CN103183492A - Asphalt polymer cement waterproof coating - Google Patents
Asphalt polymer cement waterproof coating Download PDFInfo
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- CN103183492A CN103183492A CN2013101326511A CN201310132651A CN103183492A CN 103183492 A CN103183492 A CN 103183492A CN 2013101326511 A CN2013101326511 A CN 2013101326511A CN 201310132651 A CN201310132651 A CN 201310132651A CN 103183492 A CN103183492 A CN 103183492A
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- polymer cement
- waterproof paint
- asphalt
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Abstract
The invention relates to an asphalt polymer cement waterproof coating which consists of a component A and a component B. The component A comprises the raw materials in percentage by weight as follows: 20-50% of emulsified asphalt, 30-50% of modified latex and 10-30% of water. The component B comprises the raw materials in percentage by weight as follows: 40-60% of cement, 20-40% of staffing and 1-5% of assistant. The coating provided by the invention is low in price, good in waterproofness and good in flexibility, and can resist corrosion caused by low concentration inorganic acid, base and salt. The asphalt polymer cement waterproof coating can be independently used as a film waterproof layer in waterproof and corrosion resisting projects of kitchens and bath rooms, basements and bridge floors.
Description
Technical field
The present invention relates to a kind of asphaltic base waterproof paint, be mainly used in water-tight corrosion-proof field coating, especially relate to a kind of asphalt polymer cement waterproof paint.
Technical background
Also there is poor water resistance in the polymer cement-based waterproof material at present, and work-ing life is short, can not be used for secondary and above water-proof roofing and important waterproofing work.There are shortcomings such as poor water resistance in acrylate polymer emulsion, the water-proof function of impact polymer waterproof paint during as the liquid material of polymer cement waterproof paint.Advantages such as pitch has that material source is extensive, cheap, the mineral acid of ability lower concentration, alkali and salt corrosion, and himself waterproof have certain self-healing.
Summary of the invention
This product is a kind of antiseep and etch-proof asphalt polymer cement water-proof film, has good binding property, self-healing, protected object is sealed fully, and is seamless; Acid-alkali-corrosive-resisting; Uvioresistant and biological degradation; Outstanding antistripping ability; Excellent specific property such as nontoxic, tasteless, pollution-free becomes the outstanding person in international waterproof, the aseptic production.
Emulsified bitumen in this system is to develop for this system specially, compares with common emulsified bitumen, and this emulsified bitumen has and modified latex, the better consistency of sand-cement slurry, guarantees the waterproof quality of product, improves the application property of product.
This product has been widely used in waterproof and protection against corrosion fields such as building construction, municipal traffic, petrochemical industry electric power, environment protection, oceanographic engineering, hydro project.This product and technology have embodied the development of international waterproof and corrosion-resistant field initiative.
Technical scheme involved in the present invention:
The asphalt polymer cement waterproof paint is made up of A component and B component, and the A component comprises emulsified bitumen, modified latex, and the B component comprises cement, filler, auxiliary agent, the content of various raw materials in A, the B component wherein, and (as follows) meter is as follows by weight percentage:
A component: emulsified bitumen: 20%-50%
Modified latex: 30%-50%
Water: 10-30%
The B component:
Cement: 40%-60%
Filler: 20%-40%
Auxiliary agent: 1%-5%.
Emulsified bitumen of the present invention is formed: pitch 50%-65%; Preferred 58%-63%,
Cationic emulsifier 3%-10%, preferred 3%-6%;
Nonionic emulsifying agent 3%-10%, preferred 3%-6%;
Stablizer 1%-5%, preferred 1%-3%;
All the other are water.
Pitch wherein can be rock asphalt, petroleum pitch, coal-tar pitch and composition thereof, oil heavy traffic asphaltum preferably, and its penetration degree is 60-100(1/10mm).
The application finds that after deliberation single emulsifying agent can't satisfy the asphalt polymer cement waterproof paint to the requirement of emulsified bitumen, because single emulsifying agent has fixing HLB value, it can not satisfy the complicated required HLB scope of asphalt emulsification.Therefore the present invention has selected cationic and two kinds of emulsifying agents of nonionic especially, carries out compositely in different ratios, forms compound emulsifying agent.In concrete asphalt emulsifier was selected, the used cationic asphalt emulsifier of the present invention had been selected one or more in lauryl amine, tetradecylamine, hexadecylamine, docosyl amine, coconut oleyl amine, tallow amine, hydrogenated tallow amine, oleyl amine, soybean oleyl amine, 1-aminoethyl-2-heptadecyl tetrahydroglyoxaline-2 hydrochloride, lignin amine, dodecyl benzyl dimethyl ammonium chloride, tetradecyl alkyl dimethyl ammonium chloride, the cetalkonium chloride.The present invention is in laurostearic acid single ethanol amide, lauryl diethanol amide, coconut oil single ethanol amide, lauric acid amide of ethanol, polyoxyethylene sorbitan monolaurate, octadecanoic acid ester of polyethylene glycol, the polyoxyethylene nonylphenol ether one or more to the nonionic asphalt emulsifier.It is compound to adopt mentioned emulsifier to carry out, and is conducive to eliminate list and easily produces the low problem of cloud point with non-ionic emulsifier, also can avoid single use cationic emulsifier, the problem that pitch particle is thick.Use above-mentioned composite emulsifier, can dwindle profit between the two the relative density difference and the difference of viscosity, strengthen the electromotive force of pitch particulate, be easy to form electrostatic double layer, increase the mutual repulsive force between the particle, hinder the polymerization tendency of pitch particulate.
The used stablizer of the present invention can be inorganic salt, as vitriol, nitrate, hydrochloride etc.; Also can be mineral acid or organic acid, as lipid acid, acetic acid, hydrochloric acid, tartrate etc.; Can be polyvinyl alcohol, Mierocrystalline cellulose, inner complex etc.; Also can be above-mentioned two kinds or three kinds and mix use.
Modified latex of the present invention is selected from: one or more in cationic chloroprene latex, positively charged ion styrene-butadiene latex, pure acrylic acid latex, styrene-acrylic latex, natural rubber latex, nitrile rubber, isobutylene-isoprene latex, polyisoprene latex, ethene-vinyl acetate latex, Ethylene Propylene Terpolymer latex, binary ethylene propylene rubber latex, chlorinated butyl latex, the chlorosulfonated polyethylene latex etc.
Cement of the present invention is selected from: one or more in white cement, the ash concrete etc.
Filler of the present invention is selected from: calcium carbonate, talcum powder, wollastonite powder, quartz sand etc.
Auxiliary agent of the present invention is formed: one or more in water reducer, stablizer, the thickening material etc.
Product preparation process flow process of the present invention is as follows:
Emulsified bitumen preparation technology flow process in the product of the present invention is as follows:
(1) with 50%-65% pitch earlier 110 ℃-130 ℃ dehydrations 1 hour-2 hours, mild heat to 130 is ℃-160 ℃ then, the metering back is standby;
(2) tap water is heated to 45 ℃-65 ℃, the metering back is standby;
(3) emulsifying agent, stablizer are joined in the standby hot water, stir, make aqueous emulsion, the control temperature is 45 ℃-65 ℃, and standby, emulsifying agent refers to that cationic emulsifier and nonionic emulsifying agent are composited;
(4) open the mulser system, the aqueous emulsion that meets temperature requirement that step (3) makes is poured in the emulsifying agent, pour the heated bitumen that meets temperature requirement that step (1) makes immediately into, the satisfactory emulsified bitumen preparation in the back that stirs is finished.
A component preparation method:
20%-50% emulsified bitumen, 30%-50% modified latex that step (4) is made join the stirring of a mixing bowl high speed, stir 20 minutes, and static half an hour, hour after-filtration discharging was packed.
B component technology:
40%-60% cement, 20%-40% filler and 1%-5% auxiliary agent are joined a mixing bowl high speed stir, stir discharging packing after 30 minutes.
Asphalt polymer cement waterproof paint of the present invention, cheap, application property is excellent, mineral acid, alkali and the salt corrosion of good waterproof performance, ability lower concentration, good flexibility is arranged.
The asphalt polymer cement waterproof paint can be separately as film waterproof material usefulness, and it is medium to be used for kitchen and toilet, vault and bridge deck water-proof antiseptic project.
Embodiment
Embodiment 1
Emulsified bitumen starting material in the invention product are carried out proportioning (weight ratio, down together) by following (table 1):
Table 1 emulsified bitumen formula table (100 parts of emulsified bitumens)
The emulsified bitumen manufacturing process is as follows:
(1), with pitch earlier 110 ℃-130 ℃ dehydrations 1 hour-2 hours, mild heat to 130 is ℃-160 ℃ then, the metering back is standby;
(2), tap water is heated to 45 ℃-65 ℃, the metering back is standby;
(3), emulsifying agent, stablizer are joined in the standby hot water, stir, make aqueous emulsion, the control temperature is 45 ℃-65 ℃, and is standby;
(4), open the mulser system, the aqueous emulsion that will meet temperature requirement is poured in the emulsification, pours the heated bitumen that meets temperature requirement immediately into, satisfactory emulsified bitumen preparation is finished.
Again the starting material in the invention product are carried out proportioning (weight ratio, down together) by following (table 2):
Table 2 asphalt polymer cement waterproof paint A component (100 parts of coating)
Table 3 asphalt polymer cement waterproof paint B component (100 parts of coating)
| Cement | Filler 1 | Filler 2 | Auxiliary agent |
| White cement | Calcium carbonate | Quartz sand | Water reducer |
| 50 | 30 | 18 | 2 |
The manufacturing process of asphalt polymer cement waterproof paint is as follows:
A group technology:
Emulsified bitumen, modified latex are joined a mixing bowl high speed stir, stirred 20 minutes, static half an hour, hour after-filtration discharging was packed.
B component technology:
Cement, filler and auxiliary agent are joined a mixing bowl high speed stir, stir discharging packing after 30 minutes.
Embodiment 2
The emulsified bitumen starting material are carried out proportioning (weight ratio, down together) by following (table 4):
Table 4 emulsified bitumen formula table (100 parts of emulsified bitumens)
The emulsified bitumen manufacturing process of embodiment 2 such as embodiment 1
Again the starting material in the invention product are carried out proportioning (weight ratio, down together) by following (table 5):
Table 5 asphalt polymer cement waterproof paint A component (100 parts of coating)
| Emulsified bitumen | Modified latex 1 | Modified latex 2 | Water |
| Embodiment 1 | Pure acrylic acid latex | Styrene-acrylic latex | Tap water |
| 40 | 30 | 15 | 15 |
Table 6 asphalt polymer cement waterproof paint B component (100 parts of coating)
| Cement | Filler 1 | Filler 2 | Auxiliary agent |
| White cement | Calcium carbonate | Wollastonite | Water reducer |
| 50 | 30 | 18 | 2 |
The manufacturing process of the asphalt polymer cement waterproof paint of embodiment 2 such as embodiment 1
Embodiment 3
The emulsified bitumen starting material are carried out proportioning (weight ratio, down together) by following (table 7):
Table 7 emulsified bitumen formula table (100 parts of emulsified bitumens)
The emulsified bitumen manufacturing process of embodiment 3 such as embodiment 1
Again the starting material in the invention product are carried out proportioning (weight ratio, down together) by following (table 8):
Table 8 asphalt polymer cement waterproof paint A component (100 parts of coating)
Table 9 asphalt polymer cement waterproof paint B component (100 parts of coating)
| Cement | Filler 1 | Filler 2 | Auxiliary agent |
| White cement | Calcium carbonate | Talcum powder | Water reducer |
| 50 | 33 | 15 | 2 |
The manufacturing process of the asphalt polymer cement waterproof paint of embodiment 3 such as embodiment 1
Embodiment 4
The emulsified bitumen starting material are carried out proportioning (weight ratio, down together) by following (table 10):
Table 10 emulsified bitumen formula table (100 parts of emulsified bitumens)
The emulsified bitumen manufacturing process of embodiment 4 such as embodiment 1
Again the starting material in the invention product are carried out proportioning (weight ratio, down together) by following (table 11):
Table 11 asphalt polymer cement waterproof paint A component (100 parts of coating)
Table 12 asphalt polymer cement waterproof paint B component (100 parts of coating)
| Cement | Filler 1 | Filler 2 | Auxiliary agent |
| White cement | Calcium carbonate | Quartz sand | Water reducer |
| 45 | 33 | 20 | 2 |
The manufacturing process of the asphalt polymer cement waterproof paint of embodiment 4 such as embodiment 1.
Claims (10)
1. asphalt polymer cement waterproof paint, it is characterized in that: described asphalt polymer cement waterproof paint is made up of A component and B component, the A component comprises emulsified bitumen, modified latex, the B component comprises cement, filler, auxiliary agent, the content of various raw materials in A, the B component wherein, as follows by weight percentage:
A component: emulsified bitumen: 20%-50%,
Modified latex: 30%-50%,
Water: 10%-30%,
The B component:
Cement: 40%-60%,
Filler: 20%-40%,
Auxiliary agent: 1%-5%.
2. asphalt polymer cement waterproof paint according to claim 1 is characterized in that: the weight ratio that each component of emulsified bitumen is formed is: pitch 50%-65%; Cationic emulsifier 3%-10%, nonionic emulsifying agent 3%-10%, stablizer 1%-5%, all the other are water.
3. asphalt polymer cement waterproof paint according to claim 2 is characterized in that: the weight ratio that each component of emulsified bitumen is formed is: pitch 58%-63%; Cationic emulsifier 3%-6%; Nonionic emulsifying agent 3%-6%; Stablizer 1%-3%, all the other are water.
4. asphalt polymer cement waterproof paint according to claim 2, it is characterized in that: described pitch is selected from a kind of or its mixture in rock asphalt, petroleum pitch, the coal-tar pitch.
5. asphalt polymer cement waterproof paint according to claim 2, it is characterized in that: described pitch is the oil heavy traffic asphaltum.
6. asphalt polymer cement waterproof paint according to claim 2, it is characterized in that: cationic emulsifier is selected from one or more in lauryl amine, tetradecylamine, hexadecylamine, docosyl amine, coconut oleyl amine, tallow amine, hydrogenated tallow amine, oleyl amine, soybean oleyl amine, 1-aminoethyl-2-heptadecyl tetrahydroglyoxaline-2 hydrochloride, lignin amine, dodecyl benzyl dimethyl ammonium chloride, tetradecyl alkyl dimethyl ammonium chloride, the cetalkonium chloride.The present invention is in laurostearic acid single ethanol amide, lauryl diethanol amide, coconut oil single ethanol amide, lauric acid amide of ethanol, polyoxyethylene sorbitan monolaurate, octadecanoic acid ester of polyethylene glycol, the polyoxyethylene nonylphenol ether one or more to the nonionic asphalt emulsifier.
7. asphalt polymer cement waterproof paint according to claim 2, it is characterized in that: nonionic emulsifying agent is one or more in laurostearic acid single ethanol amide, lauryl diethanol amide, coconut oil single ethanol amide, lauric acid amide of ethanol, polyoxyethylene sorbitan monolaurate, octadecanoic acid ester of polyethylene glycol, the polyoxyethylene nonylphenol ether.
8. asphalt polymer cement waterproof paint according to claim 1 is characterized in that: described stablizer is selected from one or more the mixture in inorganic salt, mineral acid, organic acid, polyvinyl alcohol, Mierocrystalline cellulose, the inner complex.
9. asphalt polymer cement waterproof paint according to claim 1, it is characterized in that: modified latex is selected from one or more in cationic chloroprene latex, positively charged ion styrene-butadiene latex, pure acrylic acid latex, styrene-acrylic latex, natural rubber latex, nitrile rubber, isobutylene-isoprene latex, polyisoprene latex, ethene-vinyl acetate latex, Ethylene Propylene Terpolymer latex, binary ethylene propylene rubber latex, chlorinated butyl latex, the chlorosulfonated polyethylene latex; Cement is selected from one or more in white cement, the ash concrete; Filler is selected from one or more in calcium carbonate, talcum powder, wollastonite powder, the quartz sand; Auxiliary agent is selected from one or more in water reducer, stablizer, the thickening material.
10. the preparation method of A, B component in the asphalt polymer cement waterproof paint is characterized in that: the emulsified bitumen preparation method:
(1) with 50%-65% pitch earlier 110 ℃-130 ℃ dehydrations 1 hour-2 hours, mild heat to 130 is ℃-160 ℃ then, the metering back is standby;
(2) tap water is heated to 45 ℃-65 ℃, the metering back is standby;
(3) with emulsifying agent, namely cationic emulsifier 3%-6% and nonionic emulsifying agent 3%-6% compositely form, stablizer 1%-5% joins in the standby hot water, stir, and make aqueous emulsion, and the control temperature is 45 ℃-65 ℃, and is standby;
(4) open the mulser system, will meet the aqueous emulsion that makes in the C step of temperature requirement and pour in the mulser, pour the heated bitumen that meets temperature requirement that step () makes immediately into, the satisfactory emulsified bitumen preparation in the back that stirs is finished;
The preparation method of A component: 20%-50% emulsified bitumen, 30%-50% modified latex that step (four) is made join the stirring of a mixing bowl high speed, stir 20 minutes, static after-filtration discharging half an hour packing;
The B method for preparing ingredients thereof:
40%-60% cement, 20%-40% filler and 1%-5% auxiliary agent are joined a mixing bowl stir, stir discharging packing after 30 minutes.
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| CN201310132651.1A CN103183492B (en) | 2013-04-17 | 2013-04-17 | Asphalt polymer cement waterproof coating |
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| CN201310132651.1A CN103183492B (en) | 2013-04-17 | 2013-04-17 | Asphalt polymer cement waterproof coating |
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| CN103833282A (en) * | 2014-02-28 | 2014-06-04 | 北京东方雨虹防水技术股份有限公司 | Emulsified asphalt waterproof mortar and preparation method thereof |
| CN104087173A (en) * | 2014-07-24 | 2014-10-08 | 苏州吉人漆业有限公司 | Ethylene propylene diene monomer regenerated rubber modified asphalt anti-rust paint |
| CN104211356A (en) * | 2014-09-11 | 2014-12-17 | 锦州东方雨虹建筑材料有限责任公司 | Emulsified asphalt modified cement-based waterproof slurry as well as preparation and use method thereof |
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| CN103833282B (en) * | 2014-02-28 | 2016-04-06 | 北京东方雨虹防水技术股份有限公司 | A kind of emulsified bitumen waterproof mortar and preparation method thereof |
| CN103833282A (en) * | 2014-02-28 | 2014-06-04 | 北京东方雨虹防水技术股份有限公司 | Emulsified asphalt waterproof mortar and preparation method thereof |
| CN104087173A (en) * | 2014-07-24 | 2014-10-08 | 苏州吉人漆业有限公司 | Ethylene propylene diene monomer regenerated rubber modified asphalt anti-rust paint |
| CN104211356A (en) * | 2014-09-11 | 2014-12-17 | 锦州东方雨虹建筑材料有限责任公司 | Emulsified asphalt modified cement-based waterproof slurry as well as preparation and use method thereof |
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| CN104479479A (en) * | 2014-12-12 | 2015-04-01 | 岳阳东方雨虹防水技术有限责任公司 | Emulsified asphalt primer coating |
| CN104478342A (en) * | 2014-12-23 | 2015-04-01 | 咸阳东方雨虹建筑材料有限公司 | Wet base surface treating agent |
| CN105694494A (en) * | 2016-03-30 | 2016-06-22 | 徐州卧牛山新型防水材料有限公司 | Emulsified asphalt and preparation method thereof, and water-based substrate treating agent for asphalt waterproof coiled materials and preparation method thereof |
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| CN106186963B (en) * | 2016-07-22 | 2019-03-08 | 葛洲坝集团项目管理有限公司 | A kind of anti-aging bitumastic material and preparation method thereof |
| CN107501971A (en) * | 2017-10-13 | 2017-12-22 | 安徽朗凯奇建材有限公司 | A kind of ground brickwork joint waterproof material and its preparation technology |
| CN108389649A (en) * | 2018-01-22 | 2018-08-10 | 宝胜高压电缆有限公司 | A kind of high-tension cable coated with novel anticorrosion material |
| CN108707375A (en) * | 2018-03-23 | 2018-10-26 | 常德市万福达环保节能建材有限公司 | A kind of polymer cement-base waterproof coating and preparation method thereof |
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| CN108997937A (en) * | 2018-08-16 | 2018-12-14 | 马鞍山市永固防水科技有限公司 | A kind of preparation method of rubber asphalt-polymer cement waterproof paint |
| CN108977080A (en) * | 2018-08-21 | 2018-12-11 | 四川蜀羊防水材料有限公司 | Weather resistant polymer modified asphalt cement water-repellent paint and preparation method thereof |
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| CN112029344A (en) * | 2020-09-10 | 2020-12-04 | 深圳港创建材股份有限公司 | Polymer cement-based coating with good compatibility and preparation method and application thereof |
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| CN103183492B (en) | 2015-02-04 |
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Effective date of registration: 20151223 Address after: 650311 Yunnan city of Kunming province Anning City Lu Biao street Fengying an Cun Wei Hui Shang Biao Cun Patentee after: Kunming Fengxing Waterproof Material Co., Ltd. Address before: 650101 in Yunnan Province in the western suburbs of Kunming Jindingshan Road No. 20 Patentee before: Kunming Fengxing Waterproof Material Co., Ltd. Patentee before: Jinzhou Dongfang Yuhong Building Materials Co., Ltd. Patentee before: Beijing Oriental Yuhong Waterproof Technology Co., Ltd. |