CN103098830A - Disinfectant and preparation method thereof - Google Patents
Disinfectant and preparation method thereof Download PDFInfo
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- CN103098830A CN103098830A CN 201110356696 CN201110356696A CN103098830A CN 103098830 A CN103098830 A CN 103098830A CN 201110356696 CN201110356696 CN 201110356696 CN 201110356696 A CN201110356696 A CN 201110356696A CN 103098830 A CN103098830 A CN 103098830A
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Abstract
The invention relates to a disinfectant and a preparation method thereof, belonging to a field of traditional Chinese medicine. A to-be-solved problem is to provide a method of preparing the disinfectant, and the traditional Chinese medicine disinfectant prepared by the method is basically harmless to humans. The method of preparing the disinfectant comprises: a, taking 10-30 parts of honeysuckle flower, 25-40 parts of fructus forsythia, 4-8 parts of coptis, 50-70 parts of dandelion, 55-65 parts of isatis root, 25-50 parts of cape jasmine, 30-45 parts of licorice and 12-20 parts of radix ophiopogonis by weight ratio, crushing, uniformly mixing, adding an ethanol solution with a concentration of 50-80 % with an amount being 3-5 times of the weight of the medicinal materials, heating for reflux, extracting for 3-4 times; and b, filtering to obtain a filtrate, ie, the disinfectant.
Description
Technical field
The present invention relates to disinfectant and preparation method thereof, belong to the field of Chinese medicines.
Background technology
Disinfectant, people often claim that also disinfectant is " chemosterilant ".Disinfectant can be divided into bactericidal agent, high effect disinfectants, middle effect disinfectants, low effect disinfectants according to the level of its effect.Bactericidal agent can be killed all microorganisms makes it reach the sterilization requirement, comprise formaldehyde, glutaraldehyde, oxirane, Peracetic acid, hydrogen peroxide, chlorine dioxide, chlorine, copper sulphate, quicklime, ethanol, etc.High effect disinfectants can be killed all bacterial propagules (comprising mycobacterium), virus, fungi and spore thereof etc., bacterial spore also there is certain killing effect, reach the high level disinfection requirement, comprise chlorine-containing disinfectant, ozone, methyl hydantoin compounds, double-chain quaternary ammonium salt etc.Middle effect disinfectants only can be killed the microorganisms such as mycobacterium, fungi, virus and bacterial propagule, reaches the sterilization requirement, comprises containing iodine disinfectant, alcohol disinfectant, phenols disinfectant etc.But low effect disinfectants is kill vegetative forms of bacteria and close nma virus only, reach the disinfectant requirement, comprise the biguanides disinfectants such as quaternary ammonium disinfectant, Chlorhexidine (chlorohexidene) such as benzalkonium bromide, metal ion class disinfectant and the Chinese herbal disinfectants such as mercury, silver, copper.The definition disinfectant of disinfectant refers to be used to killing pathogenic microorganism on communication media, make it reach the preparation of innoxious requirement, it is different from antibiotic, its Main Function in diseases prevention is that pathogenic microorganism is eliminated outside human body, cut off the route of transmission of infectious disease, reach the purpose of controlling infectious disease.People often claim that also disinfectant is " chemosterilant ".Although the chemosterilant effect is better, some disinfectant such as formaldehyde etc. equally also can be detrimental to health.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of method for preparing disinfectant, and the Chinese medicine antiseptic of the method preparation is harmless to human body basic.
The method that the present invention prepares disinfectant comprises the steps:
A, 10～30 parts of extracting honeysuckles by weight ratio, 25～40 parts of the capsules of weeping forsythia, 4～8 parts of the coptiss, 50～70 parts of dandelions, 55～65 parts of Radix Isatidis, 25～50 parts of cape jasmines, 30～45 parts, Radix Glycyrrhizae, 12～20 parts of the tubers of dwarf lilyturf, pulverize, mixing, the concentration that adds 3～5 times of medicinal material weight is the ethanolic solution of 50～80wt%, heating and refluxing extraction 3～4 times;
B, filtration, gained filtrate is disinfectant.
Wherein, in order to improve Disinfection Effect, the present invention prepares the method for disinfectant, 15～25 parts of preferred extracting honeysuckles by weight ratio in its a step, 30～35 parts of the capsules of weeping forsythia, 5～7 parts of the coptiss, 55～65 parts of dandelions, 58～62 parts of Radix Isatidis, 35～45 parts of cape jasmines, 35～40 parts, Radix Glycyrrhizae, 15～19 parts of the tubers of dwarf lilyturf.20 parts of extracting honeysuckles most preferably by weight ratio in its a step, 32 parts of the capsules of weeping forsythia, 6 parts of the coptiss, 60 parts of dandelions, 60 parts of Radix Isatidis, 40 parts of cape jasmines, 38 parts, Radix Glycyrrhizae, 16 parts of the tubers of dwarf lilyturf.
Further, in order to improve Disinfection Effect, it is that the ethanolic solution of 70～80wt% carries out refluxing extraction that the method that the present invention prepares disinfectant preferably adopts concentration, and most preferably adopting concentration is that the ethanolic solution of 75wt% carries out refluxing extraction.
Wherein, in order to improve the quality of disinfectant, the present invention prepares the method for disinfectant, preferably adopts ultrafiltration to filter.
The present invention also provides the disinfectant by the said method preparation.
The present invention has following beneficial effect: the Disinfection Effect of disinfectant of the present invention is obvious, can substantially reach the Disinfection Effect of formaldehyde, and harmless, and cost is low, and the present invention has broad application prospects for disinfectant provides a kind of new selection.
Embodiment
The method that the present invention prepares disinfectant comprises the steps:
A, 10～30 parts of extracting honeysuckles by weight ratio, 25～40 parts of the capsules of weeping forsythia, 4～8 parts of the coptiss, 50～70 parts of dandelions, 55～65 parts of Radix Isatidis, 25～50 parts of cape jasmines, 30～45 parts, Radix Glycyrrhizae, 12～20 parts of the tubers of dwarf lilyturf, pulverize, mixing, the concentration that adds 3～5 times of medicinal material weight is the ethanolic solution of 50～80wt%, heating and refluxing extraction 3～4 times;
B, filtration, gained filtrate is disinfectant.
Wherein, in order to improve Disinfection Effect, the present invention prepares the method for disinfectant, 15～25 parts of preferred extracting honeysuckles by weight ratio in its a step, 30～35 parts of the capsules of weeping forsythia, 5～7 parts of the coptiss, 55～65 parts of dandelions, 58～62 parts of Radix Isatidis, 35～45 parts of cape jasmines, 35～40 parts, Radix Glycyrrhizae, 15～19 parts of the tubers of dwarf lilyturf.20 parts of extracting honeysuckles most preferably by weight ratio in its a step, 32 parts of the capsules of weeping forsythia, 6 parts of the coptiss, 60 parts of dandelions, 60 parts of Radix Isatidis, 40 parts of cape jasmines, 38 parts, Radix Glycyrrhizae, 16 parts of the tubers of dwarf lilyturf.
Further, in order to improve Disinfection Effect, it is that the ethanolic solution of 70～80wt% carries out refluxing extraction that the method that the present invention prepares disinfectant preferably adopts concentration, and most preferably adopting concentration is that the ethanolic solution of 75wt% carries out refluxing extraction.
Wherein, in order to improve the quality of disinfectant, the present invention prepares the method for disinfectant, preferably adopts ultrafiltration to filter.
The present invention also provides the disinfectant by the said method preparation.
Below in conjunction with embodiment, the specific embodiment of the present invention is further described, does not therefore limit the present invention among described scope of embodiments.
The preparation of embodiment 1 disinfectant of the present invention
Extracting honeysuckle 10kg, capsule of weeping forsythia 25kg, coptis 4kg, dandelion 70kg, Radix Isatidis 65kg, cape jasmine 25kg, Radix Glycyrrhizae 30kg, the tuber of dwarf lilyturf, 20kg, pulverized, and crosses 20 mesh sieves, mixing, the concentration that adds 3 times of medicinal material weight is the ethanolic solution of 70wt%, heating and refluxing extraction 4 times; Ultrafiltration, gained filtrate is disinfectant.
The preparation of embodiment 2 disinfectants of the present invention
Extracting honeysuckle 30kg, capsule of weeping forsythia 25kg, coptis 8kg, dandelion 50kg, Radix Isatidis 55kg, cape jasmine 50kg, Radix Glycyrrhizae 30kg, the tuber of dwarf lilyturf, 12kg, pulverized, and crosses 20 mesh sieves, mixing, the concentration that adds 5 times of medicinal material weight is the ethanolic solution of 80wt%, heating and refluxing extraction 3 times, ultrafiltration, gained filtrate is disinfectant.
The preparation of embodiment 3 disinfectants of the present invention
Extracting honeysuckle 10kg, capsule of weeping forsythia 30kg, coptis 7kg, dandelion 60kg, Radix Isatidis 60kg, cape jasmine 30kg, Radix Glycyrrhizae 40kg, the tuber of dwarf lilyturf, 15kg, pulverized, and crosses 20 mesh sieves, mixing, the concentration that adds 4 times of medicinal material weight is the ethanolic solution of 75wt%, heating and refluxing extraction 4 times, ultrafiltration, gained filtrate is disinfectant.
The preparation of embodiment 4 disinfectants of the present invention
Extracting honeysuckle 10kg, capsule of weeping forsythia 25kg, coptis 5kg, dandelion 55kg, Radix Isatidis 64kg, cape jasmine 45kg, Radix Glycyrrhizae 35kg, the tuber of dwarf lilyturf, 16kg, pulverized, and crosses 20 mesh sieves, the ethanolic solution that to add 4 times of concentration of medicinal material weight be 60wt%, heating and refluxing extraction 3 times, ultrafiltration, gained filtrate is disinfectant.
Through test, the disinfectant of embodiment 1-4 preparation reaches the Disinfection Effect of formaldehyde substantially.
Claims (7)
1. the method for preparing disinfectant is characterized in that comprising the steps:
A, 10～30 parts of extracting honeysuckles by weight ratio, 25～40 parts of the capsules of weeping forsythia, 4～8 parts of the coptiss, 50～70 parts of dandelions, 55～65 parts of Radix Isatidis, 25～50 parts of cape jasmines, 30～45 parts, Radix Glycyrrhizae, 12～20 parts of the tubers of dwarf lilyturf, pulverize, mixing, the concentration that adds 3～5 times of medicinal material weight is the ethanolic solution of 50～80wt%, heating and refluxing extraction 3～4 times;
B, filtration, gained filtrate is disinfectant.
2. the method for preparing disinfectant according to claim 1 is characterized in that: 15～25 parts of extracting honeysuckles by weight ratio in a step, 30～35 parts of the capsules of weeping forsythia, 5～7 parts of the coptiss, 55～65 parts of dandelions, 58～62 parts of Radix Isatidis, 35～45 parts of cape jasmines, 35～40 parts, Radix Glycyrrhizae, 15～19 parts of the tubers of dwarf lilyturf.
3. the method for preparing disinfectant according to claim 1 is characterized in that: 20 parts of extracting honeysuckles by weight ratio in a step, 32 parts of the capsules of weeping forsythia, 6 parts of the coptiss, 60 parts of dandelions, 60 parts of Radix Isatidis, 40 parts of cape jasmines, 38 parts, Radix Glycyrrhizae, 16 parts of the tubers of dwarf lilyturf.
4. the described method for preparing disinfectant of according to claim 1～3 any one is characterized in that: adopting concentration is that the ethanolic solution of 70～80wt% carries out refluxing extraction.
5. the method for preparing disinfectant according to claim 4 is characterized in that: adopting concentration is that the ethanolic solution of 75wt% carries out refluxing extraction.
6. the described method for preparing disinfectant of according to claim 1～5 any one, is characterized in that: adopt ultrafiltration to filter.
7. the disinfectant that is prepared by the described method of claim 1～6 any one.
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| CN 201110356696 CN103098830A (en) | 2011-11-11 | 2011-11-11 | Disinfectant and preparation method thereof |
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| CN 201110356696 CN103098830A (en) | 2011-11-11 | 2011-11-11 | Disinfectant and preparation method thereof |
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| CN103098830A true CN103098830A (en) | 2013-05-15 |
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Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103493851A (en) * | 2013-09-25 | 2014-01-08 | 合肥智上农业开发有限公司 | Traditional Chinese medicine disinfectant prepared employing film technology |
| CN104491229A (en) * | 2014-11-26 | 2015-04-08 | 成都顺发消洗科技有限公司 | Compound sterilizing solution |
| CN104663737A (en) * | 2014-05-27 | 2015-06-03 | 陕西仁康药业有限公司 | Bacteria cleaning effervescent tablet and preparation method thereof |
| CN105685117A (en) * | 2016-03-18 | 2016-06-22 | 安徽三联泵业股份有限公司 | Spray type Chinese herbal medicine pump disinfectant and preparation method thereof |
| CN106172519A (en) * | 2016-07-21 | 2016-12-07 | 南通佰能油化有限公司 | A kind of electronic product disinfectant solution |
| CN106212575A (en) * | 2016-07-21 | 2016-12-14 | 南通铁人体育设施工程有限公司 | Furniture disinfectant |
| CN106234458A (en) * | 2016-08-20 | 2016-12-21 | 裕龙农牧科技股份有限公司 | A kind of pig farm compound Chinese herb disinfectant |
| CN106342952A (en) * | 2016-08-28 | 2017-01-25 | 广西兴胜农牧有限公司 | Disinfectant for dairy farms |
| CN106342949A (en) * | 2016-08-28 | 2017-01-25 | 广西兴胜农牧有限公司 | Disinfectant for dairy farms and method for preparing the disinfectant |
| CN106342962A (en) * | 2016-08-28 | 2017-01-25 | 广西兴胜农牧有限公司 | Method for disinfecting dairy farms |
| CN106417406A (en) * | 2016-08-28 | 2017-02-22 | 广西兴胜农牧有限公司 | Disinfectant for disinfecting dairy farm |
| CN107114425A (en) * | 2017-06-05 | 2017-09-01 | 太仓优活生物技术有限公司 | A kind of safe and harmless pure natural disinfectant |
| CN108671088A (en) * | 2018-06-20 | 2018-10-19 | 河南牧业经济学院 | A kind of livestock and poultry cultivation Chinese herbal medicine environmental protection disinfectant and preparation method thereof and application method |
| CN111298059A (en) * | 2020-03-18 | 2020-06-19 | 湖南宝护者生物技术有限公司 | Skin mucosa disinfectant prepared from Chinese herbal medicines and preparation method thereof |
| CN114176099A (en) * | 2021-12-15 | 2022-03-15 | 何连旺 | Preparation process of environment-friendly disinfectant |
-
2011
- 2011-11-11 CN CN 201110356696 patent/CN103098830A/en active Pending
Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103493851A (en) * | 2013-09-25 | 2014-01-08 | 合肥智上农业开发有限公司 | Traditional Chinese medicine disinfectant prepared employing film technology |
| CN104663737A (en) * | 2014-05-27 | 2015-06-03 | 陕西仁康药业有限公司 | Bacteria cleaning effervescent tablet and preparation method thereof |
| CN104491229A (en) * | 2014-11-26 | 2015-04-08 | 成都顺发消洗科技有限公司 | Compound sterilizing solution |
| CN105685117A (en) * | 2016-03-18 | 2016-06-22 | 安徽三联泵业股份有限公司 | Spray type Chinese herbal medicine pump disinfectant and preparation method thereof |
| CN106172519A (en) * | 2016-07-21 | 2016-12-07 | 南通佰能油化有限公司 | A kind of electronic product disinfectant solution |
| CN106212575A (en) * | 2016-07-21 | 2016-12-14 | 南通铁人体育设施工程有限公司 | Furniture disinfectant |
| CN106234458B (en) * | 2016-08-20 | 2018-09-28 | 裕龙农牧科技股份有限公司 | A kind of pig farm compound Chinese herb disinfectant |
| CN106234458A (en) * | 2016-08-20 | 2016-12-21 | 裕龙农牧科技股份有限公司 | A kind of pig farm compound Chinese herb disinfectant |
| CN106342952A (en) * | 2016-08-28 | 2017-01-25 | 广西兴胜农牧有限公司 | Disinfectant for dairy farms |
| CN106342949A (en) * | 2016-08-28 | 2017-01-25 | 广西兴胜农牧有限公司 | Disinfectant for dairy farms and method for preparing the disinfectant |
| CN106342962A (en) * | 2016-08-28 | 2017-01-25 | 广西兴胜农牧有限公司 | Method for disinfecting dairy farms |
| CN106417406A (en) * | 2016-08-28 | 2017-02-22 | 广西兴胜农牧有限公司 | Disinfectant for disinfecting dairy farm |
| CN107114425A (en) * | 2017-06-05 | 2017-09-01 | 太仓优活生物技术有限公司 | A kind of safe and harmless pure natural disinfectant |
| CN108671088A (en) * | 2018-06-20 | 2018-10-19 | 河南牧业经济学院 | A kind of livestock and poultry cultivation Chinese herbal medicine environmental protection disinfectant and preparation method thereof and application method |
| CN111298059A (en) * | 2020-03-18 | 2020-06-19 | 湖南宝护者生物技术有限公司 | Skin mucosa disinfectant prepared from Chinese herbal medicines and preparation method thereof |
| CN114176099A (en) * | 2021-12-15 | 2022-03-15 | 何连旺 | Preparation process of environment-friendly disinfectant |
| CN114176099B (en) * | 2021-12-15 | 2023-08-11 | 安徽绿阳生物科技有限公司 | Environment-friendly disinfectant preparation process |
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Application publication date: 20130515 |