CN103344628A - 钢铁中砷含量的icp-aes测量 - Google Patents
钢铁中砷含量的icp-aes测量 Download PDFInfo
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- CN103344628A CN103344628A CN2013102585301A CN201310258530A CN103344628A CN 103344628 A CN103344628 A CN 103344628A CN 2013102585301 A CN2013102585301 A CN 2013102585301A CN 201310258530 A CN201310258530 A CN 201310258530A CN 103344628 A CN103344628 A CN 103344628A
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- arsenic
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- icp
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- 229910052785 arsenic Inorganic materials 0.000 title claims abstract description 26
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 title claims abstract description 21
- 229910000831 Steel Inorganic materials 0.000 title claims abstract description 15
- 239000010959 steel Substances 0.000 title claims abstract description 15
- 238000000691 measurement method Methods 0.000 title abstract 2
- 238000000034 method Methods 0.000 claims abstract description 28
- HEDRZPFGACZZDS-UHFFFAOYSA-N chloroform Substances ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 claims abstract description 13
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229910017604 nitric acid Inorganic materials 0.000 claims abstract description 9
- 238000010438 heat treatment Methods 0.000 claims abstract description 6
- 239000012286 potassium permanganate Substances 0.000 claims abstract description 5
- 239000000243 solution Substances 0.000 claims description 43
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 18
- 238000009616 inductively coupled plasma Methods 0.000 claims description 17
- 239000012074 organic phase Substances 0.000 claims description 13
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 12
- 238000005303 weighing Methods 0.000 claims description 12
- 229910021642 ultra pure water Inorganic materials 0.000 claims description 10
- 239000012498 ultrapure water Substances 0.000 claims description 10
- 229910052742 iron Inorganic materials 0.000 claims description 9
- 239000000523 sample Substances 0.000 claims description 9
- 239000012488 sample solution Substances 0.000 claims description 8
- 239000011609 ammonium molybdate Substances 0.000 claims description 4
- APUPEJJSWDHEBO-UHFFFAOYSA-P ammonium molybdate Chemical compound [NH4+].[NH4+].[O-][Mo]([O-])(=O)=O APUPEJJSWDHEBO-UHFFFAOYSA-P 0.000 claims description 4
- 229940010552 ammonium molybdate Drugs 0.000 claims description 4
- 235000018660 ammonium molybdate Nutrition 0.000 claims description 4
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 4
- 230000008676 import Effects 0.000 claims description 4
- 230000003595 spectral effect Effects 0.000 claims description 4
- 239000012086 standard solution Substances 0.000 claims description 4
- 239000012224 working solution Substances 0.000 claims description 4
- TXUICONDJPYNPY-UHFFFAOYSA-N (1,10,13-trimethyl-3-oxo-4,5,6,7,8,9,11,12,14,15,16,17-dodecahydrocyclopenta[a]phenanthren-17-yl) heptanoate Chemical compound C1CC2CC(=O)C=C(C)C2(C)C2C1C1CCC(OC(=O)CCCCCC)C1(C)CC2 TXUICONDJPYNPY-UHFFFAOYSA-N 0.000 claims description 3
- 229910021626 Tin(II) chloride Inorganic materials 0.000 claims description 3
- 235000011150 stannous chloride Nutrition 0.000 claims description 3
- 239000001119 stannous chloride Substances 0.000 claims description 3
- 238000002354 inductively-coupled plasma atomic emission spectroscopy Methods 0.000 claims 3
- 239000011159 matrix material Substances 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 125000004108 n-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 abstract 1
- 238000005259 measurement Methods 0.000 description 4
- 238000001514 detection method Methods 0.000 description 3
- GOLCXWYRSKYTSP-UHFFFAOYSA-N Arsenious Acid Chemical compound O1[As]2O[As]1O2 GOLCXWYRSKYTSP-UHFFFAOYSA-N 0.000 description 2
- -1 As3O5) Chemical compound 0.000 description 2
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 1
- 229910000805 Pig iron Inorganic materials 0.000 description 1
- 238000003723 Smelting Methods 0.000 description 1
- MJLGNAGLHAQFHV-UHFFFAOYSA-N arsenopyrite Chemical compound [S-2].[Fe+3].[As-] MJLGNAGLHAQFHV-UHFFFAOYSA-N 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 230000005284 excitation Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000002203 pretreatment Methods 0.000 description 1
- 239000011435 rock Substances 0.000 description 1
- 238000004611 spectroscopical analysis Methods 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
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- Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
Abstract
Description
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Priority Applications (1)
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CN201310258530.1A CN103344628B (zh) | 2013-06-26 | 2013-06-26 | 钢铁中砷含量的icp-aes测量 |
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CN201310258530.1A CN103344628B (zh) | 2013-06-26 | 2013-06-26 | 钢铁中砷含量的icp-aes测量 |
Publications (2)
Publication Number | Publication Date |
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CN103344628A true CN103344628A (zh) | 2013-10-09 |
CN103344628B CN103344628B (zh) | 2016-01-20 |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103954610A (zh) * | 2014-04-10 | 2014-07-30 | 中国航空工业集团公司北京航空材料研究院 | 一种测定高铬镍钢中砷的方法 |
CN108318476A (zh) * | 2018-05-09 | 2018-07-24 | 郭秀娟 | 一种钼铁合金中微量元素锑含量的icp-aes测量方法 |
CN108645842A (zh) * | 2018-05-09 | 2018-10-12 | 郭秀娟 | 一种钼铁合金中微量元素铋含量的icp-aes测量方法 |
Citations (8)
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JP2007327797A (ja) * | 2006-06-06 | 2007-12-20 | Dowa Holdings Co Ltd | 高周波誘導結合プラズマ発光分光分析方法 |
CN101435775A (zh) * | 2008-12-23 | 2009-05-20 | 二重集团(德阳)重型装备股份有限公司 | 测定钼铁中杂质元素砷、锡、锑的方法 |
CN101620186A (zh) * | 2009-07-27 | 2010-01-06 | 中国科学院上海硅酸盐研究所 | 一种玻璃澄清剂中砷含量分析法 |
CN101776607A (zh) * | 2009-12-30 | 2010-07-14 | 中国科学院上海硅酸盐研究所 | 玻璃中总砷的分析方法 |
CN102200512A (zh) * | 2011-03-14 | 2011-09-28 | 山东省冶金科学研究院 | 钢铁中有害元素成分分析用多元素标准溶液及制备方法 |
CN102253108A (zh) * | 2011-04-13 | 2011-11-23 | 邬蓓蕾 | 高压消解icp-ms法测定原油中稀土元素含量的方法 |
CN102252880A (zh) * | 2010-05-19 | 2011-11-23 | 攀钢集团钢铁钒钛股份有限公司 | 铁矿的消解方法和检测方法 |
KR20120131768A (ko) * | 2011-05-26 | 2012-12-05 | 현대중공업 주식회사 | 유도결합플라즈마 수소화물발생기에 의한 음용수의 비소 분석방법 |
-
2013
- 2013-06-26 CN CN201310258530.1A patent/CN103344628B/zh active Active
Patent Citations (8)
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JP2007327797A (ja) * | 2006-06-06 | 2007-12-20 | Dowa Holdings Co Ltd | 高周波誘導結合プラズマ発光分光分析方法 |
CN101435775A (zh) * | 2008-12-23 | 2009-05-20 | 二重集团(德阳)重型装备股份有限公司 | 测定钼铁中杂质元素砷、锡、锑的方法 |
CN101620186A (zh) * | 2009-07-27 | 2010-01-06 | 中国科学院上海硅酸盐研究所 | 一种玻璃澄清剂中砷含量分析法 |
CN101776607A (zh) * | 2009-12-30 | 2010-07-14 | 中国科学院上海硅酸盐研究所 | 玻璃中总砷的分析方法 |
CN102252880A (zh) * | 2010-05-19 | 2011-11-23 | 攀钢集团钢铁钒钛股份有限公司 | 铁矿的消解方法和检测方法 |
CN102200512A (zh) * | 2011-03-14 | 2011-09-28 | 山东省冶金科学研究院 | 钢铁中有害元素成分分析用多元素标准溶液及制备方法 |
CN102253108A (zh) * | 2011-04-13 | 2011-11-23 | 邬蓓蕾 | 高压消解icp-ms法测定原油中稀土元素含量的方法 |
KR20120131768A (ko) * | 2011-05-26 | 2012-12-05 | 현대중공업 주식회사 | 유도결합플라즈마 수소화물발생기에 의한 음용수의 비소 분석방법 |
Non-Patent Citations (4)
Title |
---|
支国瑞 等: ""ICP-AES法直接测定钢中微量砷、锡、锑"", 《光谱实验室》, vol. 19, no. 4, 31 July 2002 (2002-07-31) * |
曹宏燕: "《冶金材料分析技术与应用》", 30 September 2008, article ""砷含量测定"" * |
杨素莲: ""ICP-AES法测定铁矿石中高含量砷"", 《冶金丛刊》, no. 5, 31 October 2010 (2010-10-31) * |
武文健 等: ""溶剂萃取ICP-AES法测定钢中磷"", 《冶金分析》, vol. 21, no. 5, 31 October 2001 (2001-10-31) * |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103954610A (zh) * | 2014-04-10 | 2014-07-30 | 中国航空工业集团公司北京航空材料研究院 | 一种测定高铬镍钢中砷的方法 |
CN103954610B (zh) * | 2014-04-10 | 2016-08-17 | 中国航空工业集团公司北京航空材料研究院 | 一种测定高铬镍钢中砷的方法 |
CN108318476A (zh) * | 2018-05-09 | 2018-07-24 | 郭秀娟 | 一种钼铁合金中微量元素锑含量的icp-aes测量方法 |
CN108645842A (zh) * | 2018-05-09 | 2018-10-12 | 郭秀娟 | 一种钼铁合金中微量元素铋含量的icp-aes测量方法 |
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Effective date of registration: 20171227 Address after: 400147 Chongqing city Yubei District Longxi street new irrigation Road No. 18 building 11 Ambassador city 24-11 Patentee after: Chongqing view Intellectual Property Service Co., Ltd. Address before: 300112 Tianjin City, North Industrial Park Xiqing District Jin Xia Lu No. 18 C District No. 6 Patentee before: Tianjin Hongyan Technology Co., Ltd. |
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Effective date of registration: 20190225 Address after: 401120 Chongqing Yubei District Longxi Street Jinlong Road 259 Finance and Information City International 4 1-6 Patentee after: Chongqing Haoting Zhongtuo Environmental Technology Co., Ltd. Address before: 400147 Guobin Town, 18 Xinji Avenue, Longxi Street, Yubei District, Chongqing City, 11 blocks, 24-11 Patentee before: Chongqing view Intellectual Property Service Co., Ltd. |
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Effective date of registration: 20201216 Address after: 274900 high tech chemical industry park, Juye County, Heze City, Shandong Province Patentee after: Heze Dijie Chemical Co.,Ltd. Address before: Room 1-6, building 4, Caixin City International, 259 Jinlong Road, Longxi street, Yubei District, Chongqing Patentee before: Chongqing Haoting Zhongtuo Environmental Technology Co.,Ltd. |
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Effective date of registration: 20210408 Address after: 550000 1-09, No.13 Zhenfu Road, Dongmen neighborhood committee, Yongjing Town, Xifeng County, Guiyang City, Guizhou Province Patentee after: Guiyang Yuguan Technical Service Center Address before: 274900 high tech chemical industry park, Juye County, Heze City, Shandong Province Patentee before: Heze Dijie Chemical Co.,Ltd. |