CN103061114B - 一种电磁屏蔽织物的制备方法 - Google Patents
一种电磁屏蔽织物的制备方法 Download PDFInfo
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- CN103061114B CN103061114B CN201310014809.5A CN201310014809A CN103061114B CN 103061114 B CN103061114 B CN 103061114B CN 201310014809 A CN201310014809 A CN 201310014809A CN 103061114 B CN103061114 B CN 103061114B
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- nickel
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- 238000002360 preparation method Methods 0.000 title claims abstract description 24
- 239000004753 textile Substances 0.000 title claims abstract description 11
- 238000007747 plating Methods 0.000 claims abstract description 109
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 56
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims abstract description 53
- 239000000126 substance Substances 0.000 claims abstract description 53
- 239000010949 copper Substances 0.000 claims abstract description 34
- 229910052751 metal Inorganic materials 0.000 claims abstract description 33
- 239000002184 metal Substances 0.000 claims abstract description 33
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims abstract description 30
- 229910052802 copper Inorganic materials 0.000 claims abstract description 30
- 229910052759 nickel Inorganic materials 0.000 claims abstract description 25
- SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 claims abstract description 18
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 16
- 239000001257 hydrogen Substances 0.000 claims abstract description 16
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 229910052709 silver Inorganic materials 0.000 claims abstract description 11
- 239000004332 silver Substances 0.000 claims abstract description 11
- 230000000536 complexating effect Effects 0.000 claims abstract description 10
- 229910001961 silver nitrate Inorganic materials 0.000 claims abstract description 9
- 238000001035 drying Methods 0.000 claims abstract 2
- 239000004744 fabric Substances 0.000 claims description 97
- 239000007788 liquid Substances 0.000 claims description 45
- 239000000243 solution Substances 0.000 claims description 33
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 20
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 20
- 235000011121 sodium hydroxide Nutrition 0.000 claims description 20
- 239000008139 complexing agent Substances 0.000 claims description 17
- 239000000872 buffer Substances 0.000 claims description 16
- 229910000906 Bronze Inorganic materials 0.000 claims description 13
- 239000010974 bronze Substances 0.000 claims description 13
- 239000003638 chemical reducing agent Substances 0.000 claims description 13
- KUNSUQLRTQLHQQ-UHFFFAOYSA-N copper tin Chemical compound [Cu].[Sn] KUNSUQLRTQLHQQ-UHFFFAOYSA-N 0.000 claims description 13
- 150000002815 nickel Chemical class 0.000 claims description 13
- 238000012545 processing Methods 0.000 claims description 13
- 239000003381 stabilizer Substances 0.000 claims description 13
- 239000004094 surface-active agent Substances 0.000 claims description 12
- 239000003795 chemical substances by application Substances 0.000 claims description 10
- 239000007864 aqueous solution Substances 0.000 claims description 8
- 101710134784 Agnoprotein Proteins 0.000 claims description 7
- 238000007670 refining Methods 0.000 claims description 7
- 239000012190 activator Substances 0.000 claims description 6
- 239000003054 catalyst Substances 0.000 claims description 6
- 229920000642 polymer Polymers 0.000 claims description 4
- 239000006172 buffering agent Substances 0.000 claims description 2
- 150000002739 metals Chemical class 0.000 claims description 2
- 238000000034 method Methods 0.000 abstract description 46
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 11
- 238000003912 environmental pollution Methods 0.000 abstract description 6
- 239000000178 monomer Substances 0.000 abstract 1
- 238000002203 pretreatment Methods 0.000 abstract 1
- 239000005020 polyethylene terephthalate Substances 0.000 description 17
- 239000001488 sodium phosphate Substances 0.000 description 16
- 229910000162 sodium phosphate Inorganic materials 0.000 description 16
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 16
- 229920004934 Dacron® Polymers 0.000 description 15
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 15
- LGQLOGILCSXPEA-UHFFFAOYSA-L nickel sulfate Chemical group [Ni+2].[O-]S([O-])(=O)=O LGQLOGILCSXPEA-UHFFFAOYSA-L 0.000 description 15
- 229910000363 nickel(II) sulfate Inorganic materials 0.000 description 15
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical group CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 14
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 10
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 10
- 238000012360 testing method Methods 0.000 description 9
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 8
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 description 8
- UMGDCJDMYOKAJW-UHFFFAOYSA-N thiourea Chemical compound NC(N)=S UMGDCJDMYOKAJW-UHFFFAOYSA-N 0.000 description 8
- 239000004327 boric acid Substances 0.000 description 7
- 150000001875 compounds Chemical class 0.000 description 7
- 238000005516 engineering process Methods 0.000 description 7
- 239000000835 fiber Substances 0.000 description 7
- 239000004310 lactic acid Substances 0.000 description 7
- 235000014655 lactic acid Nutrition 0.000 description 7
- 239000000203 mixture Substances 0.000 description 7
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical group O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 5
- 239000011248 coating agent Substances 0.000 description 5
- 238000000576 coating method Methods 0.000 description 5
- 230000000694 effects Effects 0.000 description 5
- 238000001465 metallisation Methods 0.000 description 5
- 229910052763 palladium Inorganic materials 0.000 description 5
- 229920001223 polyethylene glycol Polymers 0.000 description 5
- 239000001384 succinic acid Substances 0.000 description 5
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 4
- 229920000298 Cellophane Polymers 0.000 description 4
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical group [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 4
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical group [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 4
- 229920002334 Spandex Polymers 0.000 description 4
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 4
- 239000002253 acid Substances 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- 150000002431 hydrogen Chemical class 0.000 description 4
- 239000004745 nonwoven fabric Substances 0.000 description 4
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 4
- 239000001632 sodium acetate Substances 0.000 description 4
- 235000017281 sodium acetate Nutrition 0.000 description 4
- 239000004759 spandex Substances 0.000 description 4
- 239000011593 sulfur Substances 0.000 description 4
- 229910052717 sulfur Inorganic materials 0.000 description 4
- 238000001771 vacuum deposition Methods 0.000 description 4
- 238000009736 wetting Methods 0.000 description 4
- 239000002202 Polyethylene glycol Substances 0.000 description 3
- 235000011114 ammonium hydroxide Nutrition 0.000 description 3
- 238000001755 magnetron sputter deposition Methods 0.000 description 3
- 239000011159 matrix material Substances 0.000 description 3
- 229920000728 polyester Polymers 0.000 description 3
- 238000007788 roughening Methods 0.000 description 3
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 2
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 description 2
- 229920002125 Sokalan® Polymers 0.000 description 2
- 229920004933 Terylene® Polymers 0.000 description 2
- 230000004913 activation Effects 0.000 description 2
- 239000002390 adhesive tape Substances 0.000 description 2
- 125000005619 boric acid group Chemical group 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- ORTQZVOHEJQUHG-UHFFFAOYSA-L copper(II) chloride Chemical compound Cl[Cu]Cl ORTQZVOHEJQUHG-UHFFFAOYSA-L 0.000 description 2
- 230000005670 electromagnetic radiation Effects 0.000 description 2
- 239000003822 epoxy resin Substances 0.000 description 2
- 230000006870 function Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000004584 polyacrylic acid Substances 0.000 description 2
- 229920000647 polyepoxide Polymers 0.000 description 2
- 239000004814 polyurethane Substances 0.000 description 2
- 229920002635 polyurethane Polymers 0.000 description 2
- 239000000276 potassium ferrocyanide Substances 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 239000011780 sodium chloride Substances 0.000 description 2
- 230000000087 stabilizing effect Effects 0.000 description 2
- 238000010998 test method Methods 0.000 description 2
- XOGGUFAVLNCTRS-UHFFFAOYSA-N tetrapotassium;iron(2+);hexacyanide Chemical group [K+].[K+].[K+].[K+].[Fe+2].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-] XOGGUFAVLNCTRS-UHFFFAOYSA-N 0.000 description 2
- YWYZEGXAUVWDED-UHFFFAOYSA-N triammonium citrate Chemical group [NH4+].[NH4+].[NH4+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O YWYZEGXAUVWDED-UHFFFAOYSA-N 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- 208000016261 weight loss Diseases 0.000 description 2
- 230000004580 weight loss Effects 0.000 description 2
- KWSLGOVYXMQPPX-UHFFFAOYSA-N 5-[3-(trifluoromethyl)phenyl]-2h-tetrazole Chemical compound FC(F)(F)C1=CC=CC(C2=NNN=N2)=C1 KWSLGOVYXMQPPX-UHFFFAOYSA-N 0.000 description 1
- 241001044369 Amphion Species 0.000 description 1
- 244000207740 Lemna minor Species 0.000 description 1
- 235000006439 Lemna minor Nutrition 0.000 description 1
- 235000001855 Portulaca oleracea Nutrition 0.000 description 1
- 206010070834 Sensitisation Diseases 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000012298 atmosphere Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 229910000365 copper sulfate Inorganic materials 0.000 description 1
- 238000005202 decontamination Methods 0.000 description 1
- 230000003588 decontaminative effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- CEYULKASIQJZGP-UHFFFAOYSA-L disodium;2-(carboxymethyl)-2-hydroxybutanedioate Chemical compound [Na+].[Na+].[O-]C(=O)CC(O)(C(=O)O)CC([O-])=O CEYULKASIQJZGP-UHFFFAOYSA-L 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 238000005553 drilling Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 238000009713 electroplating Methods 0.000 description 1
- 239000007888 film coating Substances 0.000 description 1
- 238000009501 film coating Methods 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 238000006263 metalation reaction Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000009832 plasma treatment Methods 0.000 description 1
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 description 1
- 229920000053 polysorbate 80 Polymers 0.000 description 1
- VZOPRCCTKLAGPN-ZFJVMAEJSA-L potassium;sodium;(2r,3r)-2,3-dihydroxybutanedioate;tetrahydrate Chemical group O.O.O.O.[Na+].[K+].[O-]C(=O)[C@H](O)[C@@H](O)C([O-])=O VZOPRCCTKLAGPN-ZFJVMAEJSA-L 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000009991 scouring Methods 0.000 description 1
- 230000008313 sensitization Effects 0.000 description 1
- 235000017557 sodium bicarbonate Nutrition 0.000 description 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 229910001379 sodium hypophosphite Inorganic materials 0.000 description 1
- 229940074446 sodium potassium tartrate tetrahydrate Drugs 0.000 description 1
- 238000004544 sputter deposition Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000012956 testing procedure Methods 0.000 description 1
- RYCLIXPGLDDLTM-UHFFFAOYSA-J tetrapotassium;phosphonato phosphate Chemical compound [K+].[K+].[K+].[K+].[O-]P([O-])(=O)OP([O-])([O-])=O RYCLIXPGLDDLTM-UHFFFAOYSA-J 0.000 description 1
- 238000003911 water pollution Methods 0.000 description 1
Landscapes
- Chemically Coating (AREA)
- Shielding Devices Or Components To Electric Or Magnetic Fields (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
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Families Citing this family (16)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103422347B (zh) * | 2013-07-31 | 2015-07-29 | 天津新纶科技有限公司 | 一种用于化学镀的表面改性剂、表面改性处理方法和织物化学镀方法 |
CN103437026A (zh) * | 2013-08-16 | 2013-12-11 | 苏州东艺技研有限公司 | 一种防辐射聚酯纤维面料 |
CN103409876A (zh) * | 2013-08-16 | 2013-11-27 | 苏州东艺技研有限公司 | 一种防辐射聚乙烯醇纤维面料 |
CN104357816B (zh) * | 2014-11-13 | 2018-03-13 | 南通大学 | 一种铜镍导电面料的制备方法 |
CN104695212A (zh) * | 2015-03-20 | 2015-06-10 | 苏州陈恒织造有限公司 | 一种电磁屏蔽织物的制备方法 |
CN105297085B (zh) * | 2015-08-27 | 2018-10-16 | 中国科学院兰州化学物理研究所 | 一种镀镍液制备镍基镀层的方法 |
CN105821396A (zh) * | 2016-03-27 | 2016-08-03 | 华南理工大学 | 一种无钯化学镀铜的方法 |
CN107419524B (zh) * | 2017-08-03 | 2019-11-12 | 浙江三元电子科技有限公司 | 一种超薄电磁屏蔽材料 |
CN107815855A (zh) * | 2017-11-10 | 2018-03-20 | 湖南省凯纳方科技有限公司 | 一种纺织品金属化的制备方法 |
CN108330676A (zh) * | 2018-02-10 | 2018-07-27 | 朱东洋 | 一种抗拉型氨纶纤维的制备方法 |
CN108914093A (zh) * | 2018-06-05 | 2018-11-30 | 苏州巨奇光电科技有限公司 | 一种导电布的制备方法及导电布 |
CN109306460A (zh) * | 2018-09-25 | 2019-02-05 | 广州小楠科技有限公司 | 一种电磁屏蔽织物及其制备方法 |
CN110983763A (zh) * | 2019-12-18 | 2020-04-10 | 浙江蓝天制衣有限公司 | 一种适用于服装棉织物的化学镀铜的工艺 |
CN112593219B (zh) * | 2020-12-09 | 2021-09-28 | 昆山成功环保科技有限公司 | 铝基材直接化学镀铜的溶液及其应用方法 |
CN115852679B (zh) * | 2022-09-08 | 2024-08-16 | 西南科技大学 | 蚕丝织物铁活化法实现铜-镍双层化学镀 |
CN115852709A (zh) * | 2022-11-25 | 2023-03-28 | 电子科技大学长三角研究院(湖州) | 一种电磁屏蔽织物及其制备方法 |
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CN1400354A (zh) * | 2002-08-28 | 2003-03-05 | 苏州大学 | 织物表面金属化处理的方法 |
CN1570211A (zh) * | 2004-05-10 | 2005-01-26 | 夏芝林 | 镀银纤维织物的制备方法 |
CN1268803C (zh) * | 2004-01-13 | 2006-08-09 | 长沙力元新材料股份有限公司 | 一种镍铜复合金属织物及其制备方法 |
CN101876140A (zh) * | 2009-04-30 | 2010-11-03 | 昆山市同福电子材料厂 | 电磁屏蔽导电布的制备方法 |
Family Cites Families (1)
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JPS61146870A (ja) * | 1984-12-21 | 1986-07-04 | 平岡織染株式会社 | 繊維性基布の表面金属化方法 |
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Patent Citations (4)
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CN1400354A (zh) * | 2002-08-28 | 2003-03-05 | 苏州大学 | 织物表面金属化处理的方法 |
CN1268803C (zh) * | 2004-01-13 | 2006-08-09 | 长沙力元新材料股份有限公司 | 一种镍铜复合金属织物及其制备方法 |
CN1570211A (zh) * | 2004-05-10 | 2005-01-26 | 夏芝林 | 镀银纤维织物的制备方法 |
CN101876140A (zh) * | 2009-04-30 | 2010-11-03 | 昆山市同福电子材料厂 | 电磁屏蔽导电布的制备方法 |
Non-Patent Citations (1)
Title |
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JP昭61-146870A 1986.07.04 |
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