CN103843835A - Broad-spectrum net bacteria preparation with natural plant source as well as preparation method and application thereof - Google Patents
Broad-spectrum net bacteria preparation with natural plant source as well as preparation method and application thereof Download PDFInfo
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- CN103843835A CN103843835A CN201310113097.2A CN201310113097A CN103843835A CN 103843835 A CN103843835 A CN 103843835A CN 201310113097 A CN201310113097 A CN 201310113097A CN 103843835 A CN103843835 A CN 103843835A
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- bacteria preparation
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- GRWFGVWFFZKLTI-UHFFFAOYSA-N rac-alpha-Pinene Natural products CC1=CCC2C(C)(C)C1C2 GRWFGVWFFZKLTI-UHFFFAOYSA-N 0.000 description 1
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- 239000005871 repellent Substances 0.000 description 1
- 235000015639 rosmarinus officinalis Nutrition 0.000 description 1
- 238000011012 sanitization Methods 0.000 description 1
- 229930000044 secondary metabolite Natural products 0.000 description 1
- 230000035943 smell Effects 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 229940116411 terpineol Drugs 0.000 description 1
- 229960003500 triclosan Drugs 0.000 description 1
- 230000001018 virulence Effects 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a broad-spectrum net bacteria preparation with a natural plant source as well as a preparation method and an application thereof. The broad-spectrum net bacteria preparation with the natural plant source is prepared from the following raw materials by weight percent: 0.03-5% of plant pyrethrin, 0.01-2% of eucalyptus oil, 0.03-1% of thymol, 0.03-1% of mint, 1-5% of tea tree oil, 0.015-0.5% of dispersant, 0.2-30% of synergist, 0.01-3% of antioxidant, 35-51% of ethyl alcohol and the balance of water, wherein the plant pyrethrin contains 20-80% of active ingredients; and the concentration of the tea tree oil is 10-15%. The broad-spectrum net bacteria preparation with the natural plant source disclosed by the invention is prepared from a natural plant extract as a main raw material, and has a plurality of functions, also has a significant killing effect on insect pests, such as mosquitoes, acarid, ticks and the like caused by damage to human health except for antibiosis, can purify air, is friendly to a human body and the environment, and has a broad application prospect.
Description
Technical field
The invention belongs to household chemicals and field, hygiene field, be specifically related to clean bacteria preparation of a kind of natural plant wide spectrum and its preparation method and application.
Background technology
At present, at home and abroad on market, conventionally adopting chemical reagent is the preparation that primary raw material preparation has anti-tick, mosquito repellent, anti-mite, mildew-resistant, antibacterial, the effect that purifies air.For example, in the U.S., a large amount of insecticides is still take Metadelphene (DEET) as main, and permethrin takes second place and prevents and insectifuge for raw material is added on conduct in each insecticides.In Europe, the famous Sanitized of chemical company and Clariant still adopt permethrin kill mosquito, the mite of going out, adopt the triclosan bacterium of going out, adopt Zinc Pyrithione to drive fungi, using above-mentioned raw materials as medicament antibacterial, pest expelling, fewer companies adopts single phytochemicals and chemical emulsion to be mixed with mosquitocide, or adopt single phytochemicals to prepare antibacterial agent, pet spray or the bathing agent of flea, louse with it goes out.In Japan, it is that raw material is prepared the anti-mite of preparation that famous Kuraray company still adopts Zinc Pyrithione, and still adopts mosquito-repellent incense mosquito repellent.In China, a mosquito liquid has been prepared this year by Sino-foreign joint venture Shanghai Johnson, although in advertisement, declare to adopt plant eucalyptus essential oil, but in composition, comprise 0.62% tetrafluoro methyl ether chrysanthemum, its Main Ingredients and Appearance remains three kinds of different types of permethrins, and content is all 0.03%.
Adopting chemical reagent is that anti-tick, mosquito repellent, anti-mite, mildew-resistant, preparation antibacterial, the effect that purifies air prepared by primary raw material has following defect: (1) chemical reagent used all has certain toxicity, can be to human body, particularly child baby, pregnant woman are had to negative effect.(2) mosquito easily develops immunity to drugs to chemical reagent, in U.S.'s west nile virus event occurring over the years, its infection carrier is exactly mosquito, because the U.S. is used Metadelphene (DEET) mosquito repellent in a large number, mosquito develops immunity to drugs to this medicine, from this virus in 1999, since U.S.A is found, be once the most serious this year.(3) adopt mosquito repellent, bactericide prepared by chemical reagent to use extremely inconvenient, in the time using kill mosquito spray, must close the doors and windows a period of time indoor, after dispenser, also needing to open door and window ventilates, in time indoor door and window and furniture surface are removed to the residual of chemical fog agent, not only people can not be indoor, and pollute the environment.
Up to the present, also there is no both at home and abroad that a kind of to adopt multiple pure natural plant extract be the clean bacteria preparation of natural plant wide spectrum with anti-tick, mosquito repellent, anti-mite, mildew-resistant, antibacterial, the effect that purifies air prepared by raw material.
Summary of the invention
The object of the present invention is to provide that a kind of to adopt multiple natural plant extracts be clean bacteria preparation of natural plant wide spectrum with anti-tick, mosquito repellent, anti-mite, mildew-resistant, antibacterial, the effect that purifies air of preparing of raw material and its preparation method and application, the clean bacteria preparation of described natural plant wide spectrum is harmless, in the time of dispenser, without closing the doors and windows, people needn't leave indoor, and can improve room air and environment.
In order to reach above-mentioned technique effect, the present invention by the following technical solutions:
The clean bacteria preparation of a kind of natural plant wide spectrum, the clean bacteria preparation of described natural plant wide spectrum is made up of the raw material of following percentage by weight:
Plant pyrethrin 0.03%～5%;
Eucalyptus oil 0.01%～2%;
Thymol 0.03%～1%;
Peppermint 0.03%～1%;
Tea oil 1%～5%;
Dispersant 0.015%～0.5%;
Synergist 0.2%～30%;
Antioxidant 0.01%～3%;
Ethanol 35%～51%;
The water of surplus;
Wherein, described plant pyrethrin contains 20%～80% active component, and the concentration of described tea oil is 10%～15%.
According to the present invention, described dispersant is selected from one or more in rilanit special, organosilicon, sorbierite, poloxamer.
According to the present invention, described synergist is selected from the one in sesamin, citrene, neem oil, spearmint oil, tangerine oil, piperonyl butoxide.
According to the present invention, described antioxidant be selected from rosemary, Xue MingRosma rinus officinalis, 2, one or more in 6-di-tert-butyl-4-methy phenol, di-tert-butyl hydroquinone.
The preparation method of the clean bacteria preparation of described natural plant wide spectrum, comprises the following steps:
Synergist and plant pyrethrin are mixed, stir; The mixture that adds eucalyptus oil, Thymol, peppermint, tea oil, stirs; Add antioxidant, stir; Add dispersant, stir; Add second alcohol and water, stir.
According to the present invention, described step is carried out under the condition of 35～60 ℃.
According to the present invention, the rotating speed of described stirring is 500～2500rpm.
According to the present invention, the time of described stirring is 30～120 minutes.
The clean bacteria preparation of natural plant wide spectrum of the present invention can be used for anti-tick, mosquito repellent, anti-mite, mildew-resistant, antibacterial, purify air.
The clean bacteria preparation of natural plant wide spectrum of the present invention can be used as textile finish or directly sprays in textile product, making textile self produce antibody.
Beneficial effect of the present invention:
1, adopt the insecticide active substance of the composite mixture of multiple extracted form natural plant polymerization, plant self-defense function and the result with pest Adaptive change, coevolution, wherein multiple secondary metabolites confrontation human body is nontoxic, grows and disturbs normal behaviour but make bacterium, insect pest have food refusal, poisoning, anesthesia, inhibition; Strengthen receiving the inhibitory action of channel current; The ability of mixed-functional oxidase degraded medicament virulence in bacterium, insect pest body is suppressed, add that appropriate synergist has more strengthened the effect of antibacterial, pest-resistant evil (mosquito, mite, tick etc.), minimum to the mankind and warm blooded animal toxicity, fast decoupled in natural environment, noresidue, being not easy to develop immunity to drugs, is universally acknowledged desirable natural insecticide;
2, the natural plant extracts of selecting, most of super critical CO 2 technology that adopts extracts, former medicine forms with the particle that is less than 100nm, add the polymerization of dispersant, breast grain is few, generally below 1 μ m, absorption ratio is high, physical property is stable, can tolerate pressure sterilizing and cryogenic freezing, can increase the surface dissolution degree of multi-medicament because surfactant forms micelle, in the time of indoor spraying, easily adhesion, resist airborne dirt mite, all kinds of bacterium in dust, cleaning ambient, protect the health, nuisanceless generation, a kind of desirable natural air clarificant and bactericide,
3,, after the natural plant extracts of selecting and stabilizing agent, dispersant polymerization, can prevent that natural-plant-essence from being decomposed by ultraviolet light and ozone, and there is better heat endurance.
It is primary raw material preparation that the clean bacteria preparation of natural plant wide spectrum of the present invention adopts natural plant extracts, there is multi-efficiency, except antibacterial, also bring the insect pest of harm to there is significant killing action for mosquito, acarid and tick worm etc. to health, and can purify air, all friendly to human body and environment, be with a wide range of applications.
Embodiment
Below, by specific embodiment, the present invention is described in further details.Should be understood that following examples are only for the present invention is described but not for limiting scope of the present invention.
The primary raw material that the clean bacteria preparation preparation of natural plant wide spectrum of the present invention is used is as follows:
One, natural plant extracts
1, plant pyrethrin (Pyrethrums)
Plant pyrethrin comprises pyrethrin I (C
21h
28o
3), pyrethrin II (C
22h
28o
5), cinerin I, cinerin II, jasmolin I, jasmolin II, pH4～7, tagging property by force, because the element composition of plant Dalmatian chrysanthemum is very complicated, therefore there is not the practical problem that insect is developed immunity to drugs, reach the quick knockdown effect to insect by acting on the nervous system of insect, there is efficient, wide spectrum, low toxicity, insect is had to food refusal and repellent action.In the present invention, the plant pyrethrin that contains 20%～80% active component all can be used as raw material.
2, eucalyptus oil (eucalyptus oil)
Eucalyptus oil is best bactericide, and antimicrbial power is strong, chief component: 1, 8-Cineole (more than 80%), amphene, phellandrene, terpineol, acetic acid geraniol, isopentyl aldehyde, citronellal and piperitone etc.
3, Thymol (Thymol)
Thymol molecular formula C
10h
14o, has very strong sterilization, antifungal, kills acarid effect, surpasses phenol, can kill the spore of mould.
4, peppermint (peppermint)
Peppermint has extremely strong sterilization antibacterial action, composition comprises: the levorotatory menthol (menthol) of 62.3%-87.2%, left-handed menthones (menthone), methyl benzoate (methylbenzoate), australene (α-pinene), nopinene (β-pinene), α-thujene (α-thujene), β-thujene (β-thujene), 3-amylalcohol (3-pentol), 2-is alcohol (2-hexanol), 3-octanol (3-octanol), dextrorotation laurene (myrcene), citrene (limonene), Cineole (cineole), alpha-terpineol (α-terpineol) etc.
5, tea oil (Tea Tree Oil)
Tea oil claims again the Meng-1-alcohol-4-1,8-cineole etc., there is the effect of anti-inflammation, effect is four times of general chemical antiphlogistic, can eliminate and have drug-fast multiple bacillus, killing fungus, in the time of certain low concentration after medication 24h, do not have microorganism to bring back to life, have anticorrosion, anti-inflammatory, expelling parasite concurrently, the effect of killing mite, tea oil is widely used in personal care articles and air purifying preparation.
Two, dispersant
1, organosilicon 818
Organosilicon not only plays dispersion, hydrophobic, froth breaking effect, and because its unparalleled key exists, and main chain be-Si-O-, is therefore difficultly decomposed by ultraviolet light and ozone, has than the better heat endurance of other macromolecular material and resistance to irradiation and Nai Hou ability.
2, poloxamer (Poloxamer)
Poloxamer breast grain is few, and generally, below 1 μ m, absorption ratio is high.Physical property is stable, can tolerate pressure sterilizing and cryogenic freezing, can increase the surface dissolution degree of multi-medicament because surfactant forms micelle.
3, sorbierite
4, rilanit special (PEG40)
Three, synergist
1, sesamin (Sesamin)
2, citrene
3, neem oil
4, spearmint oil
5, tangerine oil
6, piperonyl butoxide (PBO)
Four, antioxidant
1, rosemary, Xue MingRosma rinus officinalis (Rosmarinus officinalis)
2,2,6-di-tert-butyl-4-methy phenol (BHT)
3, di-tert-butyl hydroquinone (DTBHQ)
Above raw material all has commercially available, and wherein, it is good that described natural plant extracts preferably adopts the raw material of super critical CO 2 technology extraction.
embodiment 1, the clean bacteria preparation of natural plant wide spectrum preparation
It is among 50% plant pyrethrin 3g that sesamin 25g is joined to concentration content, and 700～900 revs/min are stirred 90～120 minutes to evenly, temperature risen to 35～40 ℃ simultaneously;
The tea oil 1g that is 10% by eucalyptus oil 0.3g, Thymol 0.3g, peppermint 0.25g, concentration mixes, and temperature is risen to 40 ℃, joins in the mixture of above-mentioned sesamin and plant pyrethrin, and 700～900 revs/min are stirred 90～120 minutes to even;
Adding temperature is the rosemary, Xue MingRosma rinus officinalis 0.25g of 40 ℃, and 700～900 revs/min are stirred 90～120 minutes to evenly;
Adding temperature is the rilanit special 0.05g of 50 ℃, and 1700～2000 revs/min are stirred 60 minutes to evenly;
Add ethanol 35g, deionized water 34.9g, 1300～1500 revs/min are stirred 40 minutes to even;
Leave standstill 1.5 hours.
embodiment 2, the clean bacteria preparation of natural plant wide spectrum preparation
It is among 70% plant pyrethrin 1.5g that piperonyl butoxide (PBO) 12g is joined to concentration content, and 700～900 revs/min are stirred 90～120 minutes to evenly, temperature risen to 35～40 ℃ simultaneously;
The tea oil 1g that eucalyptus oil 0.25g, Thymol 0.5g, peppermint 0.6g, the concentration that is 40 ℃ by temperature is 15% mixes, join in the mixture of above-mentioned piperonyl butoxide (PBO) and plant pyrethrin, 700～900 revs/min are stirred 90～120 minutes to even;
Add temperature be 40 ℃ 2,6-di-tert-butyl-4-methy phenol (BHT) 0.08g, 700～900 revs/min are stirred 90～120 minutes to evenly;
Adding temperature is the poloxamer 0.035g of 50 ℃, and 1700～2000 revs/min are stirred 60 minutes to evenly;
Adding temperature is that ethanol 50.825g, the deionized water 33.21g of 50 ℃ is mixed, and 1300～1500 revs/min are stirred 40 minutes to evenly;
Leave standstill 1.5 hours.
embodiment 3, the clean bacteria preparation of natural plant wide spectrum preparation
It is among 20% plant pyrethrin 5g that piperonyl butoxide (PBO) 30g is joined to concentration content, and 700～900 revs/min are stirred 90～120 minutes to evenly, temperature risen to 35～40 ℃ simultaneously;
Be that eucalyptus oil 0.45g, Thymol 0.7g, the peppermint 0.6g of 40 ℃, the tea oil 1g of concentration 15% mix by temperature, join in the mixture of above-mentioned piperonyl butoxide (PBO) and plant pyrethrin, 700～900 revs/min are stirred 90～120 minutes to even;
Add temperature be 40 ℃ 2,6-di-tert-butyl-4-methy phenol (BHT) 1.2g, 700～900 revs/min are stirred 90～120 minutes to evenly;
Adding temperature is the poloxamer 0.035g of 50 ℃, and 1700～2000 revs/min are stirred 60 minutes to evenly;
Adding temperature is that ethanol 40.58g, the deionized water 21.67g of 50 ℃ is mixed, and 1300～1500 revs/min are stirred 40 minutes to evenly;
Leave standstill 1.5 hours.
embodiment 4, repelling effect detect
The clean bacteria preparation of natural plant wide spectrum of embodiment 1～3 preparation, through on probation, detection, all has good repelling effect, and wherein, the clean bacteria preparation result of natural plant wide spectrum prepared by embodiment 2 is better:
1, directly spray to mosquito, after three minutes, approximately 1/3 mosquito is knocked down, and other is driven;
2, in the time that invaded and harassed by mosquito midnight, with plant resource preparation spraying of the present invention, mosquito was not was not invaded and harassed once again, after three days, mosquito does not reproduce, within the 4th day, spray again, so repeat, be not subject to mosquito and disturb a summer, after spraying, people is all the time indoor, not abnormal, only smells one delicate fragrance of plant;
3, the dusk in summer, play soccer in garden, community, a pair of father and son is owing to not spraying medicament on skin, frequent by mosquito bite.Afterwards, sprayed medicament, child is not bitten, and adult has only been bitten flatly.
4, clean natural plant wide spectrum bacteria preparation is sprayed on fabric, Culex pipiens pallens is forced to contact detection with this fabric.Simultaneously with the fabric of spray formulation in contrast.
First according to the formula of embodiment 2, select the plant pyrethrin of variable concentrations, Different Weight to prepare mosquito screen A, mosquito screen B and mosquito screen C, wherein, mosquito screen A be the plant pyrethrin of 70% concentration to get 1.5g, mosquito screen B be that the plant pyrethrin of 50% concentration is got the plant pyrethrin 6g that 3g, mosquito screen C are 30% concentration, and A-10, A-20, B-10, B-20, C-10, C-20 refer to respectively mosquito screen washing 10 times and 20 times.Result is as shown in table 1.
Table 1, the clean bacteria preparation of natural plant wide spectrum of the present invention force contact down effect to Culex pipiens pallens
According to forcing contact method evaluation in GB/T13917.9-2009 " agriculture chemical registration hygienic insecticide indoor pharmacodynamic test and evaluation part 1: propellant ", as shown in table 1, adopting mosquito screen prepared by the clean bacteria preparation of natural plant wide spectrum of the present invention is 100% to the rate of knockdown that forces contact 30min of Culex pipiens pallens, and after mosquito screen is washed to 20 times, still have good repelling effect, drug effect reaches qualified index.
embodiment 5, antibacterial effect detect
The clean bacteria preparation of natural plant wide spectrum of the present invention is removed or on cotton, carried out pilot scale coating as spray, and submit in SGS No.SHFDO120710278FDC.1, CDC disease control to post searching ［ 2012 ］ and No. 007 cloth specimen is done to multinomial detection evaluation, shown in result table 2.
The antibacterial effect of table 2, the clean bacteria preparation of natural plant wide spectrum of the present invention detects
Detect through SGS, the clean bacteria preparation of natural plant wide spectrum of the present invention reaches 99%, SGS to the bacteriostasis rate of pneumobacillus and evaluates: have good antibacterial effect.
embodiment 6, anti-tick effect detection
Pharmacodynamics index according to Direct spraying in standard GB/T/T17322.1-1998 " indoor harmacological effect of agriculture chemical registration hygienic insecticide is evaluated propellant " is evaluated the fragmentation effect of the clean bacteria preparation of natural plant wide spectrum of the present invention to tick worm, detect sample and comprise that plants essential oil, the natural plant extracts prepared by natural plant extracts add synergist, natural plant extracts adds aqueous emulsion, natural plant extracts interpolation aqueous emulsion and synergist, result is as shown in table 3.
Table 3, the evaluating drug effect result of the clean bacteria preparation of natural plant wide spectrum of the present invention to haemaphysalis longicornis
As shown in Table 3, the plants essential oil of being prepared by natural plant extracts is 30% to the 24h lethality of haemaphysalis longicornis, and in natural plant extracts, add after synergist and/or aqueous emulsion, 24h lethality to haemaphysalis longicornis all reaches 100%, therefore, the clean bacteria preparation of natural plant wide spectrum of the present invention belongs to A level to the indoor harmacological effect of haemaphysalis longicornis.
embodiment 7, anti-mite effect detection
The clean bacteria preparation of natural plant wide spectrum of the present invention is removed or on cotton, carried out pilot scale coating as spray, simultaneously with the cotton sample in contrast of spray formulation not, drive mite evaluating drug effect according to GB/T24253-2009 " evaluation of the anti-mite performance of textile ", wherein, drive mite rate computational methods as follows:
Testing result is as shown in table 4.
Table 4, the clean bacteria preparation of natural plant wide spectrum of the present invention drive mite effect
As shown in table 4, the clean bacteria preparation 24h of natural plant wide spectrum of the present invention is 95.81% to the scattering ratio of acarid, has good anti-mite effect.
In sum, the effect that the clean bacteria preparation of natural plant wide spectrum prepared by the present invention has good mosquito repellent, antibacterial, anti-tick, anti-mite, mildew-resistant and purifies air, and its primary raw material is natural plant extracts, nontoxic to human body, environmentally friendly pollution-free, be with a wide range of applications.
Claims (10)
1. the clean bacteria preparation of natural plant wide spectrum, is characterized in that, the clean bacteria preparation of described natural plant wide spectrum is made up of the raw material of following percentage by weight:
Plant pyrethrin 0.03%～5%;
Eucalyptus oil 0.01%～2%;
Thymol 0.03%～1%;
Peppermint 0.03%～1%;
Tea oil 1%～5%;
Dispersant 0.015%～0.5%;
Synergist 0.2%～30%;
Antioxidant 0.01%～3%;
Ethanol 35%～51%;
The water of surplus;
Wherein, described plant pyrethrin contains 20%～80% active component, and the concentration of described tea oil is that the concentration of 15%～50% ， Fish rattan ketone is 50%～80%.
2. the clean bacteria preparation of natural plant wide spectrum according to claim 1, is characterized in that, described dispersant is selected from one or more in rilanit special, organosilicon, sorbierite, poloxamer.
3. the clean bacteria preparation agent of natural plant wide spectrum according to claim 1, is characterized in that, described synergist is selected from the one in sesamin, citrene, neem oil, spearmint oil, tangerine oil, piperonyl butoxide.
4. the clean bacteria preparation of natural plant wide spectrum according to claim 1, is characterized in that, described antioxidant be selected from rosemary, Xue MingRosma rinus officinalis, 2, one or more in 6-di-tert-butyl-4-methy phenol, di-tert-butyl hydroquinone.
5. according to the preparation method of the clean bacteria preparation of natural plant wide spectrum described in any one in claim 1～4, it is characterized in that, comprise the following steps:
Synergist and plant pyrethrin are mixed, stir; The mixture that adds eucalyptus oil, Thymol, peppermint, tea oil, stirs; Add antioxidant, stir; Add dispersant, stir; Add second alcohol and water, stir.
6. preparation method according to claim 5, is characterized in that, described step is carried out under the condition of 35～60 ℃.
7. preparation method according to claim 5, is characterized in that, the rotating speed of described stirring is 500～2500rpm.
8. preparation method according to claim 5, is characterized in that, the time of described stirring is 30～120 minutes.
According to the clean bacteria preparation of natural plant wide spectrum described in any one in claim 1～4 for anti-tick, mosquito repellent, anti-mite, mildew-resistant, antibacterial, the application that purifies air.
10. in textile product, make textile self produce the application of antibody according to the clean bacteria preparation of natural plant wide spectrum described in any one in claim 1～4 as textile finish or direct spraying.
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| RU2639562C1 (en) * | 2016-11-04 | 2017-12-21 | ОБЩЕСТВО С ОГРАНИЧЕННОЙ ОТВЕТСТВЕННОСТЬЮ "КОСМЕТИКО-ФАРМАЦЕВТИЧЕСКАЯ КОМПАНИЯ "ГРИН ФАРМ КОСМЕТИК" (сокращенно - ООО "КФК "ГРИН ФАРМ КОСМЕТИК") | Active biological substance "ingaliptum active plus", local action preparation obtained on its basis |
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| CN108308188A (en) * | 2018-04-18 | 2018-07-24 | 中国人民解放军海军军医大学海军医学研究所 | A kind of water-base pesticide emulsion |
| CN108308188B (en) * | 2018-04-18 | 2022-06-21 | 中国人民解放军海军特色医学中心 | Water-based insecticidal emulsion |
| CN109430295A (en) * | 2018-12-21 | 2019-03-08 | 佛山市高科合创科技有限公司 | It is a kind of using tea-seed oil as the acaricide of primary raw material and its preparation |
| CN110338197A (en) * | 2019-07-31 | 2019-10-18 | 西藏阿木达草本科技有限公司 | A kind of plant type disinfecting mite-removing element and preparation method |
| CN111206426A (en) * | 2020-02-28 | 2020-05-29 | 南通大学 | Preparation method of mosquito-repellent cotton fabric |
| CN112450229A (en) * | 2020-12-09 | 2021-03-09 | 华南农业大学 | Plant essential oil type ultraviolet sterilization synergist and ultraviolet combined sterilization method thereof |
| CN115137680A (en) * | 2022-06-17 | 2022-10-04 | 汕头市金龙日化实业有限公司 | Mosquito repellent liquid and preparation method thereof |
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