CN103341195B - A kind of preparation technology of antibacterial perfume - Google Patents
A kind of preparation technology of antibacterial perfume Download PDFInfo
- Publication number
- CN103341195B CN103341195B CN201310226120.9A CN201310226120A CN103341195B CN 103341195 B CN103341195 B CN 103341195B CN 201310226120 A CN201310226120 A CN 201310226120A CN 103341195 B CN103341195 B CN 103341195B
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- China
- Prior art keywords
- chitosan
- perfume
- essence
- microsphere
- antibacterial
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- 239000002304 perfume Substances 0.000 title claims abstract description 28
- 230000000844 anti-bacterial effect Effects 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title claims abstract description 8
- 229920001661 Chitosan Polymers 0.000 claims abstract description 23
- 239000004005 microsphere Substances 0.000 claims abstract description 15
- 239000002904 solvent Substances 0.000 claims abstract description 10
- QTBSBXVTEAMEQO-UHFFFAOYSA-N acetic acid Substances CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 230000002572 peristaltic effect Effects 0.000 claims abstract description 6
- 239000007921 spray Substances 0.000 claims abstract description 6
- 238000001035 drying Methods 0.000 claims abstract description 3
- 239000000284 extract Substances 0.000 claims abstract description 3
- 235000013599 spices Nutrition 0.000 claims abstract description 3
- 239000003205 fragrance Substances 0.000 abstract description 12
- 230000002045 lasting effect Effects 0.000 abstract description 6
- 238000001694 spray drying Methods 0.000 abstract description 6
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 239000002994 raw material Substances 0.000 abstract description 4
- 238000013268 sustained release Methods 0.000 abstract description 3
- 239000012730 sustained-release form Substances 0.000 abstract description 3
- 230000000845 anti-microbial effect Effects 0.000 abstract description 2
- 230000001408 fungistatic effect Effects 0.000 description 5
- 230000008901 benefit Effects 0.000 description 4
- 230000003115 biocidal effect Effects 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 239000003921 oil Substances 0.000 description 4
- 235000019198 oils Nutrition 0.000 description 4
- 239000008868 Flower Essence Substances 0.000 description 3
- 241000207840 Jasminum Species 0.000 description 3
- 235000010254 Jasminum officinale Nutrition 0.000 description 3
- 239000003814 drug Substances 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229920000018 Callose Polymers 0.000 description 1
- 240000007436 Cananga odorata Species 0.000 description 1
- 229920002101 Chitin Polymers 0.000 description 1
- 108010054033 Chitin deacetylase Proteins 0.000 description 1
- 241000238424 Crustacea Species 0.000 description 1
- 241000238557 Decapoda Species 0.000 description 1
- 241000371997 Eriocheir sinensis Species 0.000 description 1
- 244000178870 Lavandula angustifolia Species 0.000 description 1
- 235000010663 Lavandula angustifolia Nutrition 0.000 description 1
- 241000220317 Rosa Species 0.000 description 1
- 244000178231 Rosmarinus officinalis Species 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 238000003483 aging Methods 0.000 description 1
- 239000003242 anti bacterial agent Substances 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000003385 bacteriostatic effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 229960000935 dehydrated alcohol Drugs 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 229960004756 ethanol Drugs 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000008394 flocculating agent Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000035800 maturation Effects 0.000 description 1
- 239000011806 microball Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 231100000957 no side effect Toxicity 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 230000002085 persistent effect Effects 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
Landscapes
- Fats And Perfumes (AREA)
- Cosmetics (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
Invention broadly provides a kind of preparation technology of antibacterial perfume, essence or spice extract are dissolved in 4-12% chitosan-acetic acid solution, pump into spray dryer spout by peristaltic pump.Inlet temperature is 110 DEG C, air intake flow is 110m3/h, leaving air temp is 80 DEG C, and drop enters drying chamber together with hot-air, the solvent in drop is evaporated and discharges separated and collected by sewer pipe to obtain chitosan essence microsphere.Chitosan essence microsphere is joined in appropriate 95% ethanol or pure water solvent, load in bottle, obtain antibacterial perfume product.The present invention adopts chitosan to be that antibacterial perfume prepared by raw material, and not only raw material is easy to get, and production technology is simple, and adopts spray drying technology to carry out the preparation of sustained-release micro-spheres, solves the problem of unsuitable lasting, the good antimicrobial effect of fragrance in perfume.
Description
Technical field
The present invention relates to a kind of perfume, particularly a kind of long-acting bacteriostatic perfume.
Background technology
Perfume is requisite articles for use during people live.Both, with it having can be sprayed on, also can be sprayed on the places such as automobile, room, office, toilet.Namely being a kind of necessary article of doings, is again good assistant that is clean and environmental protect.Perfume major part on the market, just by pleasant aroma, in fact without antibacterial effect, particularly not only needs the special of the fragrance of perfume own as places such as automobile, room, offices, but also need have fungistatic effect.
201110108951.7 an antibiotic perfume.This invention is by natural aromatic vegetable oil: rose absolute, Herba Pogostemonis oil, Oleum lavandula angustifolia, ylang ylang oil, oil of rosemary, oleum bergamottae, orange blossom oil and dehydrated alcohol, distilled water form.Form through dissolving, mixing, maturation, freezing, ageing, filtration, fill.Though this invention fungistatic effect is good, but the persistent period is not long.
Chitosan also claims chitosan or chitosan chitosan; it is a kind of Natural polycations alkaline polysaccharide; its chemical name is (1; 4)-2-amino-2-deoxidation-callose; it is the product of chitin deacetylase base; and chitin is the main component of the crustacean such as shrimp, Eriocheir sinensis shell, be extensively present in nature.Chitosan has good biocompatibility and biodegradability, and its catabolite is harmful to human health, and it is worthy of note that these amino are by carrying out anti-bacteria in conjunction with negatron containing amino (NH2+) in the solution after dissolving especially.The Antibacterial activity of chitosan, makes it have a wide range of applications in fields such as medicine, weaving and food.Chitosan have degradable, safety non-toxic, can the many advantage such as bacteriostasis antibiosis, good permeability, current people have looked it for a kind of good slow-release material, and are widely used in the every field such as medicine, chemical industry, agricultural.
The chitosan sustained-release microsphere adopting spray drying method to prepare has good spherical and smooth surface, and fragrance component is scattered in chitosan microball, is dissolved in perfume solvent, not only reaches fungistatic effect, and slow releasing fragrance.
Chitosan-phospholipid complex is as natural macromolecule flocculating agent, and its bactericidal action has been familiar with and has been studied, and particularly in field of medicaments, is more and more subject to extensive concern, and its aboundresources has huge potentiality and application prospect.Strengthen the research and development to Chitosan-phospholipid complex product, make it industrialization, will produce huge economic benefit and social benefit, the contribution made new advances is done in the economic development for China.
Summary of the invention
The object of the invention is the defect in order to solve above-mentioned existence, providing a kind of use safety, the antibiotic perfume had no side effect, have stronger antibiotic and sterilizing effect, fragrance fragrance, lasting lasting, production technology is simple, the advantages such as production cost is low.Be mainly used in the places such as automobile, room, office, toilet.
A preparation technology for antibacterial perfume,
1) essence or spice extract are dissolved in 4-12% chitosan-acetic acid solution, pump into spray dryer spout by peristaltic pump.Inlet temperature is 110 DEG C, air intake flow is 110m3/h, leaving air temp is 80 DEG C, and drop enters drying chamber together with hot-air, and make the solvent in drop evaporate and be discharged by sewer pipe, separated and collected obtains chitosan essence microsphere.
2) chitosan essence microsphere is joined in appropriate 95% ethanol or pure water solvent, load in bottle, obtain antibacterial perfume product.
Through experimental study confirm, the chitosan-acetic acid solution fungistatic effect containing 8% and the lasting rate of fragrance high.
The present invention adopts chitosan to be that antibacterial perfume prepared by raw material, and not only raw material is easy to get, and production technology is simple, and adopts spray drying technology to carry out the preparation of sustained-release micro-spheres, solves the problem of unsuitable lasting, the good antimicrobial effect of fragrance in perfume.
Antibacterial perfume provided by the invention uses family, toilet fungistatic effect in hotel is obvious, and fragrance is lasting.
Jasmine flower essence 30g is dissolved in 4% chitosan-acetic acid solution by embodiment 1, pumps into spray dryer spout by peristaltic pump.Inlet temperature is 110 DEG C, air intake flow is 110m3/h, leaving air temp is 80 DEG C of chitosan perfume ingredient microspheres being obtained by spray drying method wrapping up.Chitosan essence microsphere 40g is joined in 60g pure water solvent, loads in bottle, obtain antibacterial perfume product.Result of the test: bacteriostasis rate 85.13%, fragrance remaining time is 3 days.
Embodiment 2
Jasmine flower essence 30g is dissolved in 10% chitosan-acetic acid solution by embodiment 1, pumps into spray dryer spout by peristaltic pump.Inlet temperature is 110 DEG C, air intake flow is 110m3/h, leaving air temp is 80 DEG C of chitosan perfume ingredient microspheres being obtained by spray drying method wrapping up.Chitosan essence microsphere 40g is joined in 60g pure water solvent, loads in bottle, obtain antibacterial perfume product.Result of the test: bacteriostasis rate 99.99%, fragrance remaining time is 7 days.
Embodiment 3
Jasmine flower essence 30g is dissolved in 8% chitosan-acetic acid solution by embodiment 1, pumps into spray dryer spout by peristaltic pump.Inlet temperature is 110 DEG C, air intake flow is 110m3/h, leaving air temp is 80 DEG C of chitosan perfume ingredient microspheres being obtained by spray drying method wrapping up.Chitosan essence microsphere 40g is joined in 60g pure water solvent, loads in bottle, obtain antibacterial perfume product.Result of the test: bacteriostasis rate 99.98%, fragrance remaining time is 7 days.
Claims (2)
1. a preparation technology for antibacterial perfume, is characterized in that step is as follows:
1) essence or spice extract are dissolved in 4-12% chitosan-acetic acid solution, pump into spray dryer spout by peristaltic pump;
Inlet temperature is 110 DEG C, air intake flow is 110m3/h, leaving air temp is 80 DEG C, and drop enters drying chamber together with hot-air, and make the solvent in drop evaporate and be discharged by sewer pipe, separated and collected obtains chitosan essence microsphere;
2) chitosan essence microsphere is joined in appropriate 95% ethanol or pure water solvent, load in bottle, obtain antibacterial perfume product.
2. the preparation technology of antibacterial perfume according to claim 1, is characterized in that the chitosan-acetic acid solution selecting 8%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310226120.9A CN103341195B (en) | 2013-06-08 | 2013-06-08 | A kind of preparation technology of antibacterial perfume |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310226120.9A CN103341195B (en) | 2013-06-08 | 2013-06-08 | A kind of preparation technology of antibacterial perfume |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103341195A CN103341195A (en) | 2013-10-09 |
| CN103341195B true CN103341195B (en) | 2016-03-30 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310226120.9A Expired - Fee Related CN103341195B (en) | 2013-06-08 | 2013-06-08 | A kind of preparation technology of antibacterial perfume |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103341195B (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1803200A (en) * | 2006-01-19 | 2006-07-19 | 武汉理工大学 | Antibiotic and deodorant agent for shoes and socks |
| CN101024094A (en) * | 2007-01-11 | 2007-08-29 | 南京零一新材料工程研究中心 | Biological-degradable chitosan porous hemostasis material and its preparing method |
| CN101433730A (en) * | 2008-11-28 | 2009-05-20 | 浙江林学院 | Treatment agent for domestic refuse containing plant vinegar liquor and uses thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0678978A (en) * | 1992-09-03 | 1994-03-22 | Takeshi Karita | Deodorant |
-
2013
- 2013-06-08 CN CN201310226120.9A patent/CN103341195B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1803200A (en) * | 2006-01-19 | 2006-07-19 | 武汉理工大学 | Antibiotic and deodorant agent for shoes and socks |
| CN101024094A (en) * | 2007-01-11 | 2007-08-29 | 南京零一新材料工程研究中心 | Biological-degradable chitosan porous hemostasis material and its preparing method |
| CN101433730A (en) * | 2008-11-28 | 2009-05-20 | 浙江林学院 | Treatment agent for domestic refuse containing plant vinegar liquor and uses thereof |
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| Publication number | Publication date |
|---|---|
| CN103341195A (en) | 2013-10-09 |
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| C41 | Transfer of patent application or patent right or utility model | ||
| CB03 | Change of inventor or designer information |
Inventor after: Fei Jinhua Inventor before: Ling Yuanruo |
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| COR | Change of bibliographic data | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20160224 Address after: Wujiang District of Suzhou City, Jiangsu province 215200 Song Ling Zhen Wu highway Applicant after: Wujiang Huacheng Composite Technology Co., Ltd. Address before: Wujiang City, Suzhou City, Jiangsu province 215212 Li Jian Township Street No. 30 southwest of Hong Kong Applicant before: Wujiang Lida Glazing Products Co., Ltd. |
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| C14 | Grant of patent or utility model | ||
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| CB03 | Change of inventor or designer information |
Inventor after: Ling Yuanruo Inventor before: Fei Jinhua |
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| TR01 | Transfer of patent right |
Effective date of registration: 20160325 Address after: Wujiang City, Suzhou City, Jiangsu province 215212 Li Jian Township Street No. 30 southwest of Hong Kong Patentee after: Wujiang Lida Glazing Products Co., Ltd. Address before: Wujiang District of Suzhou City, Jiangsu province 215200 Song Ling Zhen Wu highway Patentee before: Wujiang Huacheng Composite Technology Co., Ltd. |
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| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160330 Termination date: 20160608 |