CN103147278A - Temperature-regulating intelligent tent fabric and preparation method thereof - Google Patents
Temperature-regulating intelligent tent fabric and preparation method thereof Download PDFInfo
- Publication number
- CN103147278A CN103147278A CN2013100773062A CN201310077306A CN103147278A CN 103147278 A CN103147278 A CN 103147278A CN 2013100773062 A CN2013100773062 A CN 2013100773062A CN 201310077306 A CN201310077306 A CN 201310077306A CN 103147278 A CN103147278 A CN 103147278A
- Authority
- CN
- China
- Prior art keywords
- coating
- temperature
- agent
- powder
- tent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Images
Landscapes
- Paints Or Removers (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The invention relates to a temperature-regulating intelligent tent fabric and a preparation method of the temperature-regulating intelligent tent fabric. The temperature-regulating intelligent tent fabric comprises a paulin matrix and a temperature-regulating coating, wherein the temperature-regulating coating comprises doped vanadium dioxide (V (1-x)Mx)O2 nanopowder or micelle, wherein 0 <= x <= 0.03. The preparation method of the temperature-regulating intelligent tent fabric comprises the following steps of: (1) preparing doped (V(1-x)Mx)O2; and (2) applying the doped (V(1-x)Mx)O2 to the paulin matrix by coating, padding or impregnating to obtain the temperature-regulating intelligent tent fabric. The temperature-regulating intelligent tent fabric can effectively improve the temperature in a tent, greatly improve the degree of comfort of a user and play a good role in the aspects of field construction, amusement and tourism, geological exploration, rescue and relief work, field hospitals and outdoor banquets, is easy to operate, is low in cost and has a good application prospect.
Description
Technical field
The invention belongs to fabric and preparation field thereof for tent, particularly fabric and preparation method thereof for a kind of temperature-controlled smart tent.
Background technology
At present, tent is mainly used in the field construction operation, training, outdoor exhibition, sports and amusement place, Forces Command Post, field hospital encamp, the aspects such as rescue and relief work, field encampment, amusement and travel, its mounting or dismounting characteristics easy, easy to carry are that it is in the numerous areas extensive use.Although tent provides an institute of becalming and taking shelter from rain for people, its internal-external temperature difference makes numerous users quite feel uncomfortable.(totally 192 times) comparative observation when inside and outside the tent of once living to the Longnan of Gansu Province disaster area masses in regional climate center, Gansu Province weather bureau Lanzhou, temperature has carried out pursuing.Result shows: in tent, temperature is than 2.5 ℃ of the outer temperature mean heights of tent.That is to say, when the highest temperature in a day reaches 37-38 ℃, the temperature of tent inside is up to more than 40 ℃.It is generally acknowledged, ambient temperature is body sense the most comfortable in the time of 20-24 ℃.Therefore, the high temperature of tent inside can cause the discomfort on health to the user undoubtedly.
Military aspect, the tent that combat troop is used has directly affected army's fighting capacity; Civilian aspect, the comfort level of tent inside has directly determined the victims of the disaster's health status, traveller's satisfaction and various outdoor exhibition and the interior movable success or not of account.Therefore, be badly in need of a kind of can the variation and the comfort type intelligence tent of active adjustment internal temperature according to ambient temperature on tent market.
Summary of the invention
Technical problem to be solved by this invention is to provide fabric and preparation method thereof for a kind of temperature-controlled smart tent, this intelligence tent has greatly improved user's level of comfort with fabric, make the larger use value of aspect performance such as its construction operation, amusement and travel, geological prospecting, rescue and relief work, field hospital, outdoor dinner party in the wild.
A kind of temperature-controlled smart tent fabric of the present invention, comprise tarpaulin matrix and thermal control coating; Wherein, described thermal control coating comprises doped vanadium dioxide (V
1-xm
x) O
2nano-powder or micro-glue, 0≤x≤0.03.
Described tarpaulin matrix is any form (machine-processed, knitting, nonwoven fabric), the textiles of any material (natural fabric, synthetic fiber, regenerated fiber), the thin-film material of any material.
Described tarpaulin matrix is nylon taffeta or OXFORD.
Described intelligent tent also comprises waterproof coating with fabric, described waterproof coating can be coating prepared by coating prepared by aqueous binder and solvent type adhesive, specifically comprises that PVC coating, PU coating, acrylic resin type coating, silicone based coating, ethylene-propylene-diene monomer gel coating are or/and the post processing of fluorine-containing water-refusing oil-refusing finishing agent emulsion.
Described thermal control coating also comprises the functional form auxiliary agent, described functional form auxiliary agent is tackifier, flexibilizer, plasticizer, thickener, diluent, solvent, coupling agent, emulsifying agent, filler, reinforcing agent, curing agent, crosslinking agent, initator, light trigger, catalyst, promoter, polymerization inhibitor, oxidant, softening agent, age resistor, dispersant, blowing agent, defoamer, levelling agent, colouring agent, toner, bleeding agent, wetting agent, neutralizer, sagging inhibitor, anti skinning agent, drier, anti-adhesion agent, antifreezing agent, antistatic additive, the flavor agent disappears, antiseptic, mould inhibitor, mite-proof agent, anophelifuge, fire retardant, one or more in ultra-violet absorber.
Described thermal control coating for improve coating such as anticorrosion, toughness reinforcing, wear-resisting, water-fast, heat-resisting, ageing-resistant, the function such as extend using period and add some solid additive in coating, described solid additive is precipitated calcium carbonate, powdered whiting, fine heavy activation calcium, activated Calcium carbonate, calcium carbonate superfine powder, calcite in powder, calcium oxide, calcium hydroxide, light magnesium oxide, activated magnesia, light magnesium carbonate, blanc fixe, ultra-fine barium sulfate, lithopone, land plaster, mica powder, talcum powder, superfine alumina silicate, kaolin powder, feldspar powder, atlapulgite, silica flour, precipitated silica, hydrophobic silicic aerogels, silicon powder, hollow glass micro-ball, glass dust, wollastonite in powder, vermiculite power, sepiolite powder, flake asbestos, dolomite dust, trbasic zinc phosphate, rutile type titanium white, micaceous iron oxide, aluminum nitride powder, graphite powder, aluminium powder, carbonyl iron dust, nano silicon, nano titanium oxide, nano-aluminium oxide, nano-calcium carbonate, zinc oxide, nanmeter antimong trioxide, nano barium sulfate, water nano calcium carbonate, CNT, one or more in kaolin nanotube.
Also can add coloring pigment in described waterproof coating, described coloring pigment is anatase thpe white powder, chrome green, iron oxide black, iron oxide yellow, iron oxide green, colour carbon black, ultramarine, permanent yellow, fluorescein, fluorescence green, phthalocyanine blue b, one or more in Phthalocyanine Green G, CBS brightening agent.
The adhesive used is one or more in epoxy resin, phenolic resins, polyurethane resin, unsaturated polyester resin, ammoniacum oil, aldol resin, amino resins.
Described doped vanadium dioxide (V
1-xm
x) O
2phase transition temperature be 0-70 ℃.
The preparation method of fabric for a kind of temperature-controlled smart tent of the present invention comprises:
(1) prepare doped vanadium dioxide (V
1-xm
x) O
2;
Concrete preparation method: in room temperature, respectively with deionized water preparation sulfuric acid oxidation vanadium solution, ammonium tungstate solution and sodium bicarbonate solution, first ammonium tungstate solution mixed with vanadic sulfate solution and be placed in there-necked flask, with constant flow pump, sodium bicarbonate solution is splashed into to above-mentioned mixed solution under continuous stirring condition in, dropwise rear continuation stirring and make its complete reaction, gained precipitates after filtration, deionized water washs extremely without SO
4 2-, absolute ethanol washing, vacuum drying; The gained powder, as for calcining under inert atmosphere in atmosphere furnace, is obtained to phase-change material.
(2) by above-mentioned vanadium dioxide (V
1-xm
x) O
2by coating, pad or flood and be applied on tarpaulin matrix, obtain temperature-controlled smart tent fabric.
Coating in described step (2) is a kind of in blade coating, spraying, flow coat, electro-deposition.
Described blade coating is for using brush, roller or paint chipping chisel; Described spraying is aerial spraying, airless spraying, thermal spraying or electrostatic spraying; Described flow coat is dip-coating, curtain coating, roller coat or inverse roller coating.
This preparation method is not limited to the use in the tent field, is equally applicable to the textile field that parasols, sunbonnet, Curtains Fabrics, flameproof coveralls, steel-making Work Clothes etc. need the timely adjustment variations in temperature.
Intelligent tent provided by the invention adopts coating method that intelligent temperature control coating is applied on tarpaulin with fabric, and its core temperature control material is doped vanadium dioxide.Vanadium dioxide has obvious thermal induced phase transition property, and when temperature surpasses its transformation temperature (68 ℃ of left and right), crystal structure carries out reversible transition by monoclinic form to the tetragonal structure of rutile structure.Correspondingly, its phase is Metal Phase by semiconductor phase-change, follows the sudden change of optical property simultaneously.Before phase transformation, in all band scope, to ultrared transmissivity is high, reflectivity is low; After phase transformation, to ultrared transmissivity is low, reflectivity is high, thereby can see through the infra-red intensity of tarpaulin according to the variation active adjustment of ambient temperature, adjusts temperature in account, as shown in Figure 1 in good time.
The phase transition temperature of vanadium dioxide can effectively reduce by doping, and the controlled doping ratio can make transformation temperature change in 0-70 ℃ of scope.Select appropriate doped chemical and doping ratio, it is undergone phase transition in the optimum temperature range of human body, thereby make to reach through the tent of this functional form material modification the purpose of low temperature daylighting high temperature insulating.
The tarpaulin fabric mainly comprises matrix and functional form coating.Select suitable fabric matrix according to different purposes, wherein nylon taffeta is thin and light, is applicable to mountain-climbing and camps and use tent on foot; OXFORD is thick, but heavier, the tent that applicable making drives to camp or groupuscule is used, different purposes that concrete matrix selective basis is used and determining.Thermal control coating is to take the functional form that the doped vanadium dioxide slurry is main body to modify, by film forming matter, main body pigment, additional function auxiliary agent, defoamer, dispersant, plasticizer and solvent composition, adopt blade coating, spraying or flow coat mode to be applied on tarpaulin matrix, to give the excellent properties of its low temperature daylighting high temperature insulating.In addition, tarpaulin matrix also can be by padding or impregnation method is applied to the doped vanadium dioxide dispersion on matrix, thereby give the matrix function of temperature control.Face coat is waterproof coating, and top finish is determined according to specific requirement difference in using.For example, though generally speaking the PVC waterproof is good, winter temperature can harden, become fragile when low, easily produces folding line or fracture; The PU coating can not only overcome the deficiency of PVC, and waterproof effect is also comparatively desirable.After coating repeatedly, more than waterproofing pressure can reach 2000mm
beneficial effect
The present invention effectively improves the tent internal temperature, has greatly improved user's level of comfort, makes the larger use value of aspect performance such as its construction operation, amusement and travel, geological prospecting, rescue and relief work, field hospital, outdoor dinner party in the wild; Simple to operate, cost is lower, has a good application prospect.
The accompanying drawing explanation
Fig. 1 is the doped vanadium dioxide transmittance graph before and after phase transformation respectively;
The structural representation that Fig. 2 is the temperature-controlled smart tarpaulin.
The specific embodiment
Below in conjunction with specific embodiment, further set forth the present invention.Should be understood that these embodiment only are not used in and limit the scope of the invention for the present invention is described.Should be understood that in addition those skilled in the art can make various changes or modifications the present invention after the content of having read the present invention's instruction, these equivalent form of values fall within the application's appended claims limited range equally.
The preparation of doped vanadium dioxide powder
Embodiment 1
In room temperature, respectively with the sulfuric acid oxidation vanadium solution of deionized water preparation 150mL1mol/L, the sodium tungstate solution of 10mL1mol/L, the ammonium bicarbonate soln of 100mL2mol/L, first sodium tungstate solution mixed with vanadic sulfate solution and be placed in there-necked flask, stir 5-10min under stir speed (S.S.) 350-400rpm condition, then in 60min, with constant flow pump, ammonium bicarbonate soln is splashed in above-mentioned mixed solution, dropwise rear continuation and stir 1-2h, the gained precipitation is washed extremely without SO through 220nm miillpore filter filtration under diminished pressure, deionized water
4 2-, absolute ethanol washing, 45 ℃ of lower vacuum dryings obtain the yellowish-brown powder.This powder, as for 700-800 under nitrogen atmosphere in atmosphere furnace ℃ of high-temperature calcination 3h, is then continued to calcine 2-3h under 500-600 ℃ of nitrogen atmosphere, obtain phase-change material.
Embodiment 2
In room temperature, respectively with the sulfuric acid oxidation vanadium solution of deionized water preparation 100mL0.05mol/L, the ammonium tungstate solution of 5mL1mol/L, the sodium bicarbonate solution of 150mL0.1mol/L, first ammonium tungstate solution mixed with vanadic sulfate solution and be placed in there-necked flask, stir 20min under stir speed (S.S.) 270-300rpm condition, then in 100-120min, with constant flow pump, sodium bicarbonate solution is splashed in above-mentioned mixed solution, dropwise rear continuation and stir 3-5h, for the gained precipitation, 4# sand core funnel filtration under diminished pressure, deionized water washing are extremely without SO
4 2-, dry under absolute ethanol washing 1-2 time, 60 ℃ of vacuum states.The gained powder, as for 600-700 under argon gas atmosphere in atmosphere furnace ℃ of high-temperature calcination 9h, is then continued to calcine 1h under 400-500 ℃ of argon gas atmosphere, obtain phase-change material.
Embodiment 3
In room temperature, prepare respectively the sulfuric acid oxidation vanadium solution of 200mL0.5mol/L with deionized water, 10mL0.5mol/L sodium tungstate solution, 10mL0.5mol/L ammonium molybdate solution, 150mL0.5mol/L sodium carbonate liquor, first by sodium tungstate solution, ammonium molybdate solution mixes with vanadic sulfate solution and is placed in there-necked flask, stir 25-30min under stir speed (S.S.) 200-250rpm condition, then in 70-90min, with constant flow pump, sodium carbonate liquor is splashed in above-mentioned mixed solution, dropwise rear continuation and stir 8-10h, the gained precipitation is through 220nm miillpore filter filtration under diminished pressure, the deionized water washing is extremely without SO
4 2-, acetone washing, 30 ℃ of lower vacuum dryings, then 900-1000 ℃ of high-temperature calcination 2h under nitrogen atmosphere, then continue to calcine 5-8h under 700-800 ℃ of nitrogen atmosphere, obtains phase-change material.‘
Coating prepares the temperature-controlled smart tarpaulin
Embodiment 4
(1) preparation of doped vanadium dioxide thermal control paint
Dispersant (H-402) 5%
Dimethylbenzene 75%
Dispersant is joined in dimethylbenzene, after stirring, add doped vanadium dioxide powder, mixture and zirconia ceramics pearl are placed in to the ball milling instrument, under the 800rpm rotating speed, grind 6h, obtain the doped vanadium dioxide dispersion liquid, average grain diameter is in the 200nm left and right.
(2) thermal control coating arranges
By the formula consumption, above-mentioned material is mixed, add after the doped vanadium dioxide slurry made and grind 30min under the 400rpm rotating speed, be coated on nylon taffeta.
(3) waterproof coating
By formula consumption preparation coating agent, evenly coat on the matrix of processing through (2) coating weight 100g/m
2, 130 ℃ of oven dry, 180 ℃ of plasticizings, repeat coating 5 times.
This temperature-controlled smart tarpaulin phase transition temperature is 29.5 ℃, and the transmissivity to sunshine when in the time of 25 ℃, tarpaulin is 80%, 35 ℃ to sunlight transmittance is 45%, and waterproofing pressure can reach 1000mm.
Embodiment 5
(1) preparation of smart coatings
Dispersant and fire retardant is soluble in water, add doped vanadium dioxide powder after stirring, mixture and zirconia ceramics pearl are placed in to the ball milling instrument, grind 10h under the 650rpm rotating speed, obtain the doped vanadium dioxide dispersion liquid, average grain diameter is in the 170nm left and right.
(2) preparation of temperature control type tarpaulin
By the formula consumption, above-mentioned material is mixed, add after stirring after the doped vanadium dioxide slurry prepared and grind 45min under the 350rpm rotating speed, be coated on OXFORD.
(3) waterproof coating
By formula consumption preparation coating agent, evenly coat on the matrix of processing through (2) coating weight 150g/m
2, 110 ℃ of oven dry, 200 ℃ of plasticizings, repeat coating 8 times.
This temperature-controlled smart tarpaulin phase transition temperature is 41.2 ℃, and the transmissivity to sunshine when in the time of 35 ℃, tarpaulin is 73%, 45 ℃ to sunlight transmittance is 34%, and waterproofing pressure can reach 2000mm.
Embodiment 6
(1) preparation of temperature control type coating
Dispersant, ultra-violet absorber and pest-control finishing agent is soluble in water, under the 200rpm rotating speed, stir 10 minutes, then add doped vanadium dioxide powder, mixture and zirconia ceramics pearl are placed in to the ball milling instrument, grind 4h under the 1000rpm rotating speed, obtain the doped vanadium dioxide dispersion liquid, average grain diameter is in the 100nm left and right.
(2) preparation of temperature-controlled smart tarpaulin
By the formula consumption, above-mentioned material is mixed, add after the slurry made and grind 20min under the 350rpm rotating speed, be coated on OXFORD.
(3) waterproof coating
By formula consumption preparation coating agent, evenly coat on the matrix of processing through (2) coating weight 130g/m
2,
145 ℃ of oven dry, 175 ℃ of plasticizings, repeat coating 2 times.
This temperature-controlled smart tarpaulin phase transition temperature is 19.5 ℃, and the transmissivity to sunshine when in the time of 15 ℃, tarpaulin is 69%, 25 ℃ to sunlight transmittance is 32%, effective insecting driving insect, and waterproofing pressure can reach 1500mm, can be used as the desirable fabric of summer with tent.
Padding method prepares the temperature-controlled smart tarpaulin
Embodiment 7
(1) preparation of intelligent nano dispersion liquid
Doped vanadium dioxide 32%
Dispersant 8%
Water 60%
By the formula consumption, doped vanadium dioxide, dispersant, water and zirconia ceramics pearl are placed in to the ball milling instrument, under the 980rpm rotating speed, grind 5h, obtain the doped vanadium dioxide dispersion liquid, average grain diameter is in the 90nm left and right.
(2) preparation of temperature-controlled smart tarpaulin
Be mixed with finishing agent by above-mentioned formula consumption, this finishing agent is padded on nylon taffeta, two soak two rolls, 70%, 75 ℃ of lower preliminary drying 3min of pick-up, after bake 45s under 130 ℃.
(3) waterproof coating
By formula consumption preparation coating agent, evenly coat on the matrix of processing through (2) coating weight 120g/m
2, 125 ℃ of oven dry, 190 ℃ of plasticizings, repeat coating 6 times.
This temperature-controlled smart tarpaulin phase transition temperature is 35.4 ℃, and the transmissivity to sunshine when in the time of 30 ℃, tarpaulin is 85%, 40 ℃ to sunlight transmittance is 29%, and waterproofing pressure can reach 1800mm.
Embodiment 8
(1) preparation of intelligent nano dispersion liquid
By the formula consumption, doped vanadium dioxide, titanium dioxide, dispersant and zirconia ceramics pearl are placed under ball milling instrument 750rpm rotating speed and grind 3h, obtain composite dispersion liquid, average grain diameter is in the 100nm left and right.
(2) preparation of temperature-controlled smart tarpaulin
Be mixed with finishing agent by above-mentioned formula consumption, this finishing agent is padded on OXFORD, one soaks one rolls, 80%, 60 ℃ of lower preliminary drying 10min of pick-up, after bake 60s under 140 ℃.
(3) waterproof coating
By formula consumption preparation coating agent, evenly coat on the matrix of processing through (2) coating weight 135g/m
2, 100 ℃ of oven dry, 170 ℃ of plasticizings, repeat coating 8 times.
This temperature-controlled smart tarpaulin phase transition temperature is 15.8 ℃, and the transmissivity to sunshine when in the time of 10 ℃, tarpaulin is 81%, 20 ℃ to sunlight transmittance is 32%, and waterproofing pressure can reach 2000mm.
Embodiment 9
(1) preparation of intelligent heat insulation nano dispersion liquid
By the formula consumption, doped vanadium dioxide, aluminum zinc oxide, tin-antiomony oxide, hyper-dispersant, water and zirconia ceramics pearl are placed in to the ball milling instrument, under the 1000rpm rotating speed, grind 8h, obtain intelligent heat insulation dispersion liquid, average grain diameter is in the 80-100nm scope.
(2) preparation of temperature-controlled smart tarpaulin
The heat insulation dispersion liquid 55% of intelligence
Defoamer 13%
Water 32%
Be mixed with finishing agent by above-mentioned formula consumption, this finishing agent is padded on nylon taffeta, two soak two rolls, 100%, 60 ℃ of lower preliminary drying 5min of pick-up, after bake 30s under 160 ℃.
(3) waterproof coating
By formula consumption preparation coating agent, evenly coat on the matrix of processing through (2) coating weight 140g/m
2, 130 ℃ of oven dry, 190 ℃ of plasticizings.
This temperature-controlled smart tarpaulin phase transition temperature is 28.6 ℃, and the transmissivity to sunshine when in the time of 20 ℃, tarpaulin is 77%, 35 ℃ to sunlight transmittance is 38%, and waterproofing pressure can reach 2200mm.
Infusion process prepares the temperature-controlled smart tarpaulin
(1) preparation of temperature control type coating
By the formula consumption, doped vanadium dioxide, zinc oxide, titanium dioxide, dispersant, water and zirconia ceramics pearl are placed in to star formula ball milling instrument, under the 500rpm rotating speed, grind 16h, obtain composite dispersion liquid, average grain diameter is in the 120nm left and right.
(2) preparation of temperature-controlled smart tarpaulin
Be mixed with dressing liquid by above-mentioned formula consumption, bath raio 1:10, be immersed in nylon taffeta in this dressing liquid, under normal temperature, keeps 10min, the rear 75 ℃ of lower preliminary drying 4min that dewater, after bake 50s under 130 ℃.
(3) waterproof coating
By formula consumption preparation coating agent, evenly coat on the matrix of processing through (2) coating weight 120g/m
2, 140 ℃ of oven dry, 200 ℃ of plasticizings, repeat coating 7 times.
This temperature-controlled smart tarpaulin phase transition temperature is 36.7 ℃, and in the time of 30 ℃, tarpaulin to sunlight transmittance is, the transmissivity to sunshine in the time of 40 ℃ is that waterproofing pressure can reach 2500mm.
Embodiment 11
(1) preparation of temperature control type coating
By the formula consumption, doped vanadium dioxide, silica, ultra-fine barium sulfate, dispersant, water and zirconia ceramics pearl are placed in to star formula ball milling instrument, under the 350rpm rotating speed, grind 20h, obtain composite dispersion liquid, average grain diameter is in the 90nm left and right.
(2) preparation of temperature-controlled smart tarpaulin
Be mixed with dressing liquid by above-mentioned formula consumption, bath raio 1:20, be immersed in OXFORD in this dressing liquid, keeps 15min under 40 ℃, the rear 80 ℃ of lower preliminary drying 5min that dewater, after bake 60s under 150 ℃.
(3) waterproof coating
By formula consumption preparation coating agent, evenly coat on the matrix of processing through (2) coating weight 150g/m
2, 110 ℃ of oven dry, 185 ℃ of plasticizings, repeat coating 5 times.
This temperature-controlled smart tarpaulin phase transition temperature is 36.7 ℃, and the transmissivity to sunshine when in the time of 30 ℃, tarpaulin is 64%, 40 ℃ to sunlight transmittance is 19%, and waterproofing pressure can reach 2500mm.
Embodiment 12
(1) preparation of temperature control type coating
By the formula consumption, doped vanadium dioxide, lithopone, titanium dioxide, superfine alumina silicate, hyper-dispersant, water and zirconia ceramics pearl are placed in to star formula ball milling instrument, under the 850rpm rotating speed, grind 9h, obtain composite dispersion liquid, average grain diameter is in the 100nm left and right.
(2) preparation of temperature-controlled smart tarpaulin
Be mixed with dressing liquid by above-mentioned formula consumption, bath raio 1:15, be immersed in nylon taffeta in this dressing liquid, keeps 5min under 30 ℃, the rear 60 ℃ of lower preliminary drying 10min that dewater, after bake 45s under 175 ℃.
(3) waterproof coating
By formula consumption preparation coating agent, evenly coat on the matrix of processing through (2) coating weight 100g/m
2, 130 ℃ of oven dry, 190 ℃ of plasticizings, repeat coating 3 times.This temperature-controlled smart tarpaulin phase transition temperature is 29.6 ℃, and the transmissivity to sunshine when in the time of 25 ℃, tarpaulin is 71%, 35 ℃ to sunlight transmittance is 27%, and waterproofing pressure can reach 1200mm.
Claims (9)
1. a temperature-controlled smart tent fabric, it is characterized in that: intelligent tent comprises tarpaulin matrix and thermal control coating with fabric; Wherein, described thermal control coating comprises doped vanadium dioxide (V
1-xm
x) O
2nano-powder or micro-glue, 0≤x≤0.03.
2. a kind of temperature-controlled smart tent fabric according to claim 1, it is characterized in that: described intelligent tent also comprises waterproof coating with fabric, described waterproof coating is coating prepared by the coating for preparing of aqueous binder or solvent type adhesive, comprises PVC coating, PU coating, acrylic resin type coating, silicone based coating or ethylene-propylene-diene monomer gel coating.
3. a kind of temperature-controlled smart tent fabric according to claim 1, it is characterized in that: described thermal control coating also comprises the functional form auxiliary agent, described functional form auxiliary agent is tackifier, flexibilizer, plasticizer, thickener, diluent, solvent, coupling agent, emulsifying agent, filler, reinforcing agent, curing agent, crosslinking agent, initator, light trigger, catalyst, promoter, polymerization inhibitor, oxidant, softening agent, age resistor, dispersant, blowing agent, defoamer, levelling agent, colouring agent, toner, bleeding agent, wetting agent, neutralizer, sagging inhibitor, anti skinning agent, drier, anti-adhesion agent, antifreezing agent, antistatic additive, the flavor agent disappears, antiseptic, mould inhibitor, mite-proof agent, anophelifuge, fire retardant, one or more in ultra-violet absorber.
4. a kind of temperature-controlled smart tent fabric according to claim 1, it is characterized in that: described thermal control coating also comprises solid additive, described solid additive is precipitated calcium carbonate, powdered whiting, fine heavy activation calcium, activated Calcium carbonate, calcium carbonate superfine powder, calcite in powder, calcium oxide, calcium hydroxide, light magnesium oxide, activated magnesia, light magnesium carbonate, blanc fixe, ultra-fine barium sulfate, lithopone, land plaster, mica powder, talcum powder, superfine alumina silicate, kaolin powder, feldspar powder, atlapulgite, silica flour, precipitated silica, hydrophobic silicic aerogels, silicon powder, hollow glass micro-ball, glass dust, wollastonite in powder, vermiculite power, sepiolite powder, flake asbestos, dolomite dust, trbasic zinc phosphate, rutile type titanium white, micaceous iron oxide, aluminum nitride powder, graphite powder, aluminium powder, carbonyl iron dust, nano silicon, nano titanium oxide, nano-aluminium oxide, nano-calcium carbonate, zinc oxide, nanmeter antimong trioxide, nano barium sulfate, water nano calcium carbonate, CNT, one or more in kaolin nanotube.
5. a kind of temperature-controlled smart tent fabric according to claim 2, it is characterized in that: in described waterproof coating, add coloring pigment, described coloring pigment is anatase thpe white powder, chrome green, iron oxide black, iron oxide yellow, iron oxide green, colour carbon black, ultramarine, permanent yellow, fluorescein, fluorescence green, phthalocyanine blue b, one or more in Phthalocyanine Green G, CBS brightening agent.
6. a kind of temperature-controlled smart tent fabric according to claim 1, is characterized in that: described doped vanadium dioxide (V
1-xm
x) O
2phase transition temperature be 0-70 ℃.
7. the preparation method of fabric for a temperature-controlled smart tent as claimed in claim 1 comprises:
(1) prepare doped vanadium dioxide (V
1-xm
x) O
2;
(2) by above-mentioned vanadium dioxide (V
1-xm
x) O
2by coating, pad or flood and be applied on tarpaulin matrix, obtain temperature-controlled smart tent fabric.
8. the preparation method of fabric for a kind of temperature-controlled smart tent according to claim 7 is characterized in that: the coating way in described step (2) is a kind of in blade coating, spraying, flow coat, electro-deposition.
9. the preparation method of fabric for a kind of temperature-controlled smart tent according to claim 8 is characterized in that: described blade coating is for brush, roller or paint chipping chisel; Described spraying is aerial spraying, airless spraying, thermal spraying or electrostatic spraying; Described flow coat is dip-coating, curtain coating, roller coat or inverse roller coating.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013100773062A CN103147278A (en) | 2013-03-11 | 2013-03-11 | Temperature-regulating intelligent tent fabric and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013100773062A CN103147278A (en) | 2013-03-11 | 2013-03-11 | Temperature-regulating intelligent tent fabric and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103147278A true CN103147278A (en) | 2013-06-12 |
Family
ID=48545576
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2013100773062A Pending CN103147278A (en) | 2013-03-11 | 2013-03-11 | Temperature-regulating intelligent tent fabric and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103147278A (en) |
Cited By (36)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103361959A (en) * | 2013-07-05 | 2013-10-23 | 吴江龙纺纺织有限公司 | Preparation method of anti-bacterial flame-retardant fabric |
| CN103696271A (en) * | 2013-12-26 | 2014-04-02 | 安徽中天印染股份有限公司 | Preparation method of durable, anti-static, flame-retardant, anti-mite and anti-skid vehicular shell fabric |
| CN103741472A (en) * | 2013-12-17 | 2014-04-23 | 江苏金太阳纺织科技有限公司 | Antibacterial tent fabrics preparation method |
| CN103757914A (en) * | 2013-12-31 | 2014-04-30 | 苏州市轩德纺织科技有限公司 | Preparation method of wearproof and antibacterial blended fabric |
| CN103774432A (en) * | 2014-01-20 | 2014-05-07 | 南通全技纺织涂层有限公司 | Light-shading waterproof polyester taffeta fabric |
| CN103899132A (en) * | 2014-04-17 | 2014-07-02 | 四川农业大学 | Double-layer phase-change energy storage tent |
| CN104213405A (en) * | 2014-08-29 | 2014-12-17 | 句容市石狮冲压件厂 | Outdoor dustproof and waterproof warm-keeping jacket |
| CN104264483A (en) * | 2014-08-28 | 2015-01-07 | 句容市石狮冲压件厂 | Ultraviolet-proof thermal insulation coating for outdoor tent and preparation method of coating |
| CN104861805A (en) * | 2015-05-21 | 2015-08-26 | 紫荆花涂料（上海）有限公司 | Water-borne architectural color coating with light reflection function and preparation method of coating |
| CN105385254A (en) * | 2015-11-14 | 2016-03-09 | 合肥标兵凯基新型材料有限公司 | Special weather-resistant stain-resistant paint for pop-top can |
| CN105385295A (en) * | 2015-11-14 | 2016-03-09 | 合肥标兵凯基新型材料有限公司 | Modified waterborne epoxy resin paint specially used for pop can |
| CN105385265A (en) * | 2015-11-14 | 2016-03-09 | 合肥标兵凯基新型材料有限公司 | Corrosion-resistant and weatherproof paint specially used for pop can |
| CN105400360A (en) * | 2015-11-14 | 2016-03-16 | 合肥标兵凯基新型材料有限公司 | Antibacterial anti-corrosion two-component coating specially used for pop can |
| CN105671976A (en) * | 2016-03-30 | 2016-06-15 | 江阴芗菲服饰有限公司 | Scrape coating type antimicrobial acrylic fabric |
| CN105970603A (en) * | 2016-07-07 | 2016-09-28 | 上海大学 | Intelligent temperature-controlled textile product and preparation method thereof |
| CN106012561A (en) * | 2016-06-27 | 2016-10-12 | 安徽忆特斯阻燃科技有限公司 | Basalt-aramid blended asbeston with excellent thermal protection performance |
| CN106049029A (en) * | 2016-07-07 | 2016-10-26 | 上海大学 | Polydopamine-coated vanadium dioxide composite powder based intelligent temperature-regulating textile and manufacturing process thereof |
| CN106368502A (en) * | 2016-10-31 | 2017-02-01 | 广西大学 | Tent warm in winter and cool in summer |
| CN106521974A (en) * | 2016-09-21 | 2017-03-22 | 东莞市联洲知识产权运营管理有限公司 | Temperature-controlling heat-insulating temperature-reducing intelligent outdoor fabric based on microcapsules and aero-gels |
| CN106917299A (en) * | 2017-05-03 | 2017-07-04 | 天鼎丰非织造布有限公司 | Tarpaulin and its production method with filament spunbond nonwoven cloth as base fabric |
| CN107059416A (en) * | 2017-05-03 | 2017-08-18 | 天鼎丰非织造布有限公司 | Using composite short fiber non-woven fabrics as the tarpaulin of base fabric and its production method |
| CN107254779A (en) * | 2016-11-11 | 2017-10-17 | 成都杰雷遮阳工程有限公司 | A kind of preparation method of the water-fast nonwoven cloth with epoxy coating |
| CN107267048A (en) * | 2017-07-25 | 2017-10-20 | 常州市元智汇电子有限公司 | A kind of multifunctional building coating and preparation method thereof |
| CN107354733A (en) * | 2017-09-04 | 2017-11-17 | 西南大学 | Lighting wool fabric is prepared with the dithiothreitol (DTT) aqueous solution |
| CN107386776A (en) * | 2016-05-17 | 2017-11-24 | 上海大学 | A kind of wet tent of portable constant temperature control for archaeological excavation scene |
| CN107524016A (en) * | 2017-09-14 | 2017-12-29 | 张家港市双河染织有限公司 | A kind of manufacturing process of waterproof fabrics |
| CN107700225A (en) * | 2017-08-31 | 2018-02-16 | 海宁文硕科技咨询有限公司 | A kind of processing method of blended yarn weaved fabric |
| CN107779067A (en) * | 2017-09-14 | 2018-03-09 | 张家港市双河染织有限公司 | A kind of weaving water-repellent paint |
| CN107844019A (en) * | 2016-09-19 | 2018-03-27 | 苏州黑白画映影视器材有限公司 | A kind of white modeling projection screen |
| CN109605864A (en) * | 2019-01-19 | 2019-04-12 | 天津大学 | A kind of passive type tent and production method cool in summer and warm in winter based on high molecular material |
| CN110344258A (en) * | 2019-07-26 | 2019-10-18 | 兴化市大地蓝绢纺有限公司 | A kind of preparation method of heat-accumulation temperature-adjustment fabric |
| CN110499649A (en) * | 2018-05-18 | 2019-11-26 | 澳洋集团有限公司 | A kind of preparation method of heat-resistant fabric |
| CN113088192A (en) * | 2019-10-13 | 2021-07-09 | 福建恒安集团有限公司 | Intelligent temperature-adjusting non-woven fabric, intelligent temperature-adjusting coating and intelligent temperature-adjusting disposable hygienic product |
| CN113832738A (en) * | 2021-09-18 | 2021-12-24 | 海宁金义家纺有限公司 | Processing technology of decorative fabric |
| CN113981675A (en) * | 2021-11-16 | 2022-01-28 | 武汉纺织大学 | Preparation method of photo-induced heating textile |
| CN114232332A (en) * | 2022-01-04 | 2022-03-25 | 顾译雯 | Anti-yellowing wear-resistant fabric for quilt cover and preparation process thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101265374A (en) * | 2008-01-24 | 2008-09-17 | 复旦大学 | Intelligent heat-insulating film and its preparing process |
| CN101818589A (en) * | 2009-12-11 | 2010-09-01 | 广东亿龙新材科技有限公司 | PVC coating tent material |
| CN102464354A (en) * | 2010-11-05 | 2012-05-23 | 中国科学院上海硅酸盐研究所 | Rutile-phase vanadium dioxide composition, coating containing same and performance of rutile-phase vanadium dioxide composition |
-
2013
- 2013-03-11 CN CN2013100773062A patent/CN103147278A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101265374A (en) * | 2008-01-24 | 2008-09-17 | 复旦大学 | Intelligent heat-insulating film and its preparing process |
| CN101818589A (en) * | 2009-12-11 | 2010-09-01 | 广东亿龙新材科技有限公司 | PVC coating tent material |
| CN102464354A (en) * | 2010-11-05 | 2012-05-23 | 中国科学院上海硅酸盐研究所 | Rutile-phase vanadium dioxide composition, coating containing same and performance of rutile-phase vanadium dioxide composition |
Cited By (47)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103361959A (en) * | 2013-07-05 | 2013-10-23 | 吴江龙纺纺织有限公司 | Preparation method of anti-bacterial flame-retardant fabric |
| CN103741472A (en) * | 2013-12-17 | 2014-04-23 | 江苏金太阳纺织科技有限公司 | Antibacterial tent fabrics preparation method |
| CN103696271A (en) * | 2013-12-26 | 2014-04-02 | 安徽中天印染股份有限公司 | Preparation method of durable, anti-static, flame-retardant, anti-mite and anti-skid vehicular shell fabric |
| CN103757914B (en) * | 2013-12-31 | 2016-01-06 | 苏州市轩德纺织科技有限公司 | A kind of preparation method of blended yarn woven fabric of wear-resistant antibacterial |
| CN103757914A (en) * | 2013-12-31 | 2014-04-30 | 苏州市轩德纺织科技有限公司 | Preparation method of wearproof and antibacterial blended fabric |
| CN103774432A (en) * | 2014-01-20 | 2014-05-07 | 南通全技纺织涂层有限公司 | Light-shading waterproof polyester taffeta fabric |
| CN103899132A (en) * | 2014-04-17 | 2014-07-02 | 四川农业大学 | Double-layer phase-change energy storage tent |
| CN104264483A (en) * | 2014-08-28 | 2015-01-07 | 句容市石狮冲压件厂 | Ultraviolet-proof thermal insulation coating for outdoor tent and preparation method of coating |
| CN104213405A (en) * | 2014-08-29 | 2014-12-17 | 句容市石狮冲压件厂 | Outdoor dustproof and waterproof warm-keeping jacket |
| CN104861805A (en) * | 2015-05-21 | 2015-08-26 | 紫荆花涂料（上海）有限公司 | Water-borne architectural color coating with light reflection function and preparation method of coating |
| CN104861805B (en) * | 2015-05-21 | 2017-12-12 | 紫荆花涂料（上海）有限公司 | A kind of colourama reflection aqueous architectural coating and its compound method |
| CN105385254A (en) * | 2015-11-14 | 2016-03-09 | 合肥标兵凯基新型材料有限公司 | Special weather-resistant stain-resistant paint for pop-top can |
| CN105385295A (en) * | 2015-11-14 | 2016-03-09 | 合肥标兵凯基新型材料有限公司 | Modified waterborne epoxy resin paint specially used for pop can |
| CN105385265A (en) * | 2015-11-14 | 2016-03-09 | 合肥标兵凯基新型材料有限公司 | Corrosion-resistant and weatherproof paint specially used for pop can |
| CN105400360A (en) * | 2015-11-14 | 2016-03-16 | 合肥标兵凯基新型材料有限公司 | Antibacterial anti-corrosion two-component coating specially used for pop can |
| CN105385265B (en) * | 2015-11-14 | 2019-04-19 | 合肥市易远新材料有限公司 | A kind of dedicated corrosion-resistant weatherability coating of pop can |
| CN105671976A (en) * | 2016-03-30 | 2016-06-15 | 江阴芗菲服饰有限公司 | Scrape coating type antimicrobial acrylic fabric |
| CN107386776A (en) * | 2016-05-17 | 2017-11-24 | 上海大学 | A kind of wet tent of portable constant temperature control for archaeological excavation scene |
| CN106012561A (en) * | 2016-06-27 | 2016-10-12 | 安徽忆特斯阻燃科技有限公司 | Basalt-aramid blended asbeston with excellent thermal protection performance |
| CN105970603B (en) * | 2016-07-07 | 2018-11-20 | 上海大学 | A kind of intelligent temperature control textile and preparation method thereof |
| CN105970603A (en) * | 2016-07-07 | 2016-09-28 | 上海大学 | Intelligent temperature-controlled textile product and preparation method thereof |
| CN106049029A (en) * | 2016-07-07 | 2016-10-26 | 上海大学 | Polydopamine-coated vanadium dioxide composite powder based intelligent temperature-regulating textile and manufacturing process thereof |
| CN106049029B (en) * | 2016-07-07 | 2018-11-20 | 上海大学 | A kind of poly-dopamine cladding Vanadium dioxide composite powder base intelligent temperature-regulation fabric and its manufacture craft |
| CN107844019A (en) * | 2016-09-19 | 2018-03-27 | 苏州黑白画映影视器材有限公司 | A kind of white modeling projection screen |
| CN106521974B (en) * | 2016-09-21 | 2019-01-01 | 台州市莱恩克智能科技有限公司 | A kind of outdoor fabric of temperature control heat insulation and heat control intelligence based on microcapsules and aeroge |
| CN106521974A (en) * | 2016-09-21 | 2017-03-22 | 东莞市联洲知识产权运营管理有限公司 | Temperature-controlling heat-insulating temperature-reducing intelligent outdoor fabric based on microcapsules and aero-gels |
| CN106368502A (en) * | 2016-10-31 | 2017-02-01 | 广西大学 | Tent warm in winter and cool in summer |
| CN107254779A (en) * | 2016-11-11 | 2017-10-17 | 成都杰雷遮阳工程有限公司 | A kind of preparation method of the water-fast nonwoven cloth with epoxy coating |
| CN106917299A (en) * | 2017-05-03 | 2017-07-04 | 天鼎丰非织造布有限公司 | Tarpaulin and its production method with filament spunbond nonwoven cloth as base fabric |
| CN107059416A (en) * | 2017-05-03 | 2017-08-18 | 天鼎丰非织造布有限公司 | Using composite short fiber non-woven fabrics as the tarpaulin of base fabric and its production method |
| CN107267048A (en) * | 2017-07-25 | 2017-10-20 | 常州市元智汇电子有限公司 | A kind of multifunctional building coating and preparation method thereof |
| CN107700225A (en) * | 2017-08-31 | 2018-02-16 | 海宁文硕科技咨询有限公司 | A kind of processing method of blended yarn weaved fabric |
| CN108729239A (en) * | 2017-08-31 | 2018-11-02 | 海宁文硕科技咨询有限公司 | The processing method of modified blended yarn weaved fabric |
| CN107354733A (en) * | 2017-09-04 | 2017-11-17 | 西南大学 | Lighting wool fabric is prepared with the dithiothreitol (DTT) aqueous solution |
| CN107779067A (en) * | 2017-09-14 | 2018-03-09 | 张家港市双河染织有限公司 | A kind of weaving water-repellent paint |
| CN107524016A (en) * | 2017-09-14 | 2017-12-29 | 张家港市双河染织有限公司 | A kind of manufacturing process of waterproof fabrics |
| CN110499649A (en) * | 2018-05-18 | 2019-11-26 | 澳洋集团有限公司 | A kind of preparation method of heat-resistant fabric |
| CN109605864A (en) * | 2019-01-19 | 2019-04-12 | 天津大学 | A kind of passive type tent and production method cool in summer and warm in winter based on high molecular material |
| CN110344258A (en) * | 2019-07-26 | 2019-10-18 | 兴化市大地蓝绢纺有限公司 | A kind of preparation method of heat-accumulation temperature-adjustment fabric |
| CN113088192A (en) * | 2019-10-13 | 2021-07-09 | 福建恒安集团有限公司 | Intelligent temperature-adjusting non-woven fabric, intelligent temperature-adjusting coating and intelligent temperature-adjusting disposable hygienic product |
| CN113088192B (en) * | 2019-10-13 | 2022-03-25 | 福建恒安集团有限公司 | Intelligent temperature-adjusting non-woven fabric, intelligent temperature-adjusting coating and intelligent temperature-adjusting disposable hygienic product |
| CN113832738A (en) * | 2021-09-18 | 2021-12-24 | 海宁金义家纺有限公司 | Processing technology of decorative fabric |
| CN113832738B (en) * | 2021-09-18 | 2024-01-02 | 海宁金义家纺有限公司 | Processing technology of decorative fabric |
| CN113981675A (en) * | 2021-11-16 | 2022-01-28 | 武汉纺织大学 | Preparation method of photo-induced heating textile |
| CN113981675B (en) * | 2021-11-16 | 2023-07-07 | 武汉纺织大学 | Preparation method of photo-induced heating textile |
| CN114232332A (en) * | 2022-01-04 | 2022-03-25 | 顾译雯 | Anti-yellowing wear-resistant fabric for quilt cover and preparation process thereof |
| CN114232332B (en) * | 2022-01-04 | 2024-03-19 | 顾译雯 | Anti-yellowing wear-resistant fabric for quilt cover and preparation process thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103147278A (en) | Temperature-regulating intelligent tent fabric and preparation method thereof | |
| CN103224719B (en) | Fluorosilicone material for super-hydrophobic coating and its preparation method and use method | |
| CN101870842B (en) | Aqueous cold pigment double-coat multifunctional thermal-insulation external wall paint and preparation method thereof | |
| CN102399483A (en) | Organic/inorganic composite heat-insulating heat-preserving water-based building coating and preparation method thereof | |
| CN105131764B (en) | A kind of reflective insulation texture paint and preparation method thereof | |
| CN107163855A (en) | A kind of silica aerogel reflective insulation exterior wall paint and preparation method thereof | |
| CN109322156A (en) | A kind of processing method of the thermal insulation fabric with water proof fire retardant | |
| CN103740204A (en) | Intelligent temperature regulating type heat reflection heat insulation coating and preparation method thereof | |
| CN105755800A (en) | A thermal reflective coating cloth | |
| CN108360268A (en) | A kind of preparation method of indoor curtain using insulating moulding coating | |
| CN103602194A (en) | Acrylate waterproof coating material | |
| CN107879710A (en) | A kind of mould proof high UV resistant pressure knot brick | |
| CN110467878A (en) | A kind of energy saving building long-acting type heat insulation and heat control coating and preparation method | |
| CN105175655B (en) | A kind of preparation method of uvioresistant lotion | |
| CN108300002B (en) | Vanadium dioxide-based thermochromic solid-liquid composite material and preparation method and application thereof | |
| CN109826018A (en) | A kind of warming Reflection fabric of traffic police's uniform | |
| CN103061106A (en) | Low-carbon photocuring single-side moisture transport finishing agent as well as preparation method and application thereof | |
| CN109423184A (en) | A kind of self-cleaning composite coating of the transparent heat-insulated hydrophobic oleophobic of outdoor fabric and preparation process | |
| CN108018613B (en) | Preparation method of photo-sterilization, self-cleaning and far-infrared composite nano particles and multifunctional fibers thereof | |
| CN102399072B (en) | Preparation method of intelligent energy-saving coating | |
| CN102018630A (en) | Preparation of skin-color rutile type nano-titanium dioxide | |
| CN105839400A (en) | Preparation method for wettability-controllable cotton fabric | |
| CN106189519A (en) | One can photochromic water-based ultraviolet (UV) curable ceramic ink jet ink and preparation method thereof | |
| CN105036190A (en) | Preparation method for nanometer titania | |
| CN113773707A (en) | Waterproof vanadium dioxide intelligent temperature control coating and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C12 | Rejection of a patent application after its publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20130612 |