CN107550760A - A kind of gestational period egg yolk bloom, newborn class cosmetics - Google Patents

A kind of gestational period egg yolk bloom, newborn class cosmetics Download PDF

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Publication number
CN107550760A
CN107550760A CN201710870011.9A CN201710870011A CN107550760A CN 107550760 A CN107550760 A CN 107550760A CN 201710870011 A CN201710870011 A CN 201710870011A CN 107550760 A CN107550760 A CN 107550760A
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yolk
egg yolk
gestational period
bloom
egg
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CN201710870011.9A
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马述腾
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Individual
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Abstract

The present invention relates to cosmetic field, more particularly to a kind of gestational period egg yolk bloom, newborn class cosmetics, it is characterised in that raw material is prepared by following weight part ratios:Security Oleum Ovum Gallus domesticus Flavus 1~20%, emulsifying agent 2~10%, thickener 0~5%, purified water polishing to 100%.The beneficial effects of the invention are as follows:It is safe to use without carcinogenic substance BaP, organic solvent-free residual;Essence and pigment are not added, property is gentle, effective the problems such as alleviating dry gravid skin, itch, is adapted to the gestational period to use.

Description

A kind of gestational period egg yolk bloom, newborn class cosmetics
Technical field
The present invention relates to cosmetic field, more particularly to a kind of gestational period egg yolk bloom, newborn class cosmetics.
Background technology
With developing rapidly for fine chemistry industry, cosmetics are widely used in daily life nursing, but someization by people Cosmetic often contains heavy metal and hormone, if long-term use can influence itself and offspring is healthy, gestational period cosmetics safety problem, The always emphasis of pregnant and lying-in women's concern, particularly cosmetics are to the health effect of fetus, and therefore, gestational period pregnant woman can select peace The special skin care item of pregnant woman of the harmful components such as entirely, alcohol-free, mineral oil, hormone, dyestuff and heavy metal.Gravid skin is due to swashing The influence of the reasons such as element, it may appear that it is obscure to dry water shortage, the colour of skin, even pruitus the problems such as, current commercially available pregnant woman is special Apply some make up and not can solve these problems still.
Oleum Ovum Gallus domesticus Flavus are extracted by egg yolk, containing abundant lecithin and unrighted acid, additionally contain albumen The multiple nutritional components such as matter amino acids, mineral matter, vitamins, Oleum Ovum Gallus domesticus Flavus can foster skin beauty, increase skin elasticity, egg Butter also has the effect of clearing heat and detoxicating, convergence, hemostasis, analgesic, has sterilization, anti-inflammatory and the work(for repairing cells of superficial layer to skin Can, it is very suitable for the production of gestational period cosmetics.
The method for producing Oleum Ovum Gallus domesticus Flavus at present is mainly traditional cracking process, drying method, chloroform extraction, ethanol extraction method, super Critical CO2Extraction, Propane extraction, Enzymatic Extraction, chromatogram extraction method.Traditional cracking process and drying method due to high temperature and Carcinogenic substance BaP is generated, and a large amount of smoke pollution of environment are produced in producing;Chloroform extraction and ethanol extraction method are industrial Used method, using a large amount of organic solvents, the problem of organic solvent residual be present;Supercritical CO2Extraction and subcritical Propane extraction big energy-consuming, hyperbaric environment is needed, and production cost is high, although the good product quality of its separation, composition can reach single One, but this method yields poorly and industrialization is not implemented;Enzymatic Extraction has the advantages of technique is simple, but lecithin is substantially free of in product Fat composition;Chromatogram extraction method treating capacity is limited, and product composition is single, problem of solvent residual be present.It can be seen that carcinogenic substance and organic molten Agent is to produce inevitable composition in Oleum Ovum Gallus domesticus Flavus at present, and these harmful components can cause potential threat to the health of human body.
Egg oil hair products are reported for work at present, such as Application No. 201610929880.X Chinese invention patent " egg oil emulsion preparation method ", 10~25 parts of mink oil, 30~45 parts of egg oil, 1~2 part of vitamin A, vitamine D1~2 Part, vitamin e1~2 part, 100~150 parts of palm wax, 3~5 parts of tea oil, 3~5 parts of triethanolamine stearate salt, lanolin 5~ 7 parts, 1~2 part of sorbitol polyoxyethylene monolaurate, 1~2 part of propane diols, 3~5 parts of glycerine, 1 part of spices, deionized water 1000 parts mix and produce product, but not yet explicitly egg oil source, may contain carcinogenic components BaP or organic solvent residual, meeting Health is threatened.For another example, Chinese invention patent " a kind of guarantor containing egg oil of Application No. 201210163986.5 Wet micro emulsion gel and preparation method thereof ", egg oil 1%~10%, surfactant 2%~20%, cosurfactant 6%~30%, Bionical NMF 0.1%~10%, gel-type vehicle 0.02%~2%, the water of preservative 0.2%~0.8% and surplus, but its egg oil makes Extracted with ethanol, containing organic solvent residual, be not suitable for gestational period use.Therefore, solve the above problems, invent a kind of nothing The gestational period egg oiling cosmetic of harmful components is very necessary.
The content of the invention
It is an object of the invention to provide a kind of gestational period egg yolk bloom, newborn class cosmetics, without harmful substance BaP, Organic solvent-free remains, and does not add essence and pigment, and property is gentle, is adapted to the gestational period to use, to reach above-mentioned purpose, the present invention Using following technical scheme:
A kind of gestational period egg yolk bloom, newborn class cosmetics, it is characterised in that raw material is prepared by following weight part ratios:
Security Oleum Ovum Gallus domesticus Flavus 1~20%, emulsifying agent 2~10%, thickener 0~5%, purified water polishing to 100%.
The emulsifying agent is Tween 65, Tween 85, Span 80, Crodaret, polyoxyethylene caster One or more in oil, PEG 400,1,2- propane diols, glycerine.
The thickener is the one or more in xanthans, Acritamer 940, carboxymethyl hydroxyethyl cellulose, alginic acid.
A kind of security Oleum Ovum Gallus domesticus Flavus are produced according to the following steps:
(1)Freshly-slaughtered poultry yolk is stocked up:The egg for selecting freshness >=72Ha is separated using equipment progress yolk with egg white, collects yolk Film does not rupture, the complete yolk of form;
(2)Ultrasound pretreatment:Yolk is subjected to ultrasonication, 25~50kHz of processing frequency, 5~15min of processing time, with Increase the permeability of egg membrane and destroy the emulsion stability of albumen and lipid in yolk;
(3)Hot-cold processing:The egg yolk complete to ultrasonication carries out hot-cold processing, using Hot-blast Heating, temperature 45~55 DEG C, 10~20min is kept, chilling treatment is carried out afterwards, 5~8 DEG C for the treatment of temperature, 20~30min is kept, further to destroy yolk The emulsion stability of middle albumen and lipid;
(4)Configure pickling liquid:By food-grade osmotic pressure regulator of the mass fraction for 1~40%, 0.1~10% food-grade acidity tune Agent, 0.1~5% food grade antioxidants, purified water polishing to 100% are saved, after stirring and dissolving, boiling sterilization is carried out, cools to room Temperature;
(5)Pickle:Processed egg yolk is placed in pickling liquid, the two weight ratio is 1:3~1:1, add into pickling liquid Enter the edible salt of final concentration of mass fraction 4%~10%, add by several times to form salt gradient, keep clean environment, temperature 30~ 40 DEG C are pickled 36~48h, 70 DEG C of 2~5h of curing;
(6)Centrifugation:Clean after pickling the egg yolk obtained and crushed, use industrial centrifugal machine collected after centrifugation fluid;
(7)Desalination:The purified water of 2~5 times of weight is added into the fluid of collection, repeats 2~5 times, is stood after being gently mixed Layering, retain upper strata fluid;
(8)Deodorize:Due in egg yolk curing process, there is volatile flavor substance, vacuum is used to deodorize to reduce flavor substances Matter content;
(9)Decolourize:A certain amount of activated carbon is added, the pigment in Oleum Ovum Gallus domesticus Flavus and the flavor substance not purified is adsorbed, makes egg Butter color and luster and taste are purer, and this finished product is Oleum Ovum Gallus domesticus Flavus finished product.
Above-mentioned steps(4)Described osmotic pressure regulator include but is not limited to sucrose, D-mannital, glycerine, carragheen, One or more in xanthans.
Above-mentioned steps(4)Described acidity regulator include but is not limited to acetic acid, phosphoric acid, hydrochloric acid, malic acid, citric acid, One or more in lactic acid.
Above-mentioned steps(4)Described antioxidant includes but is not limited to vitamin C.
A kind of gestational period egg yolk bloom, newborn class cosmetics are produced according to the following steps:
(10)Thickener is added in purified water after being fully swelled, be transferred in vacuum emulsifying machine, by security Oleum Ovum Gallus domesticus Flavus, emulsification Agent mixes, and is added gradually to after stirring in vacuum emulsifying machine, normal temperature, rotating speed 2500~2800r/min, homogeneous 40~ 60min, irradiation sterilization are a kind of gestational period egg yolk bloom, newborn class cosmetics.
The beneficial effects of the invention are as follows:Due to Oleum Ovum Gallus domesticus Flavus extraction without high-temperature process, without using organic solvent, therefore Carcinogenic substance BaP is free of in the Oleum Ovum Gallus domesticus Flavus of extraction, organic solvent-free remains, and safety in utilization is higher;Do not add essence and color Element, property is gentle, effective the problems such as alleviating dry gravid skin, itch, is adapted to the gestational period to use.
Embodiment
Following examples are used to illustrate the present invention, but are not limited to the scope of the present invention.
Embodiment 1
In market purchasing freshness >=72Ha 1000 pieces of egg, separated using yolk-egg white seperator, collect vitellinae membrana Complete uncracked yolk, weight in wet base 17.59kg.The egg yolk of collection is ultrasonically treated using supersonic wave cleaning machine, set Power 25kHz, handle 5min.Egg yolk after ultrasound is transferred to hot-air oven, design temperature is 45 DEG C, dries 15min, transfer To refrigerator, 5 DEG C of temperature, taken out after refrigerating 30min.Pickling liquid 30kg is prepared, 9kg glycerine, 1kg second are added into rustless steel container Acid, 0.2kg vitamin Cs, purified water 19.8kg, stir, and 20min is boiled in heating, cool to room temperature, are taken out after adding refrigeration Egg yolk, be placed in clean environment, set 35 DEG C of temperature, into pickling liquid add salt 0.06kg, be gently mixed to dissolving, Often cross 1h and add salt 0.06kg, pickle 48h, be allowed to dry pickling liquid, 70 DEG C of curing 5h, clean egg yolk and crush, use industry Centrifuge is centrifuged, rotating speed 4000r/min, retains centrifugation fluid 5.4kg.Purified water 26.5kg is added into centrifugation fluid, Rear stratification is gently mixed, retains upper strata fluid, vacuum is deodorized, 40 DEG C of temperature, vacuum -0.04Mpa, time 30min, added Enter activated carbon granule 1kg, precipitation filters to obtain Oleum Ovum Gallus domesticus Flavus 5.3kg after standing 2h.0.175kg Acritamer 940s are added into 27.13kg Be swelled in purified water, after be transferred in vacuum emulsifying machine, by 5.3kg Oleum Ovum Gallus domesticus Flavus, 2.15kg Tween 65,0.3kg glycerine stir It is added step-wise in vacuum emulsifying machine, normal temperature, rotating speed 2700r/min, homogeneous 60min, irradiation sterilization, produces a kind of pregnant after uniformly It is pregnent phase egg yolk bloom, newborn class cosmetics.
Embodiment 2
In market purchasing freshness >=72Ha 2000 pieces of egg, separated using yolk-egg white seperator, collect vitellinae membrana Complete uncracked yolk, weight in wet base 36.22kg.The egg yolk of collection is ultrasonically treated using supersonic wave cleaning machine, set Power 30kHz, handle 5min.Egg yolk after ultrasound is transferred to hot-air oven, design temperature is 50 DEG C, dries 10min, transfer To refrigerator, 6 DEG C of temperature, taken out after refrigerating 30min.Pickling liquid 60kg is prepared, 9kg glycerine, 5kg sugarcanes are added into rustless steel container Sugar, 0.7kg carragheens, 1kg acetic acid, 0.5kg phosphoric acid, 0.5kg vitamin Cs, purified water 43.3kg, stir, heating is boiled 20min, cool to room temperature, add after refrigeration the egg yolk taken out, be placed in clean environment, 40 DEG C of temperature is set, to pickling liquid Middle addition salt 0.1kg, it is gently mixed to dissolving, often crosses 1h and add salt 0.12kg, pickle 48h, be allowed to dry pickling liquid, 70 DEG C ripe Change 5h, clean egg yolk and crush, centrifuged using industrial centrifugal machine, rotating speed 4000r/min, retain centrifugation fluid 11.6kg.Purified water 45.6kg is added into centrifugation fluid, is gently mixed rear stratification, retains upper strata fluid, repeats washing 2 Retain final upper strata fluid after secondary, vacuum is deodorized, and 40 DEG C, vacuum -0.04Mpa, time 30min of temperature, adds activated carbon Particle 3kg, precipitation filter to obtain Oleum Ovum Gallus domesticus Flavus 11.4kg after standing 2h.70kg purified waters are transferred in vacuum emulsifying machine, will 11.4kg Oleum Ovum Gallus domesticus Flavus, 2.7kg Tween 85,2.1kg Span 80,2.3kg PEG 400,1.25kg are polyethylene glycol hydrogenated Castor oil is added step-wise in vacuum emulsifying machine after stirring, normal temperature, rotating speed 2800r/min, homogeneous 60min, irradiation sterilization, Produce a kind of gestational period egg yolk bloom, newborn class cosmetics.

Claims (6)

1. a kind of gestational period egg yolk bloom, newborn class cosmetics, it is characterised in that raw material is prepared by following weight part ratios:
Security Oleum Ovum Gallus domesticus Flavus 1~20%, emulsifying agent 2~10%, thickener 0~5%, purified water polishing to 100%;
A kind of security Oleum Ovum Gallus domesticus Flavus are produced according to the following steps:
(1)Freshly-slaughtered poultry yolk is stocked up:The egg for selecting freshness >=72Ha is separated using equipment progress yolk with egg white, collects yolk Film does not rupture, the complete yolk of form;
(2)Ultrasound pretreatment:Yolk is subjected to ultrasonication, 25~50kHz of processing frequency, 5~15min of processing time, with Increase the permeability of egg membrane and destroy the emulsion stability of albumen and lipid in yolk;
(3)Hot-cold processing:The egg yolk complete to ultrasonication carries out hot-cold processing, using Hot-blast Heating, temperature 45~55 DEG C, 10~20min is kept, chilling treatment is carried out afterwards, 5~8 DEG C for the treatment of temperature, 20~30min is kept, further to destroy yolk The emulsion stability of middle albumen and lipid;
(4)Configure pickling liquid:By food-grade osmotic pressure regulator of the mass fraction for 1~40%, 0.1~10% food-grade acidity tune Agent, 0.1~5% food grade antioxidants, purified water polishing to 100% are saved, after stirring and dissolving, boiling sterilization is carried out, cools to room Temperature;
(5)Pickle:Processed egg yolk is placed in pickling liquid, the two weight ratio is 1:3~1:1, add into pickling liquid Enter the edible salt of final concentration of mass fraction 4%~10%, add by several times to form salt gradient, keep clean environment, temperature 30~ 40 DEG C are pickled 36~48h, 70 DEG C of 2~5h of curing;
(6)Centrifugation:Clean after pickling the egg yolk obtained and crushed, use industrial centrifugal machine collected after centrifugation fluid;
(7)Desalination:The purified water of 2~5 times of weight is added into the fluid of collection, repeats 2~5 times, is stood after being gently mixed Layering, retain upper strata fluid;
(8)Deodorize:Due in egg yolk curing process, there is volatile flavor substance, vacuum is used to deodorize to reduce flavor substances Matter content;
(9)Decolourize:A certain amount of activated carbon is added, the pigment in Oleum Ovum Gallus domesticus Flavus and the flavor substance not purified is adsorbed, makes egg Butter color and luster and taste are purer, and this finished product is Oleum Ovum Gallus domesticus Flavus finished product;
A kind of gestational period egg yolk bloom, newborn class cosmetics are produced according to the following steps:
(10)Thickener is added in purified water after being fully swelled, be transferred in vacuum emulsifying machine, by security Oleum Ovum Gallus domesticus Flavus, emulsification Agent mixes, and is added gradually to after stirring in vacuum emulsifying machine, normal temperature, rotating speed 2500~2800r/min, homogeneous 40~ 60min, irradiation sterilization are a kind of gestational period egg yolk bloom, newborn class cosmetics.
2. a kind of gestational period egg yolk bloom according to claim 1, newborn class cosmetics, it is characterised in that described emulsification Agent is Tween 65, Tween 85, Span 80, Crodaret, Emulsifier EL-60, PEG 400,1,2- One or more in propane diols, glycerine.
3. a kind of gestational period egg yolk bloom according to claim 1, newborn class cosmetics, it is characterised in that described thickening Agent is the one or more in xanthans, Acritamer 940, carboxymethyl hydroxyethyl cellulose, alginic acid.
4. a kind of gestational period egg yolk bloom according to claim 1, newborn class cosmetics, it is characterised in that step(4)Institute The one or more that the osmotic pressure regulator stated includes but is not limited in sucrose, D-mannital, glycerine, carragheen, xanthans.
5. a kind of gestational period egg yolk bloom according to claim 1, newborn class cosmetics, it is characterised in that step(4)Institute The one or more that the acidity regulator stated includes but is not limited in acetic acid, phosphoric acid, hydrochloric acid, malic acid, citric acid, lactic acid.
6. a kind of gestational period egg yolk bloom according to claim 1, newborn class cosmetics, it is characterised in that step(4)Institute The antioxidant stated includes but is not limited to vitamin C.
CN201710870011.9A 2017-09-23 2017-09-23 A kind of gestational period egg yolk bloom, newborn class cosmetics Withdrawn CN107550760A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116391850A (en) * 2023-03-14 2023-07-07 华南理工大学 Yolk oil microemulsion with high antioxidant activity and preparation method and application thereof

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103230343A (en) * 2013-04-22 2013-08-07 苏州元素集化学工业有限公司 Emulsion composition
CN103816084A (en) * 2014-02-28 2014-05-28 华南理工大学 Slow- release lotion carrier for whitening and spot removing, and preparation method thereof
CN105232374A (en) * 2015-10-21 2016-01-13 广东龙湖科技股份有限公司 Efficient moderate moist type cleansing cream
CN105764472A (en) * 2013-12-17 2016-07-13 雅芳产品公司 Glycerin-in-oil emulsion
CN106667851A (en) * 2017-02-28 2017-05-17 高宝化妆品(中国)有限公司 Traditional Chinese medicine acne removal cream and preparation method thereof
CN107083269A (en) * 2017-04-01 2017-08-22 新疆喀什昆仑翠翎鸽业有限责任公司 One kind is without BaP pigeon eggs butter and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103230343A (en) * 2013-04-22 2013-08-07 苏州元素集化学工业有限公司 Emulsion composition
CN105764472A (en) * 2013-12-17 2016-07-13 雅芳产品公司 Glycerin-in-oil emulsion
CN103816084A (en) * 2014-02-28 2014-05-28 华南理工大学 Slow- release lotion carrier for whitening and spot removing, and preparation method thereof
CN105232374A (en) * 2015-10-21 2016-01-13 广东龙湖科技股份有限公司 Efficient moderate moist type cleansing cream
CN106667851A (en) * 2017-02-28 2017-05-17 高宝化妆品(中国)有限公司 Traditional Chinese medicine acne removal cream and preparation method thereof
CN107083269A (en) * 2017-04-01 2017-08-22 新疆喀什昆仑翠翎鸽业有限责任公司 One kind is without BaP pigeon eggs butter and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116391850A (en) * 2023-03-14 2023-07-07 华南理工大学 Yolk oil microemulsion with high antioxidant activity and preparation method and application thereof

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Application publication date: 20180109