CN102876238B - High-performance nutritious waterproof shoe cream and preparation method thereof - Google Patents
High-performance nutritious waterproof shoe cream and preparation method thereof Download PDFInfo
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- CN102876238B CN102876238B CN201210344732.3A CN201210344732A CN102876238B CN 102876238 B CN102876238 B CN 102876238B CN 201210344732 A CN201210344732 A CN 201210344732A CN 102876238 B CN102876238 B CN 102876238B
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Abstract
The invention discloses high-performance nutritious waterproof shoe cream and a preparation method thereof. The high-performance nutritious waterproof shoe cream is prepared from surfactant, oleic acid, an animal fat leather fatting agent, a brightening agent, odorless kerosene, triethanolamine, mildew preventive, essence, and deionized water in a certain mass ratio, and the preparation method comprises the following steps of: preparing raw materials, mixing oil phases, mixing water phases, mixing oil and water, and filtering canned objects. The high-performance nutritious waterproof shoe cream contains fluorine-containing silicone oil and a plurality of kinds of aids, can effectively improve the antistatic and mildew proof effects of leather, enhances the bending resistance of the leather, and endows the leather with the characteristics of smoothness, softness, high elasticity, and the like.
Description
Technical field
The present invention relates to household chemicals field, be specifically related to a kind of high-performance and nourish waterproof shoe polish and preparation method thereof.
Background technology
Along with improving constantly of living standards of the people, people require also to improve constantly for the nursing efficacy of leather shoes.Now on market, shoe polish is main raw material mainly with wax, solvent, dyestuff, then add that some contribute to clean, the auxiliary agent of glazing etc., this nursing agent is not ideal to the nourishing effect of leather, after life-time service, resistance to the circumnutating property of leather is poor.In addition, both at home and abroad the trend of leather shoe cleaning is disposablely to complete and improvement mildew-resistant effect antistatic to leather shoes, and gives the features such as leather is smooth, soft, elasticity is good simultaneously.Most product efficacy are on the market more single, do not reach above-mentioned composite effect.Therefore, be necessary shoe polish of the prior art to fill a prescription and the improvement of related production technique.
Summary of the invention
The object of the invention is to overcome the defect existing in prior art, design a kind of high-performance and nourish waterproof shoe polish, this shoe polish can effectively improve the antistatic and mildew-resistant effect of leather shoes, strengthen resistance to the circumnutating property of leather, give the features such as leather is smooth, soft, elasticity is good, another object of the present invention is to design the preparation method that a kind of high-performance is nourished waterproof shoe polish simultaneously.
For achieving the above object, technical scheme of the present invention provides a kind of high-performance to nourish waterproof shoe polish, it is characterized in that, the weight percent of described footwear oil composition and component is:
Tensio-active agent 2 ~ 13%
Oleic acid 1 ~ 2%
Stearic acid 2 ~ 6%
Animal tallow leather fat 2 ~ 5%
Brightening agent 7 ~ 18%
Tasteless kerosene 10 ~ 30%
Trolamine 0.5 ~ 2.0%
Mould inhibitor 0.1 ~ 0.5%
Essence 0 ~ 0.3%
Deionized water surplus
The weight percent sum of each component is 100%, and described brightening agent contains fluorine containing silicone oil, and described brightening agent also comprises at least two kinds that are selected from E wax, S wax, OP wax, beeswax and carnauba wax.
Wherein, in described high-performance nourishing waterproof shoe polish, the weight percent of fluorine containing silicone oil is 2 ~ 5%.
Wherein, described tensio-active agent comprises nonionogenic tenside, cats product, and the weight percent that described high-performance is nourished nonionogenic tenside, cats product in waterproof shoe polish is respectively: nonionogenic tenside 1 ~ 5%, cats product 1 ~ 6%.
Preferably, described nonionogenic tenside is selected from least one in glyceryl monostearate, fatty alcohol-polyoxyethylene ether and sorbitan fatty acid ester, and described cats product is quaternary ammonium salt cationic surfactant.
Wherein, described cats product is long-chain monoalkyl quaternary ammonium salt cationic surfactant.
Wherein, described animal tallow leather fat is dark seal oil or lanolin.
Wherein, described mould inhibitor is selected from least one in nano phase ag_2 o leather fungicide, methyl p-hydroxybenzoate, BIT.
Technical scheme of the present invention also provides a kind of high-performance to nourish the preparation method of waterproof shoe polish, it is characterized in that, described preparation method is:
S1: according to the weight percent configuration raw material described in claim 1;
S2: the fat-soluble ingredient in tensio-active agent, brightening agent, oleic acid, stearic acid, animal tallow leather fat, tasteless kerosene are joined to oil phase pot, be warming up to 90 ~ 95 ℃, at this temperature, stir 10 ~ 15 minutes, raw material evenly obtains oil mixture after fusing;
S3: deionized water is joined in water pot, be warming up to 90 ~ 95 ℃, add water soluble ingredient and trolamine in tensio-active agent, stir 10 ~ 15 minutes, obtain aqueous mixture after being uniformly dissolved;
S4: gained aqueous mixture in S3 is joined in emulsification pot, start stirring, then the oil mixture of gained in S2 is joined in emulsification pot, homogenizing emulsifying is cooled to 40 ~ 45 ℃ after 30 ~ 40 minutes, add mould inhibitor and essence, then stir after 10 ~ 15 minutes standing;
S5: the product of gained in S4 is filled in packaging vessel.
Wherein, the speed stirring in described S4 is 70 ~ 90r/min.
Advantage of the present invention and beneficial effect are: the fluorine containing silicone oil adding in this invention formula is containing active group, between molecule, can interact, simultaneously can with leather surface on amino, the carboxyl isopolarity radical reaction of collagen, produce great bounding force and can form one deck organosilicone elastic film at leather surface, this tunic can make leather smooth, soft feel(ing) strengthens, and improves wear resistance and the flexible resistance of leather; The linkage force of the major key Si-O that in this fluorine containing silicone oil, silicon ehter bond forms is large, and gradient of temperature is little on the impact of its viscosity, so this shoe polish has good high and low temperature resistance;
The glazing of brightening agent has persistence, with the wetting action of fluorine containing silicone oil mixing and emulsifying and tensio-active agent, and glazing better effects if;
Adopt compound tensio-active agent, particularly added cats product, emulsification, decontamination be soft leather simultaneously, reduces electrostatic adhesion, and after using, leather delicate fragrance, softness, recover elasticity.
Embodiment
Below in conjunction with embodiment, the specific embodiment of the present invention is further described.Following examples are only for technical scheme of the present invention is more clearly described, and can not limit the scope of the invention with this.
Embodiment 1
In embodiment 1, the weight percent of high-performance nourishing waterproof footwear oil composition and component is:
Fatty alcohol-polyoxyethylene ether 3%
Glyceryl monostearate 2%
Palmityl trimethyl ammonium chloride 2%
Oleic acid 1.5%
Stearic acid 4%
Lanolin 3.5%
Beeswax 3%
Carnauba wax 2%
Fluorine containing silicone oil 3.5%
Tasteless kerosene 20%
Trolamine 1.6%
Nano phase ag_2 o leather fungicide 0.1%
Methyl p-hydroxybenzoate 0.2%
Essence 0.3%
Deionized water surplus
The weight percent sum of each component is 100%;
The preparation method that high-performance is nourished waterproof shoe polish is:
S1: according to above-mentioned weight percent configuration raw material;
S2: fatty alcohol-polyoxyethylene ether, glyceryl monostearate, oleic acid, stearic acid, lanolin, beeswax, carnauba wax, fluorine containing silicone oil, tasteless kerosene, methyl p-hydroxybenzoate are joined to oil phase pot, be warming up to 90 ℃, at this temperature, stir 10 minutes, raw material evenly obtains oil mixture after fusing;
S3: deionized water is joined in water pot, be warming up to 90 ℃, add palmityl trimethyl ammonium chloride and trolamine, stir 10 minutes, obtain aqueous mixture after being uniformly dissolved;
S4: gained aqueous mixture in S3 is joined in emulsification pot, start stirring, then the oil mixture of gained in S2 is joined in emulsification pot, homogenizing emulsifying is cooled to 40 ℃ after 30 minutes, add nano phase ag_2 o leather fungicide and essence, then stir after 10 minutes standing;
S5: the product of gained in S4 is filled in packaging vessel.
Wherein, the speed stirring in described S4 is 70r/min.
Embodiment 2:
In embodiment 2, the weight percent of high-performance nourishing waterproof footwear oil composition and component is:
Sorbitan fatty acid ester 2%
Glyceryl monostearate 3%
Cetyl trimethylammonium bromide 6%
Oleic acid 1%
Stearic acid 3%
Dark seal oil 2%
E wax 1%
OP wax 4.5%
Fluorine containing silicone oil 5%
Tasteless kerosene 25%
Trolamine 2%
Nanometer silver leather mould inhibitor 0.3%
Essence 0.1%
Deionized water surplus
The weight percent sum of each component is 100%;
The preparation method that high-performance is nourished waterproof shoe polish is:
S1: according to above-mentioned weight percent configuration raw material;
S2: sorbitan fatty acid ester, glyceryl monostearate, oleic acid, stearic acid, dark seal oil, E wax, OP wax, fluorine containing silicone oil, tasteless kerosene are joined to oil phase pot, be warming up to 93 ℃, at this temperature, stir 15 minutes, raw material evenly obtains oil mixture after fusing;
S3: deionized water is joined in water pot, be warming up to 93 ℃, add cetyl trimethylammonium bromide and trolamine, stir 15 minutes, obtain aqueous mixture after being uniformly dissolved;
S4: gained aqueous mixture in S3 is joined in emulsification pot, start stirring, then the oil mixture of gained in S2 is joined in emulsification pot, homogenizing emulsifying is cooled to 42 ℃ after 40 minutes, add nano phase ag_2 o leather fungicide and essence, then stir after 15 minutes standing;
S5: the product of gained in S4 is filled in packaging vessel.
Wherein, the speed stirring in described S4 is 80r/min.
Embodiment 3:
In embodiment 3, the weight percent of high-performance nourishing waterproof footwear oil composition and component is:
Sorbitan fatty acid ester 5%
Glyceryl monostearate 1%
Octadecyl trimethyl ammonium chloride 3%
Oleic acid 2%
Stearic acid 6%
Lanolin 5%
S wax 5%
Carnauba wax 1.5%
Fluorine containing silicone oil 2%
Tasteless kerosene 20%
Trolamine 0.5%
Nano phase ag_2 o leather fungicide 0.2%
BIT 0.2%
Essence 0.2%
Deionized water surplus
The weight percent sum of each component is 100%;
The preparation method that high-performance is nourished waterproof shoe polish is:
S1: according to above-mentioned weight percent configuration raw material;
S2: sorbitan fatty acid ester, glyceryl monostearate, oleic acid, stearic acid, lanolin, S wax, carnauba wax, fluorine containing silicone oil, tasteless kerosene are joined to oil phase pot, be warming up to 90 ℃, at this temperature, stir 15 minutes, raw material evenly obtains oil mixture after fusing;
S3: deionized water is joined in water pot, be warming up to 90 ℃, add octadecyl trimethyl ammonium chloride and trolamine, stir 15 minutes, obtain aqueous mixture after being uniformly dissolved;
S4: gained aqueous mixture in S3 is joined in emulsification pot, start stirring, then the oil mixture of gained in S2 is joined in emulsification pot, homogenizing emulsifying is cooled to 43 ℃ after 35 minutes, add nano phase ag_2 o leather fungicide, BIT and essence, then stir after 15 minutes standing;
S5: the product of gained in S4 is filled in packaging vessel.
Wherein, the speed stirring in described S4 is 90r/min.
Above-mentioned three embodiment gained high-performance are nourished the emulsification of waterproof shoe polish, decontamination soft leather simultaneously, reduce electrostatic adhesion, and after using, leather delicate fragrance, softness, recover elasticity.
The above is only the preferred embodiment of the present invention; it should be pointed out that for those skilled in the art, do not departing under the prerequisite of the technology of the present invention principle; can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (9)
1. high-performance is nourished a waterproof shoe polish, it is characterized in that, the weight percent of described footwear oil composition and component is:
Tensio-active agent 2 ~ 13%
Oleic acid 1 ~ 2%
Stearic acid 2 ~ 6%
Animal tallow leather fat 2 ~ 5%
Brightening agent 7 ~ 18%
Tasteless kerosene 10 ~ 30%
Trolamine 0.5 ~ 2.0%
Mould inhibitor 0.1 ~ 0.5%
Essence 0 ~ 0.3%
Deionized water surplus
The weight percent sum of each component is 100%, and described brightening agent contains fluorine containing silicone oil, and described brightening agent also comprises at least two kinds that are selected from E wax, S wax, OP wax, beeswax and carnauba wax.
2. according to the high-performance described in claim 1, nourish waterproof shoe polish, it is characterized in that, the weight percent that described high-performance is nourished fluorine containing silicone oil in waterproof shoe polish is 2 ~ 5%.
3. according to the high-performance described in claim 1, nourish waterproof shoe polish, it is characterized in that, described tensio-active agent comprises nonionogenic tenside, cats product, and the weight percent that described high-performance is nourished nonionogenic tenside, cats product in waterproof shoe polish is respectively: nonionogenic tenside 1 ~ 5%, cats product 1 ~ 6%.
4. according to the high-performance described in claim 3, nourish waterproof shoe polish, it is characterized in that, described nonionogenic tenside is selected from least one in glyceryl monostearate, fatty alcohol-polyoxyethylene ether and sorbitan fatty acid ester, and described cats product is quaternary ammonium salt cationic surfactant.
5. high-performance according to claim 4 is nourished waterproof shoe polish, it is characterized in that, described cats product is long-chain monoalkyl quaternary ammonium salt cationic surfactant.
6. high-performance according to claim 1 is nourished waterproof shoe polish, it is characterized in that, described animal tallow leather fat is dark seal oil or lanolin.
7. high-performance according to claim 1 is nourished waterproof shoe polish, it is characterized in that, described mould inhibitor is selected from least one in nano phase ag_2 o leather fungicide, methyl p-hydroxybenzoate, BIT.
8. high-performance is nourished a preparation method for waterproof shoe polish, it is characterized in that, described preparation method is:
S1: according to the weight percent configuration raw material described in claim 1;
S2: the fat-soluble ingredient in tensio-active agent, brightening agent, oleic acid, stearic acid, animal tallow leather fat, tasteless kerosene are joined to oil phase pot, be warming up to 90 ~ 95 ℃, at this temperature, stir 10 ~ 15 minutes, raw material evenly obtains oil mixture after fusing;
S3: deionized water is joined in water pot, be warming up to 90 ~ 95 ℃, add water soluble ingredient and trolamine in tensio-active agent, stir 10 ~ 15 minutes, obtain aqueous mixture after being uniformly dissolved;
S4: gained aqueous mixture in S3 is joined in emulsification pot, start stirring, then the oil mixture of gained in S2 is joined in emulsification pot, homogenizing emulsifying is cooled to 40 ~ 45 ℃ after 30 ~ 40 minutes, add mould inhibitor and essence, then stir after 10 ~ 15 minutes standing;
S5: the product of gained in S4 is filled in packaging vessel.
9. high-performance according to claim 8 is nourished the preparation method of waterproof shoe polish, it is characterized in that, the speed stirring in described S4 is 70 ~ 90r/min.
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| CN201210344732.3A CN102876238B (en) | 2012-09-18 | 2012-09-18 | High-performance nutritious waterproof shoe cream and preparation method thereof |
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| CN201210344732.3A CN102876238B (en) | 2012-09-18 | 2012-09-18 | High-performance nutritious waterproof shoe cream and preparation method thereof |
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| CN102876238B true CN102876238B (en) | 2014-04-02 |
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Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103992744A (en) * | 2013-02-18 | 2014-08-20 | 刘祖学 | Efficient shoe polish |
| CN103409073A (en) * | 2013-08-14 | 2013-11-27 | 吴江市利达上光制品有限公司 | Moisture-proof environment-friendly shoe polish and preparation method thereof |
| CN104974670A (en) * | 2014-12-02 | 2015-10-14 | 裴萌 | Wiping-free liquid leather shoe polish |
| CN105219539A (en) * | 2015-09-17 | 2016-01-06 | 广州佳伲思抗菌材料有限公司 | A kind of antimildew and antibacterial cleansing cream and preparation method thereof and application |
| WO2017161509A1 (en) * | 2016-03-23 | 2017-09-28 | 江阴樱花梦家庭用品有限公司 | Composition for brushing-free shoe polish and preparation method therefor |
| CN106700947B (en) * | 2016-11-29 | 2018-06-05 | 梧州市海邦科技有限公司 | A kind of bloom footwear breast |
| CN106752971A (en) * | 2016-12-09 | 2017-05-31 | 陈忠燕 | A kind of Mildew resistant shoe polish |
| CN107011808A (en) * | 2017-04-27 | 2017-08-04 | 陈秋华 | A kind of liquid shoe polish and preparation method thereof |
| CN108148508A (en) * | 2017-11-12 | 2018-06-12 | 孝感市锐思新材科技有限公司 | A kind of preparation method for leather and fur products brightener new material |
| CN108864951A (en) * | 2018-08-09 | 2018-11-23 | 台州智子科技有限公司 | A kind of shoe polish and preparation method thereof with anti-aging function |
| CN110684603A (en) * | 2019-09-26 | 2020-01-14 | 广东中联邦精细化工有限公司 | Leather cleaning agent and preparation method thereof |
| CN111234710A (en) * | 2020-02-20 | 2020-06-05 | 广州赫厉狮森汽车用品有限公司 | Automobile paint surface protective wax and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| JPH06184497A (en) * | 1992-12-16 | 1994-07-05 | Ishihara Chem Co Ltd | Polishing agent for vehicle |
| CN101712848A (en) * | 2008-10-06 | 2010-05-26 | 天津市化学试剂研究所 | Metal vibration polishing solution and preparation method thereof |
| CN101921676A (en) * | 2009-06-12 | 2010-12-22 | 刘光玲 | Leather shoe cleaning cream |
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Address after: 214400 No. 35 Yingbin Avenue, Xu Xiake Town, Jiangyin, Wuxi, Jiangsu. Patentee after: Jiangsu Xuebao Daily Chemical Co., Ltd. Address before: 214400 east side of Dongmen overpass, Jiangyin City, Wuxi, Jiangsu Patentee before: Jiangsu Xuebao Daily Chemical Co., Ltd. |
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