CN103011952A - Manufacturing method of high-concentration biological compound fertilizer - Google Patents
Manufacturing method of high-concentration biological compound fertilizer Download PDFInfo
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- CN103011952A CN103011952A CN2012105026371A CN201210502637A CN103011952A CN 103011952 A CN103011952 A CN 103011952A CN 2012105026371 A CN2012105026371 A CN 2012105026371A CN 201210502637 A CN201210502637 A CN 201210502637A CN 103011952 A CN103011952 A CN 103011952A
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Abstract
The invention relates to a manufacturing method of a high-concentration biological compound fertilizer. The high-concentration biological compound fertilizer comprises the following components in percentage by weight: 20%-25% of carbamide, 25%-30% of monoammonium phosphate, 0%-5% of ammonium sulfate, 5%-7.5% of ammonium bicarbonate, 20%-25% of potassium sulfate, 18%-20% of raw materials containing humic acids, 1%-5% of trace elements and 0.5%-1% of biological microbial inoculum. The manufacturing process of the high-concentration biological compound fertilizer comprises the following steps of: uniformly mixing a common inorganic compound fertilizer raw material adopted as a vector with the humic acids and the biological microbial inoculum; then evaporating, granulating, drying, cooling, screening, coating a film, packaging, and detecting to be qualified; and then warehousing. The high-concentration biological compound fertilizer is a multifunctional compound fertilizer prepared by mixing microorganism bacteria and a compound fertilizer and can organically combine the microbial function and the conventional compound fertilizer function, thereby improving the granular structure of soil and enhancing the utilization ratio of fertilizers; and the high-concentration biological compound fertilizer is novel in production conception and is a first selected product of a compound fertilizer manufacturer on realizing product appreciation.
Description
Technical field
The present invention relates to high-concentration biological compound manure and preparation method thereof, belong to field of fertilizer production.
Background technology
Along with the development that fertilizer industry makes rapid progress, the problem that fertilizer industry faces becomes increasingly conspicuous, and the long-term application chemical fertilizer can cause soil acidification, soil compaction, and the Common compound fertilizer utilization rate of fertilizer is low, has increased the peasant and has produced input cost.
Summary of the invention
The object of the invention is to improve existing Common compound fertilizer and biological organic fertilizer can not complementary shortcoming and a kind of high-concentration biological compound manure and preparation method thereof is provided.
For achieving the above object, the present invention takes following design:
A kind of high-concentration biological compound manure forms the components by weight percent proportioning:
Urea: 20～25, monoammonium phosphate: 25～30, ammonium sulfate: 0～5, bicarbonate of ammonia: 5～7.5
Vitriolate of tartar: 20～25, contain humic acid material: 18～20, trace element: 1～5, bacteria agent: 0.5～1.
Further, form the components by weight percent proportioning:
Urea: 25, monoammonium phosphate: 25, ammonium sulfate: 2.5, bicarbonate of ammonia: 6
Vitriolate of tartar: 25, contain humic acid material: 20, trace element: 3, bacteria agent: 0.5
Further, nitrogen, phosphorus, potassium total nutrient content are not less than 40% in the described compound fertilizer product.
Further, described bacteria agent is the composite fungus agent that a kind of or any several microbial inoculum in subtilis, bacillus laterosporus, Bacillus licheniformis and the bacillus megaterium that is in the gemma phase mixes.
Further, described bacteria agent is the composite fungus agent in subtilis, bacillus laterosporus, Bacillus licheniformis and the bacillus megaterium that is in the gemma phase, mass ratio 3:3:2:2.
Further, the described humic acid material that contains is weathered coal, brown coal, industrial or agricultural organic waste through overactivation.
A kind of method of producing above-mentioned high-concentration biological compound manure, employing contains humic acid material and does the bacteria agent carrier, with bacteria agent with contain humic acid material and mix, mix with conventional composite fertilizer material again, through steam granulation, oven dry, cooling, screening, coating, packing, detection warehousing after passing, adopt step as follows:
Step 1: various raw materials are entered in the steel basin after metering by above-mentioned components by weight percent proportioning mix;
Step 2: the raw material that mixes is delivered to after crusher in crushing in the granulating cylinder with travelling belt, by steam granulation, material humidification, heating are caused fertiliser granulates;
Step 3: the material of granulating is sent in the dram, by the hot blast exchange board material is dried, the outside shake hammer of dram does not stop to beat dram with the rotation of dram, avoids an endoparticle adhesion and causes granulating rate to descend, and the dram temperature out is 65～80 ℃;
Step 4: the material of oven dry is sent to the coating cylinder after cooling, screening, this moment, particle temperature was 35～45 ℃, anti-hard caking agent evenly is sprayed on the fertiliser granulates surface with 2 ‰ ratio, enters packing shop by lift and pack, detect warehousing after passing in batches.
Further, the temperature in the described granulating cylinder is 50～60 ℃, 80 rev/mins of rotations of granulating cylinder.
Further, the used anti-hard caking agent of described coating cylinder is commercially available anti-hard caking agent.
Excellent results of the present invention is as follows:
The present invention combines microbiobacterial agent and Common compound fertilizer raw material, and good characteristic and compound fertilizer technology combination with the fixed nitrogen of microorganism, the phosphorus of living, short potassium form a kind of new fertilizer type.The suitable food crop of this fertilizer and the diversified economy crops such as fruit tree, vegetables, respond well.
Concrete advantage is as follows:
It is the multifunctional compound fertilizer that a kind of biological organic fertilizer and inorganic fertilizer mix, and its existing bio-organic fertilizer long-lasting has again the special efficacy type of humic acids improvement soil concurrently, also has the quick-acting of inorganic fertilizer, is the innovative product of composite fertilizer enterprise.Its advantage is embodied in following 4 aspects:
1. because containing a large amount of humic acidss in the fertilizer, therefore can promote the formation of soil aggregate, increase the drought-resistant ability of crop and the shock-absorbing capacity of soil, the improvement soil compaction is increase soil fertility and plant recovery of nutrient;
2. because this fertilizer of biological bacteria can form micro-ecological environment around crop root, in this ecotope, particularly adopt the bacterial classification of this ratio, profitable strain accounts for leading, suppresses harmful bacteria and grows, and promotes healthy growth of crops;
3. this fertilizer nutritive element is comprehensive, except also having a large amount of nitrogen, phosphorus, potassium, also contains various trace elements (such as boron, iron, manganese, zinc etc., satisfying the different demands of different growth phases);
4. this fertilizer component can satisfy all nutrient requirements of plant production phase, and this fertilizer can single fertilization in the general situation of soil fertility, reduces fertilizer application frequency, reduces labour intensity and frequency.
Below in conjunction with the implementation explanation.
Embodiment:
Following examples are used for explanation the present invention, but are not used for limiting the scope of the invention.
Embodiment bacteria used thereby powder is available from the vast rich special bio tech ltd in Guangzhou; Wherein, the weight ratio of described subtilis, bacillus laterosporus, Bacillus licheniformis and bacillus megaterium is 3:3:2:2, and wherein the every gram viable count of subtilis is that 2,100 hundred million, the every gram viable count of bacillus laterosporus are that 2,500 hundred million, the every gram viable count of Bacillus licheniformis are that 2,000 hundred million, the every gram viable count of bacillus megaterium are 2,200 hundred million.
Described humic acids mainly contains organic matter (40%), humic acids total amount (42%) available from the complete holy chemical industry in Wuhai City limited liability company.
All commercially available acquisitions of used other raw material in the enforcement.
Embodiment 1:
Step 1: with following mass parts: 20 parts of urea, 30 parts of monoammonium phosphates, 5 parts of ammonium sulfate, 5 parts of bicarbonate of ammonia, 25 parts of vitriolate of tartar, 18 parts contain humic acid material, 1 part of trace element and 0.5 part of bacteria agent and add in the steel basin and mix;
Step 2: the raw material that mixes is delivered to after crusher in crushing in the granulating cylinder with travelling belt, by steam granulation, with heating material to 50 ℃, by the moving balling-up of the not stall of 80 rev/mins of granulating cylinders;
Step 3: the material of balling-up is sent in the dram, by the hot blast exchange board material is dried, the outside shake hammer of dram does not stop to beat dram with the rotation of dram, avoids an endoparticle adhesion and causes granulating rate to descend, and the dram temperature out is 65 ℃;
Step 4: the material of oven dry is sent to the coating cylinder after cooling, screening, this moment, particle temperature was 35 ℃, anti-hard caking agent evenly is sprayed on the fertiliser granulates surface with 2 ‰ ratio, enters packing shop by lift and pack, detect warehousing after passing in batches.
Embodiment 2:
Step 1: with 25 parts of urea, 25 part of one ammonium, 7.5 parts of bicarbonate of ammonia, 20 parts of vitriolate of tartar, 20 parts contain humic acid material, 5 parts of trace elements and 1 part of bacteria agent and add in the steel basin and mix;
Step 2: the raw material that mixes is delivered to after crusher in crushing in the granulating cylinder with travelling belt, by steam granulation, with heating material to 60 ℃, by the moving balling-up of the not stall of 80 rev/mins of granulating cylinders;
Step 3: the material of balling-up is sent in the dram, by the hot blast exchange board material is dried, the outside shake hammer of dram does not stop to beat dram with the rotation of dram, avoids an endoparticle adhesion and causes granulating rate to descend, and the dram temperature out is 80 ℃;
Step 4: the material of oven dry is sent to the coating cylinder after cooling, screening, this moment, particle temperature was 45 ℃, anti-hard caking agent evenly is sprayed on the fertiliser granulates surface with 2 ‰ ratio, enters packing shop by lift and pack, detect warehousing after passing in batches.
Embodiment 3:
Step 1: with 22.5 parts of urea, 27.5 part of one ammonium, 2.5 parts of ammonium sulfate, 6 parts of bicarbonate of ammonia, 22.5 parts of vitriolate of tartar, 19 parts contain humic acid material, 2.5 parts of trace elements and 0.75 part of bacteria agent and add in the steel basin and mix;
Step 2: the raw material that mixes is delivered to after crusher in crushing in the granulating cylinder with travelling belt, by steam granulation, with heating material to 55 ℃, by the moving balling-up of the not stall of 80 rev/mins of granulating cylinders;
Step 3: the material of balling-up is sent in the dram, by the hot blast exchange board material is dried, the outside shake hammer of dram does not stop to beat dram with the rotation of dram, avoids an endoparticle adhesion and causes granulating rate to descend, and the dram temperature out is 73 ℃;
Step 4: the material of oven dry is sent to the coating cylinder after cooling, screening, this moment, particle temperature was 40.5 ℃, anti-hard caking agent evenly is sprayed on the fertiliser granulates surface with 2 ‰ ratio, enters packing shop by lift and pack, detect warehousing after passing in batches.
Embodiment 4:
Step 1: with 25 parts of urea, 25 part of one ammonium, 2.5 parts of ammonium sulfate, 6 parts of bicarbonate of ammonia, 25 parts of vitriolate of tartar, 20 parts contain humic acid material, 3 parts of trace elements and 0. 5 parts of bacteria agents and add in the steel basins and mix;
Step 2: the raw material that mixes is delivered to after crusher in crushing in the granulating cylinder with travelling belt, by steam granulation, with heating material to 55 ℃, by the moving balling-up of the not stall of 80 rev/mins of granulating cylinders;
Step 3: the material of balling-up is sent in the dram, by the hot blast exchange board material is dried, the outside shake hammer of dram does not stop to beat dram with the rotation of dram, avoids an endoparticle adhesion and causes granulating rate to descend, and the dram temperature out is 73 ℃;
Step 4: the material of oven dry is sent to the coating cylinder after cooling, screening, this moment, particle temperature was 40.5 ℃, anti-hard caking agent evenly is sprayed on the fertiliser granulates surface with 2 ‰ ratio, enters packing shop by lift and pack, detect warehousing after passing in batches.
Simultaneous test 1
The high-concentration biological composite fertilizer of experiment fertilizer: embodiment 1;
Contrast fertilizer: Common compound fertilizer (N:P
2O
5: K
2O=15:15:15);
According to routine operation the high-concentration biological composite fertilizer of embodiment 1 and contrast fertilizer are applied on the vegetables respectively.
The result: detect according to quality supervised department, is waiting under the commodity amount application conditions, compare with contrast fertilizer, use the vegetables that compound manure that the embodiment of the invention 1 obtains is produced, grow fine, the output height, quality better is used cost more than 25%; Nitrate and remnant nitrite significantly reduce, and wherein nitrate content is below the 1440mg/kg, reduce more than 60% than the nuisanceless grain standard 3800mg/kg of country; Average amount of increase in production reaches about 15-22%; Use the rear soil weight and alleviate, field capacity improves, and the soil structure improved addictive successful reduces by 40% pollution of area source.
Simultaneous test 2
Experiment fertilizer: the high-concentration biological composite fertilizer of embodiment 2-3;
Contrast fertilizer: Common compound fertilizer (N:P
2O
5: K
2O=15:15:15);
According to routine operation the high-concentration biological composite fertilizer of embodiment 2-3 and contrast fertilizer are applied to respectively on wheat, the fruit tree.
The result: detect according to quality supervised department, is waiting under the commodity amount application conditions, compare with contrast fertilizer, use wheat and fruit tree that compound manure that embodiment of the invention 2-3 obtains is produced, grow fine, the output height, quality better is used cost more than 28%; Nitrate and remnant nitrite significantly reduce, and wherein nitrate content is below the 1500mg/kg, reduce more than 50% than the nuisanceless grain standard 3500mg/kg of country; Average amount of increase in production reaches about 18-25%; Use the rear soil weight and alleviate, field capacity improves, and the soil structure improved addictive successful reduces by 45% pollution of area source.
Simultaneous test 3
The high-concentration biological composite fertilizer of experiment fertilizer: embodiment 4;
Contrast fertilizer: Common compound fertilizer (N:P
2O
5: K
2O=15:15:15);
According to routine operation the high-concentration biological composite fertilizer of embodiment 4 and contrast fertilizer are applied to respectively on wheat, the fruit tree.
The result: detect according to quality supervised department, is waiting under the commodity amount application conditions, compare with contrast fertilizer, use wheat and fruit tree that compound manure that the embodiment of the invention 4 obtains is produced, grow fine, the output height, quality better is used cost more than 30%; Nitrate and remnant nitrite significantly reduce, and wherein nitrate content is below the 1300mg/kg, reduce more than 50% than the nuisanceless grain standard 3500mg/kg of country; Average amount of increase in production reaches about 24-29%; Use the rear soil weight and alleviate, field capacity improves, and the soil structure improved addictive successful reduces by 50% pollution of area source.
Claims (9)
1. high-concentration biological compound manure is characterized in that: form the components by weight percent proportioning:
Urea: 20～25, monoammonium phosphate: 25～30, ammonium sulfate: 0～5, bicarbonate of ammonia: 5～7.5
Vitriolate of tartar: 20～25, contain humic acid material: 18～20, trace element: 1～5, bacteria agent: 0.5～1.
2. high-concentration biological compound manure according to claim 1 is characterized in that: form the components by weight percent proportioning:
Urea: 25, monoammonium phosphate: 25, ammonium sulfate: 2.5, bicarbonate of ammonia: 6
Vitriolate of tartar: 25, contain humic acid material: 20, trace element: 3, bacteria agent: 0.5.
3. according to high-concentration biological compound manure claimed in claim 1, it is characterized in that: nitrogen, phosphorus, potassium total nutrient content are not less than 40% in the described compound fertilizer product.
4. according to claim 1 or 2 described high-concentration biological compound manure, it is characterized in that: described bacteria agent is the composite fungus agent that a kind of or any several microbial inoculum in subtilis, bacillus laterosporus, Bacillus licheniformis and the bacillus megaterium that is in the gemma phase mixes.
5. want 4 described high-concentration biological compound manure according to right, it is characterized in that: described bacteria agent is the composite fungus agent in subtilis, bacillus laterosporus, Bacillus licheniformis and the bacillus megaterium that is in the gemma phase, mass ratio 3:3:2:2.
6. according to claim 1 or 2 described high-concentration biological compound manure, it is characterized in that: the described humic acid material that contains is weathered coal, brown coal, industrial or agricultural organic waste through overactivation.
7. method of producing above-mentioned high-concentration biological compound manure, it is characterized in that: employing contains humic acid material and does the bacteria agent carrier, with bacteria agent with contain humic acid material and mix, mix with conventional composite fertilizer material again, through steam granulation, oven dry, cooling, screening, coating, packing, detection warehousing after passing, adopt step as follows:
Step 1: various raw materials are entered in the steel basin after metering by above-mentioned components by weight percent proportioning mix;
Step 2: the raw material that mixes is delivered to after crusher in crushing in the granulating cylinder with travelling belt, by steam granulation, material humidification, heating are caused fertiliser granulates;
Step 3: the material of granulating is sent in the dram, by the hot blast exchange board material is dried, the outside shake hammer of dram does not stop to beat dram with the rotation of dram, avoids an endoparticle adhesion and causes granulating rate to descend, and the dram temperature out is 65～80 ℃;
Step 4: the material of oven dry is sent to the coating cylinder after cooling, screening, this moment, particle temperature was 35～45 ℃, anti-hard caking agent evenly is sprayed on the fertiliser granulates surface with 2 ‰ ratio, enters packing shop by lift and pack, detect warehousing after passing in batches.
8. the method for described production high-concentration biological compound manure according to claim 6, it is characterized in that: the temperature in the described granulating cylinder is 50～60 ℃, 80 rev/mins of rotations of granulating cylinder.
9. the method for described production high-concentration biological compound manure according to claim 6, it is characterized in that: the used anti-hard caking agent of described coating cylinder is commercially available anti-hard caking agent.
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| CN104326830A (en) * | 2014-11-13 | 2015-02-04 | 中国科学院亚热带农业生态研究所 | Organic-inorganic compound fertilizer and preparation method thereof |
| CN104876764A (en) * | 2015-05-14 | 2015-09-02 | 洛阳茁壮肥业有限公司 | Compound fertilizer for vegetable planting |
| CN104876667A (en) * | 2015-05-14 | 2015-09-02 | 洛阳茁壮肥业有限公司 | Compound fertilizer for corn planting |
| CN104892104A (en) * | 2015-05-14 | 2015-09-09 | 洛阳茁壮肥业有限公司 | Composite fertilizer for wheat plantation |
| CN105801240A (en) * | 2016-01-29 | 2016-07-27 | 山东鑫圣源生物工程技术有限公司 | Fertilizer batching microbial agent and preparation method therefor |
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| CN106316691A (en) * | 2016-08-24 | 2017-01-11 | 石家庄市中嘉化肥有限公司 | Polynucleotide zinc humid acid synergistic fertilizer and preparing method thereof |
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| CN108794225A (en) * | 2018-09-18 | 2018-11-13 | 周口万德生物有机肥有限公司 | A kind of dedicated compound organic and inorganic fertilizer of fruits and vegetables |
| CN108821926A (en) * | 2018-09-18 | 2018-11-16 | 周口万德生物有机肥有限公司 | A kind of dedicated compound organic and inorganic fertilizer of corn |
| CN108840762A (en) * | 2018-09-18 | 2018-11-20 | 周口万德生物有机肥有限公司 | A kind of dedicated compound organic and inorganic fertilizer of peanut soybean |
| CN108840761A (en) * | 2018-09-18 | 2018-11-20 | 周口万德生物有机肥有限公司 | A kind of dedicated compound organic and inorganic fertilizer of wheat |
| CN109574746A (en) * | 2018-12-14 | 2019-04-05 | 河北百禾丰化肥有限公司 | A kind of microbe synergistic compound fertilizer and preparation method thereof |
| CN110357701A (en) * | 2018-04-11 | 2019-10-22 | 山东红日化工股份有限公司 | A kind of composite microbial manure and preparation method thereof for preventing and treating tomato wilt |
| CN110845271A (en) * | 2019-11-25 | 2020-02-28 | 滨州学院 | Soil remediation microbial agent and preparation method thereof |
| CN111646837A (en) * | 2020-04-30 | 2020-09-11 | 湖北绿道农业发展有限公司 | Vegetable bio-organic fertilizer, preparation method and fertilization method thereof |
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| CN104326830A (en) * | 2014-11-13 | 2015-02-04 | 中国科学院亚热带农业生态研究所 | Organic-inorganic compound fertilizer and preparation method thereof |
| CN104326830B (en) * | 2014-11-13 | 2016-11-02 | 中国科学院亚热带农业生态研究所 | A kind of compound organic and inorganic fertilizer and preparation method |
| CN104876764A (en) * | 2015-05-14 | 2015-09-02 | 洛阳茁壮肥业有限公司 | Compound fertilizer for vegetable planting |
| CN104876667A (en) * | 2015-05-14 | 2015-09-02 | 洛阳茁壮肥业有限公司 | Compound fertilizer for corn planting |
| CN104892104A (en) * | 2015-05-14 | 2015-09-09 | 洛阳茁壮肥业有限公司 | Composite fertilizer for wheat plantation |
| CN105801240A (en) * | 2016-01-29 | 2016-07-27 | 山东鑫圣源生物工程技术有限公司 | Fertilizer batching microbial agent and preparation method therefor |
| CN105859428A (en) * | 2016-05-23 | 2016-08-17 | 史丹利化肥股份有限公司 | High-concentration inorganic compound microbial fertilizer |
| CN106316691A (en) * | 2016-08-24 | 2017-01-11 | 石家庄市中嘉化肥有限公司 | Polynucleotide zinc humid acid synergistic fertilizer and preparing method thereof |
| CN107523310A (en) * | 2017-08-29 | 2017-12-29 | 宁夏顺宝现代农业股份有限公司 | It is a kind of suitable for soil conditioner of nonacid soil and preparation method thereof |
| CN110357701A (en) * | 2018-04-11 | 2019-10-22 | 山东红日化工股份有限公司 | A kind of composite microbial manure and preparation method thereof for preventing and treating tomato wilt |
| CN108794225A (en) * | 2018-09-18 | 2018-11-13 | 周口万德生物有机肥有限公司 | A kind of dedicated compound organic and inorganic fertilizer of fruits and vegetables |
| CN108821926A (en) * | 2018-09-18 | 2018-11-16 | 周口万德生物有机肥有限公司 | A kind of dedicated compound organic and inorganic fertilizer of corn |
| CN108840762A (en) * | 2018-09-18 | 2018-11-20 | 周口万德生物有机肥有限公司 | A kind of dedicated compound organic and inorganic fertilizer of peanut soybean |
| CN108840761A (en) * | 2018-09-18 | 2018-11-20 | 周口万德生物有机肥有限公司 | A kind of dedicated compound organic and inorganic fertilizer of wheat |
| CN109574746A (en) * | 2018-12-14 | 2019-04-05 | 河北百禾丰化肥有限公司 | A kind of microbe synergistic compound fertilizer and preparation method thereof |
| CN110845271A (en) * | 2019-11-25 | 2020-02-28 | 滨州学院 | Soil remediation microbial agent and preparation method thereof |
| CN111646837A (en) * | 2020-04-30 | 2020-09-11 | 湖北绿道农业发展有限公司 | Vegetable bio-organic fertilizer, preparation method and fertilization method thereof |
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Application publication date: 20130403 |