CN103341195A - Preparation technology for antibacterial perfume - Google Patents
Preparation technology for antibacterial perfume Download PDFInfo
- Publication number
- CN103341195A CN103341195A CN2013102261209A CN201310226120A CN103341195A CN 103341195 A CN103341195 A CN 103341195A CN 2013102261209 A CN2013102261209 A CN 2013102261209A CN 201310226120 A CN201310226120 A CN 201310226120A CN 103341195 A CN103341195 A CN 103341195A
- Authority
- CN
- China
- Prior art keywords
- chitosan
- perfume
- antibacterial
- essence
- preparation technology
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000002304 perfume Substances 0.000 title claims abstract description 28
- 230000000844 anti-bacterial effect Effects 0.000 title claims abstract description 18
- 238000005516 engineering process Methods 0.000 title claims abstract description 13
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- 229920001661 Chitosan Polymers 0.000 claims abstract description 25
- 239000002904 solvent Substances 0.000 claims abstract description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 230000002572 peristaltic effect Effects 0.000 claims abstract description 6
- 238000001035 drying Methods 0.000 claims abstract description 3
- 239000000284 extract Substances 0.000 claims abstract description 3
- 235000013599 spices Nutrition 0.000 claims abstract description 3
- 239000004005 microsphere Substances 0.000 claims description 12
- QTBSBXVTEAMEQO-UHFFFAOYSA-N acetic acid Substances CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 7
- 238000012856 packing Methods 0.000 claims description 5
- 239000007921 spray Substances 0.000 claims description 5
- 238000000935 solvent evaporation Methods 0.000 claims description 2
- 239000003205 fragrance Substances 0.000 abstract description 12
- 238000001694 spray drying Methods 0.000 abstract description 7
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- 239000002994 raw material Substances 0.000 abstract description 3
- 239000007788 liquid Substances 0.000 abstract 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 abstract 1
- 238000005086 pumping Methods 0.000 abstract 1
- 230000003115 biocidal effect Effects 0.000 description 5
- 230000001408 fungistatic effect Effects 0.000 description 5
- 230000002045 lasting effect Effects 0.000 description 5
- 230000008901 benefit Effects 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 239000003921 oil Substances 0.000 description 4
- 235000019198 oils Nutrition 0.000 description 4
- 239000008868 Flower Essence Substances 0.000 description 3
- 241000207840 Jasminum Species 0.000 description 3
- 235000010254 Jasminum officinale Nutrition 0.000 description 3
- 239000003814 drug Substances 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 241001597008 Nomeidae Species 0.000 description 2
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000013268 sustained release Methods 0.000 description 2
- 239000012730 sustained-release form Substances 0.000 description 2
- 229920000018 Callose Polymers 0.000 description 1
- 240000007436 Cananga odorata Species 0.000 description 1
- 229920002101 Chitin Polymers 0.000 description 1
- 108010054033 Chitin deacetylase Proteins 0.000 description 1
- 241000238424 Crustacea Species 0.000 description 1
- 241000238557 Decapoda Species 0.000 description 1
- 241000371997 Eriocheir sinensis Species 0.000 description 1
- 244000178870 Lavandula angustifolia Species 0.000 description 1
- 235000010663 Lavandula angustifolia Nutrition 0.000 description 1
- 241000220317 Rosa Species 0.000 description 1
- 244000178231 Rosmarinus officinalis Species 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 238000003483 aging Methods 0.000 description 1
- 230000000845 anti-microbial effect Effects 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 230000003385 bacteriostatic effect Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 229960000935 dehydrated alcohol Drugs 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 229960004756 ethanol Drugs 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000008394 flocculating agent Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000035800 maturation Effects 0.000 description 1
- 239000011806 microball Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 231100000957 no side effect Toxicity 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 230000002085 persistent effect Effects 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 230000002787 reinforcement Effects 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
Landscapes
- Fats And Perfumes (AREA)
- Cosmetics (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention mainly provides a preparation technology for an antibacterial perfume. The preparation technology comprises: dissolving an essence or a spice extract in an acetate solution of chitosan with a concentration of 4-12%, pumping into the nozzle of a spray drying apparatus via a peristaltic pump; under the conditions of an air inlet temperature of 110 DEG C, an air inlet flow of 110 m<3>/h and an air outlet temperature of 80 DEG C, making liquid drops and hot-air to enter into a drying chamber to evaporate the solvent in the liquid drops and discharge the solvent through a sewer pipe, separating and collecting to obtain chitosan essence microballoons; and adding into proper amount of 95% ethanol or a pure water solvent, filling into a bottle to obtain the antibacterial perfume product. By employing chitosan as one raw material, the prepared antibacterial perfume is easily available in raw materials and simple in production technology; and by employing the spray drying technology to prepare the slow-release microballoon, the problems that fragrance in the conventional perfume cannot last long enough and the antibacterial effect is bad are solved.
Description
Technical field
The present invention relates to a kind of perfume, particularly a kind of long-acting bacteriostatic perfume.
Background technology
Perfume is requisite articles for use during people live.On one's body both having can be sprayed on, also can be sprayed on places such as automobile, room, office, toilet.Namely being a kind of necessary article of doings, is again the good assistant who cleans and improve environment.In fact perfume on the market is most of does not have antibiotic effect just by the pleasant aroma, particularly not only needs the special of the fragrance of perfume own as places such as automobile, room, offices, but also need have fungistatic effect.
201110108951.7 antibiotic perfume.This invention is by natural aromatic vegetable oil: rose absolute, Herba Pogostemonis oil, Oleum lavandula angustifolia, ylang ylang oil, oil of rosemary, oleum bergamottae, orange blossom oil and dehydrated alcohol, distilled water are formed.Form through dissolving, mixing, maturation, freezing, ageing, filtration, fill.Though this invention fungistatic effect is good, but the persistent period is not long.
Chitosan also claims chitosan or chitosan chitosan; it is a kind of natural polycation alkaline polysaccharide; its chemical name is (1; 4)-2-amino-2-deoxidation-callose; it is the product of chitin deacetylase base; and chitin is the main component of crustacean shells such as shrimp, Eriocheir sinensis, extensively is present in nature.Chitosan has good biocompatibility and biodegradability, and its catabolite is harmless to health, it is worthy of note especially the dissolving after solution in contain amino (NH2+), these amino are by suppressing antibacterial in conjunction with negatron.The inhibition bacterial activity of chitosan makes it have a wide range of applications in fields such as medicine, weaving and food.But chitosan has degradable, safety non-toxic bacteriostasis antibiosis, good many advantages such as permeability, and people have looked it and are a kind of good slow release material at present, and are widely used in every field such as medicine, chemical industry, agricultural.
Adopt the chitosan sustained-release microsphere of spray drying method for preparation that good sphere and smooth surface are arranged, fragrance component is scattered in the chitosan microball, is dissolved in the perfume solvent, not only reaches fungistatic effect, and slowly discharges fragrance.
Chitosan and derivant thereof are as natural macromolecule flocculating agent, and its bactericidal action is familiar with and is studied, and particularly more and more are subjected to extensive concern in field of medicaments, and its aboundresources has great potential and application prospect.Reinforcement makes it industrialization to the research and development of chitosan and derivant product thereof, will produce huge economic benefit and social benefit, does the contribution that makes new advances for the economic development of China.
Summary of the invention
The objective of the invention is provides a kind of use safety in order to solve the defective of above-mentioned existence, and the antibiotic perfume that has no side effect has stronger antibiotic and sterilizing effect, fragrance fragrance, lasting lasting, advantage such as production technology is simple, and production cost is low.Be mainly used in places such as automobile, room, office, toilet.
A kind of preparation technology of antibacterial perfume,
1) essence or spice extract are dissolved in the 4-12% chitosan-acetic acid solution, pump into the spray dryer spout by peristaltic pump.Inlet temperature is that 110 ℃, air intake flow are that 110m3/h, leaving air temp are 80 ℃, and drop enters drying chamber with hot-air, makes the solvent evaporation in the drop and is discharged by sewer pipe, and separated and collected obtains chitosan essence microsphere.
2) chitosan essence microsphere is joined in an amount of 95% ethanol or the pure water solvent, in the bottle of packing into, namely get antibacterial perfume products.
Confirm through experimental study, contain 8% chitosan-acetic acid solution fungistatic effect and the lasting rate height of fragrance.
It is the antibacterial perfume of feedstock production that the present invention adopts chitosan, and not only raw material is easy to get, and production technology is simple, and adopt spray drying technology to carry out the preparation of sustained-release micro-spheres, has solved the problem of unsuitable lasting, the good antimicrobial effect of fragrance in the perfume.
Antibacterial perfume provided by the invention is used family, hotel toilet fungistatic effect is obvious, and fragrance is lasting.
Embodiment 1 is dissolved in jasmine flower essence 30g in 4% chitosan-acetic acid solution, pumps into the spray dryer spout by peristaltic pump.Inlet temperature is that 110 ℃, air intake flow are that 110m3/h, leaving air temp are 80 ℃ of chitosan perfume ingredient microspheres that obtained wrapping up by spray drying method.Chitosan essence microsphere 40g is joined in the 60g pure water solvent, in the bottle of packing into, namely get antibacterial perfume products.Result of the test: bacteriostasis rate 85.13%, fragrance remaining time are 3 days.
Embodiment 2
Embodiment 1 is dissolved in jasmine flower essence 30g in 10% chitosan-acetic acid solution, pumps into the spray dryer spout by peristaltic pump.Inlet temperature is that 110 ℃, air intake flow are that 110m3/h, leaving air temp are 80 ℃ of chitosan perfume ingredient microspheres that obtained wrapping up by spray drying method.Chitosan essence microsphere 40g is joined in the 60g pure water solvent, in the bottle of packing into, namely get antibacterial perfume products.Result of the test: bacteriostasis rate 99.99%, fragrance remaining time are 7 days.
Embodiment 3
Embodiment 1 is dissolved in jasmine flower essence 30g in 8% chitosan-acetic acid solution, pumps into the spray dryer spout by peristaltic pump.Inlet temperature is that 110 ℃, air intake flow are that 110m3/h, leaving air temp are 80 ℃ of chitosan perfume ingredient microspheres that obtained wrapping up by spray drying method.Chitosan essence microsphere 40g is joined in the 60g pure water solvent, in the bottle of packing into, namely get antibacterial perfume products.Result of the test: bacteriostasis rate 99.98%, fragrance remaining time are 7 days.
Claims (2)
1. the preparation technology of an antibacterial perfume is characterized in that step is as follows:
1) essence or spice extract are dissolved in the 4-12% chitosan-acetic acid solution, pump into the spray dryer spout by peristaltic pump;
Inlet temperature is that 110 ℃, air intake flow are that 110m3/h, leaving air temp are 80 ℃, and drop enters drying chamber with hot-air, makes the solvent evaporation in the drop and is discharged by sewer pipe, and separated and collected obtains chitosan essence microsphere;
2) chitosan essence microsphere is joined in an amount of 95% ethanol or the pure water solvent, in the bottle of packing into, namely get antibacterial perfume products.
2. according to the preparation technology of the described antibacterial perfume of claim 1, it is characterized in that selecting for use 8% chitosan-acetic acid solution.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310226120.9A CN103341195B (en) | 2013-06-08 | 2013-06-08 | A kind of preparation technology of antibacterial perfume |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310226120.9A CN103341195B (en) | 2013-06-08 | 2013-06-08 | A kind of preparation technology of antibacterial perfume |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103341195A true CN103341195A (en) | 2013-10-09 |
| CN103341195B CN103341195B (en) | 2016-03-30 |
Family
ID=49276053
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310226120.9A Expired - Fee Related CN103341195B (en) | 2013-06-08 | 2013-06-08 | A kind of preparation technology of antibacterial perfume |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103341195B (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0678978A (en) * | 1992-09-03 | 1994-03-22 | Takeshi Karita | Deodorant |
| CN1803200A (en) * | 2006-01-19 | 2006-07-19 | 武汉理工大学 | Antibiotic and deodorant agent for shoes and socks |
| CN101024094A (en) * | 2007-01-11 | 2007-08-29 | 南京零一新材料工程研究中心 | Biological-degradable chitosan porous hemostasis material and its preparing method |
| CN101433730A (en) * | 2008-11-28 | 2009-05-20 | 浙江林学院 | Treatment agent for domestic refuse containing plant vinegar liquor and uses thereof |
-
2013
- 2013-06-08 CN CN201310226120.9A patent/CN103341195B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0678978A (en) * | 1992-09-03 | 1994-03-22 | Takeshi Karita | Deodorant |
| CN1803200A (en) * | 2006-01-19 | 2006-07-19 | 武汉理工大学 | Antibiotic and deodorant agent for shoes and socks |
| CN101024094A (en) * | 2007-01-11 | 2007-08-29 | 南京零一新材料工程研究中心 | Biological-degradable chitosan porous hemostasis material and its preparing method |
| CN101433730A (en) * | 2008-11-28 | 2009-05-20 | 浙江林学院 | Treatment agent for domestic refuse containing plant vinegar liquor and uses thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103341195B (en) | 2016-03-30 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| CB03 | Change of inventor or designer information |
Inventor after: Fei Jinhua Inventor before: Ling Yuanruo |
|
| COR | Change of bibliographic data | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20160224 Address after: Wujiang District of Suzhou City, Jiangsu province 215200 Song Ling Zhen Wu highway Applicant after: Wujiang Huacheng Composite Technology Co., Ltd. Address before: Wujiang City, Suzhou City, Jiangsu province 215212 Li Jian Township Street No. 30 southwest of Hong Kong Applicant before: Wujiang Lida Glazing Products Co., Ltd. |
|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| CB03 | Change of inventor or designer information |
Inventor after: Ling Yuanruo Inventor before: Fei Jinhua |
|
| COR | Change of bibliographic data | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20160325 Address after: Wujiang City, Suzhou City, Jiangsu province 215212 Li Jian Township Street No. 30 southwest of Hong Kong Patentee after: Wujiang Lida Glazing Products Co., Ltd. Address before: Wujiang District of Suzhou City, Jiangsu province 215200 Song Ling Zhen Wu highway Patentee before: Wujiang Huacheng Composite Technology Co., Ltd. |
|
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160330 Termination date: 20160608 |
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| CF01 | Termination of patent right due to non-payment of annual fee |