CN103230343A - Emulsion composition - Google Patents
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- CN103230343A CN103230343A CN2013101389417A CN201310138941A CN103230343A CN 103230343 A CN103230343 A CN 103230343A CN 2013101389417 A CN2013101389417 A CN 2013101389417A CN 201310138941 A CN201310138941 A CN 201310138941A CN 103230343 A CN103230343 A CN 103230343A
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Abstract
The invention relates to an emulsion composition which is used for the care of human skin and the recuperation of hair. The composition comprises an oil phase component, an aqueous phase component and long-chain fatty acyl acidic amino acid aliphatic alcohol ester expressed by a general formula, wherein the oil phase component comprises oil, wax, higher fatty acid, higher aliphatic alcohol, aliphatic ester, polysiloxane and the like; and the aqueous phase component comprises pure water, deionized water, mineral water and the like. The composition also comprises a coemulsifier and an auxiliary agent. The emulsion composition can be applied to various skin care products to bring unique soft and moist skin feel, and can be applied to hair recuperation products to bring excellent gloss and favorable combing property to the hair.
Description
Technical field
The present invention relates to emulsion composition, specially refer to the emulsion composition for human body skin nursing, hair-conditioning.
Background technology
Emulsion is that one or more liquid are dispersed in the heterogeneous dispersion with quite stable that constitutes in another not miscible liquid with liquid pearl form.Become decentralized photo (or claiming inner phase, discontinuous phase) mutually with liquid pearl or other forms dispersed in the emulsion; Another joins together mutually, is called disperse medium (or claiming foreign minister, continuous phase).One of common emulsion is water or aqueous solution (water) mutually; Another is the phase (organic facies, common name " oil phase ") not miscible with water mutually.The foreign minister is " water ", and inner phase is called oil-in-water emulsion for the emulsion of " oil ".The foreign minister is " oil ", and inner phase then is called the emulsion of water-in-oil type for the emulsion of " water ".
No matter skin-protection product is cream frost, the emulsion of preserving moisture, moistening effect, or sunscreen product, foundation cream product, also or have the functional product of health giving quality, defying age cream for example, anti-acne cream etc. all are to be applied in human body skin, therefore, good skin sense is the basic requirement of a skin-protection product, also is the most direct factor of a skin-protection product of consumer evaluation.And for hair product, as hair conditioner, then be the cardability that requirement can be become reconciled for the glossiness that hair brings.
Summary of the invention
The technical problem to be solved in the present invention is to overcome deficiency of the prior art, and a kind of emulsion composition is provided.Be used for all kinds of skin-protection products, the skin sense that brings unique softness to moisten; Be used for the hair-conditioning product, then bring splendid glossiness and good cardability.
The present inventor realizes of the present invention by after studying for a long time by following technical measures.Though claims of the present invention particularly point out and clearly required the protection domain of the present invention " a kind of emulsion composition ", should believe that following explanation will better explain the present invention.
A kind of emulsion composition, by weight percentage composed as follows:
Oil phase component 3～70%
Water component 15～95%
Long-chain fat acyl acidic amino acid aliphatic alcohol ester with general formula (1) expression
0.05～15％
Described oil phase component comprises from oils and fats, wax, higher fatty acids, high fatty alcohol, fatty acid ester, the polysiloxanes in animal, plant, mineral or synthetic source, or their mixture;
Described water component comprises pure water, deionized water, mineral water, distilled water or their mixture;
The general formula (1) of the long-chain fat acyl acidic amino acid aliphatic alcohol ester of described expression is:
Wherein:
R
1The expression carbon number is 8 ~ 22 straight chain or the alkyl or alkenyl that contains branched chain;
R
2And R
3Expression hydrogen atom or carbon number are 8 ~ 28 straight chain or contain branched chain, the residue of saturated or unsaturated aliphatic alcohol and/or fatty alcohol ether, wherein R
2And R
3Can be identical or inequality, and R
2And R
3Can not be hydrogen atom simultaneously, and R
2And R
3The residue that does not comprise sterols;
M represents 1 or 2 positive integer;
Acidic amino acid partly is aspartic acid or glutamic acid, or their mixture.
The coemulsifier that also comprises the long-chain fat acyl acidic amino acid aliphatic alcohol ester that is different from general formula (1) expression.
Also comprise the adjuvant for nursing skin and conditioning hair.
R in described general formula (1)
1Being at least carbon number and being a kind of in 8～22 straight chain or the alkyl or alkenyl that contains branched chain, is octyl group, nonyl, decyl, dodecyl, tridecyl, myristyl, cetyl, octadecyl, eicosyl, docosyl, iso-octyl, different nonyl, isodecyl, the Fancol ID base, isotridecyl, different myristyl, isocetyl, the isooctadecane base, the Isoeicosane base, different docosyl, octenyl, the nonene base, the decene base, the laurylene base, the tridecylene base, the tetradecene base, the hexadecylene base, the octadecylene base, the isooctene base, different nonene base, the isodecyl thiazolinyl, different laurylene base, different tridecylene base, different tetradecene base, different hexadecylene base, different octadecylene base, or their mixture.
R in described general formula (1)
1Be preferably carbon number and be a kind of in 12～20 straight chain or the alkyl that contains branched chain, be dodecyl, tridecyl, myristyl, cetyl, octadecyl, eicosyl, Fancol ID base, isotridecyl, different myristyl, isocetyl, isooctadecane base, Isoeicosane base, or their mixture.
R in described general formula (1)
1More preferably carbon number is a kind of in the alkyl of 12～20 straight chain, is dodecyl, tridecyl, myristyl, cetyl, octadecyl, eicosyl, or their mixture.
R in described general formula (1)
2And R
3To be at least hydrogen atom or carbon number be 8～28 straight chain or contain branched chain, a kind of in the residue of saturated or unsaturated aliphatic alcohol and/or fatty alcohol ether, it is capryl alcohol, nonyl alcohol, decanol, lauryl alcohol, tridecanol, myristyl alcohol, palmityl alcohol, stearyl alcohol, oleyl alcohol, arachidic alcohol, behenyl alcohol, tetracosanol, hexacosyl alcohol, octacosanol, isooctanol, isononyl alcohol, isodecanol, different lauryl alcohol, different tridecanol, different tetradecyl alchohol, different hexadecanol, i-octadecanol, different eicosanol, different docosanol, different tetracosanol, isoceryl alcohol, different octacosanol, or their mixture; Capryl alcohol ether, nonyl alcohol ether, decanol ether, lauryl alcohol, tridecanol ether, Semen Myristicae alcohol ether, Petiolus Trachycarpi alcohol ether, stearic alcohol ether, oleyl alcohol ether, Semen arachidis hypogaeae alcohol ether, behenyl alcohol ether, tetracosanol ether, hexacosyl alcohol ether, octacosanol ether, isooctanol ether, isononyl alcohol ether, isodecyl alcohol ether, different lauryl alcohol ether, different tridecanol ether, different tetradecyl alchohol ether, different hexadecanol ether, i-octadecanol ether, different eicosanol ether, different docosanol ether, different tetracosanol ether, isoceryl alcohol ether, different octacosanol ether, or their mixture.
R in described general formula (1)
2And R
3To be preferably hydrogen atom or carbon number be 10～22 straight chain or contain branched chain, a kind of in the residue of saturated or unsaturated aliphatic alcohol and/or fatty alcohol ether, be decanol, lauryl alcohol, tridecanol, myristyl alcohol, palmityl alcohol, stearyl alcohol, oleyl alcohol, arachidic alcohol, behenyl alcohol, isodecanol, different lauryl alcohol, different tridecanol, different tetradecyl alchohol, different hexadecanol, i-octadecanol, different eicosanol, different docosanol, or their mixture; Fatty alcohol ether: decanol ether, lauryl alcohol, tridecanol ether, Semen Myristicae alcohol ether, Petiolus Trachycarpi alcohol ether, stearic alcohol ether, oleyl alcohol ether, Semen arachidis hypogaeae alcohol ether, behenyl alcohol ether, isodecyl alcohol ether, different lauryl alcohol ether, different tridecanol ether, different tetradecyl alchohol ether, different hexadecanol ether, i-octadecanol ether, different eicosanol ether, different docosanol ether, or their mixture.
R in described general formula (1)
2And R
3More preferably hydrogen atom or carbon number are a kind of in the residue of 10～22 straight chain or the saturated aliphatic alcohol that contains branched chain, be lauryl alcohol, tridecanol, myristyl alcohol, palmityl alcohol, stearyl alcohol, arachidic alcohol, behenyl alcohol, isodecanol, different lauryl alcohol, different tridecanol, different tetradecyl alchohol, different hexadecanol, i-octadecanol, different eicosanol, different docosanol, or their mixture.
Described long-chain fat acyl acidic amino acid aliphatic alcohol ester is: lauroyl glutamic acid lauryl alcohol ester; lauroyl glutamic acid tridecanol ester; lauroyl glutamic acid tetradecyl alchohol ester; lauroyl glutamic acid hexadecanol ester; lauroyl glutamic acid octadecanol ester; lauroyl glutamic acid eicosanol ester; the different lauryl alcohol ester of lauroyl glutamic acid; lauroyl glutamic acid isotridecanol; the different tetradecyl alchohol ester of lauroyl glutamic acid; the different hexadecanol ester of lauroyl glutamic acid; lauroyl glutamic acid i-octadecanol ester; the different eicosanol ester of lauroyl glutamic acid; tridecanoyl glutamic acid lauryl alcohol ester; tridecanoyl glutamic acid tridecanol ester; tridecanoyl glutamic acid tetradecyl alchohol ester; tridecanoyl glutamic acid hexadecanol ester; tridecanoyl glutamic acid octadecanol ester; tridecanoyl glutamic acid eicosanol ester; the different lauryl alcohol ester of tridecanoyl glutamic acid; tridecanoyl glutamic acid isotridecanol; the different tetradecyl alchohol ester of tridecanoyl glutamic acid; the different hexadecanol ester of tridecanoyl glutamic acid; tridecanoyl glutamic acid i-octadecanol ester; the different eicosanol ester of tridecanoyl glutamic acid; myristoyl glutamic acid lauryl alcohol ester; myristoyl glutamic acid tridecanol ester; myristoyl glutamic acid tetradecyl alchohol ester; myristoyl glutamic acid hexadecanol ester; myristoyl glutamic acid octadecanol ester; myristoyl glutamic acid eicosanol ester; the different lauryl alcohol ester of myristoyl glutamic acid; myristoyl glutamic acid isotridecanol; the different tetradecyl alchohol ester of myristoyl glutamic acid; the different hexadecanol ester of myristoyl glutamic acid; myristoyl glutamic acid i-octadecanol ester; the different eicosanol ester of myristoyl glutamic acid; palmityl glutamic acid lauryl alcohol ester; palmityl glutamic acid tridecanol ester; palmityl glutamic acid tetradecyl alchohol ester; palmityl glutamic acid hexadecanol ester; palmityl glutamic acid octadecanol ester; palmityl glutamic acid eicosanol ester; the different lauryl alcohol ester of palmityl glutamic acid; palmityl glutamic acid isotridecanol; the different tetradecyl alchohol ester of palmityl glutamic acid; the different hexadecanol ester of palmityl glutamic acid; palmityl glutamic acid i-octadecanol ester; the different eicosanol ester of palmityl glutamic acid; stearoyl-glutamic acid lauryl alcohol ester; stearoyl-glutamic acid tridecanol ester; stearoyl-glutamic acid tetradecyl alchohol ester; stearoyl-glutamic acid hexadecanol ester; stearoyl-glutamic acid octadecanol ester; stearoyl-glutamic acid eicosanol ester; the different lauryl alcohol ester of stearoyl-glutamic acid; the stearoyl-glutamic acid isotridecanol; the different tetradecyl alchohol ester of stearoyl-glutamic acid; the different hexadecanol ester of stearoyl-glutamic acid; stearoyl-glutamic acid i-octadecanol ester; the different eicosanol ester of stearoyl-glutamic acid; eicosane acyl glutamic acid lauryl alcohol ester; eicosane acyl glutamic acid tridecanol ester; eicosane acyl glutamic acid tetradecyl alchohol ester; eicosane acyl glutamic acid hexadecanol ester; eicosane acyl glutamic acid octadecanol ester; the different lauryl alcohol ester of eicosane acyl glutamic acid; eicosane acyl glutamic acid isotridecanol; the different tetradecyl alchohol ester of eicosane acyl glutamic acid; the different hexadecanol ester of eicosane acyl glutamic acid; eicosane acyl glutamic acid i-octadecanol ester; the different eicosanol ester of eicosane acyl glutamic acid; lauroyl aspartic acid lauryl alcohol ester; lauroyl aspartic acid tridecanol ester; lauroyl aspartic acid tetradecyl alchohol ester; lauroyl aspartic acid hexadecanol ester; lauroyl aspartic acid octadecanol ester; lauroyl aspartic acid eicosanol ester; the different lauryl alcohol ester of lauroyl aspartic acid; lauroyl aspartic acid isotridecanol; the different tetradecyl alchohol ester of lauroyl aspartic acid; the different hexadecanol ester of lauroyl aspartic acid; lauroyl aspartic acid i-octadecanol ester; the different eicosanol ester of lauroyl aspartic acid; tridecanoyl aspartic acid lauryl alcohol ester; tridecanoyl aspartic acid tridecanol ester; tridecanoyl aspartic acid tetradecyl alchohol ester; tridecanoyl aspartic acid hexadecanol ester; tridecanoyl aspartic acid octadecanol ester; tridecanoyl aspartic acid eicosanol ester; the different lauryl alcohol ester of tridecanoyl aspartic acid; tridecanoyl aspartic acid isotridecanol; the different tetradecyl alchohol ester of tridecanoyl aspartic acid; the different hexadecanol ester of tridecanoyl aspartic acid; tridecanoyl aspartic acid i-octadecanol ester; the different eicosanol ester of tridecanoyl aspartic acid; myristoyl aspartic acid lauryl alcohol ester; myristoyl aspartic acid tridecanol ester; myristoyl aspartic acid tetradecyl alchohol ester; myristoyl aspartic acid hexadecanol ester; myristoyl aspartic acid octadecanol ester; myristoyl aspartic acid eicosanol ester; the different lauryl alcohol ester of myristoyl aspartic acid; myristoyl aspartic acid isotridecanol; the different tetradecyl alchohol ester of myristoyl aspartic acid; the different hexadecanol ester of myristoyl aspartic acid; myristoyl aspartic acid i-octadecanol ester; the different eicosanol ester of myristoyl aspartic acid; palmityl aspartic acid lauryl alcohol ester; palmityl aspartic acid tridecanol ester; palmityl aspartic acid tetradecyl alchohol ester; palmityl aspartic acid hexadecanol ester; palmityl aspartic acid octadecanol ester; palmityl aspartic acid eicosanol ester; the different lauryl alcohol ester of palmityl aspartic acid; palmityl aspartic acid isotridecanol; the different tetradecyl alchohol ester of palmityl aspartic acid; the different hexadecanol ester of palmityl aspartic acid; palmityl aspartic acid i-octadecanol ester; the different eicosanol ester of palmityl aspartic acid; stearoyl aspartic acid lauryl alcohol ester; stearoyl aspartic acid tridecanol ester; stearoyl aspartic acid tetradecyl alchohol ester; stearoyl aspartic acid hexadecanol ester; stearoyl aspartic acid octadecanol ester; stearoyl aspartic acid eicosanol ester; the different lauryl alcohol ester of stearoyl aspartic acid; stearoyl aspartic acid isotridecanol; the different tetradecyl alchohol ester of stearoyl aspartic acid; the different hexadecanol ester of stearoyl aspartic acid; stearoyl aspartic acid i-octadecanol ester; the different eicosanol ester of stearoyl aspartic acid, eicosane acyl aspartic acid lauryl alcohol ester; eicosane acyl aspartic acid tridecanol ester; eicosane acyl aspartic acid tetradecyl alchohol ester; eicosane acyl aspartic acid hexadecanol ester; eicosane acyl aspartic acid octadecanol ester; the different lauryl alcohol ester of eicosane acyl aspartic acid; eicosane acyl aspartic acid isotridecanol; the different tetradecyl alchohol ester of eicosane acyl aspartic acid; the different hexadecanol ester of eicosane acyl aspartic acid; eicosane acyl aspartic acid i-octadecanol ester; the different eicosanol ester of eicosane acyl aspartic acid or their mixture.
The acidic amino acid part of described long-chain fat acyl acidic amino acid aliphatic alcohol ester is preferably glutamic acid.
In the present composition, account for composition weight percentage ratio with the long-chain fat acyl acidic amino acid aliphatic alcohol ester of general formula (1) expression and be preferably: 0.1%～10%.
In the present composition, account for composition weight percentage ratio more preferably 0.5%～5% with the long-chain fat acyl acidic amino acid aliphatic alcohol ester of general formula (1) expression.
In the oil phase component of the present composition:
Described oils and fats is: Oleum Ricini; olive oil; Oleum Arachidis hypogaeae semen; Oleum Cocois; Oleum Gossypii semen; almond oil; Apricot kernel oil; Petiolus Trachycarpi oil; palm-kernel oil; Oleum Glycines; Semen Tritici aestivi germ oil; Semen Maydis oil; Oleum sesami; Oleum Camelliae; Testa oryzae oil; American Avocado Tree oil; macadimia nut oil; candlenut oil; Jojoba oil; Oleum Hippophae; water Bulbus Allii mustard seed oil; cameline oil; cocoa butter; mother-in-law sieve's fat; Adeps Bovis seu Bubali resin; mink oil; shark liver oil Walk fish oil; Adeps Bovis seu Bubali; leaf fat; horse fat; exquisite Adeps Cervi; liquid paraffin; vaseline; lanonol; the Pilus Caprae seu Ovis fatty acid; wool oil; acetylated lanolin; Wool wax alcohols,ethoxylated; hydrogenated lanolin; cholesterol; squalane; isomery hexadecane hydrocarbon, or their mixture.
Described wax is: Brazil wax, candelilla wax, haze tallow, aromatic wax, spermaceti, Cera Flava, lanoline, paraffin, microwax, ceresine, montan wax, or their mixture.
Described higher fatty acids is: lauric acid, myristic acid, Palmic acid, stearic acid, isostearic acid, mountain Yu acid, oleic acid, or their mixture.
Described high fatty alcohol is: lauryl alcohol, myristyl alcohol, palmityl alcohol, stearyl alcohol, isooctadecanol, oleyl alcohol, behenyl alcohol, or their mixture.
Described fatty acid ester is: the different monooctyl ester of stearic acid, isopropyl myristate, isopropyl palmitate, iso-octyl palmitate, myristyl myristate, acid isopropyl, oleic acid monooctyl ester, capric acid triglyceride, lauric acid triglyceride, Dynasan 114, caprylic/capric triglyceride, ricinoleic acid glyceride, the different hard ester of isostearic acid, the different monooctyl ester of isostearic acid, glyceryl isostearate, isononyl isononanoate, geoceric acid stearyl alcohol ester, behenic acid 20 diester, the different hard ester alcohol ester of isostearic acid, or their mixture.
Described polysiloxanes is: polydimethylsiloxane, PSI, ring-type methylsiloxane, polysiloxane polyether copolymer or their mixture.
In the present composition, oil phase component accounts for composition weight percentage ratio and is preferably: 5%～55%.
In the present composition, oil phase component accounts for composition weight percentage ratio more preferably 10%～45%.
In the present composition, water ingredients constitute composition weight percentage ratio is preferably: 35%～90%.
In the present composition, water ingredients constitute composition weight percentage ratio more preferably 50%～85%.
In the present composition; includable be different from general formula (1) expression the coemulsifier of long-chain fat acyl acidic amino acid aliphatic alcohol ester be: C12～C18 alkyl carboxylate; C12～C18 alkylsulfonate; C12～C18 fatty alcohol sulfate salt; C12～C18 polyoxyethylene alkyl ether sulfate salt; C12～C18 fatty alcohol phosphates; C12～18 aliphatic alcohol polyoxyvinethene phosphate salt; (the above-mentioned salt that becomes can be potassium salt to C8～C20 alkanoyl lactate; sodium salt); triethanolamine salt; polyoxyethylene aliphatic alcohol ether; polyoxyethylene carboxylate; fatty acid glyceride; the fatty acid ester of sorbitol or anhydrous sorbitol; the fatty acid ester of polyoxyethylene sorbitol or anhydrous sorbitol; sucrose fatty acid ester; polyglyceryl fatty acid ester; alkyl polyglucoside, or their mixture.
Described be different from general formula (1) expression the coemulsifier of long-chain fat acyl acidic amino acid aliphatic alcohol ester in:
Described C12～C18 alkyl carboxylate is: dodecyl carboxylate, tridecyl carboxylate, myristyl carboxylate, cetyl carboxylate, octadecyl carboxylate, or their mixture.
Described C12～C18 alkylsulfonate is: dodecane sulfonate, tridecyl sulfonate, tetradecyl sulfonate, cetyl sulfonate, octadecyl sulfonate, or their mixture.
Described C12～C18 fatty alcohol sulfate salt is: lauryl alcohol sulfuric acid, tridecanol sulfuric acid, tetradecyl alchohol sulfuric acid, hexadecanol sulfuric acid, octadecanol sulfuric acid, or their mixture.
Described C12～C18 polyoxyethylene alkyl ether sulfate salt is: lauryl alcohol ether sulfuric acid, tridecanol ether sulfuric acid, tetradecyl alchohol ether sulfuric acid, hexadecanol ether sulfuric acid, octadecanol ether sulfuric acid, or their mixture.
Described C12～C18 fatty alcohol phosphates is: lauryl alcohol phosphate ester salt, tridecanol phosphate ester salt, tetradecyl alchohol phosphate ester salt, hexadecanol phosphate ester salt, octadecanol phosphate ester salt, or their mixture.
Described C12～18 aliphatic alcohol polyoxyvinethene phosphate salt are: lauryl alcohol ether phosphate salt, tridecanol ether phosphate salt, tetradecyl alchohol ether phosphate salt, hexadecanol ether phosphate salt, octadecanol ether phosphate salt, or their mixture.
Described C8～C20 alkanoyl lactate is: octane acyl-lactate, decane acyl-lactate, lauroyl lactate, tridecanoyl lactate, tetradecanoyl lactate, hexadecanoyl lactate, octadecanoyl lactate, or their mixture.
The salt that above-claimed cpd becomes can be potassium salt, sodium salt or triethanolamine salt.
Described polyoxyethylene aliphatic alcohol ether is: lauryl alcohol ether, tridecanol ether, different tridecanol ether, tetradecyl alchohol ether, hexadecanol ether, octadecanol ether, i-octadecanol alcohol ether, oleyl alcohol ether, or their mixture.
Described polyoxyethylene carboxylate is: polyoxyethylene laurate, polyoxyethylene myristinate, polyoxyethylene cetylate, Myrj 45, or their mixture.
Described fatty acid glyceride is: glycerol monolaurate, glycerine myristate ester, palmitin, glyceryl stearate, or their mixture.
The fatty acid ester of described sorbitol or anhydrous sorbitol is: sorbitol or anhydrous sorbitol laurate, sorbitol or anhydrous sorbitol myristinate, sorbitol or anhydrous sorbitol cetylate, sorbitol or Span60, sorbitol or sorbitan monooleate, or their mixture.
The fatty acid ester of described polyoxyethylene sorbitol or anhydrous sorbitol is: polyoxyethylene sorbitol or anhydrous sorbitol laurate, polyoxyethylene sorbitol or anhydrous sorbitol myristinate, polyoxyethylene sorbitol or anhydrous sorbitol cetylate, polyoxyethylene sorbitol or Span60, polyoxyethylene sorbitol or sorbitan monooleate, or their mixture.
Described sucrose fatty acid ester is: Surfhope SE Cosme C 1216, Sucrose myristate, sucrose palmitate, sucrose stearate, sucrose oleate, or their mixture.
Described polyglyceryl fatty acid ester is: polyglycereol laurate, polyglycereol myristinate, POGE-A POGE-B POGE-C Polyglycerin palmitate, polyglycereol stearate, polyglyceryl-isostearate, or their mixture.
Described alkyl polyglucoside is: decyl glucosides, dodecyl glucosides, myristyl glucosides, cetyl glucosides, octadecyl glucosides, eicosyl glucosides, or their mixture.
In the present composition, the includable coemulsifier that is different from the represented long-chain fat acyl acidic amino acid aliphatic alcohol ester of component general formula (1) is preferably at least a HLB value greater than 7 emulsifying agent.
In the present composition, includable adjuvant is: special composition, antiseptic, antioxidant, sunscreen, powder, coloring agent, the spice of water-soluble polymer thickening agent, wetting agent, pH regulator agent, cosmetics and efficacy cosmetic product.
In described adjuvant:
Described water-soluble polymer thickening agent is: collagen protein, hydrolysis almond protein, hydrolysis aleuronat, hydrolyzed silk protein, gelatin, arabic gum, guar gum, chitin derivativ, HANSHENGJIAO, modified cellulose class, polyethylene glycols, polyvinylpyrrolidone, esters of acrylic acid, polyacrylamide, Magnesiumaluminumsilicate, bentonite, or their mixture.
Described wetting agent is: polyhydric alcohol, lactic acid, sodium lactate, pyrrolidone carboxylic acid salt, glucose esters, sodium chondroitin sulfate, hyaluronic acid (sodium), or they are mixture.
Described pH regulator agent is: citric acid, fruit acid, potassium hydroxide, sodium hydroxide, ammonium hydroxide, triethanolamine, or their mixture.
The special composition of described cosmetics and efficacy cosmetic product is: vitamins, various plant extraction liquid, or their mixture.
Described antiseptic is: phenoxyethanol, parabens, or their mixture.
Described antioxidant is: BHT, BHA, or their mixture.
Described sunscreen is: p-aminobenzoate and derivant thereof, salicylate and derivant thereof, cinnamate derivative, hexichol (first) ketone, o-aminobenzoa, dibenzoyl methane class, Camphora analog derivative, or their mixture.
Described powder is: titanium dioxide, zinc oxide, or their mixture.
The detailed note of these adjuvant is found in Sagarin's " cosmetics, science and technology " (Cosmetics, Science and Technology) etc.The various traditional adjuvant kind and the numerous of quantity that can be used for emulsion composition can not exemplify one by one, only otherwise influence under the prerequisite of stability of the present composition, can add.
The preparation method of the present composition:
Production technology of the present invention is those skilled in the art institute method in common, be summarized as follows: (stirrer paddle is the anchor formula in that stirrer paddle is housed, frame, screw-pushing type) and in the container of homogenizer, container has chuck or metal coil pipe heating and cooling system, add water and other hydrophilic adjuvant earlier, open heating, container slowly is heated to about 70 ℃, then with oil phase with and lipophile adjuvant and coemulsifier add in another preparation pot, the preparation pot also has chuck or metal coil pipe heating and cooling system, open heating, container slowly is heated to about 70 ℃, then with oil phase suction aqueous phase, open homogenizing, keep half an hour.After confirming abundant homogenizing and reaching index of correlation, the unlatching cooling system begins to cool down, and is cooled to add volatile component, antiseptic and essence etc. about 40 ℃ again, emits the material body after fully mixing.
The skin sense is estimated:
Smear test by 10 various emulsion compositions that use the present invention to prepare through the volunteer of training, it is clean that every volunteer smears the position skin clean with need earlier, evenly be applied in an amount of emulsion composition on the skin then, smear evenly according to smearing custom at ordinary times, after treating that emulsion composition is absorbed fully by skin, evaluate according to following classification standard.
5 minutes: very soft moist skin sense.
4 minutes: soft moist skin sense.
3 minutes: slight soft skin sense.
2 minutes: do not have soft skin sense of moistening.
1 minute: the skin sense is dry and astringent, and was crude.
To evaluate the score addition, decide grade according to following standard for each compositions.
A level: 45 ~ 50 minutes.
B level: 35 ~ 44 minutes.
C level: 25 ~ 34 minutes.
D level: be lower than 25 fens.
After the present invention adopted abovementioned technology, emulsion composition was used for all kinds of skin-protection products, for example preserved moisture, the cream frost of moisturizing effect, emulsion, sunscreen product, foundation cream series products, or effect product, after being applied in skin, can both bring a kind of moist skin sense of softness of uniqueness; Also can be used for the hair-conditioning product, as hair conditioner, can come splendid glossiness and good cardability for hair carry.
The specific embodiment
Below in conjunction with specific embodiment, further set forth the present invention.Should be understood that these embodiment only are used for explanation the present invention but not limit the scope of the invention.The experimental technique of unreceipted actual conditions in the following example is usually according to normal condition or the condition of advising according to manufacturer.
Except as otherwise noted, the INCI(cosmetic composition international nomenclature International Nomenclature of Cosmetic Ingredients that all is familiar with chemical name or this area of each component) " title provides.
In embodiment and Comparative Examples, the numeral of corresponding component is this component percentage by weight in this example.
Unit in the percentage by weight among the present invention is well-known to those skilled in the art, for example refers to the weight of solute in the solution of 100 grams.
Unless otherwise defined, the same meaning that employed all specialties and scientific words and one skilled in the art are familiar with in the literary composition.In addition, any method similar or impartial to described content and material all can be applicable in the inventive method.The usefulness that preferable implementation method described in the literary composition and material only present a demonstration.
The emulsion composition of embodiment 1～24 preparation is for the skin nursing effect of partes corporis humani position; The emulsion of embodiment 25～27 preparations is the opsonic actions for human hair.
Table one:
In the table one, according to the enrich cream of embodiments of the invention 1～3 preparation, be applied in human body face after, skin sense softness is moistened non-greasy; And do not use the Comparative Examples 1 of the present composition, the skin sense is the flexibility deviation then, and greasy partially.
Table two:
In the table two, the body lotion according to embodiments of the invention 4～6 preparations is applied on the human body skin, and skin sense softness is comfortable; And do not use the Comparative Examples 2 of the present composition, the skin sense is stiff, and is uncomfortable.
Table three:
In the table three, the sunscreen cream according to embodiments of the invention 7 ~ 9 preparations is applied on human body face or the body skin, and skin sense softness is comfortable; And do not use the Comparative Examples 3 of the present composition, and skin sense drying, tight.
Table four:
In the table four, the foundation lotion according to embodiments of the invention 10 ~ 12 preparations is applied on the human body face skin, and skin sense softness is comfortable; And do not use the Comparative Examples 4 of the present composition, the skin sense is dry and astringent, coarse.
Table five:
In the table five, the hand cream according to embodiments of the invention 13 ~ 15 preparations is applied on the human hands skin, and the skin sense is soft moistens; And do not use the Comparative Examples 5 of the present composition, the skin sense is greasy, and is rough.
Table six:
In the table six, according to the massage cream of embodiments of the invention 13 ~ 15 preparations, be used for human body position skin and smear massage, the skin sense is soft moistens; And do not use the Comparative Examples 5 of the present composition, the skin sense is greasy, and is rough.
Table seven:
In the table seven, the anti-aging cream according to embodiments of the invention 19 ~ 21 preparations is applied on the human body face skin, and skin sense softness is comfortable; And do not use the Comparative Examples 7 of the present composition, the skin sense is dry and astringent, and is coarse.
Table eight:
In the table eight, the child's skin moistening cream according to embodiments of the invention 22 ~ 24 preparations is applied on the children's torso skin, and skin sense softness is comfortable; And do not use the Comparative Examples 8 of the present composition, the skin sense is dry and astringent.
Table nine:
In the table nine, according to the hair conditioner of embodiments of the invention 25 ~ 27 preparations, be used for the opsonic action of human hair, can come splendid glossiness and good cardability for hair carry.
Above-described only is preferred implementation of the present invention.Should be pointed out that for the person of ordinary skill of the art under the prerequisite that does not break away from the principle of the invention, can also make some modification and improvement, these also should be considered as belonging to protection scope of the present invention.
Claims (21)
1. emulsion composition is characterized in that: by weight percentage composed as follows:
Oil phase component 3～70%
Water component 15～95%
Long-chain fat acyl acidic amino acid aliphatic alcohol ester with general formula (1) expression
0.05～15％
Described oil phase component comprises from oils and fats, wax, higher fatty acids, high fatty alcohol, fatty acid ester, the polysiloxanes in animal, plant, mineral or synthetic source, or their mixture;
Described water component comprises pure water, deionized water, mineral water, distilled water or their mixture;
The general formula (1) of the long-chain fat acyl acidic amino acid aliphatic alcohol ester of described expression is:
Wherein:
R
1The expression carbon number is 8 ~ 22 straight chain or the alkyl or alkenyl that contains branched chain;
R
2And R
3Expression hydrogen atom or carbon number are 8 ~ 28 straight chain or contain branched chain, the residue of saturated or unsaturated aliphatic alcohol and/or fatty alcohol ether, wherein R
2And R
3Can be identical or inequality, and R
2And R
3Can not be hydrogen atom simultaneously, and R
2And R
3The residue that does not comprise sterol;
M represents 1 or 2 positive integer;
Acidic amino acid partly is aspartic acid or glutamic acid, or their mixture.
2. a kind of emulsion composition according to claim 1 is characterized in that: the coemulsifier that also comprises the long-chain fat acyl acidic amino acid aliphatic alcohol ester that is different from general formula (1) expression.
3. a kind of emulsion composition according to claim 1 is characterized in that: also comprise the adjuvant for nursing skin and conditioning hair.
4. a kind of emulsion composition according to claim 1 is characterized in that: R in described general formula (1)
1Being at least carbon number and being a kind of in 8～22 straight chain or the alkyl or alkenyl that contains branched chain, is octyl group, nonyl, decyl, dodecyl, tridecyl, myristyl, cetyl, octadecyl, eicosyl, docosyl, iso-octyl, different nonyl, isodecyl, the Fancol ID base, isotridecyl, different myristyl, isocetyl, the isooctadecane base, the Isoeicosane base, different docosyl, octenyl, the nonene base, the decene base, the laurylene base, the tridecylene base, the tetradecene base, the hexadecylene base, the octadecylene base, the isooctene base, different nonene base, the isodecyl thiazolinyl, different laurylene base, different tridecylene base, different tetradecene base, different hexadecylene base, different octadecylene base, or their mixture.
5. a kind of emulsion composition according to claim 1 is characterized in that: R in described general formula (1)
1For carbon number is 12～20 straight chain or the alkyl that contains branched chain.
6. a kind of emulsion composition according to claim 1 is characterized in that: R in described general formula (1)
1It is the alkyl of 12～20 straight chain for carbon number.
7. a kind of emulsion composition according to claim 1 is characterized in that: R in described general formula (1)
2And R
3To be at least hydrogen atom or carbon number be 8～28 straight chain or contain branched chain, a kind of in the residue of saturated or unsaturated aliphatic alcohol and/or fatty alcohol ether, it is capryl alcohol, nonyl alcohol, decanol, lauryl alcohol, tridecanol, myristyl alcohol, palmityl alcohol, stearyl alcohol, oleyl alcohol, arachidic alcohol, behenyl alcohol, tetracosanol, hexacosyl alcohol, octacosanol, isooctanol, isononyl alcohol, isodecanol, different lauryl alcohol, different tridecanol, different tetradecyl alchohol, different hexadecanol, i-octadecanol, different eicosanol, different docosanol, different tetracosanol, isoceryl alcohol, different octacosanol, or their mixture; Capryl alcohol ether, nonyl alcohol ether, decanol ether, lauryl alcohol, tridecanol ether, Semen Myristicae alcohol ether, Petiolus Trachycarpi alcohol ether, stearic alcohol ether, oleyl alcohol ether, Semen arachidis hypogaeae alcohol ether, behenyl alcohol ether, tetracosanol ether, hexacosyl alcohol ether, octacosanol ether, isooctanol ether, isononyl alcohol ether, isodecyl alcohol ether, different lauryl alcohol ether, different tridecanol ether, different tetradecyl alchohol ether, different hexadecanol ether, i-octadecanol ether, different eicosanol ether, different docosanol ether, different tetracosanol ether, isoceryl alcohol ether, different octacosanol ether, or their mixture.
8. a kind of emulsion composition according to claim 1 is characterized in that: R in described general formula (1)
2And R
3For hydrogen atom or carbon number are 10～22 straight chain or contain branched chain, the residue of saturated or unsaturated aliphatic alcohol and/or fatty alcohol ether.
9. a kind of emulsion composition according to claim 1 is characterized in that: R in described general formula (1)
2And R
3For hydrogen atom or carbon number are the residue of 10～22 straight chain or the saturated aliphatic alcohol that contains branched chain.
10. a kind of emulsion composition according to claim 1; it is characterized in that: described long-chain fat acyl acidic amino acid aliphatic alcohol ester is: lauroyl glutamic acid lauryl alcohol ester; lauroyl glutamic acid tridecanol ester; lauroyl glutamic acid tetradecyl alchohol ester; lauroyl glutamic acid hexadecanol ester; lauroyl glutamic acid octadecanol ester; lauroyl glutamic acid eicosanol ester; the different lauryl alcohol ester of lauroyl glutamic acid; lauroyl glutamic acid isotridecanol; the different tetradecyl alchohol ester of lauroyl glutamic acid; the different hexadecanol ester of lauroyl glutamic acid; lauroyl glutamic acid i-octadecanol ester; the different eicosanol ester of lauroyl glutamic acid; tridecanoyl glutamic acid lauryl alcohol ester; tridecanoyl glutamic acid tridecanol ester; tridecanoyl glutamic acid tetradecyl alchohol ester; tridecanoyl glutamic acid hexadecanol ester; tridecanoyl glutamic acid octadecanol ester; tridecanoyl glutamic acid eicosanol ester; the different lauryl alcohol ester of tridecanoyl glutamic acid; tridecanoyl glutamic acid isotridecanol; the different tetradecyl alchohol ester of tridecanoyl glutamic acid; the different hexadecanol ester of tridecanoyl glutamic acid; tridecanoyl glutamic acid i-octadecanol ester; the different eicosanol ester of tridecanoyl glutamic acid; myristoyl glutamic acid lauryl alcohol ester; myristoyl glutamic acid tridecanol ester; myristoyl glutamic acid tetradecyl alchohol ester; myristoyl glutamic acid hexadecanol ester; myristoyl glutamic acid octadecanol ester; myristoyl glutamic acid eicosanol ester; the different lauryl alcohol ester of myristoyl glutamic acid; myristoyl glutamic acid isotridecanol; the different tetradecyl alchohol ester of myristoyl glutamic acid; the different hexadecanol ester of myristoyl glutamic acid; myristoyl glutamic acid i-octadecanol ester; the different eicosanol ester of myristoyl glutamic acid; palmityl glutamic acid lauryl alcohol ester; palmityl glutamic acid tridecanol ester; palmityl glutamic acid tetradecyl alchohol ester; palmityl glutamic acid hexadecanol ester; palmityl glutamic acid octadecanol ester; palmityl glutamic acid eicosanol ester; the different lauryl alcohol ester of palmityl glutamic acid; palmityl glutamic acid isotridecanol; the different tetradecyl alchohol ester of palmityl glutamic acid; the different hexadecanol ester of palmityl glutamic acid; palmityl glutamic acid i-octadecanol ester; the different eicosanol ester of palmityl glutamic acid; stearoyl-glutamic acid lauryl alcohol ester; stearoyl-glutamic acid tridecanol ester; stearoyl-glutamic acid tetradecyl alchohol ester; stearoyl-glutamic acid hexadecanol ester; stearoyl-glutamic acid octadecanol ester; stearoyl-glutamic acid eicosanol ester; the different lauryl alcohol ester of stearoyl-glutamic acid; the stearoyl-glutamic acid isotridecanol; the different tetradecyl alchohol ester of stearoyl-glutamic acid; the different hexadecanol ester of stearoyl-glutamic acid; stearoyl-glutamic acid i-octadecanol ester; the different eicosanol ester of stearoyl-glutamic acid; eicosane acyl glutamic acid lauryl alcohol ester; eicosane acyl glutamic acid tridecanol ester; eicosane acyl glutamic acid tetradecyl alchohol ester; eicosane acyl glutamic acid hexadecanol ester; eicosane acyl glutamic acid octadecanol ester; the different lauryl alcohol ester of eicosane acyl glutamic acid; eicosane acyl glutamic acid isotridecanol; the different tetradecyl alchohol ester of eicosane acyl glutamic acid; the different hexadecanol ester of eicosane acyl glutamic acid; eicosane acyl glutamic acid i-octadecanol ester; the different eicosanol ester of eicosane acyl glutamic acid; lauroyl aspartic acid lauryl alcohol ester; lauroyl aspartic acid tridecanol ester; lauroyl aspartic acid tetradecyl alchohol ester; lauroyl aspartic acid hexadecanol ester; lauroyl aspartic acid octadecanol ester; lauroyl aspartic acid eicosanol ester; the different lauryl alcohol ester of lauroyl aspartic acid; lauroyl aspartic acid isotridecanol; the different tetradecyl alchohol ester of lauroyl aspartic acid; the different hexadecanol ester of lauroyl aspartic acid; lauroyl aspartic acid i-octadecanol ester; the different eicosanol ester of lauroyl aspartic acid; tridecanoyl aspartic acid lauryl alcohol ester; tridecanoyl aspartic acid tridecanol ester; tridecanoyl aspartic acid tetradecyl alchohol ester; tridecanoyl aspartic acid hexadecanol ester; tridecanoyl aspartic acid octadecanol ester; tridecanoyl aspartic acid eicosanol ester; the different lauryl alcohol ester of tridecanoyl aspartic acid; tridecanoyl aspartic acid isotridecanol; the different tetradecyl alchohol ester of tridecanoyl aspartic acid; the different hexadecanol ester of tridecanoyl aspartic acid; tridecanoyl aspartic acid i-octadecanol ester; the different eicosanol ester of tridecanoyl aspartic acid; myristoyl aspartic acid lauryl alcohol ester; myristoyl aspartic acid tridecanol ester; myristoyl aspartic acid tetradecyl alchohol ester; myristoyl aspartic acid hexadecanol ester; myristoyl aspartic acid octadecanol ester; myristoyl aspartic acid eicosanol ester; the different lauryl alcohol ester of myristoyl aspartic acid; myristoyl aspartic acid isotridecanol; the different tetradecyl alchohol ester of myristoyl aspartic acid; the different hexadecanol ester of myristoyl aspartic acid; myristoyl aspartic acid i-octadecanol ester; the different eicosanol ester of myristoyl aspartic acid; palmityl aspartic acid lauryl alcohol ester; palmityl aspartic acid tridecanol ester; palmityl aspartic acid tetradecyl alchohol ester; palmityl aspartic acid hexadecanol ester; palmityl aspartic acid octadecanol ester; palmityl aspartic acid eicosanol ester; the different lauryl alcohol ester of palmityl aspartic acid; palmityl aspartic acid isotridecanol; the different tetradecyl alchohol ester of palmityl aspartic acid; the different hexadecanol ester of palmityl aspartic acid; palmityl aspartic acid i-octadecanol ester; the different eicosanol ester of palmityl aspartic acid; stearoyl aspartic acid lauryl alcohol ester; stearoyl aspartic acid tridecanol ester; stearoyl aspartic acid tetradecyl alchohol ester; stearoyl aspartic acid hexadecanol ester; stearoyl aspartic acid octadecanol ester; stearoyl aspartic acid eicosanol ester; the different lauryl alcohol ester of stearoyl aspartic acid; stearoyl aspartic acid isotridecanol; the different tetradecyl alchohol ester of stearoyl aspartic acid; the different hexadecanol ester of stearoyl aspartic acid; stearoyl aspartic acid i-octadecanol ester; the different eicosanol ester of stearoyl aspartic acid, eicosane acyl aspartic acid lauryl alcohol ester; eicosane acyl aspartic acid tridecanol ester; eicosane acyl aspartic acid tetradecyl alchohol ester; eicosane acyl aspartic acid hexadecanol ester; eicosane acyl aspartic acid octadecanol ester; the different lauryl alcohol ester of eicosane acyl aspartic acid; eicosane acyl aspartic acid isotridecanol; the different tetradecyl alchohol ester of eicosane acyl aspartic acid; the different hexadecanol ester of eicosane acyl aspartic acid; eicosane acyl aspartic acid i-octadecanol ester; the different eicosanol ester of eicosane acyl aspartic acid or their mixture.
11. a kind of emulsion composition according to claim 1 is characterized in that: its acidic amino acid partly is glutamic acid in the long-chain fat acyl acidic amino acid aliphatic alcohol ester of general formula (1) expression.
12. a kind of emulsion composition according to claim 1 is characterized in that: it is 0.1%～10% that the long-chain fat acyl acidic amino acid aliphatic alcohol ester of general formula (1) expression accounts for composition weight percentage ratio.
13. a kind of emulsion composition according to claim 1 is characterized in that: it is 0.5%～5% that the long-chain fat acyl acidic amino acid aliphatic alcohol ester of general formula (1) expression accounts for composition weight percentage ratio.
14. a kind of emulsion composition according to claim 1 is characterized in that: it is 5%～55% that oil phase component accounts for composition weight percentage ratio.
15. a kind of emulsion composition according to claim 1 is characterized in that: it is 10%～45% that oil phase component accounts for composition weight percentage ratio.
16. a kind of emulsion composition according to claim 1 is characterized in that: water ingredients constitute composition weight percentage ratio is 35%～90%.
17. a kind of emulsion composition according to claim 1 is characterized in that: water ingredients constitute composition weight percentage ratio is 50%～85%.
18. according to claim 1; or 2 described a kind of emulsion composition; it is characterized in that: be different from general formula (1) expression the coemulsifier of long-chain fat acyl acidic amino acid aliphatic alcohol ester be: C12～C18 alkyl carboxylate; C12～C18 alkylsulfonate; C12～C18 fatty alcohol sulfate salt; C12～C18 polyoxyethylene alkyl ether sulfate salt; C12～C18 fatty alcohol phosphates; C12～18 aliphatic alcohol polyoxyvinethene phosphate salt; C8～C20 alkanoyl lactate; the above-mentioned salt that becomes can be potassium salt; sodium salt; triethanolamine salt; polyoxyethylene aliphatic alcohol ether; polyoxyethylene carboxylate; fatty acid glyceride; the fatty acid ester of sorbitol or anhydrous sorbitol; the fatty acid ester of polyoxyethylene sorbitol or anhydrous sorbitol; sucrose fatty acid ester; polyglyceryl fatty acid ester; alkyl polyglucoside, or their mixture.
19. according to claim 1 or 2 described a kind of emulsion compositions, it is characterized in that: described be different from general formula (1) expression the coemulsifier of long-chain fat acyl acidic amino acid aliphatic alcohol ester be the HLB value greater than 7 emulsifying agent.
20. according to claim 1 or 3 described a kind of emulsion compositions, it is characterized in that: described adjuvant is: special composition, antiseptic, antioxidant, sunscreen, powder, coloring agent, the spice of water-soluble polymer thickening agent, wetting agent, pH regulator agent, cosmetics and efficacy cosmetic product.
21. according to right 1 or 2 or 3 described a kind of emulsion compositions, it is characterized in that: described emulsion composition is used for the effect of partes corporis humani position skin nursing, also can be used for the opsonic action of human hair.
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| CN103932905A (en) * | 2014-05-15 | 2014-07-23 | 苏州元素集化学工业有限公司 | Composition inducing to form lyotropic liquid crystal structure |
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| CN107550760A (en) * | 2017-09-23 | 2018-01-09 | 马述腾 | A kind of gestational period egg yolk bloom, newborn class cosmetics |
| CN109665787A (en) * | 2019-02-28 | 2019-04-23 | 陈辉 | A kind of manufacturing method of construction wall grouting material |
| CN110694305A (en) * | 2019-11-04 | 2020-01-17 | 青岛中宝硅材料科技有限公司 | Defoaming agent and preparation method thereof |
| CN111170883A (en) * | 2020-01-06 | 2020-05-19 | 岳阳科罗德联合化学工业有限公司 | Fatty acyl amino acid polyhydroxy ester compound and preparation method thereof |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103932905A (en) * | 2014-05-15 | 2014-07-23 | 苏州元素集化学工业有限公司 | Composition inducing to form lyotropic liquid crystal structure |
| CN103961268A (en) * | 2014-05-15 | 2014-08-06 | 苏州元素集化学工业有限公司 | Clean composition with lyotropic liquid crystal structure |
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| CN107550760A (en) * | 2017-09-23 | 2018-01-09 | 马述腾 | A kind of gestational period egg yolk bloom, newborn class cosmetics |
| CN109665787A (en) * | 2019-02-28 | 2019-04-23 | 陈辉 | A kind of manufacturing method of construction wall grouting material |
| CN110694305A (en) * | 2019-11-04 | 2020-01-17 | 青岛中宝硅材料科技有限公司 | Defoaming agent and preparation method thereof |
| CN111170883A (en) * | 2020-01-06 | 2020-05-19 | 岳阳科罗德联合化学工业有限公司 | Fatty acyl amino acid polyhydroxy ester compound and preparation method thereof |
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