CN107569443A - A kind of Oleum Ovum Gallus domesticus Flavus micro emulsion eyelashes, eyebrow nutrient solution - Google Patents
A kind of Oleum Ovum Gallus domesticus Flavus micro emulsion eyelashes, eyebrow nutrient solution Download PDFInfo
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- CN107569443A CN107569443A CN201710870773.9A CN201710870773A CN107569443A CN 107569443 A CN107569443 A CN 107569443A CN 201710870773 A CN201710870773 A CN 201710870773A CN 107569443 A CN107569443 A CN 107569443A
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- gallus domesticus
- ovum gallus
- domesticus flavus
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Abstract
The present invention relates to cosmetic field, more particularly to a kind of Oleum Ovum Gallus domesticus Flavus micro emulsion eyelashes, eyebrow nutrient solution, it is characterised in that raw material is prepared by following weight part ratios：Security Oleum Ovum Gallus domesticus Flavus 1~1.5%, superoxide dismutase 0.1~0.3%, emulsifying agent 1~1.5%, assistant for emulsifying agent 0.5~0.75%, purified water polishing to 100%.The beneficial effects of the invention are as follows：It is safe to use without carcinogenic substance BaP, organic solvent-free residual；Micro emulsion particle diameter is 50~55nm, easily absorbs, contains two kinds of active ingredients, it is possible to provide nutrition needed for eyelashes and eyebrow growth, can also extend the growth cycle of eyelashes and eyebrow, make eyelashes and eyebrows bushed together elongated；Do not stimulated gently using simple, no greasy feeling, easy cleaning, property, be adapted to long-term use.
Description
Technical field
The present invention relates to cosmetic field, more particularly to a kind of Oleum Ovum Gallus domesticus Flavus micro emulsion eyelashes, eyebrow nutrient solution.
Background technology
Micro emulsion is also referred to as nano-emulsion, is a kind of a kind of flowing being made up of water, oil and surfactant and auxiliary agent, transparent, hot
Mechanics is stable, the liquid of isotropy, usual micro emulsion outward appearance clarification, transparent or semitransparent, and size droplet diameter is typically in 10~
Between 100nm.Bioavilability of the micro emulsion commonly used to improve oral or external used medicine, and without greasy feeling, it is washable remove, to skin
It is nonirritant with mucous membrane.
Oleum Ovum Gallus domesticus Flavus are extracted by egg yolk, and folk remedy uses it for the treatment of alopecia, and effect is preferable, and the modern times face
Bed research it has proven convenient that Oleum Ovum Gallus domesticus Flavus contain a variety of lipids, vitamin, more than blood egg oil can make after depilation the growth of mouse fur plus
It hurry up.The method for producing Oleum Ovum Gallus domesticus Flavus at present is mainly traditional cracking process, drying method, chloroform extraction, ethanol extraction method, overcritical
CO2Extraction, Propane extraction, Enzymatic Extraction, chromatogram extraction method.Traditional cracking process and drying method are generated due to high temperature
Carcinogenic substance BaP, and produce a large amount of smoke pollution of environment in producing；Chloroform extraction and ethanol extraction method is industrially are adopted
Method, using a large amount of organic solvents, the problem of organic solvent residual be present；Supercritical CO2Extraction and Propane
Extraction big energy-consuming, hyperbaric environment is needed, and production cost is high, although the good product quality of its separation, composition can reach single,
This method, which yields poorly, is not implemented industrialization；Enzymatic Extraction has the advantages of technique is simple, but be substantially free of in product lecithin into
Point；Chromatogram extraction method treating capacity is limited, and product composition is single, problem of solvent residual be present.It can be seen that carcinogenic substance and organic solvent are
Inevitable composition in Oleum Ovum Gallus domesticus Flavus is produced at present, these harmful components can cause potential threat to the health of human body.
Oleum Ovum Gallus domesticus Flavus are used as can be directly as eyelashes nutrient solution, but feels greasy, uncomfortable after, and bioavilability
Low, using effect is bad, and egg oil microemulsion can effectively solve these problems.At present to yolk oil microemulsion and its eyelashes, eyebrow
The invention of nutrient solution there is no report.
The content of the invention
It is an object of the invention to provide a kind of Oleum Ovum Gallus domesticus Flavus micro emulsion eyelashes, eyebrow nutrient solution, without harmful substance BaP,
Organic solvent-free remains, and has nontoxic non-stimulated, extension eyelashes, eyebrow growth cycle, there is provided eyelashes, the work(of eyebrow maintenance composition
Effect, to reach above-mentioned purpose, the present invention uses following technical scheme：
A kind of Oleum Ovum Gallus domesticus Flavus micro emulsion eyelashes, eyebrow nutrient solution, it is characterised in that raw material is prepared by following weight part ratios：
Security Oleum Ovum Gallus domesticus Flavus 1~1.5%, superoxide dismutase 0.1~0.3%, emulsifying agent 1~1.5%, assistant for emulsifying agent 0.5~
0.75%th, purified water polishing is to 100%.
The emulsifying agent is in Tween 80, Cremophor RH-40, Cremophor EL-35, Solutol HS-15
One or more.
The assistant for emulsifying agent is the one or more in PEG 400, transcutol P, 1,2- propane diols, glycerine.
A kind of security Oleum Ovum Gallus domesticus Flavus are produced according to the following steps：
（1）Freshly-slaughtered poultry yolk is stocked up：The egg for selecting freshness >=72Ha is separated using equipment progress yolk with egg white, collects yolk
Film does not rupture, the complete yolk of form；
（2）Ultrasound pretreatment：Yolk is subjected to ultrasonication, 25~50kHz of processing frequency, 5~15min of processing time, with
Increase the permeability of egg membrane and destroy the emulsion stability of albumen and lipid in yolk；
（3）Hot-cold processing：The egg yolk complete to ultrasonication carries out hot-cold processing, using Hot-blast Heating, temperature 45~55
DEG C, 10~20min is kept, chilling treatment is carried out afterwards, 5~8 DEG C for the treatment of temperature, 20~30min is kept, further to destroy yolk
The emulsion stability of middle albumen and lipid；
（4）Configure pickling liquid：By food-grade osmotic pressure regulator of the mass fraction for 1~40%, 0.1~10% food-grade acidity tune
Agent, 0.1~5% food grade antioxidants, purified water polishing to 100% are saved, after stirring and dissolving, boiling sterilization is carried out, cools to room
Temperature；
（5）Pickle：Processed egg yolk is placed in pickling liquid, the two weight ratio is 1:3~1：1, add into pickling liquid
Enter the edible salt of final concentration of mass fraction 4%~10%, add by several times to form salt gradient, keep clean environment, temperature 30~
40 DEG C are pickled 36~48h, 70 DEG C of 2~5h of curing；
（6）Centrifugation：Clean after pickling the egg yolk obtained and crushed, use industrial centrifugal machine collected after centrifugation fluid；
（7）Desalination：The purified water of 2~5 times of weight is added into the fluid of collection, repeats 2~5 times, is stood after being gently mixed
Layering, retain upper strata fluid；
（8）Deodorize：Due in egg yolk curing process, there is volatile flavor substance, vacuum is used to deodorize to reduce flavor substances
Matter content；
（9）Decolourize：A certain amount of activated carbon is added, the pigment in Oleum Ovum Gallus domesticus Flavus and the flavor substance not purified is adsorbed, makes egg
Butter color and luster and taste are purer, and this finished product is Oleum Ovum Gallus domesticus Flavus finished product.
Above-mentioned steps（4）Described osmotic pressure regulator include but is not limited to sucrose, D-mannital, glycerine, carragheen,
One or more in xanthans.
Above-mentioned steps（4）Described acidity regulator include but is not limited to acetic acid, phosphoric acid, hydrochloric acid, malic acid, citric acid,
One or more in lactic acid.
Above-mentioned steps（4）Described antioxidant includes but is not limited to vitamin C.
A kind of Oleum Ovum Gallus domesticus Flavus micro emulsion eyelashes, eyebrow nutrient solution are produced according to the following steps：
（10）Emulsification：Purified water is transferred in vacuum emulsifying machine, superoxide dismutase dissolving is added, by security egg yolk
It is added gradually to after being stirred after oil, emulsifying agent, assistant for emulsifying agent mixing in vacuum emulsifying machine, normal temperature, rotating speed 2500~
2800r/min, homogeneous 40~60min, obtain light blue clear or translucent liquid, and irradiation sterilization is a kind of Oleum Ovum Gallus domesticus Flavus
Micro emulsion eyelashes, eyebrow nutrient solution.
The beneficial effects of the invention are as follows：Due to Oleum Ovum Gallus domesticus Flavus extraction without high-temperature process, without using organic solvent, therefore
Carcinogenic substance BaP is free of in the Oleum Ovum Gallus domesticus Flavus of extraction, organic solvent-free remains, and safety in utilization is higher；Micro emulsion particle diameter be 50~
55nm, easily absorb, contain two kinds of active ingredients, it is possible to provide nutrition needed for eyelashes and eyebrow growth, can also extend eyelashes and eyebrow
Growth cycle, eyelashes and eyebrows bushed together can be made elongated；Do not stimulated gently, fitted using simple, no greasy feeling, easy cleaning, property
Close long-term use of.
Embodiment
Following examples are used to illustrate the present invention, but are not limited to the scope of the present invention.
Embodiment 1
In market purchasing freshness >=72Ha 1000 pieces of egg, separated using yolk-egg white seperator, collect vitellinae membrana
Complete uncracked yolk, weight in wet base 17.59kg.The egg yolk of collection is ultrasonically treated using supersonic wave cleaning machine, set
Power 25kHz, handle 5min.Egg yolk after ultrasound is transferred to hot-air oven, design temperature is 45 DEG C, dries 15min, transfer
To refrigerator, 5 DEG C of temperature, taken out after refrigerating 30min.Pickling liquid 30kg is prepared, 9kg glycerine, 1kg second are added into rustless steel container
Acid, 0.2kg vitamin Cs, purified water 19.8kg, stir, and 20min is boiled in heating, cool to room temperature, are taken out after adding refrigeration
Egg yolk, be placed in clean environment, set 35 DEG C of temperature, into pickling liquid add salt 0.06kg, be gently mixed to dissolving,
Often cross 1h and add salt 0.06kg, pickle 48h, be allowed to dry pickling liquid, 70 DEG C of curing 5h, clean egg yolk and crush, use industry
Centrifuge is centrifuged, rotating speed 4000r/min, retains centrifugation fluid 5.4kg.Purified water 26.5kg is added into centrifugation fluid,
Rear stratification is gently mixed, retains upper strata fluid, vacuum is deodorized, 40 DEG C of temperature, vacuum -0.04Mpa, time 30min, added
Enter activated carbon granule 1kg, precipitation filters to obtain Oleum Ovum Gallus domesticus Flavus 5.3kg after standing 2h.0.35kg superoxide dismutases are dissolved in
In 336.53kg purified waters, it is transferred in vacuum emulsifying machine, by 5.3kg Oleum Ovum Gallus domesticus Flavus, 5.3kgTween 80,2.65kgPEG 400
It is added step-wise to after stirring in vacuum emulsifying machine, normal temperature, rotating speed 2800r/min, homogeneous 60min, obtains light blue translucent
Liquid, irradiation sterilization, produce a kind of Oleum Ovum Gallus domesticus Flavus micro emulsion eyelashes, eyebrow nutrient solution.
Embodiment 2
In market purchasing freshness >=72Ha 2000 pieces of egg, separated using yolk-egg white seperator, collect vitellinae membrana
Complete uncracked yolk, weight in wet base 36.22kg.The egg yolk of collection is ultrasonically treated using supersonic wave cleaning machine, set
Power 30kHz, handle 5min.Egg yolk after ultrasound is transferred to hot-air oven, design temperature is 50 DEG C, dries 10min, transfer
To refrigerator, 6 DEG C of temperature, taken out after refrigerating 30min.Pickling liquid 60kg is prepared, 9kg glycerine, 5kg sugarcanes are added into rustless steel container
Sugar, 0.7kg carragheens, 1kg acetic acid, 0.5kg phosphoric acid, 0.5kg vitamin Cs, purified water 43.3kg, stir, heating is boiled
20min, cool to room temperature, add after refrigeration the egg yolk taken out, be placed in clean environment, 40 DEG C of temperature is set, to pickling liquid
Middle addition salt 0.1kg, it is gently mixed to dissolving, often crosses 1h and add salt 0.12kg, pickle 48h, be allowed to dry pickling liquid, 70 DEG C ripe
Change 5h, clean egg yolk and crush, centrifuged using industrial centrifugal machine, rotating speed 4000r/min, retain centrifugation fluid
11.6kg.Purified water 45.6kg is added into centrifugation fluid, is gently mixed rear stratification, retains upper strata fluid, repeats washing 2
Retain final upper strata fluid after secondary, vacuum is deodorized, and 40 DEG C, vacuum -0.04Mpa, time 30min of temperature, adds activated carbon
Particle 3kg, precipitation filter to obtain Oleum Ovum Gallus domesticus Flavus 11.4kg after standing 2h.1.425kg superoxide dismutases are dissolved in
In 919.13kg purified waters, be transferred in vacuum emulsifying machine, by 11.4kg Oleum Ovum Gallus domesticus Flavus, 8.35kgCremophor EL-35,
4kgSolutol HS-15,3.1kg transcutol P, 2.6kg glycerine are added step-wise to vacuum emulsifying machine after stirring
In, normal temperature, rotating speed 2600r/min, homogeneous 50min, light blue transparency liquid is obtained, irradiation sterilization, it is micro- to produce a kind of Oleum Ovum Gallus domesticus Flavus
Newborn eyelashes, eyebrow nutrient solution.
Claims (6)
1. a kind of Oleum Ovum Gallus domesticus Flavus micro emulsion eyelashes, eyebrow nutrient solution, it is characterised in that raw material is prepared by following weight part ratios：
Security Oleum Ovum Gallus domesticus Flavus 1~1.5%, superoxide dismutase 0.1~0.3%, emulsifying agent 1~1.5%, assistant for emulsifying agent 0.5~
0.75%th, purified water polishing is to 100%；
A kind of security Oleum Ovum Gallus domesticus Flavus are produced according to the following steps：
（1）Freshly-slaughtered poultry yolk is stocked up：The egg for selecting freshness >=72Ha is separated using equipment progress yolk with egg white, collects yolk
Film does not rupture, the complete yolk of form；
（2）Ultrasound pretreatment：Yolk is subjected to ultrasonication, 25~50kHz of processing frequency, 5~15min of processing time, with
Increase the permeability of egg membrane and destroy the emulsion stability of albumen and lipid in yolk；
（3）Hot-cold processing：The egg yolk complete to ultrasonication carries out hot-cold processing, using Hot-blast Heating, temperature 45~55
DEG C, 10~20min is kept, chilling treatment is carried out afterwards, 5~8 DEG C for the treatment of temperature, 20~30min is kept, further to destroy yolk
The emulsion stability of middle albumen and lipid；
（4）Configure pickling liquid：By food-grade osmotic pressure regulator of the mass fraction for 1~40%, 0.1~10% food-grade acidity tune
Agent, 0.1~5% food grade antioxidants, purified water polishing to 100% are saved, after stirring and dissolving, boiling sterilization is carried out, cools to room
Temperature；
（5）Pickle：Processed egg yolk is placed in pickling liquid, the two weight ratio is 1:3~1：1, add into pickling liquid
Enter the edible salt of final concentration of mass fraction 4%~10%, add by several times to form salt gradient, keep clean environment, temperature 30~
40 DEG C are pickled 36~48h, 70 DEG C of 2~5h of curing；
（6）Centrifugation：Clean after pickling the egg yolk obtained and crushed, use industrial centrifugal machine collected after centrifugation fluid；
（7）Desalination：The purified water of 2~5 times of weight is added into the fluid of collection, repeats 2~5 times, is stood after being gently mixed
Layering, retain upper strata fluid；
（8）Deodorize：Due in egg yolk curing process, there is volatile flavor substance, vacuum is used to deodorize to reduce flavor substances
Matter content；
（9）Decolourize：A certain amount of activated carbon is added, the pigment in Oleum Ovum Gallus domesticus Flavus and the flavor substance not purified is adsorbed, makes egg
Butter color and luster and taste are purer, and this finished product is Oleum Ovum Gallus domesticus Flavus finished product；
A kind of Oleum Ovum Gallus domesticus Flavus micro emulsion eyelashes, eyebrow nutrient solution are produced according to the following steps：
（10）Emulsification：Purified water is transferred in vacuum emulsifying machine, superoxide dismutase dissolving is added, by security egg yolk
It is added gradually to after being stirred after oil, emulsifying agent, assistant for emulsifying agent mixing in vacuum emulsifying machine, normal temperature, rotating speed 2500~
2800r/min, homogeneous 40~60min, obtain light blue clear or translucent liquid, and irradiation sterilization is a kind of Oleum Ovum Gallus domesticus Flavus
Micro emulsion eyelashes, eyebrow nutrient solution.
2. a kind of Oleum Ovum Gallus domesticus Flavus micro emulsion eyelashes according to claim 1, eyebrow nutrient solution is characterized in that described emulsification
Agent is the one or more in Tween 80, Cremophor RH-40, Cremophor EL-35, Solutol HS-15.
3. a kind of Oleum Ovum Gallus domesticus Flavus micro emulsion eyelashes according to claim 1, eyebrow nutrient solution, which is characterized in that, described helps breast
Agent is the one or more in PEG 400, transcutol P, 1,2- propane diols, glycerine.
4. a kind of Oleum Ovum Gallus domesticus Flavus micro emulsion eyelashes according to claim 1, eyebrow nutrient solution, it is characterised in that step（4）Institute
The one or more that the osmotic pressure regulator stated includes but is not limited in sucrose, D-mannital, glycerine, carragheen, xanthans.
5. a kind of Oleum Ovum Gallus domesticus Flavus micro emulsion eyelashes according to claim 1, eyebrow nutrient solution, it is characterised in that step（4）Institute
The one or more that the acidity regulator stated includes but is not limited in acetic acid, phosphoric acid, hydrochloric acid, malic acid, citric acid, lactic acid.
6. a kind of Oleum Ovum Gallus domesticus Flavus micro emulsion eyelashes according to claim 1, eyebrow nutrient solution, it is characterised in that step（4）Institute
The antioxidant stated includes but is not limited to vitamin C.
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| CN201710870773.9A CN107569443A (en) | 2017-09-23 | 2017-09-23 | A kind of Oleum Ovum Gallus domesticus Flavus micro emulsion eyelashes, eyebrow nutrient solution |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116196237A (en) * | 2023-05-04 | 2023-06-02 | 山东博科医用材料有限公司 | Antioxidant slow-release enzyme preparation |
| CN116391850A (en) * | 2023-03-14 | 2023-07-07 | 华南理工大学 | Yolk oil microemulsion with high antioxidant activity and preparation method and application thereof |
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| CN102670466A (en) * | 2012-05-24 | 2012-09-19 | 中国中医科学院中药研究所 | Moisture-retaining micro-emulsion gel containing egg yolk oil, and preparation method thereof |
| CN103816084A (en) * | 2014-02-28 | 2014-05-28 | 华南理工大学 | Slow- release lotion carrier for whitening and spot removing, and preparation method thereof |
| CN106377445A (en) * | 2016-10-20 | 2017-02-08 | 八步区科学技术情报研究所 | Preparation method of yolk oil emulsion |
| CN106420417A (en) * | 2016-10-20 | 2017-02-22 | 八步区科学技术情报研究所 | Preparation method of jojoba wax emulsion |
| CN106539740A (en) * | 2016-10-20 | 2017-03-29 | 八步区科学技术情报研究所 | Mink oil skin protection liquid and preparation method thereof |
| CN107083269A (en) * | 2017-04-01 | 2017-08-22 | 新疆喀什昆仑翠翎鸽业有限责任公司 | One kind is without BaP pigeon eggs butter and preparation method thereof |
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2017
- 2017-09-23 CN CN201710870773.9A patent/CN107569443A/en not_active Withdrawn
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102670466A (en) * | 2012-05-24 | 2012-09-19 | 中国中医科学院中药研究所 | Moisture-retaining micro-emulsion gel containing egg yolk oil, and preparation method thereof |
| CN103816084A (en) * | 2014-02-28 | 2014-05-28 | 华南理工大学 | Slow- release lotion carrier for whitening and spot removing, and preparation method thereof |
| CN106377445A (en) * | 2016-10-20 | 2017-02-08 | 八步区科学技术情报研究所 | Preparation method of yolk oil emulsion |
| CN106420417A (en) * | 2016-10-20 | 2017-02-22 | 八步区科学技术情报研究所 | Preparation method of jojoba wax emulsion |
| CN106539740A (en) * | 2016-10-20 | 2017-03-29 | 八步区科学技术情报研究所 | Mink oil skin protection liquid and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116391850A (en) * | 2023-03-14 | 2023-07-07 | 华南理工大学 | Yolk oil microemulsion with high antioxidant activity and preparation method and application thereof |
| CN116391850B (en) * | 2023-03-14 | 2024-05-17 | 华南理工大学 | Yolk oil microemulsion with high antioxidant activity and preparation method and application thereof |
| CN116196237A (en) * | 2023-05-04 | 2023-06-02 | 山东博科医用材料有限公司 | Antioxidant slow-release enzyme preparation |
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