CN102899167B - Tobacco flavor with uniform and stable fragrance and preparation method thereof - Google Patents
Tobacco flavor with uniform and stable fragrance and preparation method thereof Download PDFInfo
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- CN102899167B CN102899167B CN201210387797.6A CN201210387797A CN102899167B CN 102899167 B CN102899167 B CN 102899167B CN 201210387797 A CN201210387797 A CN 201210387797A CN 102899167 B CN102899167 B CN 102899167B
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- angelicae sinensis
- dwarf lilyturf
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Abstract
The invention discloses a tobacco flavor with uniform and stable and a preparation method thereof. The tobacco flavor is an extract with a relative density of 1.02 to 1.20 which is extracted by 60-95 mass percent ethanol from a mixture, wherein the mixture comprises red date, Chinese angelica and dwarf lilyturf tuber in a weight ratio of 0.2-30.0:0.5-20.0:0.5-30.0. The tobacco flavor can degrade cigarette tar. When combined with natural tobacco plant fragrance, the tobacco flavor makes cigarettes fresh, elegant, sweet, pure, mild, light, transparent and thus greatly enhances the quality of cigarettes. The invention also discloses a method for preparing the tobacco flavor. The method can make a uniform, stable and sweet liquid flavor additive without impurities, and the content of the fragrance source component of the tobacco flavor is over 80%.
Description
Technical field
The present invention relates to tobacco additive agent technical field, refer to particularly tobacco aromatics using that a kind of fragrance is even, stable and preparation method thereof.
Background technology
Along with Harm reduction techniques being fallen to deepening continuously and the continuous lifting of country to flue gas quality index control accuracy of burnt technical study, at present, tobacco industry has been determined based on keeping and developing the Thoughts that Chinese-style cigarette suction taste feature is carried out fundamental research and applied research, and has been classified < < essence and flavoring agent Core Technology Research > > one of as following cigarette science and technology four large problems in essence spice for cigarette research.Within 2005, this project starts smoothly, to making a breakthrough from three aspects: the one, basic, Research on Regularity; The 2nd, the breakthrough of essence and flavoring agent utilisation technology; The 3rd, the exploration in flavoring and casing mode.Chinese-style cigarette core competitiveness is to form selling point style, embodies personalization and the differentiation of " Chinese-style cigarette ", adapts to sucking of consumers in general and is accustomed to and consumer need.Using domestic tobacco leaf as raw material basis, keep and development Chinese style flue-cured tobacco tabacco fragrance feature, further form significantly strong " Chinese-style cigarette " flue gas style simultaneously.Flavoring and casing scientifically in cigarette, the just important means of the personalized style of outstanding cigarette product.
Blending technology is the core of essence and flavoring agent technology, and it combines multiple perfume material according to certain ratio and compatibility, thereby reaches specific fragrance characteristic and functional effect, can significantly improve cigarette odor-absorbing, and gives the specific style of cigarette grace.And the security of raising smoking, other objectionable constituent that reduce in tar content and flue gas are important directions for Chinese-style cigarette research.Yet the many fragrance matters in tobacco are but present among tar, are accompanied by the reduction of tar content, and smoke is thin out, fragrance reduces, and cigarette product keeps not losing original style, just more can be accepted by human consumer.Therefore, when reducing coke tar in cigarette, flavouring and improve flue gas concentration and fragrance, thus improve the inner quality of Chinese-style cigarette product, also only by means of the scientific and technological content of flavoring and casing technology.
Summary of the invention
The object of the invention is to overcome existing spices easily because of the reduction of tar in cigarettes amount, and fragrance is reduced, the defect losing its relish, provides even, stable tobacco aromatics using of a kind of fragrance and preparation method thereof.
For achieving the above object, even, the stable tobacco aromatics using of fragrance that the present invention is designed, the extract that the prepared relative density of extraction using alcohol mixing raw material that it is is 60% ~ 95% via mass ratio is 1.02 ~ 1.20, described mixing raw material comprises red date, Radix Angelicae Sinensis, the tuber of dwarf lilyturf, and wherein red date, Radix Angelicae Sinensis, the weight ratio between the tuber of dwarf lilyturf are: 0.2 ~ 30.0:0.5 ~ 20.0:0.5 ~ 30.0.
In described mixing raw material, red date, Radix Angelicae Sinensis, the weight ratio between the tuber of dwarf lilyturf are preferably: 10.0 ~ 30.0:7.0 ~ 15.0:5 ~ 25.0.
In described mixing raw material, also comprise auxiliary material, the weight ratio between red date, Radix Angelicae Sinensis, the tuber of dwarf lilyturf and auxiliary material is: 0.2 ~ 30.0:0.5 ~ 20.0:0.5 ~ 30.0:0.1 ~ 10.0, are preferably 10.0 ~ 30.0:7.0 ~ 15.0:5 ~ 25.0:0.5 ~ 3.0; Described auxiliary material is selected from a kind of in eight treasures (choice ingredients of certain special dishes) red-spotted stonecrop, Root of Indigowoad, the Radix Astragali, Radix Codonopsis, ginseng palpus, Radix Glycyrrhizae, Grosvenor Momordica.
Preferred mixing raw material proportioning is: red date, Radix Angelicae Sinensis, the tuber of dwarf lilyturf and eight treasures (choice ingredients of certain special dishes) red-spotted stonecrop, its weight ratio is: 1.0:1.5:2.0:3.0.
The present invention also provides the preparation method of even, the stable tobacco aromatics using of a kind of fragrance, the steps include:
1) the alcohol solution dipping mixing raw material that is 60% ~ 95% by mass ratio 15 ~ 30 days;
2) by the liquid of extruding in the ethanolic soln of immersion mixing raw material and mixing raw material in the lump suction filtration, obtain ethanol extract;
3) ethanol extract is passed through to fractionation by distillation ethanol, the described tobacco aromatics using that acquisition relative density is 1.02 ~ 1.20;
Wherein, described mixing raw material comprises red date, Radix Angelicae Sinensis, the tuber of dwarf lilyturf, and red date, Radix Angelicae Sinensis, the weight ratio between the tuber of dwarf lilyturf are: 0.2 ~ 30.0:0.5 ~ 20.0:0.5 ~ 30.0, are preferably 10.0 ~ 30.0:7.0 ~ 15.0:5 ~ 25.0.
Wherein, in described step 1), the weight ratio of ethanolic soln and mixing raw material is 1:2 ~ 10.
In described mixing raw material, also comprise auxiliary material, the weight ratio between red date, Radix Angelicae Sinensis, the tuber of dwarf lilyturf and auxiliary material is: 0.2 ~ 30.0:0.5 ~ 20.0:0.5 ~ 30.0:0.1 ~ 10.0, are preferably 10.0 ~ 30.0:7.0 ~ 15.0:5 ~ 25.0:0.5 ~ 3.0; Described auxiliary material is selected from a kind of in eight treasures (choice ingredients of certain special dishes) red-spotted stonecrop, Root of Indigowoad, the Radix Astragali, Radix Codonopsis, ginseng palpus, Radix Glycyrrhizae, Grosvenor Momordica.
Preferred mixing raw material proportioning is: red date, Radix Angelicae Sinensis, the tuber of dwarf lilyturf and eight treasures (choice ingredients of certain special dishes) red-spotted stonecrop, its weight ratio is: 1.0:1.5:2.0:3.0.
In the mixing raw material of tobacco aromatics using of the present invention, the main effect of each composition is as follows:
(1) red date (Ziziphus jujubaMill) is a kind of dungarunga that is grown in Temperate Region in China, originates in China, in various places, Chinese north and south, has distribution.Spending little how honey, is a kind of nectariferous plant; Pattern is faint yellow, has fragrant breath.Fruit is jujube, and ellipse is yellow during prematurity, ripe rear maroon.Can eat raw and also can be made into dry fruit or preserved fruit etc.Nutritious, be rich in ferro element and VITAMIN.Contain a large amount of glucides, be mainly glucose, also contain fructose, sucrose, and the oligose being formed by glucose and fructose, arabinan and galacturonan etc.; And contain the multivitamins such as a large amount of vitamins Cs, riboflavin, VitB1, carotene, nicotinic acid, and there is stronger tonic effect, can improve immune function of human body, strengthen resistance against diseases.
(2) Radix Angelicae Sinensis (Angelica sinensis) per nnial herb, at distribution in China in Gansu, the ground such as Yunnan, Sichuan, Qinghai, Shaanxi, Hunan, Hubei, Guizhou, all there is cultivation various places.Sweet, the micro-hardship of Radix Angelicae Sinensis taste, numb feeling in the tongue slightly, with main root slightly long, supporting root is few, glossy, section yellow-white, the person of giving off a strong fragrance be for well.Radix Angelicae Sinensis is generally divided into Radix Angelicae Sinensis body (containing Radix Angelicae Sinensis) and Radix Angelicae Sinensis, and multiplex Radix Angelicae Sinensis, contains multiple organic composition and the trace elements such as a large amount of volatile oil, VITAMIN, organic acid, experimental study shows, Radix Angelicae Sinensis can be expanded peripheral blood vessel, reduces vascular resistance, increases circulating liquid measure etc.
(3) having another name called dwarf lilyturf, book band grass, Radix Ophiopogonis the tuber of dwarf lilyturf (Ophitopogin japonicum (L.f) Ker.-Gawl.), is Liliaceae Ophiopogon perennial evergreen herbaceous plant.Fibrous root is more sturdy, and often expand at the top of root or middle part becomes spindle shape meat fritter.Surface yellow-white or light yellowish-white, has thin longitudinal grin.Matter is pliable and tough, section yellow-white, and translucent, center pillar is tiny.The micro-perfume (or spice) of gas, sweet, the micro-hardship of taste.Sweet cold clear and rich, the heat of the kind lung that clears away heart-fire and yin-nourishing relieving restlessness, holding concurrently can clear and rich stomach and intestine and quench the thirst and moisturize.
Beneficial effect of the present invention: the tobacco aromatics using degradable cigarette coke tar providing, this perfume of tobacco and natural herbal plant natural combination, simple and elegant and Tianjin is sweet, alcohol and extremely, fragrance is elegant, and the property sent out is good thoroughly, has enriched the fragrance of cigarette, has greatly promoted the quality of cigarette.The natural herbal plant with nourishing function is added in cigarette product after concentrating through reasonable compatibility, extraction, there is remarkable increase cigarette flavor amount, promote cigarette rhythm, set off nature cigarette perfume, reduce the sense of promoting the production of body fluid of flue gas drying sense, enhancing flue gas Hui Tian, the effect of raising cigarette comfort level, effectively remove cigarette foreign gas, improve and modification fragrance, make flue gas soft, fragrance is fine and smooth, the obvious improved texts of flue gas quality.The present invention also provides the preparation method of above-mentioned tobacco aromatics using, can make even, stable, fragrant and sweet liquid perfume additive, has removed impurity, forms the crucial aroma component relative content of its odour characteristics more than 80%.
Embodiment
Below in conjunction with specific embodiment, the present invention is described in further detail.
Embodiment 1
Getting red date, Radix Angelicae Sinensis, the tuber of dwarf lilyturf is 30.0:20.0:0.5 preparation mixing raw material by weight, and mixing raw material is prepared tobacco aromatics using in the steps below:
1) the alcohol solution dipping mixing raw material that is 75% by mass ratio 15 days, the weight ratio of ethanolic soln and mixing raw material is 1:5;
2) by the liquid of extruding in the ethanolic soln of immersion mixing raw material and mixing raw material in the lump suction filtration, obtain ethanol extract, suction filtration can adopt qualitative filter paper suction filtration, to obtain clear filtrate;
3) ethanol extract is passed through to fractionation by distillation ethanol, obtain tobacco aromatics using.
The tobacco aromatics using of making adds in blank cigarette and please comment cigarette expert to smoke panel test by 0.5% of pipe tobacco weight, the results are shown in Table 1.
Embodiment 2
Get red date, Radix Angelicae Sinensis, the tuber of dwarf lilyturf, ginseng palpus by weight being 0.2:20.0:30.0:10.0 preparation mixing raw material, mixing raw material is prepared tobacco aromatics using in the steps below:
1) the alcohol solution dipping mixing raw material that is 60% by mass ratio 25 days, the weight ratio of ethanolic soln and mixing raw material is 1:2;
2) by the liquid of extruding in the ethanolic soln of immersion mixing raw material and mixing raw material in the lump suction filtration, obtain ethanol extract, suction filtration can adopt qualitative filter paper suction filtration, to obtain clear filtrate;
3) ethanol extract is passed through to fractionation by distillation ethanol, obtain tobacco aromatics using.
The tobacco aromatics using of making adds in blank cigarette and please comment cigarette expert to smoke panel test by 0.8% of pipe tobacco weight, the results are shown in Table 1.
Embodiment 3
Get red date, Radix Angelicae Sinensis, the tuber of dwarf lilyturf, Grosvenor Momordica by weight being 20.0:10.0:1.0:1.0 preparation mixing raw material, mixing raw material is prepared tobacco aromatics using in the steps below:
1) the alcohol solution dipping mixing raw material that is 65% by mass ratio 15 days, the weight ratio of ethanolic soln and mixing raw material is 1:10;
2) by the liquid of extruding in the ethanolic soln of immersion mixing raw material and mixing raw material in the lump suction filtration, obtain ethanol extract, suction filtration can adopt qualitative filter paper suction filtration, to obtain clear filtrate;
3) ethanol extract is passed through to fractionation by distillation ethanol, obtain tobacco aromatics using.
The tobacco aromatics using of making adds in blank cigarette and please comment cigarette expert to smoke panel test by 0.7% of pipe tobacco weight, the results are shown in Table 1.
Embodiment 4
Get red date, Radix Angelicae Sinensis, the tuber of dwarf lilyturf, Radix Glycyrrhizae by weight being 10.0:2.0:3.0:5.0 preparation mixing raw material, mixing raw material is prepared tobacco aromatics using in the steps below:
1) the alcohol solution dipping mixing raw material that is 85% by mass ratio 30 days, the weight ratio of ethanolic soln and mixing raw material is 1:7;
2) by the liquid of extruding in the ethanolic soln of immersion mixing raw material and mixing raw material in the lump suction filtration, obtain ethanol extract, suction filtration can adopt qualitative filter paper suction filtration, to obtain clear filtrate;
3) ethanol extract is passed through to fractionation by distillation ethanol, obtain tobacco aromatics using.
The tobacco aromatics using of making adds in blank cigarette and please comment cigarette expert to smoke panel test by 0.7% of pipe tobacco weight, the results are shown in Table 1.
Embodiment 5
Get red date, Radix Angelicae Sinensis, the tuber of dwarf lilyturf, the Radix Astragali by weight being 1.0:0.5:10.0:10.0 preparation mixing raw material, mixing raw material is prepared tobacco aromatics using in the steps below:
1) the alcohol solution dipping mixing raw material that is 80% by mass ratio 25 days, the weight ratio of ethanolic soln and mixing raw material is 1:3;
2) by the liquid of extruding in the ethanolic soln of immersion mixing raw material and mixing raw material in the lump suction filtration, obtain ethanol extract, suction filtration can adopt qualitative filter paper suction filtration, to obtain clear filtrate;
3) ethanol extract is passed through to fractionation by distillation ethanol, obtain tobacco aromatics using.
The tobacco aromatics using of making adds in white cigarette and please comment cigarette expert to smoke panel test by 0.5% of pipe tobacco weight, the results are shown in Table 1.
Embodiment 6
Get red date, Radix Angelicae Sinensis, the tuber of dwarf lilyturf, Radix Codonopsis by weight being 3.0:20.0:15.0:4.0 preparation mixing raw material, mixing raw material is prepared tobacco aromatics using in the steps below:
1) the alcohol solution dipping mixing raw material that is 90% by mass ratio 30 days, the weight ratio of ethanolic soln and mixing raw material is 1:6;
2) by the liquid of extruding in the ethanolic soln of immersion mixing raw material and mixing raw material in the lump suction filtration, obtain ethanol extract, suction filtration can adopt qualitative filter paper suction filtration, to obtain clear filtrate;
3) ethanol extract is passed through to fractionation by distillation ethanol, obtain tobacco aromatics using.
The tobacco aromatics using of making adds in blank cigarette and please comment cigarette expert to smoke panel test by 0.5% of pipe tobacco weight, the results are shown in Table 1.
Embodiment 7
Get red date, Radix Angelicae Sinensis, the tuber of dwarf lilyturf, Root of Indigowoad by weight being 25.0:11.0:25.0:0.1 preparation mixing raw material, mixing raw material is prepared tobacco aromatics using in the steps below:
1) the alcohol solution dipping mixing raw material that is 95% by mass ratio 15 days, the weight ratio of ethanolic soln and mixing raw material is 1:8;
2) by the liquid of extruding in the ethanolic soln of immersion mixing raw material and mixing raw material in the lump suction filtration, obtain ethanol extract, suction filtration can adopt qualitative filter paper suction filtration, to obtain clear filtrate;
3) ethanol extract is passed through to fractionation by distillation ethanol, obtain tobacco aromatics using.
The tobacco aromatics using of making adds in blank cigarette and please comment cigarette expert to smoke panel test by 0.8% of pipe tobacco weight, the results are shown in Table 1.
Embodiment 8
Get red date, Radix Angelicae Sinensis, the tuber of dwarf lilyturf, eight treasures (choice ingredients of certain special dishes) red-spotted stonecrop by weight being 1.0:1.5:2.0:3.0 preparation mixing raw material, mixing raw material is prepared tobacco aromatics using in the steps below:
1) the alcohol solution dipping mixing raw material that is 75% by mass ratio 20 days, the weight ratio of ethanolic soln and mixing raw material is 1:4;
2) by the liquid of extruding in the ethanolic soln of immersion mixing raw material and mixing raw material in the lump suction filtration, obtain ethanol extract, suction filtration can adopt qualitative filter paper suction filtration, to obtain clear filtrate;
3) ethanol extract is passed through to fractionation by distillation ethanol, obtain tobacco aromatics using.
The tobacco aromatics using of making adds in blank cigarette and please comment cigarette expert to smoke panel test by 0.8% of pipe tobacco weight, the results are shown in Table 1.
Table 1 smoking result
| embodiment | smoking result |
| 1 | obviously improve mouthfeel, pleasant impression is comfortable, alcohol and flue gas. |
| 2 | significantly increase flue gas concentration, cover assorted gas, make the soft exquisiteness of flue gas. |
| 3 | obviously increase flue gas concentration, cover assorted gas, flue gas elegance is comfortable. |
| 4 | significantly improve flue gas concentration, strengthened fragrant and sweet breath, the property sent out is strong thoroughly. |
| 5 | obviously improve cigarette flavor, oral cavity is comfortable clean, and cigarette is fragrant to be coordinated. |
| 6 | obviously increase flue gas concentration, flue gas is fine and smooth, and soft, pleasant impression is comfortable. |
| 7 | significantly increase flue gas concentration, improve mouthfeel, pleasant impression is comfortable. |
| 8 | obviously improve cigarette flavor, flue gas is elegant, obviously improves cigarette quality. |
Claims (7)
1. the tobacco aromatics using that fragrance is even, stable, it is characterized in that: the extract that the prepared relative density of extraction using alcohol mixing raw material that it is is 60%～95% via mass ratio is 1.02～1.20, described mixing raw material is comprised of red date, Radix Angelicae Sinensis, the tuber of dwarf lilyturf and auxiliary material, and the weight ratio between red date, Radix Angelicae Sinensis, the tuber of dwarf lilyturf and auxiliary material is: 0.2～30.0:0.5～20.0:0.5～30.0:0.1～10.0; Described auxiliary material is selected from a kind of in eight treasures (choice ingredients of certain special dishes) red-spotted stonecrop, Root of Indigowoad, the Radix Astragali, Radix Codonopsis, ginseng palpus, Radix Glycyrrhizae, Grosvenor Momordica.
2. even, the stable tobacco aromatics using of fragrance according to claim 1, is characterized in that: the weight ratio between described red date, Radix Angelicae Sinensis, the tuber of dwarf lilyturf and auxiliary material is: 10.0～30.0:7.0～15.0:5～25.0:0.5～3.0.
3. even, the stable tobacco aromatics using of fragrance according to claim 1, it is characterized in that: described auxiliary material is eight treasures (choice ingredients of certain special dishes) red-spotted stonecrop, and the weight ratio between described red date, Radix Angelicae Sinensis, the tuber of dwarf lilyturf and eight treasures (choice ingredients of certain special dishes) red-spotted stonecrop is: 1.0:1.5:2.0:3.0.
4. a preparation method for even, the stable tobacco aromatics using of fragrance, the steps include:
1) the alcohol solution dipping mixing raw material that is 60%～95% by mass ratio 15～30 days;
2) by the liquid of extruding in the ethanolic soln of immersion mixing raw material and mixing raw material in the lump suction filtration, obtain ethanol extract;
3) ethanol extract is passed through to fractionation by distillation ethanol, the described tobacco aromatics using that acquisition relative density is 1.02～1.20;
Wherein, described mixing raw material is comprised of red date, Radix Angelicae Sinensis, the tuber of dwarf lilyturf and auxiliary material, and the weight ratio between red date, Radix Angelicae Sinensis, the tuber of dwarf lilyturf and auxiliary material is: 0.2～30.0:0.5～20.0:0.5～30.0:0.1～10.0; Described auxiliary material is selected from a kind of in eight treasures (choice ingredients of certain special dishes) red-spotted stonecrop, Root of Indigowoad, the Radix Astragali, Radix Codonopsis, ginseng palpus, Radix Glycyrrhizae, Grosvenor Momordica.
5. the preparation method of even, the stable tobacco aromatics using of fragrance according to claim 4, is characterized in that: in described step 1), the weight ratio of ethanolic soln and mixing raw material is 1:2～10.
6. the preparation method of even, the stable tobacco aromatics using of fragrance according to claim 4, is characterized in that: the weight ratio between described red date, Radix Angelicae Sinensis, the tuber of dwarf lilyturf and auxiliary material is: 10.0～30.0:7.0～15.0:5～25.0:0.5～3.0.
7. the preparation method of even, the stable tobacco aromatics using of fragrance according to claim 4, it is characterized in that: described auxiliary material is eight treasures (choice ingredients of certain special dishes) red-spotted stonecrop, and the weight ratio between described red date, Radix Angelicae Sinensis, the tuber of dwarf lilyturf and eight treasures (choice ingredients of certain special dishes) red-spotted stonecrop is: 1.0:1.5:2.0:3.0.
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| CN106753790A (en) * | 2016-12-05 | 2017-05-31 | 湖北中烟工业有限责任公司 | Uniform, stable tobacco aromaticss of fragrance and preparation method thereof |
| CN107510090B (en) * | 2017-08-16 | 2019-03-19 | 湖北中烟工业有限责任公司 | A kind of preparation method and applications for the additive inhibiting burley tobaccos bitter taste |
| CN108813528A (en) * | 2018-04-28 | 2018-11-16 | 深圳市大百汇技术有限公司 | Food additives and preparation method thereof and cigarette |
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