CN103349289A - Preparation method of fish oil soft capsules - Google Patents
Preparation method of fish oil soft capsules Download PDFInfo
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- CN103349289A CN103349289A CN2013102353963A CN201310235396A CN103349289A CN 103349289 A CN103349289 A CN 103349289A CN 2013102353963 A CN2013102353963 A CN 2013102353963A CN 201310235396 A CN201310235396 A CN 201310235396A CN 103349289 A CN103349289 A CN 103349289A
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Abstract
The invention discloses a preparation method of fish oil soft capsules, and relates to the field of health-care food. The method comprises the steps of material preparing, liquid cement preparing, capsule pressing, setting, drying, capsule washing, and screening. With the method provided by the invention, a complete preparation process of the fish oil capsules is completed. A content prepared by mixing fish oil and vitamin E is subjected to tablet pressing and setting treatments with the liquid cement prepared under certain conditions, such that the odor of fish oil can be further removed, and product taste can be ensured. With the drying and capsule washing process, the quality of the product satisfies the requirement of capsule raw material. Also, with the treatment of the process, fish oil oxidation can be prevented. With the screening step, the quality of the capsules is ensured. The entire process is completed on a same line, such that nutrient loss caused by fish oil instability is avoided.
Description
Technical field
The present invention relates to field of health care food, relate in particular to a kind of preparation method of fish oil soft capsule.
Background technology
Be rich in human body necessary ω-3 polyunsaturated fatty acid EPA and DHA in the fish oil, have help infant intelligent development, improve eyesight, reduce blood in human body in clearing gallbladder sterol and low-density lipoprotein content, anticoagulation, anti-inflammatory and the different physiological roles such as anticancer.Fish oil is in a liquid state at normal temperatures, has a fish like smell; Contain a plurality of pairs of keys among EPA and the DHA, very responsive to light, heat and oxygen, usually need low temperature, seal and keep in Dark Place, greatly limited the application of fish oil in field of food industry.The fish oil that is rich in EPA and DHA is carried out the fishy smell that microencapsulation can be covered fish oil, fish oil is changed over pressed powder from liquid state, protection fish oil is avoided the impact of extraneous poor environment, reduces oxidation, improves fish oil stability, prolongs the shelf life of food.
Because fish oil has special stench flavor, in the extractive process of fish oil, generally carry out the deodorizing of the first step by deodorization process, but in subsequent technique, may not affect finished product mouthfeel out as not doing further processing, traditional fish-oil capsule manufacturing process mainly is with fish oil preparation and the combination of capsule process division, but in this process, exist fish oil easily oxidized, and cause the loss of nutritional labeling because of the unstability of fish oil.
Summary of the invention
Technical problem to be solved by this invention provides and a kind ofly prevents that fish oil is oxidized, guarantees fish oil stability, the further preparation method of the fish oil soft capsule of deodorizing.
In order to realize purpose of the present invention, technical scheme provided by the invention: a kind of preparation technology of fish oil soft capsule, it is characterized in that, preparation technology carries out as follows:
1. prepare burden: fish oil and vitamin E are mixed, get the content feed liquid;
2. glue preparation: will glycerine and purified water mix after heating, continue heating after then adding gelatin, vacuumize again, deaeration, filtration, insulation, get glue;
3. pelleting: the content feed liquid that 1. step is made mixes the glue of 2. preparing with step and inserts in the soft capsule pellet press and be pressed into soft capsule;
4. typing: 3. step is made soft capsule carry out heat treatment;
5. dry: as 4. step to be made soft capsule carry out the drying processing;
6. wash ball: dry after 5. step is made the soft capsule washing;
7. screening: reject substandard product;
Preferably, described step 2. in the glue preparation glycerine and purified water Hybrid Heating temperature be 65-65 ℃, add and continue heating-up temperature behind the gelatin and be 80-85 ℃.
Preferably, described step 2. in the glue preparation vacuum be 0.02Mpa-0.06Mpa, with the filtration of 90-120 orders, holding temperature is 55-60 ℃, the time is 2-3h.
Preferably, described step 2. in the glue preparation process proportioning of gelatin, glycerine and purified water be 1:0.42:1.
Preferably, 3. in the pelleting process, temperature is 20 ℃ to described step, and relative humidity is 40%.
Preferably, described step is 18-22 ℃ of temperature in the type-approval process 4., relative humidity 35%-40%, time 4-6h.
Preferably, described step is 22-26 ℃ of temperature in the dry run 5., relative humidity 35%-40%, time 18-24h.
Preferably, 6. described step washes that lotion is 95% ethanol in the ball process, dries temperature and is 25-28 ℃, and relative humidity is not higher than 40%, and the time is 8-12h.
Preferably, described preparation technology's cleanliness factor is: dust particle diameter is not less than 0.5 μ m, and the grain number is lower than 3500000/m
3
Preferably, described preparation technology's cleanliness factor is: dust particle diameter is not less than 5 μ m, and the grain number is lower than 20000/m
3
Adopt the beneficial effect of above technical scheme to be: by method of the present invention, the complete preparation technology that finished fish-oil capsule, fish oil and vitamin E mix the content that makes, by carrying out pelleting, heat treatment with the glue that makes under certain condition, can further remove the stench flavor that fish oil has, guarantee to make the mouthfeel of product; By dry and wash ball technique, both can make product quality meet the requirement of capsule raw material again, it is oxidized that the processing of this process can be avoided fish oil in addition; Screening has guaranteed to make the quality of capsule.The simultaneously omnidistance collinear processing of this technique, the nutrition leak of having avoided the unstability because of fish oil to cause.
Whole preparation technology finishes in certain clean area, has guaranteed the cleaning of working environment, at utmost reduce because of environment in the capsule preparation process on the impact of content and glue.
Description of drawings
Fig. 1 is process chart of the present invention.
The specific embodiment
Describe preferred embodiment of the present invention in detail below in conjunction with accompanying drawing.
Embodiment 1:
Referring to Fig. 1, a kind of preparation method of fish oil soft capsule comprises preparation technology and technology of the package, and described preparation technology carries out as follows:
One, batching
1. prepare before producing: check operation room by the standard of clearing out a gathering place, can produce after qualified.
2. neck is expected: get the required raw and auxiliary material of this batch output.
3. prepare burden: supplementary material by the respectively weighing of prescription that feeds intake, is had people's weighing during weighing, have a people to check, after the weighing, put into the material temporary room and put respectively.
4. clear out a gathering place: equipment, operation room and Work tool are cleaned.
5. the preparation of content: fish oil and vitamin E were mixed 30 minutes, filter with 100 orders, get the content feed liquid, treat pelleting usefulness.
Two, glue preparation
Add gelatin with glycerine, when pouring into of purified water glue tank is heated to 60 ℃, and ceaselessly be heated with stirring to 80 ℃, time is 2 hours, stirs, and is evacuated to 0.02Mpa, deaeration, filter with 90 orders, filter good glue and be pushed between heat-preserving container deposits, with 55 ℃ of insulations, get glue after having at least leave standstill in 1 hour, treat pelleting usefulness.
Three, pelleting
1. be ready to corresponding mould, get used glue and content material from the heat-preserving container storage chamber.
2. check whether workshop moisture temperature meets the requirements, check pelleting chamber status indicator whether correctly, whether be in state to be produced, whether the checkout facility machine can run well, wait all confirm errorless after, begin to produce.
3. pelleting: use first paraffin (food grade) to lubricate pellet press, again content feed liquid and glue are put the soft capsule that is pressed into the 1.0g/ grain in the soft capsule pellet press, production process guarantees to meet the standard operation requirement.Should note at any time carrying out centre product control in the operating process, to guarantee to produce qualified product.
4. the soft capsule content uniformity be controlled at ± 5% in, detected once every 60 minutes, the rubber THICKNESS CONTROL is at 0.70mm, left-right deviation must not surpass 0.02mm.60 ℃ of glue holding temperature controls.
Four, typing
The capsule and pill that presses must carry out 4 hours typing, 18 ℃ of temperature, relative humidity 35% through rotating cage.
Five, drying
1. after the capsule and pill typing, divide into canopy silk car, per car dress 2kg sends into hothouse and carries out drying, should per hour stir once when dry.
2. drying parameter: baking temperature is controlled at 22 ℃, relative humidity 35%, and 18 hours time, rubber moisture should be controlled at 12%-16%.
Six, wash ball
1. capsule and pill dry good after, pour into and wash ball in the ultrasonic wave soft capsule washing machine, 50 kilograms on every machine washing ball is put into the ultrasonic wave soft capsule washing machine after clean rag is moistening with 95% ethanol and was rotated 5-10 minutes with capsule and pill.
2. dry: washed capsule and pill is put into 25 ℃ in canopy silk car, and relative humidity 35%, 8 hour treats that 95% ethanol waves to the greatest extent.
Seven, screening
1. capsule and pill is sent into after washed and is chosen the ball chamber and carry out the lamp inspection, choose the ball personnel and must wear aseptic gloves and mouth mask, underproof oil vacuole ball, skin bubble ball, impurity ball, obvious irregular ball, adhesion ball, canopy silk-screen trace ball are rejected, can case after the passed examination, change terminal over to, indicate the name of an article, specification, lot number, quantity.And to factory's laboratory censorship, survey sense organ, heavy, disintegration time limited.
2. clear out a gathering place: equipment, operation room and Work tool are cleaned, also in time fill in the record of clearing out a gathering place by QA inspector's inspection behind all clear, QA inspector sends out the quality certification reserved copy and duplicate of clearing out a gathering place after the passed examination, and original is affixed on this batch, and copy is affixed on next group.
Eight, inner packing
1. prepare before producing: check operation room by the standard of clearing out a gathering place, can produce after qualified.
2. neck is expected: get raw material from terminal, check material name, specification, lot number, weight when getting, and again weighing, reclaim after the confirmation, signed documentarily by the handing-over both sides.Get the required inner packaging material of this batch output.Used inner packaging material must have survey report, can use after the assay was approved, and be got by the special messenger, and the special messenger counts granting.
3. inner packing specification
Packing specification: 100 every bottle.Packaging material: solid medicinal vinyon bottle.
4. inner packing is complete, and statistical magnitude is filled in label and is attached on the Turnover Box, and label substance has the name of an article, specification, lot number, weight, date, operator, then sends into the external packing zone by pass-through box.
Preparation technology that it should be noted that the present embodiment finishes in certain clean area, and its standard is: dust particle diameter 〉=0.5 μ m, grain number≤3500000/m
3, dust particle diameter 〉=5 μ m, grain number≤20000/m
3,Every three months detects once, and sedimentation bacterium/ware≤10 are detected once per month, 18-26 ℃ of temperature, and humidity 45-65%, pressure reduction 〉=10 handkerchiefs checks twice every day at least.
Embodiment 2:
All the other are identical with described embodiment 1, and difference is, among the preparation technology:
Two, glue preparation: add gelatin with glycerine, when pouring into of purified water glue tank is heated to 63 ℃, the proportioning of gelatin, glycerine and purified water is 1:0.42:1, and ceaselessly is heated with stirring to 83 ℃, and the time is 3 hours, stir, be evacuated to 0.04Mpa, deaeration is filtered with 95 orders, filtering good glue is pushed between heat-preserving container deposits, with 60 ℃ of insulations, after having at least leave standstill in 1 hour glue, treat that pelleting uses.
Four, typing: the capsule and pill that presses must carry out 5 hours typing, 20 ℃ of temperature, relative humidity 40% through rotating cage.
Five, drying: baking temperature is controlled at 25 ℃, relative humidity 40%, and 20 hours time, rubber moisture should be controlled at 12%-16%
Six, wash ball: washed capsule and pill is put into 27 ℃ in canopy silk car, and relative humidity 40%, 10 hour treats that 95% ethanol waves to the greatest extent.
Embodiment 3:
All the other are identical with described embodiment 1, and difference is, among the preparation technology:
Two, glue preparation: add gelatin with glycerine, when pouring into of purified water glue tank is heated to 65 ℃, and ceaselessly be heated with stirring to 85 ℃, time is 3 hours, stirs, and vacuumizes 0.06Mpa, deaeration, filter with 100 orders, filter good glue and be pushed between heat-preserving container deposits, with 65 ℃ of insulations, get glue after having at least leave standstill in 1 hour, treat pelleting usefulness.
Three, pelleting: the workshop temperature should be 20 ℃, relative humidity 40%.
Four, typing: the capsule and pill that presses must carry out 6 hours typing, 22 ℃ of temperature, relative humidity 40% through rotating cage.
Five, drying: baking temperature is controlled at 27 ℃, relative humidity 40%, 24 hours time.
Six, wash ball: washed capsule and pill is put into 28 ℃ in canopy silk car, and relative humidity 40%, 12 hour treats that 95% ethanol waves to the greatest extent.
By method of the present invention, the complete preparation technology that finished fish-oil capsule, fish oil and vitamin E mix the content that makes, by carrying out pelleting, heat treatment with the glue that makes under certain condition, can further remove the stench flavor that fish oil has, guarantee to make the mouthfeel of product; By dry and wash ball technique, both can make product quality meet the requirement of capsule raw material again, it is oxidized that the processing of this process can be avoided fish oil in addition; Screening has guaranteed to make the quality of capsule.The simultaneously omnidistance collinear processing of this technique, the nutrition leak of having avoided the unstability because of fish oil to cause.
Whole preparation technology finishes in certain clean area, has guaranteed the cleaning of working environment, at utmost reduce because of environment in the capsule preparation process on the impact of content and glue.
Above-described only is preferred embodiment of the present invention, should be pointed out that for the person of ordinary skill of the art, under the prerequisite that does not break away from the invention design, can also make some distortion and improvement, and these all belong to protection scope of the present invention.
Claims (10)
1. the preparation technology of a fish oil soft capsule is characterized in that, preparation technology carries out as follows:
1. prepare burden: fish oil and vitamin E are mixed, get the content feed liquid;
2. glue preparation: will glycerine and purified water mix after heating, continue heating after then adding gelatin, vacuumize again, deaeration, filtration, insulation, get glue;
3. pelleting: the content feed liquid that 1. step is made mixes the glue of 2. preparing with step and inserts in the soft capsule pellet press and be pressed into soft capsule;
4. typing: 3. step is made soft capsule carry out heat treatment;
5. dry: as 4. step to be made soft capsule carry out the drying processing;
6. wash ball: dry after 5. step is made the soft capsule washing;
7. screening: reject substandard product.
2. the preparation method of a kind of fish oil soft capsule according to claim 1 is characterized in that: described step 2. in the glue preparation glycerine and purified water Hybrid Heating temperature be 65-65 ℃, add and continue heating-up temperature behind the gelatin and be 80-85 ℃.
3. the preparation method of a kind of fish oil soft capsule according to claim 1 is characterized in that: described step 2. in the glue preparation vacuum be 0.02Mpa-0.06Mpa, 90-120 orders filter, holding temperature is 55-60 ℃, the time is 2-3h.
4. the preparation method of a kind of fish oil soft capsule according to claim 1 is characterized in that: described step 2. in the glue preparation process proportioning of gelatin, glycerine and purified water be 1:0.42:1.
5. the preparation method of a kind of fish oil soft capsule according to claim 1 is characterized in that: 3. in the pelleting process, temperature is 20 ℃ to described step, and relative humidity is 40%.
6. the preparation method of a kind of fish oil soft capsule according to claim 1 is characterized in that: described step is 18-22 ℃ of temperature in the type-approval process 4., relative humidity 35%-40%, time 4-6h.
7. the preparation method of a kind of fish oil soft capsule according to claim 1 is characterized in that: described step is 22-26 ℃ of temperature in the dry run 5., relative humidity 35%-40%, time 18-24h.
8. the preparation method of a kind of fish oil soft capsule according to claim 1 is characterized in that: 6. described step washes that lotion is 95% ethanol in the ball process, dries temperature and is 25-28 ℃, and relative humidity is not higher than 40%, and the time is 8-12h.
9. the preparation method of a kind of fish oil soft capsule according to claim 1, it is characterized in that: described preparation technology's cleanliness factor is: dust particle diameter is not less than 0.5 μ m, and a grain number is lower than 3500000/m
3
10. the preparation method of a kind of fish oil soft capsule according to claim 1, it is characterized in that: described preparation technology's cleanliness factor is: dust particle diameter is not less than 5 μ m, and a grain number is lower than 20000/m
3
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104082751A (en) * | 2014-06-29 | 2014-10-08 | 宁波市成大机械研究所 | Deep sea fish oil soft capsule containing astaxanthin |
| CN105192696A (en) * | 2015-08-17 | 2015-12-30 | 北京元莱健康管理有限公司 | Composition for protecting eyeground and nutrition retinas and resisting blue light damage and preparation method of composition |
| CN105192699A (en) * | 2015-09-30 | 2015-12-30 | 深圳市生命力生物保健科技江苏有限公司 | Fish oil soft capsules and preparation method thereof |
| CN107114792A (en) * | 2017-05-10 | 2017-09-01 | 山东禹王制药有限公司 | A kind of preparation method of enteric soft capsules |
| CN108201135A (en) * | 2018-01-17 | 2018-06-26 | 广东长兴生物科技股份有限公司 | A kind of fish oil soft capsule and preparation method thereof |
| CN108208685A (en) * | 2017-12-18 | 2018-06-29 | 丁玉琴 | A kind of preparation method of fish oil soft capsule |
| CN109172537A (en) * | 2018-10-18 | 2019-01-11 | 江西师范大学 | A kind of preparation method of fish oil soft capsule |
| CN110604772A (en) * | 2019-10-25 | 2019-12-24 | 宁夏北方生物科技有限公司 | Chinese wolfberry oil capsule for assisting in reducing blood fat and enhancing immunity and preparation method thereof |
| CN112890197A (en) * | 2021-03-10 | 2021-06-04 | 湖南文理学院 | Fish oil product with health promotion effect |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104082751A (en) * | 2014-06-29 | 2014-10-08 | 宁波市成大机械研究所 | Deep sea fish oil soft capsule containing astaxanthin |
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| CN108201135A (en) * | 2018-01-17 | 2018-06-26 | 广东长兴生物科技股份有限公司 | A kind of fish oil soft capsule and preparation method thereof |
| CN109172537A (en) * | 2018-10-18 | 2019-01-11 | 江西师范大学 | A kind of preparation method of fish oil soft capsule |
| CN109172537B (en) * | 2018-10-18 | 2021-04-30 | 江西师范大学 | Preparation method of fish oil soft capsules |
| CN110604772A (en) * | 2019-10-25 | 2019-12-24 | 宁夏北方生物科技有限公司 | Chinese wolfberry oil capsule for assisting in reducing blood fat and enhancing immunity and preparation method thereof |
| CN112890197A (en) * | 2021-03-10 | 2021-06-04 | 湖南文理学院 | Fish oil product with health promotion effect |
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Application publication date: 20131016 |