CN107501971A - A kind of ground brickwork joint waterproof material and its preparation technology - Google Patents
A kind of ground brickwork joint waterproof material and its preparation technology Download PDFInfo
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- CN107501971A CN107501971A CN201710949930.5A CN201710949930A CN107501971A CN 107501971 A CN107501971 A CN 107501971A CN 201710949930 A CN201710949930 A CN 201710949930A CN 107501971 A CN107501971 A CN 107501971A
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- pitch
- waterproof material
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- brickwork joint
- cement
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L95/00—Compositions of bituminous materials, e.g. asphalt, tar, pitch
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
- C04B28/06—Aluminous cements
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
- C08J3/03—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
- C04B2111/00663—Uses not provided for elsewhere in C04B2111/00 as filling material for cavities or the like
- C04B2111/00672—Pointing or jointing materials
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2395/00—Bituminous materials, e.g. asphalt, tar or pitch
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/002—Physical properties
- C08K2201/006—Additives being defined by their surface area
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Structural Engineering (AREA)
- Medicinal Chemistry (AREA)
- Materials Engineering (AREA)
- Ceramic Engineering (AREA)
- Civil Engineering (AREA)
- Inorganic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Curing Cements, Concrete, And Artificial Stone (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
A kind of ground brickwork joint waterproof material, including following parts by weight material：30 50 parts of coal tar pitch, 15 23 parts of neoprene latex, 45 parts of emulsifying agent, 0.5 3 parts of softening agent, 14 26 parts of sulphate aluminium cement, 2 10 parts of B943 defoamers, 20 30 parts of distilled water；Also include, 1 8% accelerator calcium chloride and 0.5 1% polycarboxylic acid water reducing agent；Wherein, emulsifying agent is BH Z1；Softening agent is castor oil.The invention provides a kind of ground brickwork joint waterproof material and its preparation technology, this pitch-cement composite material is formed by emulsified asphalt and cement composition, this is high molecular polymer and the inierpeneirating network structure of inorganic material, it has the intensity of cement Seed harvest, again because the intervention of asphalt emulsion adds the diffusivity of slurries, there is good water proofing property.
Description
Technical field
The invention belongs to field of waterproof materials, and in particular to a kind of ground brickwork joint waterproof material and its preparation technology.
Background technology
Certain gap can be all produced after floor tile finishing, gap must carry out waterproof for a long time, only waterproof is done
Gap wiping will not leak after good.Water-repellent paint can be divided into 3 kinds according to development history journey at present, and the first water-repellent paint is ancient
Pitch, second is exactly modified pitch, and the third is exactly common high-molecular coating at present.High molecular water-proof paint has reaction
Type and emulsion-type and solvent-borne type, wherein being preferred option with solvent-borne type.Execution conditions are not high, and effect is good.And inorganic grouting material because
The features such as its is economic and environment-friendly, the favor of people is constantly subjected to, but it is present that concrete castability is poor, setting time is long, pliability is poor, body
Product shrinks the shortcomings of big, equally limits the application and development of inorganic grouting material.Prepare Organic-inorganic composite injection material
Expected into it is presently the most important the problem of.
Patent CN103045067 discloses a kind of cement concrete bridge deck waterproof material and preparation method thereof, described anti-
Water material is by isocyanates and Pluronic polyols generation carbamate, adds common heavy traffic paving asphalt and be catalyzed through tertiary amines
Agent, composite anti-foaming agent and ethyl acetate is composite modified forms；Alleviate the bridge structure caused by infiltration to destroy, delay highway
Bridge service life, but it is mainly used in bridge deck water-proof, it is impossible to stitch with being directly used as with waterproof material, and it is existing relevant open
Patent in never have mention dedicated for ground seam waterproof material.The invention provides a kind of ground brickwork joint waterproof material and its
Preparation technology, because the part-structure cell surface for forming pitch powder is smaller with hydroxyl, imino group isoreactivity group, particle diameter
More be advantageous to these groups and the cross-linking reaction of-NCO group, so that product properties increases, this pitch-cementitious composite material
Material is formed by emulsified asphalt and cement composition, and this is high molecular polymer and the inierpeneirating network structure of inorganic material, and it has
There is the intensity of cement Seed harvest, and because the intervention of asphalt emulsion adds the diffusivity of slurries, there is excellent water resistance.
The content of the invention
It is an object of the invention to provide a kind of ground brickwork joint waterproof material and its preparation technology, this pitch-cement are multiple
Condensation material is formed by emulsified asphalt and cement composition, and this is high molecular polymer and the inierpeneirating network structure of inorganic material,
It has the intensity of cement Seed harvest, and because the intervention of asphalt emulsion adds the diffusivity of slurries, has good waterproof
Property.
In order to achieve the above object, the technical solution adopted by the present invention is：A kind of ground brickwork joint waterproof material, including it is following
Parts by weight material：
Also include, 1-8% accelerator calcium chloride and 0.5-1% polycarboxylic acid water reducing agent；
Wherein, emulsifying agent BH-Z1；Softening agent is castor oil.
The preparation technology of this ground brickwork joint waterproof material, step include：
1) raw material is weighed in proportion；
2) asphalt emulsification：Distilled water and emulsifying agent are added in pitch, pitch heating and melting is mixed with ultrasonic emulsification
Close uniform, addition neoprene latex and softening agent mixing in pitch after emulsification；
3) preparation of pitch-cement composite material：The pitch obtained in step 2) is mixed with sulphate aluminium cement, added
Enter B943 defoamers, accelerator and water reducer mixing, stirring 30-60min in the case where rotating speed is 1000-2000r/min is dripped
Green grass or young crops-cementitious composite waterproof material.
Preferably, the coal tar pitch crosses 200 mesh sieves.
Preferably, the specific surface area of the sulphate aluminium cement is 600-800m2/Kg。
Preferably, the calcium chloride is pure to analyze.
The beneficial effects of the invention are as follows：
After 1. the emulsification of pitch dissolves pitch heating, by the effect of mechanical shearing, make tiny bitumen particle point
It is dispersed in the aqueous solution of emulsifying agent, forms that the particle diameter of oil-in-water asphalt emulsion pitch powder is smaller, and its surface area is bigger, point
Divergence is bigger, bigger with the contact surface of matrix polyurethane material, and the abundant infiltration being more beneficial between the two combines and stress point
Dissipate.Further, since the part-structure cell surface of composition pitch powder is smaller with hydroxyl, imino group isoreactivity group, particle diameter
More be advantageous to these groups and the cross-linking reaction of-NCO group, so that product properties increases.
2. modified sulphate aluminium cement specific surface area is close to Novel super-thin cement.Such a modified novel concrete
Itself it is a kind of preferably high performance water proof material, it has the excellent permeability similar to organic chemistry grouting liquid, has more
High intensity and durability, and there is the feature of environmental protection, it is pollution-free to surrounding environment, it is high anti-to be provided simultaneously with quick hardening sulphoaluminate cement
Ooze the features such as performance, water absorption rate are low and wear-resisting.
Embodiment
With reference to specific embodiment mode, the present invention is described in further detail, to make those skilled in the art join
Book word can be implemented according to this as directed.Obviously, described embodiment is only part of the embodiment of the present invention, rather than entirely
The embodiment in portion.
Embodiment 1：
1) raw material is weighed in proportion：
2) asphalt emulsification：Distilled water and emulsifying agent are added in the pitch for crossing 200 mesh sieves, by pitch heating and melting ultrasound
Ripple emulsion process is well mixed, and neoprene latex and the mixing of softening agent castor oil are added in pitch after emulsification；
3) preparation of pitch-cement composite material：The pitch obtained in step 2) is mixed with sulphate aluminium cement, added
Enter the polycarboxylic acid water reducing agent mixing of B943 defoamers, 1-8% accelerator calcium chloride and 0.5-1%, be 1000r/ in rotating speed
40min is stirred under min and obtains pitch-cementitious composite waterproof material.
Comparative example 1：
1) raw material is weighed in proportion：
2) asphalt emulsification：Distilled water and emulsifying agent are added in the pitch for crossing 200 mesh sieves, by pitch heating and melting ultrasound
Ripple emulsion process is well mixed, and neoprene latex and the mixing of softening agent castor oil are added in pitch after emulsification；
3) preparation of pitch-cement composite material：The pitch obtained in step 2) is mixed with sulphate aluminium cement, added
Enter the polycarboxylic acid water reducing agent mixing of B943 defoamers, 1-8% accelerator calcium chloride and 0.5-1%, be 1000r/ in rotating speed
40min is stirred under min and obtains pitch-cementitious composite waterproof material.Relative to waterproof material in embodiment 1, wherein in raw material
Asphalt is replaced with into coal tar pitch.
Comparative example 2：
1) raw material is weighed in proportion：
2) asphalt emulsification：Distilled water and emulsifying agent are added in the pitch for crossing 200 mesh sieves, by pitch heating and melting ultrasound
Ripple emulsion process is well mixed, and neoprene latex and the mixing of softening agent castor oil are added in pitch after emulsification；
3) preparation of pitch-cement composite material：The pitch obtained in step 2) is mixed with ordinary portland cement, added
The polycarboxylic acid water reducing agent mixing of B943 defoamers, 1-8% accelerator calcium chloride and 0.5-1%, is 1000r/min in rotating speed
Lower stirring 40min obtains pitch-cementitious composite waterproof material.
Relative to waterproof material in embodiment 1, sulphate aluminium cement is wherein replaced with into ordinary portland cement in raw material.
The waterproof material being prepared in embodiment 1 and comparative example 1-2 is tested, detects the obtained contrast of performance
Information is as shown in the table：
The data shown in upper table are contrasted, the waterproof material being prepared in embodiment 1 in comparative example 1-2 relative to preparing
Obtained waterproof material performance and tensile strength will get well, and be not only as the use of asphalt and sulphate aluminium cement, also
Because this pitch-cement composite material is high molecular polymer and the inierpeneirating network structure of inorganic material, it has cement knot
The intensity of stone body, and because the intervention of asphalt emulsion adds the diffusivity of slurries, there is good water proofing property.
Although embodiment of the present invention is disclosed as above, it is not restricted in specification and embodiment listed
With it can be applied to various suitable the field of the invention completely, can be easily for those skilled in the art
Other modification is realized, therefore under the universal limited without departing substantially from claim and equivalency range, it is of the invention and unlimited
In specific details and shown here as the example with description.
Claims (5)
1. a kind of ground brickwork joint waterproof material, it is characterised in that including following parts by weight material：
Also include, 1-8% accelerator calcium chloride and 0.5-1% polycarboxylic acid water reducing agent；
Wherein, emulsifying agent BH-Z1；Softening agent is castor oil.
2. the preparation technology of a kind of ground brickwork joint waterproof material described in a kind of claim 1, it is characterised in that step includes：
1) raw material is weighed in proportion；
2) asphalt emulsification：Distilled water and emulsifying agent are added in pitch, pitch heating and melting is mixed with ultrasonic emulsification
It is even, neoprene latex and softening agent mixing are added in pitch after emulsification；
3) preparation of pitch-cement composite material：The pitch obtained in step 2) is mixed with sulphate aluminium cement, added
B943 defoamers, accelerator and water reducer mixing, it is to be dripped to stir 30-60min in the case where rotating speed is 1000-2000r/min
Green grass or young crops-cementitious composite waterproof material.
3. according to a kind of ground brickwork joint waterproof material described in claim 1, it is characterised in that the coal tar pitch crosses 200 mesh
Sieve.
4. according to a kind of ground brickwork joint waterproof material described in claim 1, it is characterised in that the sulphate aluminium cement
Specific surface area is 600-800m2/Kg。
5. according to a kind of ground brickwork joint waterproof material described in claim 1, it is characterised in that the calcium chloride is analysis
It is pure.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710949930.5A CN107501971A (en) | 2017-10-13 | 2017-10-13 | A kind of ground brickwork joint waterproof material and its preparation technology |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710949930.5A CN107501971A (en) | 2017-10-13 | 2017-10-13 | A kind of ground brickwork joint waterproof material and its preparation technology |
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| Publication Number | Publication Date |
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| CN107501971A true CN107501971A (en) | 2017-12-22 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201710949930.5A Pending CN107501971A (en) | 2017-10-13 | 2017-10-13 | A kind of ground brickwork joint waterproof material and its preparation technology |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101580366A (en) * | 2008-04-11 | 2009-11-18 | 清华大学 | Mortar and concrete modified by emulsified asphalt |
| CN103183492A (en) * | 2013-04-17 | 2013-07-03 | 昆明风行防水材料有限公司 | Asphalt polymer cement waterproof coating |
| CN104211356A (en) * | 2014-09-11 | 2014-12-17 | 锦州东方雨虹建筑材料有限责任公司 | Emulsified asphalt modified cement-based waterproof slurry as well as preparation and use method thereof |
| CN104478342A (en) * | 2014-12-23 | 2015-04-01 | 咸阳东方雨虹建筑材料有限公司 | Wet base surface treating agent |
| CN104530729A (en) * | 2014-12-23 | 2015-04-22 | 天津市科垣新型建材有限公司 | Redispersible asphalt powder, and preparation method and application thereof |
-
2017
- 2017-10-13 CN CN201710949930.5A patent/CN107501971A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101580366A (en) * | 2008-04-11 | 2009-11-18 | 清华大学 | Mortar and concrete modified by emulsified asphalt |
| CN103183492A (en) * | 2013-04-17 | 2013-07-03 | 昆明风行防水材料有限公司 | Asphalt polymer cement waterproof coating |
| CN104211356A (en) * | 2014-09-11 | 2014-12-17 | 锦州东方雨虹建筑材料有限责任公司 | Emulsified asphalt modified cement-based waterproof slurry as well as preparation and use method thereof |
| CN104478342A (en) * | 2014-12-23 | 2015-04-01 | 咸阳东方雨虹建筑材料有限公司 | Wet base surface treating agent |
| CN104530729A (en) * | 2014-12-23 | 2015-04-22 | 天津市科垣新型建材有限公司 | Redispersible asphalt powder, and preparation method and application thereof |
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Application publication date: 20171222 |
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| RJ01 | Rejection of invention patent application after publication |