CN103301054A - Collagen gel capable of moisturizing, revitalizing and nourishing as well as preparation method and application thereof - Google Patents
Collagen gel capable of moisturizing, revitalizing and nourishing as well as preparation method and application thereof Download PDFInfo
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Abstract
The invention belongs to the field of cosmetics, and particularly relates to a collagen gel capable of moisturizing, revitalizing and nourishing. The collagen gel comprises glycerinum, butanediol, dipropylene glycol, propylene glycol, trehalose, glycine betaine, colostrums, hydrolyzed collagen, phospholipid, xanthan gum, pyridoxine, PCA ((pyrrolidone hydroxy acid)) sodium, sodium lactate, Beta-glucose, polysorbate 20, polysorbate 80, imidazolidinyl urea, iodopropynyl butylcarbamate, EDTA (Ethylene Diamine Tetraacetic Acid) disodium, essence and purified water. The gel is mild and has no simulation, is remarkable in moistening effect, can nourish the skin deeply, is applicable to moistening of a collagen mask, bottoming for massaging and acoustic wave beauty therapy when in a professional care, and also can be used as nutrient lotions for efficiently moistening when in home health care. The collagen gel is applicable to dry and dry skin and mature skin.
Description
Technical field
The present invention relates to cosmetic field, be specifically related to a kind of have moisturizing and tax collagen dew that nourishes alive and its preparation method and application.
Background technology
The fundamental of healthy skin is smooth, full, high resilience.Along with the increase at age, the Moisture factor content in the keratodermatitis reduces gradually, causes the hydratability of skin to descend, and shows as xerosis cutis, wrinkling, lax, presents aging outward appearance.It is one of pathomechanism of this old and feeble outward appearance that skin beauty water content reduces gradually.When cuticular water content is lower than 10%, the crack appears in the horn cell layer that xerosis cutis, desquamation, imbricate are arranged in parallel.Skin barrier is damaged, easily is subject to the erosion of external environment physical factor such as wind and cold, cold and hot and biological factor such as microorganism, and the water in the skin, electrolyte be easily evaporation or run off also.Therefore, keeping the water content of skin, guarantee that the moisture in the horny layer is to keep skin softness and elastic key factor, also is the most important basic means of improving looks.
Moisturizing class cosmetics promote the percutaneous moisture absorption just by simulated skin natural moisture preserving system through following mechanism.A. locking water substance increases the water concentration of skin surface, forms the interior stream gradient to skin; B. form hydrophobic barrier, reduce and lose through the severe edema due to hypofunction of the spleen, thereby cause that skin surface moisture increases, and also can form resorbent interior stream gradient.Perhaps A and B act on simultaneously.Also have a kind of gradually approved mechanism, directly or indirectly affect the characteristic of the inner albumen of horny layer or the exchange of lipid water after namely the external material is absorbed by horny layer.By above approach, keep skin to contain suitable moisture, thereby keep healthy beautiful skin.It is pointed out that cuticular hydration status is a complexity and delicate balance sysmte, need to keep a steady-state level, that is to say that water can not be too much, can not be very few, because two states all may damage organ.
Yet add the wetting agent composition in the cosmetic formulations, add have moisturizing, the oils and fats of lock water function, emulsifying agent etc., spread upon the water holding capacity that can help to improve skin on the skin, the degree of hydration of skin is improved, can be in short-term and play for a long time moisture-keeping function.We know, the state that the cell of aging skin presents is exactly that cell metabolism is slow, refuse can't be discharged, and when effective product used on skin, it can't absorb, the product active ingredient can't be entered, and it is slow that skin improves effect, even do not have effect.100% effective product uses aging skin, because cell can't absorb, causes active ingredient to enter about 10%-20%, even still less.
Beautiful, graceful, careful is the pursuit of women's invariability, and the peace favoured beauty makes in conjunction with hard-core technology and advanced prescription, aims at all kinds of skin quality the most succinct, perfect skin maintenance course for the treatment of is provided.To pursue in top quality, the remarkable female life of liking to be beautiful of enjoying to obtain scarce top U.S. flesh elaboration.Whitening, anti-ageing, clean pox, moisturizing, antiallergic, slim have successively been developed ... the planning course for the treatment of is maintained in peace each series of products of favoured beauty and the SPA that arranges in pairs or groups nursing and house, except the beautiful teacher's for the treatment of that can in top salon, arrange in pairs or groups professional skill and technique, experience outside nursing course for the treatment of of body, the heart, spirit unification; More perfectly be that peace favoured beauty series provides nursing at home hard-cover bottle, be in and also can enjoy top care! And the moisturizing series of products that contain high efficiency composition moisturizing composition have comprised more than 30 of the different size such as collagen dew, the gentle fair-skinned cleansing milk of collagen moisturizing, collagen protection foundation cream breast, collagen moisturizing essence, collagen moisture surge treatment formula and prescription, effect and have planted product.
Summary of the invention
For moisturizing and the tax skin that nourishes alive, improve the availability of Moisture factor, improve the cell state of the skin that wears out, pacifying on favoured beauty's series of products, the invention discloses a kind of collagen dew that has moisturizing and compose the nourishing of living.
Collagen of the present invention reveals and comprises glycerol, butanediol, dipropylene glycol, propylene glycol, trehalose, betanin, colostrum, hydrolytic collagen, phospholipid, xanthan gum, pyridoxin, Anjidew NL50, sodium lactate, Beta-glucose, polysorbate 20, polyoxyethylene sorbitan monoleate, imidazolidinyl urea, iodine propilolic alcohol butyl mephenesin Carbamate, EDETATE SODIUM, essence and pure water.
The present invention further defines the content that this collagen reveals each composition (by weight percent meter :) and is glycerol 2%～8%, butanediol 0.2%～1%, dipropylene glycol 0.1%～1%, propylene glycol 0.5%～1.5%, trehalose 0.1%～0.5%, betanin 0.1%～0.8%, colostrum 0.05%～0.2%, hydrolytic collagen 0.1%～0.5%, phosphatidase 10 .05%～0.2%, xanthan gum 0.1%～0.5%, pyridoxin 0.05%～0.2%, Anjidew NL50 0.05%～0.2%, sodium lactate 0.05%～0.2%, Beta-glucose 0.05%～0.2%, polysorbate 20 0.05%～0.2%, polyoxyethylene sorbitan monoleate 0.05%～0.2%, imidazolidinyl urea 0.05%～0.2%, iodine propilolic alcohol butyl mephenesin Carbamate 0.05%～0.2%, EDETATE SODIUM 0.05%～0.2%, essence 0.05%～0.2%, surplus are pure water.
The present invention is further preferred this collagen the reveals content of each composition (by weight percent meter :) is glycerol 5%, butanediol 0.6%, dipropylene glycol 0.5%, propylene glycol 1%, trehalose 0.2%, betanin 0.3%, colostrum 0.1%, hydrolytic collagen 0.2%, phosphatidase 10 .1%, xanthan gum 0.2%, pyridoxin 0.1%, Anjidew NL50 0.1%, sodium lactate 0.1%, Beta-glucose 0.1%, polysorbate 20 0.1%, polyoxyethylene sorbitan monoleate 0.1%, imidazolidinyl urea 0.1%, iodine propilolic alcohol butyl mephenesin Carbamate 0.1%, EDETATE SODIUM 0.1%, essence 0.1%, and surplus is pure water.
Collagen described above reveals, and preferably, the specification that above-mentioned collagen reveals is 120mL.
Collagen described above reveals, and preferably, the specification that above-mentioned collagen reveals is 500mL.
The preparation method that collagen described above reveals, preferably, the preparation that above-mentioned collagen reveals comprises following steps:
1. add to add ENTA-2Na at pure water, be stirred to fully dissolving after, add PVC sodium, sodium lactate, to complete swelling, add polysorbate 20, polyoxyethylene sorbitan monoleate, heating up is stirred to fully dissolving, is incubated 20 minutes;
2. add the Beta-glucose, be stirred to fully dissolving; Add again butanediol and hydrolytic collagen and stir to fully dissolving, obtain component A;
3. xanthan gum is joined in the glycerol, be stirred to fully dissolving, form glycerol mixture; Glycerol mixture is joined among the component A, stir, temperature rises to 80 ℃, obtains B component;
4. dipropylene glycol, trehalose, betanin, colostrum, phospholipid and pyridoxin are mixed, heated and stirred is dissolved to 80 ℃ fully, obtains component C;
5. under the stirring state, in B component, add component C, stir, be incubated 20 minutes, begin cooling, temperature adds propylene glycol after being down to 60 ℃, add imidazolidinyl urea and iodine propilolic alcohol butyl mephenesin Carbamate, essence below 45 ℃, stir, be cooled to room temperature and get final product.
The application that collagen described above reveals, preferably, during special and professional care, can apply to collagen mask moistening, massage bottoming, sound wave is beautiful treats.
The application that collagen described above reveals preferably, during nursing at home, then can be used as the nutrition astringent of potent moisturizing.
The application that collagen described above reveals, preferably, this collagen reveals and is suitable for any skin, and the skin that especially is suitable for hydropenia, dryness, aging, wrinkle uses.
Moisturizing of the present invention with concrete effect and the relative theory of composing each composition in the collagen dew that nourishes of living is:
Contain multiple biochemical, it nourishes the factor can infiltrate rapidly skin bottom, replenishes the needed nutrient of skin and moisture, gives skin gloss and elasticity, makes the colour of skin more thoroughly fair-skinned and moist.
Hydrolytic collagen Collagen Solution increases the skin hydratability, prevents that wrinkle is aging.
Trehalose, i.e. Seamollient Sargassum mucopolysaccharide body is the moisturizing composition of a high-efficiency, and not only sense of touch is good to be used for skin; Soft and smooth, and can prevent the pigment evaporation, and have the effects such as calmness, antiinflammatory.
Pyridoxin, namely Vitamin B6 Vitamin B6 be the anti-dermatitis vitamin of name, can alleviate stimulations, prevention sensitivity.
Compared with prior art, the present invention has following beneficial effect:
This collagen reveals gentleness not to stimulate, and moisturizing power is superpower, and absorbs fast yet.Contain hydrophilic collagen albumen and phospholipid, cooperate collagen mask to use, can significantly promote skin to the absorbing power of collagen.This collagen reveals and claims again the Joker product, of many uses, energy and multiple skin care products cooperate use, be rich in precious nutrient, can effectively increase the water content of skin, and can promote the absorption of nutrition, the composition that contains simultaneously colostrum protein, can effectively prevent the generation of wrinkle, delay skin aging allows skin found existing youthful vigor and gloss.This collagen reveals the astringent that uses at aging skin, can also promote the osmotic absorption of follow-up nutrition product.
Because it is the Joker product, so 1. it can be used as bottoming before massage; 2. available ultrasound wave imports, and can allow skin absorb more nutritional labeling; 3. directly working as astringent behind the clean skin uses; 4. can be used for soaking into disposable face paper and directly apply face, can effectively improve immediately the phenomenon of drying, decortication; 5. can be used as before bottoming of facial film; 6. can dilute any product; 7. can be used for the moistening of collagen mask; 8. can be used for transferring mantle etc.So its using method can be applied in a flexible way.
The measure of merit of transdermal dehydration TEWL can recognize, collagen of the present invention reveals the transdermal moisture evaporation that can effectively reduce skin, improves or repair the barrier function of skin, and skin is had direct or indirect moistening effect.
Learn by the right test of short-term moistening effect squadron skin beauty water, the degree of hydration that this collagen reveals skin is significantly improved, particularly after use in the time range of 0～45min, prolongation along with the time, moistening effect decreases, still have obvious raising but (105min) skin beauty water is right in the testing time scope, illustrate that this collagen reveals and has obvious moistening effect, the right raising degree of skin beauty water is up to 180%.
Learn by the right test of long-term moistening effect squadron's skin beauty water, the degree of hydration that collagen of the present invention reveals skin is significantly improved, the final degree of hydration that improves skin reaches 30%, and (6 week) skin beauty water is right in the testing time scope is in the increase stage always, illustrate that this collagen dew has obvious moistening effect, the right raising degree of skin beauty water is up to 177%.
Description of drawings:
Accompanying drawing 1: the effect of transdermal dehydration TEWL
Specific embodiment
Further explain the present invention below in conjunction with embodiment, but embodiment does not do any type of restriction to the present invention.
Embodiment 1,
Percent meter by weight: glycerol 5%, butanediol 0.6%, dipropylene glycol 0.5%, propylene glycol 1%, trehalose 0.2%, betanin 0.3%, colostrum 0.1%, hydrolytic collagen 0.2%, phosphatidase 10 .1%, xanthan gum 0.2%, pyridoxin 0.1%, Anjidew NL50 0.1%, sodium lactate 0.1%, Beta-glucose 0.1%, polysorbate 20 0.1%, polyoxyethylene sorbitan monoleate 0.1%, imidazolidinyl urea 0.1%, iodine propilolic alcohol butyl mephenesin Carbamate 0.1%, EDETATE SODIUM 0.1%, essence 0.1%, surplus is pure water.Press the specification preparation of 120ml.
According to above-mentioned prescription, do following preparation:
1. add to add ENTA-2Na at pure water, be stirred to fully dissolving after, add PVC sodium, sodium lactate, to complete swelling, add polysorbate 20, polyoxyethylene sorbitan monoleate, heating up is stirred to fully dissolving, is incubated 20 minutes;
2. add the Beta-glucose, be stirred to fully dissolving; Add again butanediol and hydrolytic collagen and stir to fully dissolving, obtain component A;
3. xanthan gum is joined in the glycerol, be stirred to fully dissolving, form glycerol mixture; Glycerol mixture is joined among the component A, stir, temperature rises to 80 ℃, obtains B component;
4. dipropylene glycol, trehalose, betanin, colostrum, phospholipid and pyridoxin are mixed, heated and stirred is dissolved to 80 ℃ fully, obtains component C;
5. under the stirring state, in B component, add component C, stir, be incubated 20 minutes, begin cooling, temperature adds propylene glycol after being down to 60 ℃, add imidazolidinyl urea and iodine propilolic alcohol butyl mephenesin Carbamate, essence below 45 ℃, stir, be cooled to room temperature and get final product.
Embodiment 2
Percent meter by weight: glycerol 2%, butanediol 0.2%, dipropylene glycol 0.1%, propylene glycol 0.5%, trehalose 0.1%, betanin 0.1%, colostrum 0.05%, hydrolytic collagen 0.1%, phosphatidase 10 .05%, xanthan gum 0.1%, pyridoxin 0.05%, Anjidew NL50 0.05%, sodium lactate 0.05%, Beta-glucose 0.05%, polysorbate 20 0.05%, polyoxyethylene sorbitan monoleate 0.05%, imidazolidinyl urea 0.05%, iodine propilolic alcohol butyl mephenesin Carbamate 0.05%, EDETATE SODIUM 0.05%, essence 0.05%, surplus is pure water.Press the specification preparation of 500ml.
Preparation method such as embodiment 1.
Embodiment 3
Percent meter by weight: glycerol 8%, butanediol 1%, dipropylene glycol 1%, propylene glycol 1.5%, trehalose 0.5%, betanin 0.8%, colostrum 0.2%, hydrolytic collagen 0.5%, phosphatidase 10 .2%, xanthan gum 0.5%, pyridoxin 0.2%, Anjidew NL50 0.2%, sodium lactate 0.2%, Beta-glucose 0.2%, polysorbate 20 0.2%, polyoxyethylene sorbitan monoleate 0.2%, imidazolidinyl urea 0.2%, iodine propilolic alcohol butyl mephenesin Carbamate 0.2%, EDETATE SODIUM 0.2%, essence 0.2%, surplus is pure water.Press the specification preparation of 500ml.
Preparation method such as embodiment 1.
Comparative Examples 4,
Do not add colostrum, the other the same as in Example 1 in the prescription.
Comparative Examples 5,
Do not add hydrolytic collagen, the other the same as in Example 1 in the prescription.
Comparative Examples 6,
Do not add pyridoxin, the other the same as in Example 1 in the prescription.
The effect test of embodiment 7, transdermal dehydration TEWL
The prepared collagen of experiment product: embodiment of the invention 1-3 reveals.
The prepared collagen of reference substance: Comparative Examples 4-6 reveals, the moisturizer of commercially available routine.
Instrument: Tewameter TM300 capacitance measuring tester
The variation that transdermal dehydration (Transepidermal water loss, TEWL) measure neighbor skin surface moisture vapor is pressed.The situation of TEWL value representation horny layer moisture loss is the major criterion of estimating stratum corneum barrier function.The TEWL value of skin is lower, illustrates that the barrier function of skin is better, otherwise then poorer.TEWL is very important parameter to the function of assessment moisture of skin protective layer, has obtained in the world widely approval.Protective layer of skin is more intact, and the content of moisture will be higher, and the numerical value of skin moisture loss TEWL is just lower, and the unit of TEWL is: g/hm
2With experiment product of the present invention, reference substance, place left and right forearm inboard respectively the coating experiment product and reference substance.By the test of Tewameter TM300 capacitance measuring tester, TEWL is assessed.The result shows in the accompanying drawings.
The moisturizer of high-quality can improve the stratum corneum barrier function of skin, reduces the dehydration of horny layer transdermal.Transdermal dehydration reduction value is larger, illustrates that the moisture retention water moistening effect is better.The volunteer uses the skin transdermal dehydration of moisture retention water different time to change as shown in Figure 1.The transdermal dehydration value of initial contrast is at 60-65g g/hm
2Between.Service test product and reference substance are during to 120min, and the transdermal dehydration of embodiment 1-3 is all at 20g/hm
2Below, and the transdermal dehydration of embodiment 1 is 18g/hm
2Reduction amplitude to the dehydration of dry skin transdermal is larger, improvement and repairing effect to stratum corneum barrier function are more obvious, although and reference substance transdermal dehydration in 60min all has the reduction of similarity degree, but the reduction amplitude is significantly less than collagen dew of the present invention behind the 60min, illustrate that collagen of the present invention reveals the transdermal moisture evaporation that can effectively reduce skin, improve or repair the barrier function of skin, skin is had direct or indirect moistening effect.
Embodiment 8, cosmetic result test
8.1 test crowd
Number: 30 people, label 1-30
Age: between 20～40 years old
Sex: women 24 people, male 6 people
Health status: experimenter's skin health, without the dermatosis allergies
8.2 select tested position
Because extremity comparatively speaking do not have individual differences, select as tested position, choose examinee's the inboard 3cm of left and right forearm * 3cm area as tested district.It is inboard that trial target is coated in left and right forearm immediately.
8.3 below 20 ± 2 ℃, relative humidity (RH) is below 50 ± 5% in room temperature for test condition
8.4 instrument and reagent
Corneometer one cover, one of Hygrothermograph
Trial target: embodiment 1 prepared collagen reveals
8.4 testing experiment
8.4.1 short term tests result:
When judging the moistening effect intensity of moisture-keeping cosmetics, the suitable primary coating of doing to finish in the short time is tested, i.e. the performance of keeping humidity certificate test.
With adding organism cuticlar water stress test in the test of 1 coating mensuration of moisture-keeping cosmetics short-term horny layer moisture content, can resolve moistening effect.This law determines whether it has moisture retention when being mainly used in selecting wetting agent in the prescription, and wetting agent and substrate relatively determine optimum concentration.
8.4.1.1 before the makeup application, measure the horny layer moisture content at tested position.
8.4.1.2 with latex finger cot with sample with 1.25L/cm
2The coating of coating even density; Instant, the horny layer moisture content after 15,30,45,60,75,90,105,120 minutes after the coating of determination test product; The horny layer moisture content of respectively being tested the position is got the meansigma methods of 5 measured values; Measurement result sees Table 1, table 2.
The skin beauty water of the front 15 bit test person different times of table 1. is right
| Time min | 001 | 002 | 003 | 004 | 005 | 006 | 007 | 010 | 013 | 014 | 015 |
| Contrast | 23.08 | 19.04 | 25.38 | 28.86 | 34.16 | 17.86 | 30.70 | 29.94 | 35.40 | 42.20 | 23.26 |
| 0 | 58.25 | 65.46 | 100.00 | 80.92 | 75.84 | 60.54 | 74.70 | 43.68 | 73.26 | 85.00 | 67.36 |
| 15 | 45.29 | 39.22 | 63.95 | 45.98 | 56.82 | 48.74 | 50.90 | 40.32 | 39.04 | 58.44 | 65.46 |
| 30 | 32.90 | 33.22 | 39.56 | 39.12 | 48.34 | 35.30 | 40.10 | 30.36 | 45.92 | 47.42 | 39.44 |
| 45 | 30.56 | 32.58 | 49.12 | 33.02 | 38.78 | 36.04 | 41.50 | 35.90 | 42.42 | 39.44 | 37.74 |
| 60 | 29.12 | 30.88 | 45.28 | 31.42 | 36.72 | 31.78 | 36.40 | 33.88 | 39.18 | 39.72 | 37.14 |
| 75 | 32.28 | 29.04 | 33.68 | 32.48 | 34.74 | 29.42 | 36.40 | 32.08 | 33.88 | 36.42 | 39.88 |
| 90 | 33.06 | 30.90 | 45.56 | 35.56 | 29.94 | 32.40 | 33.OO | 42.28 | 39.64 | 35.60 | ? |
| 105 | 34.70 | 31.64 | 40.48 | 33.76 | 38.80 | ? | ? | 39.26 | 38.28 | ? | ? |
Annotate: blank expression missed should the time test.
The right raising degree of 15 bit test persons different time skin beauty water in 120min behind the table 2.
| Time min | 016 | 017 | 018 | 019 | 020 | 021 | 022 | 025 | 028 | 029 | 030 |
| Contrast | 0.00 | 0.00 | O.00 | 0.00 | 0.00 | 0.00 | 0.00 | 0.OO | 0.00 | O.00 | 0.00 |
| 0 | 1.01 | 2.60 | 2.68 | 1.90 | 1.52 | 2.33 | 1.36 | 0.09 | O.91 | 0.92 | 1.47 |
| 15 | O.80 | 1.52 | 1.53 | 0.95 | 0.18 | 1.97 | 0.89 | O.2l | -O.12 | 0.15 | 1.38 |
| 30 | 0.65 | 1.84 | 1.52 | 0.45 | O.19 | O.92 | 0.05 | 0.1l | 0.20 | 0.10 | 0.35 |
| 45 | O.56 | 1.65 | 1.90 | 0.06 | 0.17 | 0.93 | -0.01 | 0.10 | 0.08 | -0.04 | 0.19 |
| 60 | O.35 | 1.56 | 1.82 | O.33 | 0.27 | 0.91 | 0.08 | -0.10 | -O.03 | -0.03 | 0.17 |
| 75 | 0.49 | 1.47 | 1.33 | O.01 | 0.22 | 0.85 | O.17 | O.07 | -O.08 | -0.06 | 0.28 |
| 90 | 0.45 | 1.69 | 1.65 | 0.29 | O.24 | 1.06 | 0.27 | 0.17 | 0.10 | -0.06 | 0.10 |
| 105 | 0.51 | 1.60 | 1.80 | ? | ? | ? | 0.29 | 0.23 | 0.15 | 0.19 | 0.13 |
Annotate: blank expression missed should the time test.
The right raising degree of skin beauty water=(right (during the test)-skin beauty water of skin beauty water right (contrast))/right (contrast) * 100% of skin beauty water
8.4.1.3 the short-term moistening effect of trial target
Can be found out by table 1,2, the degree of hydration that collagen reveals skin is significantly improved, particularly after use in the time range of 0～45min, prolongation along with the time, moistening effect decreases, still have obvious raising but (105min) skin beauty water is right in the testing time scope, illustrate that this collagen reveals and has obvious moistening effect, the right raising degree of skin beauty water is up to 180%.
8.4.2 long-term effect test
For the direct moistening effect of moisture-keeping cosmetics, the long-term service tests such as the impact that the cuticular seasonal variety of suitable work long-time observation organism gives and the metamorphosis of skin surface.
8.4.2.1 before the makeup application, measure the horny layer moisture content at tested position.
8.4.2.2 with latex finger cot with trial target with 1.25L/cm
2The coating of coating even density; Smeared in right amount cosmetics at WA with before going to bed by being tested the position every day.The time of smearing was 6 weeks.
8.4.2.3 the horny layer moisture content in l week before measuring respectively makeup application, after the coating, 2 weeks, 3 weeks, 4 weeks, 5 all and 6 weeks; Each is tested the horny layer moisture content at position and is got mensuration 5 times, gets its meansigma methods; Measurement result sees Table 2.
The skin beauty water of 15 bit test person different times is right behind the table l.
| Time week | 17 | 18 | 20 | 21 | 22 | 23 | 25 | 26 | 27 | 29 | 30 |
| Contrast | 20.9 | 19.8 | 27.38 | 28.32 | 33.6 | 19.6 | 21.06 | 29.94 | 31.4 | 22.2 | 18.28 |
| 1 | 38.5 | 37.24 | 35.92 | 38.38 | 28.34 | 29.42 | 29.94 | 38.6 | 28.8 | ? | ? |
| 2 | 38.7 | 30.7 | 36.56 | 39.82 | 43：22 | 29.36 | 39.62 | 35.9 | 37.84 | 34.22 | 21.3 |
| 3 | 39.5 | 38.7 | 36.34 | 36.38 | ? | ? | 40.96 | 33.4 | 18.56 | 39.22 | 29.34 |
| 4 | 38.7 | 29.2 | 45.7 | 39.78 | 39.4 | 39.32 | 38.76 | 37.4 | 41.12 | 27.08 | ? |
| 5 | 33.8 | ? | ? | ? | 38.08 | 38.4 | 37.16 | 30.08 | 31.4 | 49.08 | 38.88 |
| 6 | 35.1 | 30.3 | 40.6 | 43.3 | 39.6 | 36.6 | 39.6 | 36.1 | 37.8 | 24.4 | ? |
Annotate: blank expression experimenter tests the same day and goes out, and does not have test.
The right variation percentage ratio of the front 15 bit test person different time skin beauty waters of table 2.
| Time week | Ol | 02 | 03 | 04 | 05 | 06 | 07 | 10 | 13 | 14 | 15 |
| |
0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 |
| 1 | 0.8 | 0.7 | 0.9 | 0.6 | 0.5 | 0.6 | 0.6 | 0.9 | 0.9 | ? | 0.90 |
| 2 | 0.95 | 0.85 | 0.95 | 0.75 | 0.45 | 0.85 | 0.88 | 0.95 | 1.00 | ? | 0.90 |
| 3 | 0.55 | 0.95 | 1.25 | 0.65 | 0.55 | 0.65 | 0.84 | 0.95 | 1.05 | 0.85 | ? |
| 4 | O.65 | O.85 | 1.65 | O.85 | O.95 | O.75 | O.88 | 1.00 | 1.05 | O.95 | ? |
| 5 | O.8 | O.8 | 1.8 | 1.0 | O.90 | O.92 | O.91 | 1.22 | ? | O.8 | O.90 |
| 6 | O.77 | O.87 | 1.77 | 1.25 | O.88 | O.89 | O.90 | 1.35 | 1.20 | O.90 | O.90 |
Annotate: blank expression experimenter tests the same day and goes out, and does not have test.
The right raising degree of skin beauty water=(right (during the test)-skin beauty water of skin beauty water right (contrast))/right (contrast) * 100% of skin beauty water
8.4.2.4 the long-term moistening effect of trial target
Can be found out by table 1,2, the degree of hydration that collagen of the present invention reveals skin is significantly improved, the final degree of hydration that improves skin reaches 30%, and (6 week) skin beauty water is right in the testing time scope is in the increase stage always, illustrate that this collagen dew has obvious moistening effect, the right raising degree of skin beauty water is up to 177%.And this collagen reveals through the long-term generation that effectively prevents wrinkle on probation, has delayed skin aging, allows skin open up existing youthful vigor and gloss.
The above only is embodiments of the invention; be not so limit claim of the present invention; every equivalent structure or equivalent flow process conversion that utilizes description of the present invention to do; or directly or indirectly be used in other relevant technical fields, all in like manner be included within the scope of patent protection of the present invention.
Claims (10)
1. one kind has moisturizing and composes the collagen dew of living and nourishing, it is characterized in that, comprise glycerol, butanediol, dipropylene glycol, propylene glycol, trehalose, betanin, colostrum, hydrolytic collagen, phospholipid, xanthan gum, pyridoxin, Anjidew NL50, sodium lactate, Beta-glucose, polysorbate 20, polyoxyethylene sorbitan monoleate, imidazolidinyl urea, iodine propilolic alcohol butyl mephenesin Carbamate, EDETATE SODIUM, essence and pure water.
2. collagen as claimed in claim 1 reveals, it is characterized in that, following composition is according to the percetage by weight meter: glycerol 2%～8%, butanediol 0.2%～1%, dipropylene glycol 0.1%～1%, propylene glycol 0.5%～1.5%, trehalose 0.1%～0.5%, betanin 0.1%～0.8%, colostrum 0.05%～0.2%, hydrolytic collagen 0.1%～0.5%, phosphatidase 10 .05%～0.2%, xanthan gum 0.1%～0.5%, pyridoxin 0.05%～0.2%, Anjidew NL50 0.05%～0.2%, sodium lactate 0.05%～0.2%, Beta-glucose 0.05%～0.2%, polysorbate 20 0.05%～0.2%, polyoxyethylene sorbitan monoleate 0.05%～0.2%, imidazolidinyl urea 0.05%～0.2%, iodine propilolic alcohol butyl mephenesin Carbamate 0.05%～0.2%, EDETATE SODIUM 0.05%～0.2%, essence 0.05%～0.2%, surplus are pure water.
3. collagen as claimed in claim 2 reveals, it is characterized in that, percent meter by weight: glycerol 5%, butanediol 0.6%, dipropylene glycol 0.5%, propylene glycol 1%, trehalose 0.2%, betanin 0.3%, colostrum 0.1%, hydrolytic collagen 0.2%, phosphatidase 10 .1%, xanthan gum 0.2%, pyridoxin 0.1%, Anjidew NL50 0.1%, sodium lactate 0.1%, Beta-glucose 0.1%, polysorbate 20 0.1%, polyoxyethylene sorbitan monoleate 0.1%, imidazolidinyl urea 0.1%, iodine propilolic alcohol butyl mephenesin Carbamate 0.1%, EDETATE SODIUM 0.1%, essence 0.1%, surplus is pure water.
4. collagen as claimed in claim 3 reveals, and it is characterized in that, the specification that this collagen reveals is 120mL.
5. collagen as claimed in claim 3 reveals, and it is characterized in that, the specification that this collagen reveals is 500mL.
6. the preparation method that the described collagen of claim 1-5 reveals is characterized in that, this preparation method may further comprise the steps:
1. add to add ENTA-2Na at pure water, be stirred to fully dissolving after, add PVC sodium, sodium lactate, to complete swelling, add polysorbate 20, polyoxyethylene sorbitan monoleate, heating up is stirred to fully dissolving, is incubated 20 minutes;
2. add the Beta-glucose, be stirred to fully dissolving; Add again butanediol and hydrolytic collagen and stir to fully dissolving, obtain component A;
3. xanthan gum is joined in the glycerol, be stirred to fully dissolving, form glycerol mixture; Glycerol mixture is joined among the component A, stir, temperature rises to 80 ℃, obtains B component;
4. dipropylene glycol, trehalose, betanin, colostrum, phospholipid and pyridoxin are mixed, heated and stirred is dissolved to 80 ℃ fully, obtains component C;
5. under the stirring state, in B component, add component C, stir, be incubated 20 minutes, begin cooling, temperature adds propylene glycol after being down to 60 ℃, add imidazolidinyl urea and iodine propilolic alcohol butyl mephenesin Carbamate, essence below 45 ℃, stir, be cooled to room temperature and get final product.
7. the described collagen of the claim 1-6 application of revealing is characterized in that, during special and professional care, can apply to collagen mask moistening, massage bottoming, sound wave is beautiful treats.
8. the application that the described collagen of claim 1-6 reveals is characterized in that, during nursing at home, then can be used as the nutrition astringent of potent moisturizing.
9. the application that the described collagen of claim 1-6 reveals is characterized in that, this collagen reveals and is suitable for any skin.
10. the application that the described collagen of claim 1-6 reveals is characterized in that, this collagen reveals the skin that is suitable for hydropenia, dryness, aging, wrinkle to be used.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104187474A (en) * | 2014-08-27 | 2014-12-10 | 金湘范 | Original juice of sprout and seedling plant as well as preparation method and application of original juice |
| CN104666236A (en) * | 2015-02-13 | 2015-06-03 | 安婕妤化妆品科技股份有限公司 | Moisturizing skincare mask |
| US10251833B2 (en) * | 2014-07-11 | 2019-04-09 | Mary Kay Inc. | Pore minimizer |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1878531A (en) * | 2003-11-06 | 2006-12-13 | 荷兰联合利华有限公司 | Improved cosmetic composition comprising vitamin b3, vitamin b6 and an organic acid |
| CN101190174A (en) * | 2006-12-01 | 2008-06-04 | 高宝化妆品（中国）有限公司 | Moisture-keeping crease-shedding skin-care cream and preparation method thereof |
| CN101966135A (en) * | 2010-09-30 | 2011-02-09 | 江苏隆力奇生物科技股份有限公司 | Toning lotion and preparation method thereof |
| CN102048654A (en) * | 2010-12-22 | 2011-05-11 | 曹才建 | Skin aging-resisting stock solution |
| CN102349863A (en) * | 2011-11-01 | 2012-02-15 | 广东海洋大学 | Preparation method of algal polysaccharides toner |
| CN102462640A (en) * | 2010-11-20 | 2012-05-23 | 上海海洋大学 | Ocean fish skin collagen hydrating and anti-aging cosmetic and preparation method thereof |
| CN102988216A (en) * | 2012-11-30 | 2013-03-27 | 兰晶 | Moisturizing and anti-allergic emulsion |
-
2013
- 2013-06-27 CN CN201310264259.2A patent/CN103301054B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1878531A (en) * | 2003-11-06 | 2006-12-13 | 荷兰联合利华有限公司 | Improved cosmetic composition comprising vitamin b3, vitamin b6 and an organic acid |
| CN101190174A (en) * | 2006-12-01 | 2008-06-04 | 高宝化妆品（中国）有限公司 | Moisture-keeping crease-shedding skin-care cream and preparation method thereof |
| CN101966135A (en) * | 2010-09-30 | 2011-02-09 | 江苏隆力奇生物科技股份有限公司 | Toning lotion and preparation method thereof |
| CN102462640A (en) * | 2010-11-20 | 2012-05-23 | 上海海洋大学 | Ocean fish skin collagen hydrating and anti-aging cosmetic and preparation method thereof |
| CN102048654A (en) * | 2010-12-22 | 2011-05-11 | 曹才建 | Skin aging-resisting stock solution |
| CN102349863A (en) * | 2011-11-01 | 2012-02-15 | 广东海洋大学 | Preparation method of algal polysaccharides toner |
| CN102988216A (en) * | 2012-11-30 | 2013-03-27 | 兰晶 | Moisturizing and anti-allergic emulsion |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10251833B2 (en) * | 2014-07-11 | 2019-04-09 | Mary Kay Inc. | Pore minimizer |
| US11033487B2 (en) | 2014-07-11 | 2021-06-15 | Mary Kay Inc. | Pore minimizer |
| US11833243B2 (en) | 2014-07-11 | 2023-12-05 | Mary Kay Inc. | Pore minimizer |
| CN104187474A (en) * | 2014-08-27 | 2014-12-10 | 金湘范 | Original juice of sprout and seedling plant as well as preparation method and application of original juice |
| CN104666236A (en) * | 2015-02-13 | 2015-06-03 | 安婕妤化妆品科技股份有限公司 | Moisturizing skincare mask |
| CN104666236B (en) * | 2015-02-13 | 2016-02-17 | 安婕妤化妆品科技股份有限公司 | A kind of preserving moisture and protecting skin facial film |
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|---|---|
| CN103301054B (en) | 2014-03-26 |
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