CN103211723A - Pudding-shaped cream composition for skin nursing and preparation method thereof - Google Patents
Pudding-shaped cream composition for skin nursing and preparation method thereof Download PDFInfo
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- CN103211723A CN103211723A CN2012102122860A CN201210212286A CN103211723A CN 103211723 A CN103211723 A CN 103211723A CN 2012102122860 A CN2012102122860 A CN 2012102122860A CN 201210212286 A CN201210212286 A CN 201210212286A CN 103211723 A CN103211723 A CN 103211723A
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Abstract
The invention discloses a pudding-shaped cream composition for skin nursing and a preparation method thereof. The cream composition is characterized in that: the cream composition has pudding-shaped appearance, after dug with a spoon, the cream can remove a flat shape after a certain time, and when contacting skin, the cream has advantages of rapid demulsification and excellent moisture retention effect. The preparation method comprises: (1) based on a mass ratio, weighting grease, heating to 55 DEG C for dissolving, and uniformly stirring; (2) based on a mass ratio, weighting polyol, sorbitol fatty acid ester, sorbitan sesquioleate, polyether modified cetanol ester of polypropylene glycol unit and a thickening agent, adding them in water, heating to 55 DEG C, after stirring for dissolving, adding a neutralizer weighted by a substance weight ratio, after stirring for dissolving, adding grease prepared based on the step (1), homogenizing for 5min by a high speed shearing homogenizer, and stirring for cooling, to obtain the pudding-shaped cream. Personal nursing cream in the invention has pudding-shaped appearance, and the cream has a rapid-dissolving characteristic when coated on the skin, and can be applied in personal cosmetics.
Description
Technical field
The present invention relates to a kind of skin nursing with pudding-like cream cream composition and preparation method thereof, belong to cosmetic field.
Background technology
The cream frost is that a kind of common skin nursing applies some make up.Traditional cream frost generally is oil-in-water (O/W) and Water-In-Oil (W/O) form, realizes oil, the biphase uniform mixing of water by emulsifying agent.The present invention then adopts the collocation by emulsifying agent and polymer, make polymer encase oil earlier again by being emulsified into the form of water packet aggregation thing bag oil (O/P/W), the cream frost of this emulsifying type has unique pudding-like outward appearance, the mastic that dug with spoon can recover smooth shape behind certain hour, touch the characteristics that skin has fast emulsion breaking in use.
The preparation of cream frost need realize that the conventional emulsification temperature need heat 70-80 ℃ by emulsifying process.The emulsifying temperature of pudding-like cream cream composition of the present invention only need be heated to 55 ℃, not only can save the required heat of heating, also reduces heating-up temperature time and temperature fall time simultaneously, has improved production efficiency, has energy-conservation, low-carbon (LC), advantage efficiently.
Summary of the invention
The object of the present invention is to provide a kind of skin nursing pudding-like cream cream composition and preparation method thereof.
To achieve the object of the present invention, the present invention has adopted following technical scheme:
A kind of skin nursing pudding-like cream cream composition is characterized in that comprising following components in weight percentage:
Oils and fats 5-20%;
Span 0.5-3%;
The unitary polyether-modified spermaceti alcohol ester 0.5-2% of polypropylene glycol;
The smooth sesquialter fatty acid ester of Pyrusussuriensis 0.1-0.5%;
Thickening agent 0.3-2%;
Polyhydric alcohol 5-15%;
Nertralizer 0.1-2%;
The deionized water surplus.
Oils and fats in the above-mentioned composition is two or more a mixture of Parleam, dicaprylyl carbonate, caprylic/capric triglyceride, spermol ethylhexoate, hydrogenated polydecene, C12-15 alcohol benzoate, isomery hexadecane, polydimethylsiloxane, Cyclomethicone.
Span in the above-mentioned composition is one or more combinations in sorbitol polyethers-20 5 isostearate, sorbitol polyethers-30 5 isostearate, sorbitol polyethers-40 5 isostearate, sorbitol polyethers-50 5 isostearate, sorbitol polyethers-20 tetraoctyl stearate, sorbitol polyethers-30 tetraoctyl stearate, sorbitol polyethers-40 tetraoctyl stearate, sorbitol polyethers-50 tetraoctyl stearate.
The smooth sesquialter fatty acid ester of Pyrusussuriensis in the above-mentioned composition is one or more combinations in the smooth sesquialter isostearate of Pyrusussuriensis, the smooth sesquioleate of Pyrusussuriensis, the smooth sesquistearate of Pyrusussuriensis;
The unitary polyether-modified spermaceti alcohol ester of polypropylene glycol in the above-mentioned composition is one or more combinations in PPG-4-spermol polyethers-20, PPG-5-spermol polyethers-20, the PPG-8-spermol polyethers-20;
Thickening agent in the above-mentioned composition is one or more combinations in acrylic acid (ester) class/behenyl alcohol polyethers-25 methacrylate copolymer, acrylic acid (ester) class/stearyl alcohol polyethers-20 methacrylate copolymer, acrylic acid (ester) class/stearyl alcohol polyethers-20 methacrylate cross linked polymer.
Nertralizer in the above-mentioned composition is one or more combinations in sodium hydroxide, potassium hydroxide, triethanolamine, aminomethyl propanol, the arginine.
Polyhydric alcohol in the above-mentioned composition is glycerol, propylene glycol, butanediol, dipropylene glycol, 1, one or more combinations in ammediol, sorbitol, the Polyethylene Glycol-8.
Pudding-like cream cream composition of the present invention can also suitably add as required and is fit to the common composition that cosmetics use except containing as above component, as compositions such as chelating agen, antioxidant, antiseptic, essence.
The preparation method of pudding-like cream cream composition of the present invention, concrete steps are:
(1) oils and fats is put into oil cauldron and be heated to 55 ℃, mix, it is dissolved fully, stand-by.
(2) water, polyhydric alcohol are put into the emulsifying pot and be heated to 55 ℃, mix, it is dissolved fully, stand-by.
(3) Span, the unitary polyether-modified spermaceti alcohol ester of polypropylene glycol, the smooth sesquialter fatty acid ester of Pyrusussuriensis are put into the emulsifying pot and be heated to 55 ℃, mix after the dissolving, homogenizing 5 minutes dissolves it fully, and is stand-by.
(4) nertralizer is dropped into the emulsifying pot, stir after the dissolving, homogenizing 2 minutes.
(5) oils and fats is drawn into the emulsifying pot, uses high speed shear homogenizer homogenizing 5 minutes while stirring, stir.
(6) cool to 40 ℃ and add essence, antiseptic, active matter, stir.
(7) evacuation stirs, and cools to 35 ℃ of dischargings, gets final product.
The specific embodiment
Below come by specific embodiment that the present invention is further illustrated, but these embodiment are not limitations of the present invention just in order to illustrate.
Embodiment 1 pudding-like cream cream composition (I)
Prescription sees Table 1.
Table 1
Preparation method is as follows:
(1) A component input is put into oil cauldron and be heated to 55 ℃, mix, it is dissolved fully, stand-by.
(2) B component input is put into the emulsifying pot and be heated to 55 ℃, mix, it is dissolved fully, stand-by.
(3) the C component is dropped into the emulsifying pot, put into the emulsifying pot and be heated to 55 ℃, mix after the dissolving, homogenizing 5 minutes dissolves it fully, and is stand-by.
(4) the D component is dropped into the emulsifying pot, stir homogenizing 2 minutes after the dissolving.
(5) the A component is drawn into the emulsifying pot, uses high speed shear homogenizer homogenizing 5 minutes while stirring, stir.
(6) cool to 40 ℃ with E component adding emulsifying pot, stir.
(7) stir, evacuation cools to 35 ℃ of dischargings, gets final product.
Embodiment 2 pudding-like cream cream compositions (II)
Composite formula sees Table 2.
Table 2
Preparation method is as follows:
(1) A component input is put into oil cauldron and be heated to 55 ℃, mix, it is dissolved fully, stand-by.
(2) B component input is put into the emulsifying pot and be heated to 55 ℃, mix, it is dissolved fully, stand-by.
(3) the C component is dropped into the emulsifying pot, put into the emulsifying pot and be heated to 55 ℃, mix after the dissolving, homogenizing 5 minutes dissolves it fully, and is stand-by.
(4) the D component is dropped into the emulsifying pot, stir homogenizing 2 minutes after the dissolving.
(5) the A component is drawn into the emulsifying pot, uses high speed shear homogenizer homogenizing 5 minutes while stirring, stir.
(6) cool to 40 ℃ with E component adding emulsifying pot, stir.
(7) stir, evacuation cools to 35 ℃ of dischargings, gets final product.
Embodiment 3 pudding-like cream cream compositions (III)
Prescription sees Table 3.
Table 3
Preparation method is as follows:
(1) A component input is put into oil cauldron and be heated to 55 ℃, mix, it is dissolved fully, stand-by.
(2) B component input is put into the emulsifying pot and be heated to 55 ℃, mix, it is dissolved fully, stand-by.
(3) the C component is dropped into the emulsifying pot, put into the emulsifying pot and be heated to 55 ℃, mix after the dissolving, homogenizing 5 minutes dissolves it fully, and is stand-by.
(4) the D component is dropped into the emulsifying pot, stir homogenizing 2 minutes after the dissolving.
(5) the A component is drawn into the emulsifying pot, uses high speed shear homogenizer homogenizing 5 minutes while stirring, stir.
(6) cool to 40 ℃ with E component adding emulsifying pot, stir.
(7) stir, evacuation cools to 35 ℃ of dischargings, gets final product.
Embodiment 4 moisture-keeping efficacy evaluation experimentals
1, experimental principle: the hydration status that adopts Comermeter CM825 test keratodermatitis.After test probe and the contact skin, test the relative variation of capacitance, can obtain characterizing relative value's (degree of hydration rate of change) of hydration status by the calculating of instrument internal.Degree of hydration is more little, moisture is more little, and moisture is big more conversely.The calculating of degree of hydration is calculated by formula (1)
2, experimental apparatus: Comermeter CM825 (German Courage+Khazaha company
3, experimental technique: 20 of healthy volunteers, 10 of male, 10 of women, the age is in 25-50 year.At isoperibol (22 ± 1 ℃), relative humidity 50 ± 5% is had a rest after 1 hour.Get an amount of sample (sample that adopts pudding-like cream cream composition (III) to work it out) and be coated in experimenter's left hand forearm inboard (4cm * 4cm) and right forearm inboard (4cm * 4cm).Blank (not being coated with) is tested simultaneously.Be coated with the degree of hydration state of testing skin in 1 hour, 2 hours, 4 hours, 5 hours of sample respectively.
4, experimental result: the results are shown in the shown in Figure 1 of accompanying drawing.
The result shows that the degree of hydration of sample still has 40.66% after 5 hours, illustrates that pudding-like cream cream composition (III) has the good moisture preserving effect.
Claims (9)
1. a skin nursing is with pudding-like cream cream composition.This pudding-like cream frost is characterised in that to have unique pudding-like outward appearance, after the mastic surface is dug, can recover smooth shape behind the certain hour of mastic surface with spoon, touch skin in use and one be coated with gently, have the characteristics of fast emulsion breaking, and have well instant moistening effect.This pudding-like cream cream composition is characterised in that and comprises following components in weight percentage:
Oils and fats 5-20%;
Span 0.5-3%;
The unitary polyether-modified spermaceti alcohol ester 0.5-2% of polypropylene glycol;
The smooth sesquialter fatty acid ester of Pyrusussuriensis 0.1-0.5%;
Thickening agent 0.3-2%;
Polyhydric alcohol 5-15%;
Nertralizer 0.1-2%;
The deionized water surplus.
2. compositions according to claim 1, wherein said oils and fats are the mixture of Parleam, dicaprylyl carbonate, isomery hexadecane, Cyclomethicone.
3. compositions according to claim 1, wherein said Span are any one or the multiple combination in sorbitol polyethers-20 isostearate, sorbitol polyethers-30 5 isostearate, sorbitol polyethers-40 5 isostearate, sorbitol polyethers-50 isostearate, sorbitol polyethers-20 tetraoctyl stearate, sorbitol polyethers-30 tetraoctyl stearate, sorbitol polyethers-40 tetraoctyl stearate, sorbitol polyethers-50 tetraoctyl stearate.
4. compositions according to claim 1, the smooth sesquialter fatty acid ester of wherein said Pyrusussuriensis are any one or the multiple combination in the smooth sesquialter isostearate of Pyrusussuriensis, the smooth sesquioleate of Pyrusussuriensis, the smooth sesquistearate of Pyrusussuriensis.
5. compositions according to claim 1, the unitary polyether-modified spermaceti alcohol ester of wherein said polypropylene glycol are any one and the multiple combination in PPG-4-spermol polyethers-20, PPG-5-spermol polyethers-20, the PPG-8-spermol polyethers-20.
6. compositions according to claim 1, wherein said thickening agent are any one or the multiple combination in acrylic acid (ester) class/behenyl alcohol polyethers-25 methacrylate copolymer, acrylic acid (ester) class/stearyl alcohol polyethers-20 methacrylate copolymer, acrylic acid (ester) class/stearyl alcohol polyethers-20 methacrylate cross linked polymer.
7. compositions according to claim 1, wherein said nertralizer are any one or the multiple combination in sodium hydroxide, potassium hydroxide, triethanolamine, aminomethyl propanol, the arginine.
8. compositions as claimed in claim 1, wherein said polyhydric alcohol are glycerol, propylene glycol, butanediol, dipropylene glycol, 1, any one in ammediol, sorbitol, the Polyethylene Glycol-8 or multiple combination.
9. the described a kind of skin nursing of claim 1 is characterized in that concrete steps are with the preparation method of pudding-like cream cream composition:
(1) oils and fats is put into oil cauldron and be heated to 55 ℃, mix, it is dissolved fully, stand-by.
(2) water, polyhydric alcohol are put into the emulsifying pot and be heated to 55 ℃, mix, it is dissolved fully, stand-by.
(3) Span, the unitary polyether-modified spermaceti alcohol ester of polypropylene glycol, the smooth sesquialter fatty acid ester of Pyrusussuriensis are put into the emulsifying pot and be heated to 55 ℃, mix after the dissolving, homogenizing 5 minutes dissolves it fully, and is stand-by.
(4) nertralizer is dropped into the emulsifying pot, stir after the dissolving, homogenizing 2 minutes.
(5) oils and fats is drawn into the emulsifying pot, uses high speed shear homogenizer homogenizing 5 minutes while stirring, stir.
(6) cool to 40 ℃ and add essence, antiseptic, active matter, stir.
(7) evacuation stirs, and cools to 35 ℃ of dischargings, gets final product.
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| Application Number | Priority Date | Filing Date | Title |
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| CN2012102122860A CN103211723A (en) | 2012-06-26 | 2012-06-26 | Pudding-shaped cream composition for skin nursing and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN2012102122860A CN103211723A (en) | 2012-06-26 | 2012-06-26 | Pudding-shaped cream composition for skin nursing and preparation method thereof |
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| CN103211723A true CN103211723A (en) | 2013-07-24 |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN87107781A (en) * | 1986-11-10 | 1988-08-31 | B·F谷德里奇公司 | Stablize and the topical skin composition of energy fast emulsion breaking |
| CN1633975A (en) * | 2004-10-25 | 2005-07-06 | 江苏隆力奇生物科技股份有限公司 | Skin-care gel |
| CN102421413A (en) * | 2009-03-11 | 2012-04-18 | Elc管理有限责任公司 | Topical compositions comprising fermented exracts of traditional chinese medicinal (tcm) ingredients, and methods of making and using same |
-
2012
- 2012-06-26 CN CN2012102122860A patent/CN103211723A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN87107781A (en) * | 1986-11-10 | 1988-08-31 | B·F谷德里奇公司 | Stablize and the topical skin composition of energy fast emulsion breaking |
| CN1633975A (en) * | 2004-10-25 | 2005-07-06 | 江苏隆力奇生物科技股份有限公司 | Skin-care gel |
| CN102421413A (en) * | 2009-03-11 | 2012-04-18 | Elc管理有限责任公司 | Topical compositions comprising fermented exracts of traditional chinese medicinal (tcm) ingredients, and methods of making and using same |
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Application publication date: 20130724 |