0.5 hour, drop to 60 ℃ from 80 ℃, and located to keep temperature 5.5 hours at 60 ℃;
(3) mixing after freeze-drying slurry is adopted the ultramicro grinding crusher machine, crosses 200 order mesh screens to obtain freeze-dried powder, afterwards freeze-dried powder is incapsulated shell and under aseptic condition packing namely get described dictyophora phalloidea Sparassis crispa freeze dried superfines capsule finished product.
2. a kind of dictyophora phalloidea Sparassis crispa freeze dried superfines capsule preparation method thereof according to claim 1 is characterized in that: also comprise following operation: the dictyophora phalloidea Sparassis crispa freeze dried superfines capsule finished product of gained employing co-60 radiation after will packing.
3. a kind of dictyophora phalloidea Sparassis crispa freeze dried superfines capsule preparation method thereof according to claim 1, it is characterized in that: described capsule shells is No. 1 capsule shells, and the described freeze-dried powder of 290mg of packing in every seed lac softgel shell.
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Cited By (2)
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| CN106262798A (en) * | 2016-10-10 | 2017-01-04 | 贵州高山生物科技有限公司 | Dictyophora rubrovalvata volva dry powder and preparation method and application |
| CN114698831A (en) * | 2022-04-28 | 2022-07-05 | 贵州省现代农业发展研究所(贵州省现代农村发展研究中心、贵州省农村经济与社会发展科学研究所、贵州省农产品加工研究所) | Instant bamboo fungus flavor nutrition powder for reducing cholesterol and preparation method thereof |
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| CN106262798A (en) * | 2016-10-10 | 2017-01-04 | 贵州高山生物科技有限公司 | Dictyophora rubrovalvata volva dry powder and preparation method and application |
| CN114698831A (en) * | 2022-04-28 | 2022-07-05 | 贵州省现代农业发展研究所(贵州省现代农村发展研究中心、贵州省农村经济与社会发展科学研究所、贵州省农产品加工研究所) | Instant bamboo fungus flavor nutrition powder for reducing cholesterol and preparation method thereof |
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