CN103274587A - Glass strengthening method and preparation method of OGS (one glass solution) touch screen - Google Patents
Glass strengthening method and preparation method of OGS (one glass solution) touch screen Download PDFInfo
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- CN103274587A CN103274587A CN2013102310474A CN201310231047A CN103274587A CN 103274587 A CN103274587 A CN 103274587A CN 2013102310474 A CN2013102310474 A CN 2013102310474A CN 201310231047 A CN201310231047 A CN 201310231047A CN 103274587 A CN103274587 A CN 103274587A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/50—Glass production, e.g. reusing waste heat during processing or shaping
- Y02P40/57—Improving the yield, e-g- reduction of reject rates
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Abstract
The invention relates to a glass strengthening method which comprises the steps as follows: a cation exchange method is adopted for primary strengthening treatment on glass to be strengthened, wherein the radius of the cation participating in exchange is larger than that of the sodion; the outer peripheral edge part of the glass after primary strengthening treatment is subjected to polishing treatment; and acid-proof films are attached to the upper and lower surfaces of the glass after the polishing treatment, and the glass is placed in an aqueous solution containing hydrofluoric acid for secondary strengthening treatment. The glass strengthening method can increase the strength of the glass effectively. Besides, the invention further provides a preparation method of touch screen glass.
Description
Technical field
The present invention relates to the glass processing technical field, particularly relate to the preparation method of a kind of glass reinforced method and OGS touch-screen.
Background technology
In order effectively to reduce the touch-control module cost, satisfy the lightening market trend of terminal consumption electronic product simultaneously, greatly develop the OGS technology in the industry.The OGS technology refers to directly form the technology of ITO conducting film and sensor on protective glass, a glass plays the dual function of protective glass and touch sensor simultaneously.The G/G touch technology that the OGS technology is more traditional has a lot of advantages, as, can save a slice glass substrate, can save one bonding process on the production process, thereby be conducive to reduce production costs, improve the product yield.And adopt about the thickness little 0.4mm of the electronic product that obtains than the electronic product that adopts the G/G touch technology to obtain of OGS technology, thereby make electronic product satisfy market to lightening requirement.
The intensity of protective glass is very important for electronic product; though and the surface of glass seems very complete very smooth, in fact there is a large amount of tiny cracks, particularly the glass through cutting; there is a large amount of tiny cracks in its incision, and tiny crack can cause glass intensity to reduce greatly.Therefore, need carry out intensive treatment to strengthen the intensity of protective glass to protective glass.But traditional enhancement method is desirable not enough to the intensity that strengthens protective glass.
Summary of the invention
Based on this, be necessary to provide a kind of glass reinforced method of effectively reinforcing glass intensity.
A kind of glass reinforced method comprises the steps:
The glass that adopts base exchange method to treat intensive treatment carries out primary reinforcement to be handled, and wherein, participates in the cationic radius of exchange greater than the radius of sodium ion;
Outer peripheral edge portion to the described glass after handling through primary reinforcement is carried out polished finish;
Two surfaces up and down at the described glass after polished finish attach anti-sorrel, carry out the secondary intensive treatment in the aqueous solution of hydrofluoric acid.
Therein among embodiment, in described primary reinforcement treating processes, when the cationite that adopts is the saltpetre fused solution, described glass is soaked in handled in the saltpetre fused solution 6~7 hours, wherein, the temperature of saltpetre fused solution is 400~450 ℃.
Therein among embodiment, in described primary reinforcement treating processes, when the cationite that adopts is the saltpetre fused solution, two surfaces up and down at glass apply saltpetre fusion liquid layer, then, be placed on and strengthen in the stove, in 400~450 ℃ of following intensive treatment 6~7 hours.
Among embodiment, the reinforcement degree of depth that the primary reinforcement of described glass is handled is 20 μ m therein.
Among embodiment, described glass also comprises the step that described glass is cleaned after primary reinforcement is handled therein.
Among embodiment, the step of described cleaning is specially therein: adopt ultrapure water that described glass is carried out spray Cleaning for High Capacity earlier, adopt ultrapure water that described glass is carried out ultrasonic cleaning then.
Above-mentioned glass reinforced method is utilized base exchange method that glass is carried out primary reinforcement and is handled, make the bigger positively charged ion of radius occupy the position of the less sodium ion of radius, thereby change the composition of glass surface, reach the purpose of eliminating the glass surface tiny crack, make the internal structure of glass join more closely, form higher bearing stress, thereby reach the purpose of reinforcing glass intensity.Outer peripheral edge portion (the normally cut out portion of glass) to glass is carried out the tiny crack that the outer peripheral edges place of glass can be effectively eliminated in polished finish, realizes the purpose of reinforcing glass intensity.Further, adopt hydrofluoric acid that the outer peripheral edge portion of glass is carried out the secondary intensive treatment, destroy the silica film of outer peripheral edge portion, make the tiny crack of outer peripheral edge portion uniformly by etching off, or make crest truncation, the radius-of-curvature of tiny crack become big, thereby reduce the stress concentration phenomenon, further strengthen the intensity of glass.Above-mentioned glass reinforced method adopts base exchange method, polished finish and hydrofluoric acid corroding method that glass is strengthened comprehensively and effectively, and therefore, above-mentioned glass reinforced method is the intensity of reinforcing glass effectively.
A kind of preparation method of OGS touch-screen comprises the steps:
The glass that adopts base exchange method to treat intensive treatment carries out primary reinforcement to be handled, and wherein, participates in the cationic radius of exchange greater than the radius of sodium ion;
One side of the described glass after handling through primary reinforcement is made the ITO pattern;
The described glass that is manufactured with the ITO pattern is cut;
Outer peripheral edge portion to the described glass after cutting process is carried out polished finish;
Two surfaces up and down at the described glass after polished finish attach anti-sorrel, carry out the secondary intensive treatment in hydrofluoric acid solution.
Therein among embodiment, in described cutting process, when the glass of the described ITO of being manufactured with pattern is rectangle and size when conforming to OGS touch-screen size, the rounding cutting is carried out at four angles of the glass of the described ITO of being manufactured with pattern.
Therein among embodiment, in described cutting process, when the size of the glass of the described ITO of being manufactured with pattern does not conform to OGS touch-screen size, glass to the described ITO of being manufactured with pattern tentatively cuts the rectangle intermediates that are met OGS touch-screen size, again the rounding cutting is carried out at four angles of described intermediates.
Among embodiment, described tentatively being cut into adopts diamond custting machine to cut therein, and described rounding is cut into the CNC cutting.
The OGS touch-screen for preparing by the preparation method of above-mentioned OGS touch-screen has intensity and light transmission preferably preferably, is not easy breakage, has long work-ing life.
Description of drawings
Fig. 1 is the schema of the glass reinforced method of an embodiment;
Fig. 2 is preparation method's the schema of the OGS touch-screen of an embodiment;
Fig. 3 is for carrying out the procedure chart of cutting step to glass among Fig. 2.
Embodiment
Preparation method to glass reinforced method and OGS touch-screen is further detailed below in conjunction with accompanying drawing.
As shown in Figure 1, the glass reinforced method of an embodiment comprises the steps:
Step S110, the glass that adopts base exchange method to treat intensive treatment carry out primary reinforcement to be handled, and wherein, participates in the cationic radius of exchange greater than the radius of sodium ion.
The glass for the treatment of intensive treatment is silicate glass, and it contains sodium ion.In the present embodiment, glass is the corning glass that is used for touch-screen that Corning Incorporated produces.Certainly, glass can be the Asahi Glass glass that is used for touch-screen that Asahi Glass glass limited-liability company produces.
Owing to contain the sodium ion of positive monovalence in the glass, thereby the positively charged ion that participates in exchange is preferably the potassium ion that is all alkali-metal positive monovalence.Be appreciated that participating in the cationic of exchange can be other positively charged ions, as the rubidium ion of positive monovalence.
In the present embodiment, in the primary reinforcement treating processes, the cationite that adopts is the saltpetre fused solution, glass is soaked in handled in the saltpetre fused solution 6~7 hours, wherein, the temperature of saltpetre fused solution is 400~450 ℃, and the temperature of saltpetre fused solution is lower than the second-order transition temperature of glass (Tg).Aforesaid method can obtain the result of intensive treatment preferably in the short period of time, has higher industrialization production efficiency.The saltpetre fused solution also can be for the fused solution of other salt close with the saltpetre fusing point, as the fused solution of rubidium nitrate.
Be appreciated that in other embodiments, in the primary reinforcement treating processes, the cationite that adopts can be the saltpetre fused solution, applies saltpetre fusion liquid layer on two surfaces up and down of glass, then, be placed on and strengthen in the stove, in 400~450 ℃ of following intensive treatment 6~7 hours.
In the present embodiment, the reinforcement degree of depth that the primary reinforcement of glass is handled is preferably 20 μ m, can eliminate the tiny crack of glass surface preferably, does not influence the original performance of glass again, as, the light transmission of glass.
In the present embodiment, glass also comprises the step that glass is cleaned after primary reinforcement is handled.The step of cleaning is specially: adopt ultrapure water that glass is carried out spray Cleaning for High Capacity earlier, adopt ultrapure water that glass is carried out ultrasonic cleaning then, farthest remove and be attached to saltpetre on glass.
Step S120 carries out polished finish to the outer peripheral edge portion of the glass after handling through primary reinforcement.
Outer peripheral edge portion (the normally cut out portion of glass) to glass is carried out the tiny crack that the outer peripheral edges place of glass can be effectively eliminated in polished finish, realizes the purpose of reinforcing glass intensity.
Step S130 attaches anti-sorrel on two surfaces up and down of the glass after polished finish, carries out the secondary intensive treatment in the aqueous solution of hydrofluoric acid.
Adopt hydrofluoric acid that the outer peripheral edge portion of glass is carried out the secondary intensive treatment, destroy the silica film of outer peripheral edge portion, make the tiny crack of outer peripheral edge portion uniformly by etching off, or make crest truncation, the radius-of-curvature of tiny crack become big, thereby reduce the stress concentration phenomenon, further strengthen the intensity of glass.
The time of secondary intensive treatment can not be too short, can not be long.The time of secondary intensive treatment is too short, and strengthening effect may be undesirable.The overlong time of secondary intensive treatment, hydrofluoric acid may pass through osmosis, enters between anti-sorrel and the glass surface, and then the etching glass surface.And the time of secondary intensive treatment is relevant with the concentration of the aqueous solution of hydrofluoric acid.Therefore, in the present embodiment, the massfraction of hydrofluoric acid is preferably 5%~40%, and the time of secondary intensive treatment is preferably 5~20 minutes.
Above-mentioned glass reinforced method is utilized base exchange method that glass is carried out primary reinforcement and is handled, make the bigger positively charged ion of radius occupy the position of the less sodium ion of radius, thereby change the composition of glass surface, reach the purpose of eliminating the glass surface tiny crack, make the internal structure of glass join more closely, form higher bearing stress, thereby reach the purpose of reinforcing glass intensity.Outer peripheral edge portion (the normally cut out portion of glass) to glass is carried out the tiny crack that the outer peripheral edges place of glass can be effectively eliminated in polished finish, realizes the purpose of reinforcing glass intensity.Further, adopt hydrofluoric acid that the outer peripheral edge portion of glass is carried out the secondary intensive treatment, destroy the silica film of outer peripheral edge portion, make the tiny crack of outer peripheral edge portion uniformly by etching off, or make crest truncation, the radius-of-curvature of tiny crack become big, thereby reduce the stress concentration phenomenon, further strengthen the intensity of glass.Above-mentioned glass reinforced method adopts base exchange method, polished finish and hydrofluoric acid corroding method that glass is strengthened comprehensively and effectively, and therefore, above-mentioned glass reinforced method is the intensity of reinforcing glass effectively.
As shown in Figure 2, present embodiment also provides a kind of preparation method of OGS touch-screen, comprises the steps:
Step S210, the glass that adopts base exchange method to treat intensive treatment carry out primary reinforcement to be handled, and wherein, participates in the cationic radius of exchange greater than the radius of sodium ion.
Step S220, a side of the glass after handling through primary reinforcement is made ITO(Single ITO, individual layer ITO) pattern.
Step S230 cuts the glass that is manufactured with the ITO pattern.
As shown in Figure 3, in the present embodiment, the size that is manufactured with the glass 320 of ITO pattern does not conform to OGS touch-screen size, need earlier the glass 320 that is manufactured with the ITO pattern tentatively to be cut the rectangle intermediates 330 that are met OGS touch-screen size, again the rounding cutting is carried out at four angles of middle product, obtained the product 350 of well cutting.Wherein, tentatively be cut into and adopt diamond custting machine 310 that it is cut, rounding is cut into CNC cutting (Computer numerical control, numerically-controlled machine) 340.Wherein, the process of CNC cutting is: adopt four angles of the sharpening abrading glass of high speed rotating, and spray water in grinding place.
Being appreciated that in other embodiments, is that rectangle and size conform to OGS touch-screen size if be manufactured with the glass of ITO pattern, only need carry out the rounding cutting to four angles of the glass that is manufactured with the ITO pattern.
Step S240 carries out polished finish to the outer peripheral edge portion of the glass after cutting process.
In the present embodiment, preferably whole outer peripheral edge portion of the glass after cutting process are carried out polished finish.Certainly, also can be only to carrying out polished finish because the rounding cutting produces otch.
Step S250 attaches anti-sorrels on two surfaces up and down through the glass of polished finish, carries out the secondary intensive treatment in hydrofluoric acid solution.
Among the preparation method of above-mentioned OGS touch-screen with above-mentioned glass reinforced method in corresponding step all identical.The OGS touch-screen for preparing by the preparation method of above-mentioned OGS touch-screen has intensity and light transmission preferably preferably, is not easy breakage, has long work-ing life.
The above embodiment has only expressed several embodiment of the present invention, and it describes comparatively concrete and detailed, but can not therefore be interpreted as the restriction to claim of the present invention.Should be pointed out that for the person of ordinary skill of the art without departing from the inventive concept of the premise, can also make some distortion and improvement, these all belong to protection scope of the present invention.Therefore, the protection domain of patent of the present invention should be as the criterion with claims.
Claims (10)
1. a glass reinforced method is characterized in that, comprises the steps:
The glass that adopts base exchange method to treat intensive treatment carries out primary reinforcement to be handled, and wherein, participates in the cationic radius of exchange greater than the radius of sodium ion;
Outer peripheral edge portion to the described glass after handling through primary reinforcement is carried out polished finish;
Two surfaces up and down at the described glass after polished finish attach anti-sorrel, carry out the secondary intensive treatment in the aqueous solution of hydrofluoric acid.
2. glass reinforced method according to claim 1, it is characterized in that, in described primary reinforcement treating processes, when the cationite that adopts is the saltpetre fused solution, described glass is soaked in handled in the saltpetre fused solution 6~7 hours, wherein, the temperature of saltpetre fused solution is 400~450 ℃.
3. glass reinforced method according to claim 1, it is characterized in that, in described primary reinforcement treating processes, when the cationite that adopts is the saltpetre fused solution, two surfaces up and down at glass apply saltpetre fusion liquid layer, then, be placed on and strengthen in the stove, in 400~450 ℃ of following intensive treatment 6~7 hours.
4. according to claim 2 or 3 described glass reinforced methods, it is characterized in that the reinforcement degree of depth that the primary reinforcement of described glass is handled is 20 μ m.
5. glass reinforced method according to claim 1 is characterized in that, described glass also comprises the step that described glass is cleaned after primary reinforcement is handled.
6. glass reinforced method according to claim 5 is characterized in that, the step of described cleaning is specially: adopt ultrapure water that described glass is carried out spray Cleaning for High Capacity earlier, adopt ultrapure water that described glass is carried out ultrasonic cleaning then.
7. the preparation method of an OGS touch-screen is characterized in that, comprises the steps:
The glass that adopts base exchange method to treat intensive treatment carries out primary reinforcement to be handled, and wherein, participates in the cationic radius of exchange greater than the radius of sodium ion;
One side of the described glass after handling through primary reinforcement is made the ITO pattern;
The described glass that is manufactured with the ITO pattern is cut;
Outer peripheral edge portion to the described glass after cutting process is carried out polished finish;
Two surfaces up and down at the described glass after polished finish attach anti-sorrel, carry out the secondary intensive treatment in hydrofluoric acid solution.
8. the preparation method of OGS touch-screen according to claim 7, it is characterized in that, in described cutting process, when the glass of the described ITO of being manufactured with pattern is rectangle and size when conforming to OGS touch-screen size, the rounding cutting is carried out at four angles of the glass of the described ITO of being manufactured with pattern.
9. the preparation method of OGS touch-screen according to claim 7, it is characterized in that, in described cutting process, when the size of the glass of the described ITO of being manufactured with pattern does not conform to OGS touch-screen size, glass to the described ITO of being manufactured with pattern tentatively cuts the rectangle intermediates that are met OGS touch-screen size, again the rounding cutting is carried out at four angles of described intermediates.
10. the preparation method of OGS touch-screen according to claim 9 is characterized in that, described tentatively being cut into adopts diamond custting machine to cut, and described rounding is cut into the CNC cutting.
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Cited By (14)
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CN103482858A (en) * | 2013-09-05 | 2014-01-01 | 江西沃格光电科技有限公司 | Secondary strengthening method of toughened glass |
CN103482859A (en) * | 2013-09-05 | 2014-01-01 | 江西沃格光电科技有限公司 | Method for preparing chemical toughened glass |
CN103626401A (en) * | 2013-12-03 | 2014-03-12 | 汕头超声显示器(二厂)有限公司 | Touch screen glass chemical secondary strengthening method |
CN104598065A (en) * | 2013-10-30 | 2015-05-06 | 达鸿先进科技股份有限公司 | Touch panel process method, touch panel structure and touch device thereof |
CN104669069A (en) * | 2013-12-03 | 2015-06-03 | 汕头超声显示器(二厂)有限公司 | Edge polishing method for OGS capacitive touch screen |
CN104944790A (en) * | 2014-03-31 | 2015-09-30 | 东友精细化工有限公司 | Glass-reinforcing composition and method of manufacturing touchscreen glass using the same |
CN105405742A (en) * | 2014-09-11 | 2016-03-16 | 深圳莱宝高科技股份有限公司 | Method for processing substrate |
CN105461232A (en) * | 2014-09-11 | 2016-04-06 | 深圳莱宝高科技股份有限公司 | Substrate treatment method |
CN106167357A (en) * | 2015-05-19 | 2016-11-30 | 旭硝子株式会社 | The manufacture method of chemically reinforced glass |
CN106495505A (en) * | 2016-09-29 | 2017-03-15 | 浙江星星科技股份有限公司 | A kind of intensifying method of fingerprint button glass |
CN106746633A (en) * | 2016-12-06 | 2017-05-31 | 巢湖市伟业玻璃有限公司 | For pressure-resistant high strength glass and preparation method on gas range display panel |
CN106775149A (en) * | 2016-12-02 | 2017-05-31 | 东莞市平波电子有限公司 | A kind of OGS touch screen and preparation method thereof |
CN107272954A (en) * | 2017-06-19 | 2017-10-20 | 合肥市惠科精密模具有限公司 | A kind of flexible touch screen |
CN113121125A (en) * | 2021-04-14 | 2021-07-16 | 万津实业(赤壁)有限公司 | Processing method for 2.5D float glass |
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CN103108842A (en) * | 2010-08-24 | 2013-05-15 | 康宁股份有限公司 | Method of strengthening edge of glass article |
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CN103108842A (en) * | 2010-08-24 | 2013-05-15 | 康宁股份有限公司 | Method of strengthening edge of glass article |
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CN103482859A (en) * | 2013-09-05 | 2014-01-01 | 江西沃格光电科技有限公司 | Method for preparing chemical toughened glass |
CN103482858A (en) * | 2013-09-05 | 2014-01-01 | 江西沃格光电科技有限公司 | Secondary strengthening method of toughened glass |
CN104598065A (en) * | 2013-10-30 | 2015-05-06 | 达鸿先进科技股份有限公司 | Touch panel process method, touch panel structure and touch device thereof |
CN104669069B (en) * | 2013-12-03 | 2017-04-26 | 汕头超声显示器(二厂)有限公司 | Edge polishing method for OGS capacitive touch screen |
CN103626401A (en) * | 2013-12-03 | 2014-03-12 | 汕头超声显示器(二厂)有限公司 | Touch screen glass chemical secondary strengthening method |
CN104669069A (en) * | 2013-12-03 | 2015-06-03 | 汕头超声显示器(二厂)有限公司 | Edge polishing method for OGS capacitive touch screen |
CN104944790A (en) * | 2014-03-31 | 2015-09-30 | 东友精细化工有限公司 | Glass-reinforcing composition and method of manufacturing touchscreen glass using the same |
TWI634198B (en) * | 2014-03-31 | 2018-09-01 | 東友精細化工有限公司 | Glass-reinforcing composition and method of manufacturing touchscreen glass using the same |
CN104944790B (en) * | 2014-03-31 | 2019-04-09 | 东友精细化工有限公司 | The composition of strengthened glass and the method for manufacturing touched panel glass with it |
CN105461232B (en) * | 2014-09-11 | 2019-04-16 | 深圳莱宝高科技股份有限公司 | A kind of substrate processing method using same |
CN105405742A (en) * | 2014-09-11 | 2016-03-16 | 深圳莱宝高科技股份有限公司 | Method for processing substrate |
CN105461232A (en) * | 2014-09-11 | 2016-04-06 | 深圳莱宝高科技股份有限公司 | Substrate treatment method |
CN105405742B (en) * | 2014-09-11 | 2020-04-14 | 深圳莱宝高科技股份有限公司 | Substrate processing method |
CN106167357A (en) * | 2015-05-19 | 2016-11-30 | 旭硝子株式会社 | The manufacture method of chemically reinforced glass |
CN106167357B (en) * | 2015-05-19 | 2020-07-03 | Agc株式会社 | Method for producing chemically strengthened glass |
CN106495505A (en) * | 2016-09-29 | 2017-03-15 | 浙江星星科技股份有限公司 | A kind of intensifying method of fingerprint button glass |
CN106775149A (en) * | 2016-12-02 | 2017-05-31 | 东莞市平波电子有限公司 | A kind of OGS touch screen and preparation method thereof |
CN106746633A (en) * | 2016-12-06 | 2017-05-31 | 巢湖市伟业玻璃有限公司 | For pressure-resistant high strength glass and preparation method on gas range display panel |
CN107272954A (en) * | 2017-06-19 | 2017-10-20 | 合肥市惠科精密模具有限公司 | A kind of flexible touch screen |
CN113121125A (en) * | 2021-04-14 | 2021-07-16 | 万津实业(赤壁)有限公司 | Processing method for 2.5D float glass |
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Application publication date: 20130904 |