CN103025720B - 用于制备缩醛和缩酮的方法以及由此制备的缩醛和缩酮 - Google Patents

用于制备缩醛和缩酮的方法以及由此制备的缩醛和缩酮 Download PDF

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Publication number
CN103025720B
CN103025720B CN201180035811.XA CN201180035811A CN103025720B CN 103025720 B CN103025720 B CN 103025720B CN 201180035811 A CN201180035811 A CN 201180035811A CN 103025720 B CN103025720 B CN 103025720B
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China
Prior art keywords
ethyl levulinate
reactor
product
glycerol
acid
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Chinese (zh)
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CN103025720A (zh
Inventor
B·D·马伦
M·D·斯考特
A·J·卢瓦吉
S·A·多南
F·荆
V·拜达纳拉扬纳
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GF Biochemicals Ltd
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Segetis Inc
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
    • C07D317/08—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
    • C07D317/10—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings
    • C07D317/12—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, directly attached to ring carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
    • C07D317/08—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
    • C07D317/10—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings
    • C07D317/14—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D317/30—Radicals substituted by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
    • C07D317/08—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
    • C07D317/10—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings
    • C07D317/14—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D317/18—Radicals substituted by singly bound oxygen or sulfur atoms
    • C07D317/24—Radicals substituted by singly bound oxygen or sulfur atoms esterified
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Medicinal Preparation (AREA)
CN201180035811.XA 2010-08-03 2011-08-03 用于制备缩醛和缩酮的方法以及由此制备的缩醛和缩酮 Active CN103025720B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US37036510P 2010-08-03 2010-08-03
US61/370,365 2010-08-03
PCT/US2011/046463 WO2012018939A2 (en) 2010-08-03 2011-08-03 Methods for the manufacture of acetals and ketals, and the acetals and ketals produced thereby

Publications (2)

Publication Number Publication Date
CN103025720A CN103025720A (zh) 2013-04-03
CN103025720B true CN103025720B (zh) 2016-06-01

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Country Status (11)

Country Link
US (2) US20120035376A1 (https=)
EP (1) EP2601184B1 (https=)
JP (1) JP5886856B2 (https=)
KR (1) KR20130136955A (https=)
CN (1) CN103025720B (https=)
AU (1) AU2011285715B2 (https=)
BR (1) BR112013000575A2 (https=)
CA (2) CA2806352C (https=)
MX (1) MX336783B (https=)
SG (1) SG187044A1 (https=)
WO (1) WO2012018939A2 (https=)

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CN103069343B (zh) * 2010-08-12 2015-09-09 赛格提斯有限公司 羧基酯缩酮除去组合物、其制造方法及应用
US9212176B2 (en) 2010-11-11 2015-12-15 Segetis, Inc. Polyketal adducts, methods of manufacture and uses thereof
BR112013010073A2 (pt) 2010-11-11 2016-07-05 Segetis Inc adutos de éster polihidróxi cetálico, métodos de fabricação e seus usos
ITPN20130066A1 (it) 2013-11-11 2015-05-12 Fluos S A S Di Giuseppe Chiaradia & C Plastificanti per polimeri
WO2016028837A1 (en) 2014-08-20 2016-02-25 Resinate Materials Group, Inc. Polyester polyols from recycled polymers and waste streams
US9850400B2 (en) 2014-08-20 2017-12-26 Resinate Materials Group, Inc. Digestion of keratin
US9951171B2 (en) 2014-08-20 2018-04-24 Resinate Materials Group, Inc. Polyester polyols from recycled polymers and waste streams
US9580546B2 (en) 2014-10-29 2017-02-28 Resinate Materials Group, Inc. Polymeric plasticizer compositions
US9890243B2 (en) 2014-10-29 2018-02-13 Resinate Materials Group, Inc. Polymeric plasticizer compositions
CN110078701A (zh) * 2019-03-29 2019-08-02 郑州大学 一种农林废弃物制备生物质基缩酮酯的方法
US10773192B1 (en) * 2019-04-09 2020-09-15 Bitfury Ip B.V. Method and apparatus for recovering dielectric fluids used for immersion cooling
CN113929654B (zh) * 2021-10-26 2022-09-02 郑州大学 一种乙酰丙酸甘油缩酮甲酯的连续合成方法及应用
WO2024115796A1 (en) 2022-12-02 2024-06-06 Specialty Operations France Bio-based compounds

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US20080242721A1 (en) * 2005-11-22 2008-10-02 Aromagen Corporation Glycerol Levulinate Ketals and Their Use
WO2010036884A1 (en) * 2008-09-25 2010-04-01 Segetis, Inc. Ketal ester derivatives
CN101896474A (zh) * 2007-10-09 2010-11-24 希凯迪斯股份有限公司 制备缩酮和乙缩醛的方法

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US20080242721A1 (en) * 2005-11-22 2008-10-02 Aromagen Corporation Glycerol Levulinate Ketals and Their Use
CN101896474A (zh) * 2007-10-09 2010-11-24 希凯迪斯股份有限公司 制备缩酮和乙缩醛的方法
WO2010036884A1 (en) * 2008-09-25 2010-04-01 Segetis, Inc. Ketal ester derivatives

Also Published As

Publication number Publication date
BR112013000575A2 (pt) 2016-07-05
EP2601184A4 (en) 2014-01-15
US20150080585A1 (en) 2015-03-19
SG187044A1 (en) 2013-02-28
EP2601184A2 (en) 2013-06-12
CA2806352A1 (en) 2012-02-09
MX336783B (es) 2016-02-02
US20120035376A1 (en) 2012-02-09
AU2011285715B2 (en) 2016-04-21
JP2013537536A (ja) 2013-10-03
MX2013001158A (es) 2013-10-28
KR20130136955A (ko) 2013-12-13
CA2806352C (en) 2019-09-24
JP5886856B2 (ja) 2016-03-16
CN103025720A (zh) 2013-04-03
CA3051232C (en) 2021-08-31
US9593093B2 (en) 2017-03-14
EP2601184B1 (en) 2015-12-16
CA3051232A1 (en) 2012-02-09
AU2011285715A1 (en) 2013-01-31
WO2012018939A3 (en) 2012-08-09
WO2012018939A2 (en) 2012-02-09

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Effective date of registration: 20160823

Address after: The Republic of Malta Valletta

Patentee after: GFBIOCHEMICALS LIMITED

Address before: American Minnesota

Patentee before: Segetis, Inc.