CN103006518A - Method for preparing novel nutrient recovery type skin-care facial mask - Google Patents
Method for preparing novel nutrient recovery type skin-care facial mask Download PDFInfo
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- CN103006518A CN103006518A CN2013100046706A CN201310004670A CN103006518A CN 103006518 A CN103006518 A CN 103006518A CN 2013100046706 A CN2013100046706 A CN 2013100046706A CN 201310004670 A CN201310004670 A CN 201310004670A CN 103006518 A CN103006518 A CN 103006518A
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Abstract
The invention relates to a method for preparing a novel nutrient recovery type skin-care facial mask. A method for making an efficient cheap facial mask product which contains natural biological materials as the main moisturizing, nutrient and film forming components is designed. The method comprises the step of extracting sericin in natural colorful cocoons by a special method instead of the traditional animal collagen, substituting the compound components of konjaku flour and xanthan gum for hyaluronic acid as the main film forming materials, and simultaneously blending the materials with curacao aloe powder, thereby obtaining the novel facial mask product. The novel facial mask product has the effects of keeping the skin fine and smooth, removing free radicals, supplementing moisture and collagen and the like. The product obtained by the method provided by the invention has multiple bioactivities, is advantageous for the skin to absorbing various active ingredients, and also has obvious effects on softening the skin, preventing and treating acnes, age pigments, freckles and pachulosis, diminishing inflammation and relieving itching, keeping the skin fine and white and the like.
Description
Technical field
The present invention relates to the production technology of facial treatment mask, particularly relate to the preparation method of making a kind of novel nourishing rehabilitation type facial treatment mask as primary raw material take natural colorful silk glue protein and Rhizoma amorphophalli powder and xanthan gum, Aloe vulgaris powder, belong to the Cosmetic Manufacture technical field.
Background technology
Facial film is comparatively popular in recent years a kind of novel cosmetic, has been widely used in the beauty and skin care industry.Facial film forms a skim at skin surface, and its energy tensioning the skin opens facial pore, and blood circulation promoting when facial film is washed off or come off, because the dirt in the pore that opens can be taken away by facial film, makes skin of face become clean.
The use of natural biologic material in facial film become trend.Collagen protein begins to be applied in the mask product as a kind of effective green cosmetic material.Collagen protein on the market mostly is animal collagen, general molecular weight is all more than 300,000 dalton, because molecular weight is larger, no matter be for oral administration or external, will be through conversion, the again required collagen protein of synthesized human after entering human body, and in the process of conversion, part can convert the protein of fat or other kinds to, and absorbance is limited, so cosmetic result is also limited.In addition, the main component of moisturizing film forming is hyaluronic acid, and is expensive, causes product cost to improve.The quantity of facial film and kind have very large development in recent years, but functional component abundant and be easy to absorb, green face pack product that film-formation result is good, with low cost still lacks.
The coloring matter of natural colorful cocoon all comes from the synthetic of Folium Mori or silkworm body self, thereby its silk fabric natural health, can avoid chemical dye to the harm of human body.The natural colorful cocoon often is dropped as refuse at chromatic cocoon shell and the husks behind filature, in fact the sericin composition that wherein enriches has good performance of keeping humidity and skin moistening effect to skin, and also have a following function: thus antioxidant activity, suppress that TYR enzyme check melanin forms, the activating skin cell, promote regeneration, the anti-ageing cosmetology effect of waiting for a long time of cell.Natural colorful silk glue contains sericin and the natural pigment such as flavonoid, carotenoid, sericin wherein can make skin keep certain moisture, characteristic and skin moisture-keeping functions with stronger decomposition free radical activity, that flavone, carotenoid etc. possess is antibiotic, anti-ultraviolet, antioxidation etc. be to the function of body-care, generation that can also check melanin, delaying skin is wrinkling aging.Therefore natural colorful silk glue protein substitutes traditional collagen protein better biological activity.
Xanthan gum is a kind of extracellular polysaccharide that produces through microbial fermentation, and colorless and odorless is nontoxic, meets the water-soluble colloid that is expanded into, and good thickening property and film property are arranged, and is a kind of good biological slow-released material, is conducive to the release of biological effective components and allows absorption of human body.
Rhizoma amorphophalli is a kind of perennial grass wood plant, Rhizoma amorphophalli powder is that its underground oblate spheroid tuber is processed, contain abundant cellulose and trace element, also have 16 seed amino acids, the main component konjak glucomannan (KGM) in the Rhizoma amorphophalli powder is a kind of natural plant polyose, and KGM is medium-sized nonionic linear polysaccharide contained in the Rhizoma amorphophalli tuber, with β-1 by glucose and mannose, 4 glycosidic bonds are a kind of good dietary fibers in conjunction with the macromolecular compound that forms, the tool hydrophilic, gelation, caking property, edibility, antibiotic property, the characteristics such as film property, be characterized in that consumption is low, intensity is high, and the transparency is good.KGM and xanthan gum blend can form the good gel of film property later, and the network size of this gel formation is released very suitable running micromolecule polypeptide and protide composition, and it is very beneficial that skin is absorbed plurality of active ingredients.
Aloe is liliaceous succulent plant, be widely used in the cosmetics at present, but the kind of Aloe has hundreds of, and the most typical with the Aloe vulgaris Aloe of health care arranged.Aloe vulgaris is commonly referred to as bar bar Aloe, and Aloe Barbadensis Miller claims again aloe vera, desert Bulbus Lilii, and it is to be applied at present the most widely kind of beauty treatment aspect.On European Cosmetic Market, the cosmetics take Aloe as raw material can be found everywhere, and accounts for more than 80% according to statistics.The Aloe vulgaris Aloe has the multiple efficacies composition of a series of therapeutic efficiency and nourishes rough skin; to softening skin, restraining and preventing and treating acne, senile plaque, freckle, pachylosis and anti-inflammatory anti-itch, the delicate Bai Jie of protection skin etc. has remarkable efficacy.
Summary of the invention
The objective of the invention is to design a kind of efficient cheap mask product manufacture method take natural biologic material as main moisture-keeping nutrient and film-forming components, this product is to substitute traditional animal collagen with the sericin that extracts in the natural colorful cocoon by ad hoc approach, composite parts with Rhizoma amorphophalli powder and xanthan gum replaces hyaluronic acid as main filmogen, be equipped with simultaneously the Aloe vulgaris powder, make novel mask product, make it have the smooth exquisiteness of the skin of allowing, remove free radical, keep the skin wet and the effect such as collagen protein.
The present invention is achieved in that a kind of preparation method of novel nourishing rehabilitation type facial treatment mask:
1. the extraction of colourful silk glue protein: husks, the cocoon shell of the chromatic cocoon that dries pulverized be the fragment of 1-3mm size, then measure raw materials quality 30-60 distilled water doubly, the raw material fragment be impregnated in the aqueous solution, make the abundant swelling 20-50min of husks shell, then under normal pressure, boil, make the sericin in cocoon one shell partly be eluted in the solution, and to a certain degree hydrolysis, when liquor capacity was concentrated into original 1/10-1/5, stopped heating was cooled to room temperature.The neutral protease that adds husks chitin amount 1.5-2.5% in solution carries out enzymolysis, hydrolysis temperature is 20-35 ℃, pH value is 6.8-7.7, continues enzymolysis 120-240min, makes the sericin in the solution be hydrolyzed to the active sericin that mean molecule quantity is 5000-20000Da.Then solution is heated to boiling and keeps 10-30min, enzyme denaturing is lived.Undissolvable silkworm silk residue is pulled out, and with a small amount of distilled water wash 2-5 time, and washings are merged in the hydrolyzed solution.Silkworm silk is dried to constant weight under 50-70 ℃ of temperature, and weighing silkworm silk deducts silkworm silk weight with husks shell original weight, can calculate the sericin quality of dissolving in the eluent.The sericin hydrolyzed solution is heated under 60-90 ℃ of temperature, is concentrated into the 1/4-1/2 of original volume, naturally cool to room temperature after, obtain the concentrated solution of sericin.Then in sericin bioactive peptide solution, add 95% ethanol with volume, fully mix 5-30 min, make sericin bioactive peptide flocculation sediment, sedimentation and filtration is collected, vacuum drying is crushed to the 100-200 order to constant weight, obtains being rich in the colourful silk glue protein of flavonoid and carotene constituents.
2. the making of Aloe vulgaris powder: get bright Aloe Barbadensis Miller and clean, remove the edge ratchet, cut base portion and top, with the juice extractor juice of squeezing out, remove the aloe fibre filament after filtering, collect and extract Aloe original juice, through 100 ℃ of sterilizations of high temperature 3-10 min.With Aloe original juice liquid spray dryer spray drying, the material that sprays just just is subject to high temperature and is to be heated moment when atomisation, component material is still kept its activity after drying, and dried polyoses grain is tiny evenly, is suitable for fully dissolving in the follow-up process for preparation product main body.The drying process with atomizing parameter is: 50 ℃-90 ℃ of inlet temperature, drying time 1.0-1.5S, peristaltic pump inlet amount 20-100ml/h, dry air flux 20-150m
3/ h, the fluid tip of ejector are 0.5-2.5mm, obtain the Aloe vulgaris powder finished product of uniform granularity.
3. the making of Rhizoma amorphophalli powder-xanthan gum composite membrane-forming powder body: the Rhizoma amorphophalli tuber is cleaned the rear section of peeling dry, tentatively be crushed to diameter 100 μ m-500 μ m granules, press Rhizoma amorphophalli powder and xanthan gum with the mass ratio adding xanthan gum dry product mix homogeneously of 18:2, further be crushed to the micropowders of 10 μ m-50 μ m.
4. above key component is fully mixed by following component with other helper component, both a kind of novel nourishing rehabilitation type facial treatment mask, its component batching side of matching well (%/w): Rhizoma amorphophalli powder-xanthan gum composite membrane-forming powder body 10-20, Aloe vulgaris powder 2.0-4.5, colourful silk glue protein 2.0-5.0, Vitamin E acetate mixture 0.5-2.0, glycerol 2.0-4.0, antiseptic methyl isothiazoline 0.1-0.6, Jojoba oil 1.0-2.5, essence 0.2-1.0, deionized water adds to 100.
Major advantage of the present invention is:
1. the protein material among the present invention is natural colorful silk glue protein, its molecular weight is 5000-20000, and traditional collagen molecules amount is all more than 300,000 dalton, therefore natural colorful silk glue protein is more suitable for being absorbed by the skin, and can make skin keep certain moisture, characteristic and skin moisture-keeping functions with stronger decomposition free radical activity, flavonoid wherein, carotene constituents etc. is not had by general collagen material especially, possess antibiotic, anti-ultraviolet, thereby suppressing TYR enzyme check melanin forms, the function of the health care such as antioxidation, but delaying skin is wrinkling aging.Therefore natural colorful silk glue protein substitutes the more multiple biological activity that has of traditional collagen protein in this product.
2. general silk glue protein extraction is to adopt the aqueous alkali extraction, and the sericin of acquisition is mingled with the inorganic base composition easily, and is unfavorable to skin.The present invention adopts the neutral protein enzymatic isolation method, has both guaranteed the safety of extract, makes again protein molecular obtain fully hydrolysis, has obviously improved the high efficiency of technique.
3. the main filmogen among the present invention is the complex of food stage xanthan gum and Rhizoma amorphophalli powder, has replaced expensive traditional hyaluronic acid, has both guaranteed filming performance, by having made cost nearly 10 times.Xanthan gum is a kind of good biological slow-released material, is conducive to the release of biological effective components and allows absorption of human body.Rhizoma amorphophalli powder contains abundant cellulose and trace element, also have 16 seed amino acids, main component konjak glucomannan (KGM) wherein is a kind of good dietary fiber, the characteristics such as good gelation, antibiotic property, film property are arranged, KGM and xanthan gum blend can form the good gel of film property later, the network size of this gel formation is released very suitable running micromolecule polypeptide and protide composition, and it is very beneficial that skin is absorbed plurality of active ingredients.
4. the Aloe powder in the product in the product of the present invention derives from Aloe Barbadensis Miller juice.The kind of Aloe has hundreds of, but has the kind of health care limited, and is the most typical with Aloe vulgaris.Aloe is widely used in cosmetics industry such as the multiple cosmetics such as protective skin cream, shampoo, bath foam and fancy soap at present, but uses very rare in mask product.Product of the present invention contains the Aloe vulgaris fine powder; multiple efficacies with a series of therapeutic efficiency and nourishes rough skin; to softening skin, preventing and treating acne, senile plaque, freckle, pachylosis and anti-inflammatory anti-itch, the delicate Bai Jie of protection skin etc. has remarkable efficacy.
The specific embodiment
A kind of preparation method of novel nourishing rehabilitation type facial treatment mask:
1, the husks cocoon shell of the chromatic cocoon that dries is pulverized is the fragment of 2mm size, then measure the distilled water of 50 times of quality of husks husk as raw material, the raw material fragment be impregnated in the aqueous solution, make its abundant swelling 40min, then under normal pressure, boil, make the sericin in the raw material partly be eluted in the solution, and to a certain degree hydrolysis, that stopped heating is cooled to room temperature when solution is concentrated into 1/6 of original volume.The neutral protease that adds husks shell 2.0% quality in solution carries out enzymolysis, and hydrolysis temperature is 25 ℃, and pH value is 7.0, continues enzymolysis 200min, makes the sericin in the solution be hydrolyzed to the active sericin that mean molecule quantity is 10000-20000Da.Then solution is heated to 100 ℃ and keeps 25min, enzyme denaturing is lived.Undissolvable silkworm silk residue is pulled out, and with a small amount of distilled water wash 3 times, and washings are merged in the hydrolyzed solution.Silkworm silk is dried to constant weight under 60 ℃ of temperature, and weighing silkworm silk deducts silkworm silk weight with cocoon husk as raw material weight, can calculate the sericin quality of dissolving in the eluent.The sericin hydrolyzed solution is heated under 80 ℃ of temperature, is concentrated into 1/3 of original volume, naturally cool to room temperature after, obtain the concentrated solution of sericin.Then in sericin bioactive peptide solution, add 95% ethanol with volume, fully mix 20 min, make the sericin flocculation sediment, sedimentation and filtration is collected, vacuum drying is crushed to 200 orders to constant weight, obtains being rich in the colourful silk glue protein of flavonoid and carotene constituents.
2, get bright Aloe Barbadensis Miller and clean, remove the edge ratchet, cut base portion and top, with the juice extractor juice of squeezing out, remove the aloe fibre filament after filtering, collect and extract Aloe original juice, through 100 ℃ of sterilizations of high temperature 5min.With Aloe original juice liquid spray dryer spray drying, the drying process with atomizing parameter is: 70 ℃ of inlet temperature, drying time 1.5S, peristaltic pump inlet amount 90ml/h, dry air flux 50m
3/ h, the fluid tip of ejector are 1.5mm, obtain the Aloe vulgaris powder finished product of uniform granularity.
3, the Rhizoma amorphophalli tuber being cleaned the rear section of peeling dries, tentatively be crushed to diameter 200 μ m granules, press Rhizoma amorphophalli powder and xanthan gum with the mass ratio adding xanthan gum dry product of 18:2, mix homogeneously, further be crushed to the micropowders of 30-40 μ m, namely get Rhizoma amorphophalli powder-xanthan gum composite membrane-forming powder body.
4. above key component is fully mixed by following charge ratio (%/w) with other helper component: Rhizoma amorphophalli powder-xanthan gum composite membrane-forming powder body 20, Aloe vulgaris powder 4.0, colourful silk glue protein 3.0, Vitamin E acetate mixture 1.0, glycerol 3.0, antiseptic methyl isothiazoline 0.3, Jojoba oil 1.5, essence 0.3, deionized water adds to 100, namely obtains a kind of novel nourishing rehabilitation type facial treatment mask.
Claims (1)
1. the preparation method of a novel nourishing rehabilitation type facial treatment mask is characterized in that:
1) extraction of colourful silk glue protein: husks, the cocoon shell of the chromatic cocoon that dries pulverized be the fragment of 1-3mm size, then measure raw materials quality 30-60 distilled water doubly, the raw material fragment be impregnated in the aqueous solution, make the abundant swelling 20-50min of husks shell, then under normal pressure, boil, make the sericin in cocoon one shell partly be eluted in the solution, and to a certain degree hydrolysis, when liquor capacity was concentrated into original 1/10-1/5, stopped heating was cooled to room temperature; The neutral protease that adds husks chitin amount 1.5-2.5% in solution carries out enzymolysis, hydrolysis temperature is 20-35 ℃, pH value is 6.8-7.7, continues enzymolysis 120-240min, makes the sericin in the solution be hydrolyzed to the active sericin that mean molecule quantity is 5000-20000Da; Then solution is heated to boiling and keeps 10-30min, enzyme denaturing is lived; Undissolvable silkworm silk residue is pulled out, and with a small amount of distilled water wash 2-5 time, and washings are merged in the hydrolyzed solution; Silkworm silk is dried to constant weight under 50-70 ℃ of temperature, and weighing silkworm silk deducts silkworm silk weight with husks shell original weight, can calculate the sericin quality of dissolving in the eluent; The sericin hydrolyzed solution is heated under 60-90 ℃ of temperature, is concentrated into the 1/4-1/2 of original volume, naturally cool to room temperature after, obtain the concentrated solution of sericin; Then in sericin bioactive peptide solution, add 95% ethanol with volume, fully mix 5-30 min, make sericin bioactive peptide flocculation sediment, sedimentation and filtration is collected, vacuum drying is crushed to the 100-200 order to constant weight, obtains being rich in the colourful silk glue protein of flavonoid and carotene constituents;
2) making of Aloe vulgaris powder: get bright Aloe Barbadensis Miller and clean, remove the edge ratchet, cut base portion and top, with the juice extractor juice of squeezing out, remove the aloe fibre filament after filtering, collect and extract Aloe original juice, through 100 ℃ of sterilizations of high temperature 3-10 min; With Aloe original juice liquid spray dryer spray drying, the material that sprays just just is subject to high temperature and is to be heated moment when atomisation, component material is still kept its activity after drying, and dried polyoses grain is tiny evenly, is suitable for fully dissolving in the follow-up process for preparation product main body; The drying process with atomizing parameter is: 50 ℃-90 ℃ of inlet temperature, drying time 1.0-1.5S, peristaltic pump charging 20-100ml/h, dry air flux 20-150m
3/ h, the fluid tip of ejector are 0.5-2.5mm, obtain the Aloe vulgaris powder finished product of uniform granularity;
3) making of Rhizoma amorphophalli powder-xanthan gum composite membrane-forming powder body: the Rhizoma amorphophalli tuber is cleaned the rear section of peeling dry, tentatively be crushed to diameter 100 μ m-500 μ m granules, press Rhizoma amorphophalli powder and xanthan gum with the mass ratio adding xanthan gum dry product mix homogeneously of 18:2, further be crushed to the micropowders of 10 μ m-50 μ m;
4) above key component is fully mixed by following component with other helper component, both a kind of novel nourishing rehabilitation type facial treatment mask, its component batching side of matching well (%/w): Rhizoma amorphophalli powder-xanthan gum composite membrane-forming powder body 10-20, Aloe vulgaris powder 2.0-4.5, colourful silk glue protein 2.0-5.0, Vitamin E acetate mixture 0.5-2.0, glycerol 2.0-4.0, antiseptic methyl isothiazoline 0.1-0.6, Jojoba oil 1.0-2.5, essence 0.2-1.0, deionized water adds to 100.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104825349A (en) * | 2015-04-21 | 2015-08-12 | 浙江大学湖州市南太湖现代农业科技推广中心 | Method for producing kin care gel application agent from biomass raw material |
| CN104873425A (en) * | 2015-05-22 | 2015-09-02 | 周维新 | After-sun repair mask capsule |
| CN106074315A (en) * | 2016-08-24 | 2016-11-09 | 广东芭薇生物科技股份有限公司 | A kind of facial mask liquid with multiple skin-care effect and preparation method thereof |
| CN109276457A (en) * | 2018-11-28 | 2019-01-29 | 大连美图生物科技有限公司 | It is a kind of to contain the facial mask film cloth and preparation method thereof for solidifying essence |
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| CN1228438A (en) * | 1998-12-01 | 1999-09-15 | 浙江丝绸工学院 | Sericin polypeptide extracted from frison, husks and waste silk and its extracting method |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104825349A (en) * | 2015-04-21 | 2015-08-12 | 浙江大学湖州市南太湖现代农业科技推广中心 | Method for producing kin care gel application agent from biomass raw material |
| CN104873425A (en) * | 2015-05-22 | 2015-09-02 | 周维新 | After-sun repair mask capsule |
| CN106074315A (en) * | 2016-08-24 | 2016-11-09 | 广东芭薇生物科技股份有限公司 | A kind of facial mask liquid with multiple skin-care effect and preparation method thereof |
| CN109276457A (en) * | 2018-11-28 | 2019-01-29 | 大连美图生物科技有限公司 | It is a kind of to contain the facial mask film cloth and preparation method thereof for solidifying essence |
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Application publication date: 20130403 |