CN102964324A - 含4-四氢吡喃结构的液晶化合物及其组合物和应用 - Google Patents
含4-四氢吡喃结构的液晶化合物及其组合物和应用 Download PDFInfo
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- CN102964324A CN102964324A CN201210387567XA CN201210387567A CN102964324A CN 102964324 A CN102964324 A CN 102964324A CN 201210387567X A CN201210387567X A CN 201210387567XA CN 201210387567 A CN201210387567 A CN 201210387567A CN 102964324 A CN102964324 A CN 102964324A
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- Prior art keywords
- oco
- liquid crystal
- nitrae
- isosorbide
- compound
- Prior art date
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- 239000004973 liquid crystal related substance Substances 0.000 title claims abstract description 46
- 150000001875 compounds Chemical class 0.000 title claims abstract description 43
- 239000000203 mixture Substances 0.000 title claims abstract description 21
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 11
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical group [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000001301 oxygen Substances 0.000 claims abstract description 7
- 239000007788 liquid Substances 0.000 claims description 23
- 125000000217 alkyl group Chemical group 0.000 claims description 15
- 229910052801 chlorine Inorganic materials 0.000 claims description 10
- 229910052731 fluorine Inorganic materials 0.000 claims description 10
- 229910052799 carbon Inorganic materials 0.000 claims description 8
- 150000001721 carbon Chemical group 0.000 claims description 8
- 125000002769 thiazolinyl group Chemical group 0.000 claims description 8
- 125000003545 alkoxy group Chemical group 0.000 claims description 7
- 150000001336 alkenes Chemical class 0.000 claims description 6
- 229910052736 halogen Inorganic materials 0.000 claims description 4
- 150000002367 halogens Chemical class 0.000 claims description 4
- 229910052739 hydrogen Inorganic materials 0.000 claims description 4
- 229910052717 sulfur Inorganic materials 0.000 claims description 4
- 125000003342 alkenyl group Chemical group 0.000 claims description 2
- 125000002347 octyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 2
- 230000003287 optical effect Effects 0.000 abstract description 9
- 238000009776 industrial production Methods 0.000 abstract description 2
- 238000002360 preparation method Methods 0.000 abstract description 2
- 239000002994 raw material Substances 0.000 abstract description 2
- 238000000926 separation method Methods 0.000 abstract 1
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 22
- 238000006243 chemical reaction Methods 0.000 description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 13
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 11
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 9
- 239000012044 organic layer Substances 0.000 description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 6
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 6
- 238000001035 drying Methods 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 238000001953 recrystallisation Methods 0.000 description 6
- 238000010025 steaming Methods 0.000 description 6
- MZRVEZGGRBJDDB-UHFFFAOYSA-N N-Butyllithium Chemical compound [Li]CCCC MZRVEZGGRBJDDB-UHFFFAOYSA-N 0.000 description 4
- 238000010992 reflux Methods 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 3
- 239000004974 Thermotropic liquid crystal Substances 0.000 description 3
- 235000019441 ethanol Nutrition 0.000 description 3
- 238000003810 ethyl acetate extraction Methods 0.000 description 3
- 238000001914 filtration Methods 0.000 description 3
- 238000005984 hydrogenation reaction Methods 0.000 description 3
- UKVIEHSSVKSQBA-UHFFFAOYSA-N methane;palladium Chemical compound C.[Pd] UKVIEHSSVKSQBA-UHFFFAOYSA-N 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- 238000011056 performance test Methods 0.000 description 3
- -1 separatory Substances 0.000 description 3
- JOXIMZWYDAKGHI-UHFFFAOYSA-N toluene-4-sulfonic acid Chemical compound CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 description 3
- ZPSJGADGUYYRKE-UHFFFAOYSA-N 2H-pyran-2-one Chemical compound O=C1C=CC=CO1 ZPSJGADGUYYRKE-UHFFFAOYSA-N 0.000 description 2
- 239000004990 Smectic liquid crystal Substances 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 239000000758 substrate Substances 0.000 description 2
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 1
- 239000004991 Lytropic liquid crystal Substances 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 239000004988 Nematic liquid crystal Substances 0.000 description 1
- 230000018199 S phase Effects 0.000 description 1
- 239000008186 active pharmaceutical agent Substances 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 238000012512 characterization method Methods 0.000 description 1
- 230000003098 cholesteric effect Effects 0.000 description 1
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol group Chemical group [C@@H]1(CC[C@H]2[C@@H]3CC=C4C[C@@H](O)CC[C@]4(C)[C@H]3CC[C@]12C)[C@H](C)CCCC(C)C HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 1
- 210000002858 crystal cell Anatomy 0.000 description 1
- 125000004093 cyano group Chemical group *C#N 0.000 description 1
- 125000000113 cyclohexyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 description 1
- 238000013213 extrapolation Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 125000000623 heterocyclic group Chemical group 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 229910052740 iodine Inorganic materials 0.000 description 1
- 239000011630 iodine Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- JMJRYTGVHCAYCT-UHFFFAOYSA-N oxan-4-one Chemical compound O=C1CCOCC1 JMJRYTGVHCAYCT-UHFFFAOYSA-N 0.000 description 1
- 125000004430 oxygen atom Chemical group O* 0.000 description 1
- 125000000843 phenylene group Chemical group C1(=C(C=CC=C1)*)* 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 238000010572 single replacement reaction Methods 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
Landscapes
- Liquid Crystal Substances (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Description
Claims (10)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201210387567.XA CN102964324B (zh) | 2012-10-13 | 2012-10-13 | 含4-四氢吡喃结构的液晶化合物及其组合物和应用 |
Applications Claiming Priority (1)
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CN201210387567.XA CN102964324B (zh) | 2012-10-13 | 2012-10-13 | 含4-四氢吡喃结构的液晶化合物及其组合物和应用 |
Publications (2)
Publication Number | Publication Date |
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CN102964324A true CN102964324A (zh) | 2013-03-13 |
CN102964324B CN102964324B (zh) | 2016-02-17 |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106543178A (zh) * | 2015-09-16 | 2017-03-29 | 阜阳欣奕华材料科技有限公司 | 一种化合物、液晶组合物及液晶显示器 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1806028A (zh) * | 2003-05-27 | 2006-07-19 | 默克专利股份有限公司 | 含有四氢吡喃环的液晶化合物 |
CN100509792C (zh) * | 2002-11-27 | 2009-07-08 | 默克专利股份有限公司 | 四氢吡喃衍生物 |
US20100059710A1 (en) * | 2008-09-11 | 2010-03-11 | Bum-Gyu Choi | Novel pyran derivative, its preparation method, liquid crystal composition and liquid crystal display device comprising the same |
CN101868439A (zh) * | 2007-09-06 | 2010-10-20 | 智索株式会社 | 具有侧向氟的4、5环液晶性化合物、液晶组成物以及液晶显示元件 |
TW201113353A (en) * | 2009-08-19 | 2011-04-16 | Chisso Corp | Tetrahydropyran compound, liquid crystal composition and liquid crystal display device |
-
2012
- 2012-10-13 CN CN201210387567.XA patent/CN102964324B/zh active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100509792C (zh) * | 2002-11-27 | 2009-07-08 | 默克专利股份有限公司 | 四氢吡喃衍生物 |
CN1806028A (zh) * | 2003-05-27 | 2006-07-19 | 默克专利股份有限公司 | 含有四氢吡喃环的液晶化合物 |
CN101868439A (zh) * | 2007-09-06 | 2010-10-20 | 智索株式会社 | 具有侧向氟的4、5环液晶性化合物、液晶组成物以及液晶显示元件 |
US20100059710A1 (en) * | 2008-09-11 | 2010-03-11 | Bum-Gyu Choi | Novel pyran derivative, its preparation method, liquid crystal composition and liquid crystal display device comprising the same |
TW201113353A (en) * | 2009-08-19 | 2011-04-16 | Chisso Corp | Tetrahydropyran compound, liquid crystal composition and liquid crystal display device |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106543178A (zh) * | 2015-09-16 | 2017-03-29 | 阜阳欣奕华材料科技有限公司 | 一种化合物、液晶组合物及液晶显示器 |
CN106543178B (zh) * | 2015-09-16 | 2019-01-04 | 阜阳欣奕华材料科技有限公司 | 一种化合物、液晶组合物及液晶显示器 |
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CN102964324B (zh) | 2016-02-17 |
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Address after: 212212 Yangtze River bridge, Jiangsu, Yangzhong, Yangzhong on the eastern side of the road Patentee after: JIANGSU HECHENG DISPLAY TECHNOLOGY Co.,Ltd. Address before: 212212 Yangtze River bridge, Jiangsu, Yangzhong, Yangzhong on the eastern side of the road Patentee before: Jiangsu Hecheng Display Technology Co.,Ltd. |
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Effective date of registration: 20200428 Address after: No. 9, camphor Road, economic development zone, Daguan District, Anqing, Anhui Patentee after: ANQING FEIKAI NEW MATERIAL Co.,Ltd. Address before: 212212 Jiangsu, Zhenjiang, Yangzhong, Yangzhong, Yangtze River bridge on the east side Patentee before: JIANGSU HECHENG DISPLAY TECHNOLOGY Co.,Ltd. |
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Effective date of registration: 20210708 Address after: Room 711, Building 2, Courtyard 1, Jinhang Middle Road, Shunyi District, Beijing 101300 Patentee after: Beijing culture science and technology finance leasing Limited by Share Ltd. Address before: 246000 No. 9, Xiang Zhang Road, Daguan District Economic Development Zone, Anqing, Anhui Patentee before: ANQING FEIKAI NEW MATERIAL Co.,Ltd. |
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Effective date of registration: 20230417 Address after: 246000 No. 9, Xiang Zhang Road, Daguan District Economic Development Zone, Anqing, Anhui Patentee after: ANQING FEIKAI NEW MATERIAL Co.,Ltd. Address before: Room 711, Building 2, Courtyard 1, Jinhang Middle Road, Shunyi District, Beijing 101300 Patentee before: Beijing culture science and technology finance leasing Limited by Share Ltd. |