CN103127541A - Stonewort mosquito repel air freshener and preparation thereof - Google Patents

Stonewort mosquito repel air freshener and preparation thereof Download PDF

Info

Publication number
CN103127541A
CN103127541A CN 201210251157 CN201210251157A CN103127541A CN 103127541 A CN103127541 A CN 103127541A CN 201210251157 CN201210251157 CN 201210251157 CN 201210251157 A CN201210251157 A CN 201210251157A CN 103127541 A CN103127541 A CN 103127541A
Authority
CN
China
Prior art keywords
charophyta
quintessence oil
air freshener
spice
pure water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN 201210251157
Other languages
Chinese (zh)
Inventor
张猛
王瑞祥
李砧
石瑛
李艳晖
谢树莲
曲耀
唐坚强
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Taiyuan Normal University
Original Assignee
Taiyuan Normal University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Taiyuan Normal University filed Critical Taiyuan Normal University
Priority to CN 201210251157 priority Critical patent/CN103127541A/en
Publication of CN103127541A publication Critical patent/CN103127541A/en
Pending legal-status Critical Current

Links

Landscapes

  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention relates to a stonewort mosquito repel air freshener. The stonewort mosquito repel air freshener is characterized by comprises ingredients, by weight, 10% to 15% of stonewort essential oil, 1% to 5% of solubilizer, 0.5% to 1% of preservative, and appropriate perfume, and the rest is water. The stonewort mosquito repel air freshener has natural fragrance, and meanwhile has excellent mosquito repel effect.

Description

A kind of charophyta mosquito killing air freshener and preparation method thereof
Technical field
The present invention relates to charophyta anophelifuge product with fresh air, be specifically related to the air freshener with mosquito repellent function that a kind of quintessence oil that adopts lower algae plant charophyta is made as main effective ingredient.
Background technology
The main component that the product with fresh air of selling on the market at present uses is o-dichlorohenzene, and it is the main component of camphor ball, and relevant report shows that o-dichlorohenzene can weaken pulmonary function, and respiratory system is impacted.And how present product with fresh air does not have the effect of anophelifuge, even the product of this effect is arranged, the antibacterial main component of its anophelifuge mostly is cinerins material and other chemosynthesis product, and there is relevant report to show, the pyrethrin compounds can cause toxic action to Fish, and life-time service is also disadvantageous to people's health.
Charophyta is the low water plant of waiting, and is widely distributed, easily cultivates, and growth cycle is short, and output is large, contains organic acid, phenols, terpenoid etc. in its quintessence oil to have obvious antibacterial repelling effect and harmless composition, has light fragrant grass delicate fragrance.Show according to experiment, the charophyta quintessence oil has repellent effect preferably to culex pipiens pallens and Aedes albopictus.
In prior art, still uncommon about the applied research of charophyta.Patent 200610012617.0 discloses a kind of mosquito incense that uses charophyta to make, and has played and has not used chemicals to carry out the effect of anophelifuge.It is large that but traditional mosquito incense has a volume, and the burning ashes are arranged, and produces the shortcoming of smog pollution indoor environment, more and more do not accepted by the modern house life.
Summary of the invention
For solving problems of the prior art, both fully developed the natural fragrance taste of charophyta, take full advantage of again the repelling effect of charophyta, the present invention attempts charophyta is applied to product with fresh air, through repetition test, successful selection suitable adjuvant, the charophyta composition is successfully added in air freshener as primary raw material, and constantly test, proposed optimum proportioning raw materials scheme.
The invention provides a kind of charophyta mosquito killing air freshener, it is characterized in that, the raw material components of percent meter comprises by weight: charophyta quintessence oil: 10%-15%, solubilizing agent: 1%-5%, antiseptic: 0.5%-1%, spice are appropriate, and all the other are pure water.
Wherein said solubilizing agent can be polysorbate60 or Tween 80, and described antiseptic can be sodium benzoate.
The present invention also provides a kind of preparation method of charophyta mosquito killing air freshener, comprises the steps: a) to select fresh charophyta, cleans and removes impurity, the grinding of drying in the shade under room temperature; B) the charophyta powder that first water and step a is made according to the weight ratio ratio mixing of 10: 1 after, therefrom extract with steam distillation and obtain semi-finished product charophyta quintessence oil, the vapour pressure of vapor distillation is 0.05-0.5Mpa, distillation time is 1-3 hour; C) the semi-finished product charophyta quintessence oil that step b is made carries out concentrating under reduced pressure to be processed, and obtains required charophyta quintessence oil; D) the charophyta quintessence oil that step c is made adds in pure water, adds while stirring polysorbate60 or Tween 80, fully mixing; E) liquid that steps d is made and sodium benzoate, spice mix, and fully stir.
Compare the present invention with prior art with product and have following characteristics: (1) charophyta wide material sources, extensive growth in water body is cultivated easily, and output is very large, and growth cycle is short, and the time-to-live is long, is conducive to the wide geographic area need of production.(2) this product is that a kind of pure natural plant is the product that primary raw material is made, and it does not contain the antibacterial mosquito component of chemosynthesis, is a kind of new product of safety non-toxic.(3) charophyta quintessence oil manufacture method is simple, and the main composition that can be used as various products with fresh air adds, and makes the kind variation of this type of product with fresh air, and small investment is beneficial to and promotes and produce.(4) having overcome traditional mosquito incense has the burning ashes, pollutes the shortcoming of room air.
The specific embodiment
The preparation of charophyta mosquito killing air freshener:
Composition of raw materials: the raw material components of percent meter and content thereof comprise by weight: charophyta quintessence oil 10%-15%, polysorbate60 or Tween 80 are 1%-5%, and sodium benzoate is 0.5%-1%, and spice is appropriate, and all the other are pure water.
Embodiment one
Select fresh charophyta, clean and remove impurity, the grinding of drying in the shade under room temperature; With water and the charophyta powder that makes according to the weight ratio ratio mixing of 10: 1 after, therefrom extract with steam distillation and obtain semi-finished product charophyta quintessence oil, the vapour pressure of vapor distillation is 0.05Mpa, distillation time is 1 hour; The semi-finished product charophyta quintessence oil that makes is carried out concentrating under reduced pressure process, obtain required charophyta quintessence oil; The charophyta quintessence oil that makes is added in pure water, add while stirring polysorbate60, fully mixing; The liquid and sodium benzoate, the spice that make are mixed, fully stir.
In the present embodiment, the raw material components of percent meter and content thereof are by weight: charophyta quintessence oil 10%, polysorbate60 are 1%, and sodium benzoate is 0.5%, and spice is appropriate, and all the other are pure water.
The air freshener of example preparation, use GB GB-T13917.4-1992 agriculture chemical registration hygienic insecticide indoor harmacological effect detection method to detect thus.The air freshener 200ml of this example preparation is put into one The lower end can the airtight cylinder of opening in, mosquito half (KT50) time used of knocking down is 6.2min, can play good repelling effect; In stability test, place the 24h taking-up in the refrigerators of-5 ℃ ± 2 ℃ and return to the room temperature observation, without precipitation with without metachromatism, opaque products is haze-free, the couveuse of 40 ℃ ± 1 ℃ is placed the 24h taking-up and is returned to the room temperature observation, and without precipitation with without metachromatism, opaque products is haze-free.
Embodiment two
Select fresh charophyta, clean and remove impurity, the grinding of drying in the shade under room temperature; With water and the charophyta powder that makes according to the weight ratio ratio mixing of 10: 1 after, therefrom extract with steam distillation and obtain semi-finished product charophyta quintessence oil, the vapour pressure of vapor distillation is 0.25Mpa, distillation time is 2 hours; The semi-finished product charophyta quintessence oil that makes is carried out concentrating under reduced pressure process, obtain required charophyta quintessence oil; The charophyta quintessence oil that makes is added in pure water, add while stirring Tween 80, fully mixing; The liquid and sodium benzoate, the spice that make are mixed, fully stir.
In the present embodiment, the raw material components of percent meter and content thereof are by weight: charophyta quintessence oil 12%, Tween 80 are 3%, and sodium benzoate is 0.8%, and spice is appropriate, and all the other are pure water.
Use the air freshener of example preparation thus, GB GB-T13917.4-1992 agriculture chemical registration hygienic insecticide indoor harmacological effect detection method detects.The air freshener 200ml of this example preparation is put into one
Figure BSA00000751772800041
The lower end can the airtight cylinder of opening in, mosquito half (KT50) time used of knocking down is 5.8min, can play good repelling effect; In stability test, place the 24h taking-up in the refrigerators of-5 ℃ ± 2 ℃ and return to the room temperature observation, without precipitation with without metachromatism, opaque products is haze-free, the couveuse of 40 ℃ ± 1 ℃ is placed the 24h taking-up and is returned to the room temperature observation, and without precipitation with without metachromatism, opaque products is haze-free.
Embodiment three
Select fresh charophyta, clean and remove impurity, the grinding of drying in the shade under room temperature; With water and the charophyta powder that makes according to the ratio mixing of 10: 1 after, therefrom extract with steam distillation and obtain semi-finished product charophyta quintessence oil, the vapour pressure of vapor distillation is 0.5Mpa, distillation time is 3 hours; The semi-finished product charophyta quintessence oil that makes is carried out concentrating under reduced pressure process, obtain required charophyta quintessence oil; The charophyta quintessence oil that makes is added in pure water, add while stirring polysorbate60, fully mixing; The liquid and sodium benzoate, the spice that make are mixed, fully stir.
In the present embodiment, the raw material components of percent meter and content thereof are by weight: charophyta quintessence oil 15%, polysorbate60 are 5%, and sodium benzoate is 1%, and spice is appropriate, and all the other are pure water.
Use the air freshener of example preparation thus, GB GB-T13917.4-1992 agriculture chemical registration hygienic insecticide indoor harmacological effect detection method detects.The air freshener 200ml of this example preparation is put into one
Figure BSA00000751772800042
The lower end can the airtight cylinder of opening in, mosquito half (KT50) time used of knocking down is 5.6min, can play good repelling effect; In stability test, place the 24h taking-up in the refrigerators of-5 ℃ ± 2 ℃ and return to the room temperature observation, without precipitation with without metachromatism, opaque products is haze-free, the couveuse of 40 ℃ ± 1 ℃ is placed the 24h taking-up and is returned to the room temperature observation, and without precipitation with without metachromatism, opaque products is haze-free.
In design of the present invention and process of the test, the inventor has mainly made following effort:
1, the charophyta that has creatively proposed to have simultaneously low cost, fragrant odour, to have advantages such as repelling effect is incorporated in air freshener as important source material, overcome the shortcoming that traditional mosquito incense pollutes indoor environment, avoided simultaneously using the chemical substance of adding in the conventional air freshener, reduced the murder by poisoning composition.
2, through repetition test, by adding appropriate antiseptic and solubilizing agent, successfully the charophyta quintessence oil is added in air freshener, and evidence repelling effect and the stability of product.
The above is only preferred embodiment of the present invention, and is in order to limit the present invention, within the spirit and principles in the present invention not all, any modification of making, is equal to replacement, improvement etc., within all should being included in the scope of protection of the invention.

Claims (6)

1. a charophyta mosquito killing air freshener, is characterized in that, the raw material components of percent meter comprises by weight:
Charophyta quintessence oil: 10%-15%,
Solubilizing agent: 1%-5%,
Antiseptic: 0.5%-1%,
Spice is appropriate,
All the other are pure water.
2. charophyta mosquito killing air freshener as claimed in claim 1, is characterized in that, described solubilizing agent is polysorbate60 or Tween 80, and described antiseptic is sodium benzoate.
3. charophyta mosquito killing air freshener as claimed in claim 2, is characterized in that, the shared percentage by weight of each raw material components is the charophyta quintessence oil: 10%, solubilizing agent: 1%, antiseptic: 0.5%, spice is appropriate, and all the other are pure water.
4. charophyta mosquito killing air freshener as claimed in claim 2, is characterized in that, the shared percentage by weight of each raw material components is the charophyta quintessence oil: 12%, solubilizing agent: 3%, antiseptic: 0.8%, spice is appropriate, and all the other are pure water.
5. charophyta mosquito killing air freshener as claimed in claim 2, is characterized in that, the shared percentage by weight of each raw material components is the charophyta quintessence oil: 15%, solubilizing agent: 5%, antiseptic: 1%, spice is appropriate, and all the other are pure water.
6. one kind for the preparation of the method as the described charophyta mosquito killing air freshener of any one in claim 2-5, comprises the steps:
A) select fresh charophyta, clean and remove impurity, the grinding of drying in the shade under room temperature;
B) the charophyta powder that water and step a is made according to the weight ratio ratio mixing of 10: 1 after, therefrom extract with steam distillation and obtain semi-finished product charophyta quintessence oil, the vapour pressure of vapor distillation is 0.05-0.5Mpa, distillation time is 1-3 hour;
C) the semi-finished product charophyta quintessence oil that step b is made carries out concentrating under reduced pressure to be processed, and obtains required charophyta quintessence oil;
D) the charophyta quintessence oil that step c is made adds in pure water, adds while stirring polysorbate60 or Tween 80, fully mixing;
E) liquid that steps d is made mixes with sodium benzoate, spice, fully stirs.
CN 201210251157 2012-07-19 2012-07-19 Stonewort mosquito repel air freshener and preparation thereof Pending CN103127541A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 201210251157 CN103127541A (en) 2012-07-19 2012-07-19 Stonewort mosquito repel air freshener and preparation thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 201210251157 CN103127541A (en) 2012-07-19 2012-07-19 Stonewort mosquito repel air freshener and preparation thereof

Publications (1)

Publication Number Publication Date
CN103127541A true CN103127541A (en) 2013-06-05

Family

ID=48488402

Family Applications (1)

Application Number Title Priority Date Filing Date
CN 201210251157 Pending CN103127541A (en) 2012-07-19 2012-07-19 Stonewort mosquito repel air freshener and preparation thereof

Country Status (1)

Country Link
CN (1) CN103127541A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110325222A (en) * 2017-01-25 2019-10-11 生活技术有限公司 The method for cleaning the surface in inner space and technical equipment using benign bacterium

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110325222A (en) * 2017-01-25 2019-10-11 生活技术有限公司 The method for cleaning the surface in inner space and technical equipment using benign bacterium

Similar Documents

Publication Publication Date Title
CN107136133B (en) A kind of preparation method of aqua type plant electric mosquito repellent liquid
CN106310326A (en) Air freshener and preparation method thereof
CN111685134A (en) Mite-removing and bacterium-inhibiting composition containing plant essential oil and application thereof
CN104094977A (en) Composition with insect-expelling sterilization disinfection effects and application thereof
CN103843835A (en) Broad-spectrum net bacteria preparation with natural plant source as well as preparation method and application thereof
CN106619213A (en) Preparation method of controlled-release natural plant mosquito repellent
CN110215532A (en) A kind of plants essential oil water solvent combinations object and preparation method thereof
CN107372685A (en) A kind of plants essential oil solid mosquito repelling agent and preparation method thereof
CN106689133B (en) A kind of composition and its lure of tea geometrid sex pheromone
CN107873701A (en) A kind of aerosol for expelling parasite, sterilizing and mite killing and preparation method thereof
CN102784407A (en) Mosquito dispelling and air refreshing stonewort sustained release agent, and its preparation method
CN105597126A (en) Botanical disinfection deodorant
WO2010057362A1 (en) A composition for preventing mosquito bite, the preparation and the use thereof
KR101715284B1 (en) mixture of natural substance for repelling mosquitoes and controlling pest and methods for preparing sprayed composition or smoking agent using the same
CN103141530B (en) Plant essential oil-containing mosquito repellent
KR101954909B1 (en) Natural pest control composition using vegetable oils and manufacturing method thereof
CN108815546B (en) Lemon-flavored natural plant freshener with insect expelling and antibacterial functions
CN103127541A (en) Stonewort mosquito repel air freshener and preparation thereof
CN105638790A (en) Deodorizing mosquito repellent and preparation method thereof
CN114982791A (en) Green pollution-free biological slow release agent for expelling insect pests and preparation method thereof
CN114366788B (en) Mite-killing composition and preparation process thereof
CN106070360A (en) Sterilizing culicifuge incense
CN1158927C (en) Prepn. of incense used as herbal mosquito repelling agent
CN104208735A (en) Multifunctional anti-influenza solid aromatic agent and preparation method thereof
CN104938530A (en) Botanical electric warming mosquito incense mat synergist and electric warming mosquito incense mat

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C02 Deemed withdrawal of patent application after publication (patent law 2001)
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20130605