CN103266028A - Lilac skincare liquid detergent - Google Patents
Lilac skincare liquid detergent Download PDFInfo
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- CN103266028A CN103266028A CN2013102073106A CN201310207310A CN103266028A CN 103266028 A CN103266028 A CN 103266028A CN 2013102073106 A CN2013102073106 A CN 2013102073106A CN 201310207310 A CN201310207310 A CN 201310207310A CN 103266028 A CN103266028 A CN 103266028A
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- lilac
- flos caryophylli
- liquid detergent
- detergent
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Abstract
The invention discloses a lilac skincare liquid detergent. The lilac skincare liquid detergent comprises the following raw materials in parts by weight: 4-6 parts of sodium lauroamphoacetate, 4-6 parts of coco-betaine, 2-4 parts of N,N-dimethyldecylamine-N-amine oxide, 5-7 parts of lauryl glucoside, 0.05-0.15 part of lilac extractive and 80 parts of water. According to the lilac skincare liquid detergent, nonionic surfactants and ampholytic surfactants are compounded, the conventional anionic surfactants are abandoned, the irritation on the surface of a hand is greatly reduced when the good decontamination and washing effects are guaranteed, and meanwhile, the compounded lilac extractive has pleasant aroma and an antibiosis function.
Description
Technical field:
The present invention relates to a kind of liquid detergent, particularly a kind of Flos Caryophylli skin-care detergent.
Background technology:
Liquid washing agent is a big class in the synthetic detergent, and the output maximum is washing powder in the synthetic detergent, and with fastest developing speed is liquid washing agent.Because liquid washing agent has many good qualities than solid detergent at aspects such as kind, performance, production technique, therefore manufacturing enterprise competitively develops both at home and abroad.
Liquid washing agent is that it has the characteristic of surfactant soln with water or other organic solvents articles for washing as base-material.The liquid product that generally will have cleaning function is called liquid washing agent.Be divided into liquid detergent, fabric liquid washing agent, shampoo and skin cleaner and hard surface cleaner according to purposes or function.
Liquid detergent is mainly used in wash dining set, tea set and kitchen tools etc.; Also can be used for washing fruit, vegetables and the heavy clothing of greasy dirt.It is the indispensable washing product of catering industry and family.
Dish washing detergent belongs to allotment type product, and development is very rapid at home in recent years.At present dish washing detergent on the market is a feast for the eyes, have superpower, that concentrated type is arranged and the strong sterilizing power of detersive power etc.Along with the progressively enhancing of people's environmental consciousness, dish washing detergent development in future direction will be to be main flow with the environment-friendly and green type.Except the function that strong detersive power, harmless, sterilization and disinfection, gentle high bubble are arranged, also should degrade easily, free from environmental pollution.The effective constituent of dish washing detergent mainly is tensio-active agent, and traditional dish washing detergent is raw material with synthetic surfactant (as LAS, AS, AES, SAS etc.) mainly.Maybe can't degrade but they are difficult for degraded mostly, environment is polluted.Therefore, exploitation environment-protection type tableware washing composition has been complied with the trend in epoch, and especially in Europe, the U.S. and Japan, the use of environment protecting tableware washing composition is quite general.But at home, the development of environment-protection type tableware washing composition is slower, and particularly functional liquid detergent is just fewer.
Summary of the invention:
At the prior art above shortcomings, technical problem to be solved by this invention provides a kind of Flos Caryophylli skin-care detergent.
Technical problem of the present invention is achieved by following technical proposals:
A kind of Flos Caryophylli skin-care detergent is made up of the raw material of following weight part: lauroyl both sexes guanidine-acetic acid sodium 4-6 part, coco betaine 4-6 part, N, N-dimethyl decyl-N-amine oxide 2-4 part, dodecyl glucoside 5-7 part, Flos Caryophylli extract 0.05-0.15 part, 80 parts in water.
With lauroyl both sexes guanidine-acetic acid sodium, coco betaine, N, N-dimethyl decyl-N-amine oxide, dodecyl glucoside and Flos Caryophylli extract are added to the water, and are heated to 40-60 ℃, mix, and can make this Flos Caryophylli skin-care detergent.
Below, raw material involved in the present invention is made simple introduction:
Lauroyl both sexes guanidine-acetic acid sodium, SODIUM LAUROAMPHOACETATE, CAS number: 156028-14-7.
Coco betaine, COCO-BETAINE, CAS number: 68424-94-2.
N, N-dimethyl decyl-N-amine oxide, English name 1-Decanamine, N, N-dimethyl-, N-oxide, CAS No.2605-79-0.
The dodecyl glucoside, CAS accession number: 110615-47-9.
The Flos Caryophylli extract, claim again: cloves (EUGENIA CARYOPHYLLUS) flower extract, the INCI title: EUGENIA CARYOPHYLLUS (CLOVE) FLOWER EXTRACT, on the books in " international makeup raw material standard Chinese catalogue (version in 2010) ".CAS accession number: 84961-50-2.Flos Caryophylli extract of the present invention can pass through commercially available getting, and also can adopt ordinary method preparation and gets.As: after the Flos Caryophylli pulverizing, add the deionized water of 6-10 times of weight, soaked 1-3 hour, ultrasonic extraction 10-15 minute, filter, centrifugal, discard precipitation with supernatant concentration, make the Flos Caryophylli extract, control Flos Caryophylli extract density is 1.02-1.08g/cm
3
Flos Caryophylli skin-care detergent of the present invention, adopt nonionogenic tenside and amphoterics composite, abandoned traditional anion surfactant, when guaranteeing good decontamination washing effect, greatly reduce the pungency to watch face, composite Flos Caryophylli extract of while, the pleasant aroma, and have anti-microbial effect.
Embodiment:
Following embodiment further specifies of the present invention, rather than limits the scope of the invention.In the present invention, if no special instructions, each raw material is 100% in working substance content all.
Embodiment 1
With 5 kilograms in lauroyl both sexes guanidine-acetic acid sodium, 5 kilograms of coco betaine, N, 0.1 kilogram of N-dimethyl decyl-3 kilograms of N-amine oxides, 6 kilograms of dodecyl glucosides and Flos Caryophylli extract add in 80 kilograms the deionized water, be heated to 50 ℃, mix, be cooled to room temperature, can make this liquid detergent.
Comparative Examples 1
0.1 kilogram of 13 kilograms in lauroyl both sexes guanidine-acetic acid sodium, 6 kilograms of dodecyl glucosides and Flos Caryophylli extract added in 80 kilograms the deionized water, be heated to 50 ℃, mix, be cooled to room temperature, can make this liquid detergent.
Comparative Examples 2
0.1 kilogram of 13 kilograms of coco betaine, 6 kilograms of dodecyl glucosides and Flos Caryophylli extract added in 80 kilograms the deionized water, be heated to 50 ℃, mix, be cooled to room temperature, can make this liquid detergent.
Comparative Examples 3
With N, 0.1 kilogram of N-dimethyl decyl-13 kilograms of N-amine oxides, 6 kilograms of dodecyl glucosides and Flos Caryophylli extract add in 80 kilograms the deionized water, are heated to 50 ℃, mix, and are cooled to room temperature, can make this liquid detergent.
Test case 1:
Detergency test:
1) preparation of artificial dirt
Mixing oil prescription: be the 0.5:0.5:1 preparation with butter, lard, vegetables oil mass ratio, and add the glyceryl monostearate of its total mass 5%, this is artificial dirt.
Artificial dirt put be heated to 180 ℃ on the electric furnace, stir and keep this temperature 10min, beaker is moved to magnetic stirrer stir, naturally cool to temperature required standby.The temperature of defiling is recommended reference: when room temperature is 20 ℃, need 80 ℃ of oil temperature; When room temperature is 25 ℃, need 45 ℃ of oil temperature; When room temperature is lower than 17 ℃ or when being higher than 27 ℃, test should not be carried out, and need carry out at air conditioning room.Should use the vertical spotter of attached freezing plant in case of necessity.
2) preparation of dirty sheet
With the slide glass upper edge 10mm line that draws, be limited in this below line to show to defile; With the slide glass lower edge 5mm line that draws, be limited in this below line to show the unnecessary greasy dirt of wiping.
3) newly purchase slide glass and need in detergent solution, boil 15min after, the clear water washing to do not hang the globule put again soak 1h in the acid wash liquid after, clear water rinsing and distilled water flushing are put after the loft drier drying standby.
4) preparation of standard dish washing detergent
Take by weighing 14 parts of sodium alkyl benzene sulfonates, 1 part of ethoxylated alkyl sulfate, 5 parts of dehydrated alcohols, 5 parts in urea adds water to 100 parts, and mixing is regulated pH to 7-8 with hydrochloric acid or sodium hydroxide, and is standby.
5) defile
The slide glass of cleaning is one group with four puts on the weighing frame, with analytical balance accurately weigh (accurately to 1mg) be m0, the slide glass after weighing is sandwiched on the film airing stand one by one, clip should be clipped in along the line on the slide glass more than, film airing stand put to ward off prepares in the dish to defile.
When treating that greasy dirt remains on definite temperature, one by one slide glass is taken off from film airing stand together with clip, hand-held clip immerses in the greasy dirt slide glass to 10mm goes up following (1-2) s along the line, slowly taking-up, after treating that the following speed of greasy dirt is slack-off, hang back and prepare dirty sheet on the original film airing stand successively.After greasy dirt solidifies, dirty sheet taken off with filter paper or absorbent cotton the unnecessary greasy dirt in base and both sides in the dirty sheet lower edge 5mm is wiped, speckle with the absorbent cotton wiped clean of sherwood oil again with the tweezers folder.After hanging 4h under the room temperature, on the weighing frame, be m1 with the accurate weighing of analytical balance.Dirty amount should guarantee (0.5 ± 0.05) g on every group of dirt this moment sheet.
6) testing sequence
The slide glass of the known amount of defiling is inserted preparation washing in the corresponding wash stand.
Spotter is connected power supply, and wash temperature is set to 30 ℃, and velocity of rotation is set to 160r/min, and washing time is set to 3min.
Take by weighing the 5.00g sample to be tested in 2500mL hard water; after shaking up; measure the 800mL test solution respectively in three washing becks of vertical spotter; when treating that the test solution temperature rises to 30 ℃; rapidly the dirty sheet of known weight is put into washing beck accordingly together with wash stand; after last wash stand is put into washing beck, begin to count soak time, rapidly agitator is installed simultaneously, when soaking 1min; start spotter; begin washing, during 3min, the machine auto stop; rapidly agitator is taken off; take out wash stand, press from both sides one by one and hang on the original film airing stand washing the dirty sheet in back, hanging and dirty sheet being put the weighing of corresponding weighing frame behind the 3h that dries in the air is m2.
(5) result represent to deoil rate ω=(m1-m2)/(m1-m0)
In the formula: m0---slide glass quality before defiling, g; M1---the back slide glass quality of defiling, g; M2---the quality of the dirty sheet in washing back, g.
The rate of deoiling test chart
| ? | The rate of deoiling ω, % |
| Embodiment 1 | 43.8 |
| The standard dish washing detergent | 38.2 |
| Comparative Examples 1 | 37.7 |
| Comparative Examples 2 | 38.1 |
| Comparative Examples 3 | 38.0 |
Flos Caryophylli skin-care detergent of the present invention, adopt nonionogenic tenside and amphoterics composite, abandoned traditional anion surfactant, and amphoterics lauroyl both sexes guanidine-acetic acid sodium, coco betaine and N as can be seen from the above table, N-dimethyl decyl-N-amine oxide and nonionogenic tenside dodecyl glucoside composite (embodiment 1) synergy, compare with nonionogenic tenside dodecyl glucoside composite (Comparative Examples 1-3) with single amphoterics, detersive power obviously improves.
Test case 2:
The pungency test
The simulation irritant experiment carries out in the laboratory, and experimenter (each 5 people of men and women) washs in the water-detergent solution of 1wt%, 25 ± 2 ℃ of water temperatures, and institute's water is conventional tap water, washs every day 2 times, each 3 hours, continuous 1 week.Average after marking according to the standard of following table for the pungency of wrist-watch skin, it is more high to mark again, and pungency is more little.
Pungency test data table
| ? | Scoring |
| Embodiment 1 | 100 |
| The standard dish washing detergent | 50 |
| Comparative Examples 1 | 95 |
| Comparative Examples 2 | 90 |
| Comparative Examples 3 | 95 |
Embodiment 2
For prolonging the quality guaranteed period of the present invention, the contriver has made following research pioneeringly.
In the prepared liquid detergent of embodiment 1, add 0.05 kilogram of composite environmental-friendly sanitas.Described composite environmental-friendly sanitas, formed by weight by following component: 1,3-dihydroxymethyl-5,20 parts of 40 parts of 5-T10s (CAS:6640-58-0), 40 parts of iodine propiolic alcohol butyl mephenesin Carbamates (CAS:55406-53-6) and tennecetins (CAS:7681-93-8).
Namely, this Flos Caryophylli skin-care detergent is made up of the raw material of following weight part: 5 kilograms in lauroyl both sexes guanidine-acetic acid sodium, 5 kilograms of coco betaine, N, 3 kilograms of N-dimethyl decyls-N-amine oxide, 6 kilograms of dodecyl glucosides, 0.1 kilogram of Flos Caryophylli extract, 80 kilograms in water, 0.05 kilogram of composite environmental-friendly sanitas.
By adding the sanitas of specific proportioning on the basis of embodiment 1, prolonged the quality guaranteed period of this Flos Caryophylli skin-care detergent greatly.By 10 days 1 quality guaranteed perioves of embodiment, extend to 18 months.In addition, contrast, with the general single sanitas 1 of the industry of the composite environmental-friendly sanitas among the embodiment 2,3-dihydroxymethyl-5, the 5-T10 is replaced, and add-on is constant, and its quality guaranteed period only is December.
Claims (2)
1. a Flos Caryophylli skin-care detergent is characterized in that, is made up of following raw material: lauroyl both sexes guanidine-acetic acid sodium, coco betaine, N, N-dimethyl decyl-N-amine oxide, dodecyl glucoside, Flos Caryophylli extract and water.
2. Flos Caryophylli skin-care detergent as claimed in claim 1, it is characterized in that, raw material by following weight part is formed: lauroyl both sexes guanidine-acetic acid sodium 4-6 part, coco betaine 4-6 part, N, N-dimethyl decyl-N-amine oxide 2-4 part, dodecyl glucoside 5-7 part, Flos Caryophylli extract 0.05-0.15 part, 80 parts in water.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310207310.6A CN103266028B (en) | 2013-05-28 | 2013-05-28 | Lilac skincare liquid detergent |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310207310.6A CN103266028B (en) | 2013-05-28 | 2013-05-28 | Lilac skincare liquid detergent |
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| CN103266028A true CN103266028A (en) | 2013-08-28 |
| CN103266028B CN103266028B (en) | 2014-07-16 |
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| CN201310207310.6A Active CN103266028B (en) | 2013-05-28 | 2013-05-28 | Lilac skincare liquid detergent |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103275820A (en) * | 2013-05-28 | 2013-09-04 | 上海艳紫化工科技有限公司 | Mango seed oil skin-protecting detergent |
| CN104046525A (en) * | 2014-04-25 | 2014-09-17 | 天津天狮生物发展有限公司 | Plastic tableware washing detergent and preparation method |
| CN105482915A (en) * | 2016-02-01 | 2016-04-13 | 东莞品派实业投资有限公司 | Skin-protecting bactericidal cleanser essence |
| CN106336964A (en) * | 2016-08-24 | 2017-01-18 | 祝家程 | Disinfectant detergent |
| CN108102812A (en) * | 2016-11-24 | 2018-06-01 | 陈君君 | A kind of Chinese honey locust Ginger detergent and its concocting method |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101268177A (en) * | 2005-07-22 | 2008-09-17 | 霍尼韦尔国际公司 | Cleaner composition, article and method |
| CN102151238A (en) * | 2010-12-14 | 2011-08-17 | 李少杰 | Clove sanitizer and preparation method thereof |
-
2013
- 2013-05-28 CN CN201310207310.6A patent/CN103266028B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101268177A (en) * | 2005-07-22 | 2008-09-17 | 霍尼韦尔国际公司 | Cleaner composition, article and method |
| CN102151238A (en) * | 2010-12-14 | 2011-08-17 | 李少杰 | Clove sanitizer and preparation method thereof |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103275820A (en) * | 2013-05-28 | 2013-09-04 | 上海艳紫化工科技有限公司 | Mango seed oil skin-protecting detergent |
| CN103275820B (en) * | 2013-05-28 | 2015-01-21 | 安徽省林锦记食品工业有限公司 | Mango seed oil skin-protecting detergent |
| CN104046525A (en) * | 2014-04-25 | 2014-09-17 | 天津天狮生物发展有限公司 | Plastic tableware washing detergent and preparation method |
| CN105482915A (en) * | 2016-02-01 | 2016-04-13 | 东莞品派实业投资有限公司 | Skin-protecting bactericidal cleanser essence |
| CN106336964A (en) * | 2016-08-24 | 2017-01-18 | 祝家程 | Disinfectant detergent |
| CN108102812A (en) * | 2016-11-24 | 2018-06-01 | 陈君君 | A kind of Chinese honey locust Ginger detergent and its concocting method |
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| Publication number | Publication date |
|---|---|
| CN103266028B (en) | 2014-07-16 |
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Effective date of registration: 20190923 Address after: 233010 Incubation Workshop, 414 Changle Road, Yuhui District, Bengbu City, Anhui Province Patentee after: Bengbu Xingshi Intellectual Property Operations Co., Ltd. Address before: 201111 Shanghai city Minhang District Yuanjiang Road No. 5500 building first room E2128 Patentee before: Shanghai Yanzi Chemical Technology Co., Ltd. |
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