CN111234710A - Automobile paint surface protective wax and preparation method thereof - Google Patents
Automobile paint surface protective wax and preparation method thereof Download PDFInfo
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- CN111234710A CN111234710A CN202010105447.0A CN202010105447A CN111234710A CN 111234710 A CN111234710 A CN 111234710A CN 202010105447 A CN202010105447 A CN 202010105447A CN 111234710 A CN111234710 A CN 111234710A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/06—Other polishing compositions
- C09G1/08—Other polishing compositions based on wax
- C09G1/10—Other polishing compositions based on wax based on mixtures of wax and natural or synthetic resin
- C09G1/12—Other polishing compositions based on wax based on mixtures of wax and natural or synthetic resin mixtures of wax and silicon-containing polycondensates
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Abstract
The invention discloses an automobile paint surface protective wax and a preparation method thereof. The automobile paint surface protective wax comprises the following components in percentage by weight: 1-2% of emulsifier, 15-20% of filler, 3-6% of ethylene glycol, 20-30% of odorless kerosene, 6-10% of polyethylene wax, 4-8% of natural carnauba wax, 10-15% of polysiloxane, 2-5% of stearic acid, 0.2-0.5% of corrosion inhibitor, 0.1-0.3% of color paste and the balance of water. According to the invention, water is used as a solvent, the volatilization of the solvent in the construction process hardly causes pollution to the air environment, and the paint has the effects of decontamination, polishing, protection, antifouling and the like, has excellent glossiness, and is good in system stability and lasting in effect; the invention adopts a production process of high-temperature homogeneous emulsification, the filler is dispersed more uniformly and finely, fine scratches cannot be generated on the paint surface during construction, and the reasonable emulsification of the oil phase material and the water phase material ensures that the constructed paint surface is not greasy and has good hydrophobicity and is not easy to be stuck with ash.
Description
Technical Field
The invention relates to the technical field of automobile maintenance, in particular to automobile paint surface protective wax and a preparation method thereof.
Background
With the rapid development of the automobile industry, people pay more and more attention to automobile maintenance, and the market demand of automobile protective wax products is vigorous. At present, the widely used automobile protective wax at home and abroad is mostly divided into two types of functional products, one type of protective wax is soft wax, the effect is mainly decontamination, the soft wax is prepared by a normal-temperature stirring emulsification process, fillers cannot be well dispersed, particle diameters are uneven, technicians are easy to scratch and circle lines during construction, and meanwhile, the application of the normal-temperature emulsification process to glazing materials (such as wax powder) is limited, and the materials cannot be compatible in a system because the materials cannot be dissolved at normal temperature, so that the glazing and film forming effects cannot be good. The other kind of protective wax is solid wax, the effect of the protective wax is mainly polishing and antifouling, the solid wax belongs to a pure solvent system, the process flow of high-temperature hot melting and cooling and curing forming is adopted, the oil content is high to achieve the effect of high gloss, but the painted surface is greasy after construction, and an oil film is not cured generally, so that dust in the air is easy to bond in the driving process, and the cleaning frequency is increased. Meanwhile, most manufacturers select wax which is generally low-price synthetic wax to reduce the production cost and play a role in glazing protection, but the materials are low in hardness and melting point, poor in adhesion force after being constructed on a paint surface, and poor in durability of a protective layer caused by high-temperature weather driving, and the original effect cannot be achieved after the automobile is generally washed for two to three times. The two types of protective wax need to be packaged separately, the construction of workers cannot be completed in one step, the construction needs to be performed twice, the labor cost is increased, and meanwhile, the maintenance cost of consumers is greatly increased.
Disclosure of Invention
The invention aims to provide an automobile paint surface protective wax and a preparation method thereof, and aims to solve the technical problems.
In order to achieve the purpose, the technical scheme of the invention is as follows:
in a first aspect, the present invention provides an automobile paint protective wax, which comprises, by weight: 1-2% of emulsifier, 15-20% of filler, 3-6% of ethylene glycol, 20-30% of odorless kerosene, 6-10% of polyethylene wax, 4-8% of natural carnauba wax, 10-15% of polysiloxane, 2-5% of stearic acid, 0.2-0.5% of corrosion inhibitor, 0.1-0.3% of color paste and the balance of water.
Preferably, the emulsifier is selected from one or two of morpholine and span-80.
Preferably, the filler is selected from any one or two of diatomite, kaolin and quartz sand.
Preferably, the corrosion inhibitor is selected from one or two of triethanolamine, benzotriazole, mercapto benzothiazole and methyl benzotriazole.
In a second aspect, the present invention provides a method for preparing the automobile paint protective wax according to the first aspect, comprising the following steps:
(1) adding water, an emulsifier, a filler and ethylene glycol into a water phase pot, starting a steam heating valve for heating, simultaneously starting a dispersion machine in the water phase pot for mixing, stirring and dispersing, and heating to a preset temperature to obtain a water phase;
(2) adding odorless kerosene, polyethylene wax, natural carnauba wax, polysiloxane and stearic acid into an oil phase pot, starting a steam heating valve for heating, simultaneously starting a dispersion machine in the oil phase pot for mixing, stirring and dispersing, and heating to a preset temperature to obtain an oil phase;
(3) sucking the water phase into an emulsifying pot through a vacuum pump, starting a homogenizer in the emulsifying pot, adding the oil phase, continuing homogenizing for 3-10 min, cooling to 65-75 ℃, adding a corrosion inhibitor and color paste, stirring uniformly, cooling, filling and warehousing.
Preferably, the preset temperature in the step (1) is 80-100 ℃.
Preferably, the heating rate in the step (1) is 5-10 ℃/min.
Preferably, the stirring speed of the disperser in the step (1) is 300-500 r/min.
Preferably, the preset temperature in the step (2) is 80-100 ℃.
Preferably, the stirring speed of the disperser in the step (2) is 200-400 r/min.
Preferably, the heating rate in the step (2) is 5-10 ℃/min.
Preferably, the rotation speed of the homogenizer in the step (3) is 1500-2500 r/min.
Compared with the prior art, the invention has the beneficial effects that:
in addition, the invention has the effects of decontamination, polishing, protection, antifouling and the like, and has excellent glossiness, good system stability and lasting effect; the invention adopts a production process of high-temperature homogeneous emulsification, the filler is dispersed more uniformly and finely, fine scratches cannot be generated on the paint surface during construction, and the reasonable emulsification of the oil phase material and the water phase material ensures that the constructed paint surface is not greasy and has good hydrophobicity and is not easy to be stuck with ash.
Detailed Description
The following further describes the embodiments of the present invention. It should be noted that the description of the embodiments is provided to help understanding of the present invention, but the present invention is not limited thereto. In addition, the technical features involved in the embodiments of the present invention described below may be combined with each other as long as they do not conflict with each other.
Example 1
The preparation method of the automobile paint protective wax provided by the embodiment comprises the following steps:
(1) comprises the following components in percentage by weight: span-801.5%, diatomite 18%, ethylene glycol 4%, odorless kerosene 25%, polyethylene wax 8%, natural carnauba wax 6%, polysiloxane 12%, stearic acid 3%, triethanolamine 0.3%, color paste 0.2%, and the balance of deionized water.
(2) Adding deionized water, span-80, diatomite and ethylene glycol into a deionized water phase pot, starting a steam heating valve to heat at a heating rate of 9 ℃/min, simultaneously starting a dispersion machine in the deionized water phase pot to mix, stir and disperse at a stirring rate of 350r/min, and obtaining a deionized water phase after heating to a preset temperature of 90 ℃;
(3) adding odorless kerosene, polyethylene wax, natural carnauba wax, polysiloxane and stearic acid into an oil phase pot, starting a steam heating valve to heat at a heating rate of 6 ℃/min, simultaneously starting a dispersion machine in the oil phase pot to mix, stir and disperse at a stirring rate of 300r/min, and heating to a preset temperature of 80-100 ℃ to obtain an oil phase;
(4) sucking deionized water phase into an emulsifying pot through a vacuum pump, starting a homogenizer (the rotating speed is 2000r/min) in the emulsifying pot, then adding an oil phase, continuing homogenizing for 5min, then cooling to 70 ℃, adding triethanolamine and color paste, stirring uniformly, naturally cooling for 8h, finally filling into a single independent packaging hand-spraying kettle, sealing and warehousing.
The product obtained in this example was tested and the results are shown in the following table:
example 2
The preparation method of the automobile paint protective wax provided by the embodiment comprises the following steps:
(1) comprises the following components in percentage by weight: span-802%, diatomite 15%, ethylene glycol 5%, odorless kerosene 20%, polyethylene wax 10%, natural carnauba wax 8%, polysiloxane 10%, stearic acid 2%, triethanolamine 0.2%, color paste 0.1%, and the balance of deionized water.
(2) Adding deionized water, span-80, diatomite and ethylene glycol into a deionized water phase pot, starting a steam heating valve to heat at a heating rate of 5 ℃/min, simultaneously starting a dispersion machine in the deionized water phase pot to mix, stir and disperse at a stirring rate of 300r/min, and obtaining a deionized water phase after heating to a preset temperature of 80 ℃;
(3) adding odorless kerosene, polyethylene wax, natural carnauba wax, polysiloxane and stearic acid into an oil phase pot, starting a steam heating valve to heat at a heating rate of 5 ℃/min, simultaneously starting a dispersion machine in the oil phase pot to mix, stir and disperse at a stirring rate of 200r/min, and heating to a preset temperature of 80 ℃ to obtain an oil phase;
(4) sucking deionized water phase into an emulsifying pot through a vacuum pump, starting a homogenizer (the rotating speed is 1500r/min) in the emulsifying pot, then adding an oil phase, continuing homogenizing for 10min, then cooling to 65 ℃, adding triethanolamine and color paste, stirring uniformly, naturally cooling for 8h, finally filling into a single independent packaging hand-spraying kettle, sealing and warehousing.
The product obtained in this example was tested and the results are shown in the following table:
example 3
The preparation method of the automobile paint protective wax provided by the embodiment comprises the following steps:
(1) comprises the following components in percentage by weight: span-801%, diatomite 20%, ethylene glycol 3%, odorless kerosene 30%, polyethylene wax 6%, natural carnauba wax 4%, polysiloxane 15%, stearic acid 5%, triethanolamine 0.5%, color paste 0.3%, and the balance of deionized water.
(2) Adding deionized water, span-80, diatomite and ethylene glycol into a deionized water phase pot, starting a steam heating valve to heat at a heating rate of 5 ℃/min, simultaneously starting a dispersion machine in the deionized water phase pot to mix, stir and disperse at a stirring rate of 500r/min, and obtaining a deionized water phase after heating to a preset temperature of 100 ℃;
(3) adding odorless kerosene, polyethylene wax, natural carnauba wax, polysiloxane and stearic acid into an oil phase pot, starting a steam heating valve to heat at a heating rate of 5 ℃/min, simultaneously starting a dispersion machine in the oil phase pot to mix, stir and disperse at a stirring rate of 400r/min, and heating to a preset temperature of 100 ℃ to obtain an oil phase;
(4) sucking deionized water phase into an emulsifying pot through a vacuum pump, starting a homogenizer (the rotating speed is 2500r/min) in the emulsifying pot, then adding an oil phase, continuing homogenizing for 10min, then cooling to 75 ℃, adding triethanolamine and color paste, stirring uniformly, naturally cooling for 8h, finally filling into a single independent packaging hand-spraying kettle, sealing and warehousing.
The product obtained in this example was tested and the results are shown in the following table:
example 4
The preparation method of the automobile paint protective wax provided by the embodiment comprises the following steps:
(1) comprises the following components in percentage by weight: span-801.5%, diatomite 16%, ethylene glycol 6%, odorless kerosene 24%, polyethylene wax 7%, natural carnauba wax 5%, polysiloxane 12%, stearic acid 4%, triethanolamine 0.4%, color paste 0.2%, and the balance of deionized water.
(2) Adding deionized water, span-80, diatomite and ethylene glycol into a deionized water phase pot, starting a steam heating valve to heat at a heating rate of 5 ℃/min, simultaneously starting a dispersion machine in the deionized water phase pot to mix, stir and disperse at a stirring rate of 400r/min, and obtaining a deionized water phase after heating to a preset temperature of 85 ℃;
(3) adding odorless kerosene, polyethylene wax, natural carnauba wax, polysiloxane and stearic acid into an oil phase pot, starting a steam heating valve to heat at a heating rate of 8 ℃/min, simultaneously starting a dispersion machine in the oil phase pot to mix, stir and disperse at a stirring rate of 300r/min, and heating to a preset temperature of 80 ℃ to obtain an oil phase;
(4) and (2) sucking the deionized water phase into an emulsifying pot through a vacuum pump, starting a homogenizer (the rotating speed is 2200r/min) in the emulsifying pot, then adding the oil phase, continuing homogenizing for 3-10 min, then cooling to 70 ℃, adding triethanolamine and color paste, stirring uniformly, naturally cooling for 8h, finally filling into a single independent packaging hand-spraying pot, sealing and warehousing.
The product obtained in this example was tested and the results are shown in the following table:
example 5
The preparation method of the automobile paint protective wax provided by the embodiment comprises the following steps:
(1) comprises the following components in percentage by weight: 1.8% of morpholine, 17% of kaolin, 4% of ethylene glycol, 26% of odorless kerosene, 7% of polyethylene wax, 5% of natural carnauba wax, 11% of polysiloxane, 3% of stearic acid, 0.3% of triethanolamine, 0.2% of color paste and the balance of deionized water.
(2) Adding deionized water, morpholine, kaolin and ethylene glycol into a deionized water phase pot, starting a steam heating valve to heat at a heating rate of 6 ℃/min, simultaneously starting a dispersion machine in the deionized water phase pot to mix, stir and disperse at a stirring rate of 400r/min, and obtaining a deionized water phase after heating to a preset temperature of 90 ℃;
(3) adding odorless kerosene, polyethylene wax, natural carnauba wax, polysiloxane and stearic acid into an oil phase pot, starting a steam heating valve to heat at a heating rate of 6 ℃/min, simultaneously starting a dispersion machine in the oil phase pot to mix, stir and disperse at a stirring rate of 300r/min, and heating to a preset temperature of 90 ℃ to obtain an oil phase;
(4) sucking deionized water phase into an emulsifying pot through a vacuum pump, starting a homogenizer (the rotating speed is 2200r/min) in the emulsifying pot, then adding an oil phase, continuing homogenizing for 5min, then cooling to 70 ℃, adding triethanolamine and color paste, stirring uniformly, naturally cooling for 8h, finally filling into a single independent packaging hand-spraying kettle, sealing and warehousing.
The product obtained in this example was tested and the results are shown in the following table:
example 6
The preparation method of the automobile paint protective wax provided by the embodiment comprises the following steps:
(1) comprises the following components in percentage by weight: span-801.5%, kaolin 18%, ethylene glycol 4%, odorless kerosene 27%, polyethylene wax 7%, natural carnauba wax 6%, polysiloxane 13%, stearic acid 3%, benzotriazole 0.4%, color paste 0.2%, and the balance of deionized water.
(2) Adding deionized water, span-80, kaolin and ethylene glycol into a deionized water phase pot, starting a steam heating valve to heat at a heating rate of 9 ℃/min, simultaneously starting a dispersion machine in the deionized water phase pot to mix, stir and disperse at a stirring rate of 400r/min, and obtaining a deionized water phase after heating to a preset temperature of 90 ℃;
(3) adding odorless kerosene, polyethylene wax, natural carnauba wax, polysiloxane and stearic acid into an oil phase pot, starting a steam heating valve to heat at a heating rate of 9 ℃/min, simultaneously starting a dispersion machine in the oil phase pot to mix, stir and disperse at a stirring rate of 300r/min, and heating to a preset temperature of 90 ℃ to obtain an oil phase;
(4) sucking deionized water phase into an emulsifying pot through a vacuum pump, starting a homogenizer (the rotating speed is 2000r/min) in the emulsifying pot, then adding an oil phase, continuing homogenizing for 6min, then cooling to 70 ℃, adding benzotriazole and color paste, stirring uniformly, naturally cooling for 8h, finally filling into a single independent packaging hand-spraying pot, sealing the box and warehousing.
The product obtained in this example was tested and the results are shown in the following table:
the embodiments of the present invention have been described in detail, but the present invention is not limited to the described embodiments. It will be apparent to those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, and the scope of protection is still within the scope of the invention.
Claims (10)
1. The automobile paint surface protecting wax is characterized by comprising the following components in percentage by weight: 1-2% of emulsifier, 15-20% of filler, 3-6% of ethylene glycol, 20-30% of odorless kerosene, 6-10% of polyethylene wax, 4-8% of natural carnauba wax, 10-15% of polysiloxane, 2-5% of stearic acid, 0.2-0.5% of corrosion inhibitor, 0.1-0.3% of color paste and the balance of water.
2. The automobile finish protecting wax as claimed in claim 1, wherein the emulsifier is selected from one or two of morpholine and span-80.
3. The automobile paint protection wax as claimed in claim 1, wherein the filler is selected from any one or two of diatomaceous earth, kaolin, and quartz sand.
4. The wax as claimed in claim 1, wherein the corrosion inhibitor is one or two selected from triethanolamine, benzotriazole, mercaptobenzothiazole and tolytriazole.
5. A method for preparing the automobile paint protective wax according to any one of claims 1 to 4, which comprises the following steps:
(1) adding water, an emulsifier, a filler and ethylene glycol into a water phase pot, starting a steam heating valve for heating, simultaneously starting a dispersion machine in the water phase pot for mixing, stirring and dispersing, and heating to a preset temperature to obtain a water phase;
(2) adding odorless kerosene, polyethylene wax, natural carnauba wax, polysiloxane and stearic acid into an oil phase pot, starting a steam heating valve for heating, simultaneously starting a dispersion machine in the oil phase pot for mixing, stirring and dispersing, and heating to a preset temperature to obtain an oil phase;
(3) sucking the water phase into an emulsifying pot through a vacuum pump, starting a homogenizer in the emulsifying pot, adding the oil phase, continuing homogenizing for 3-10 min, cooling to 65-75 ℃, adding a corrosion inhibitor and color paste, stirring uniformly, cooling, filling and warehousing.
6. The method for preparing the automobile paint protection wax according to claim 5, wherein the preset temperature in the step (1) is 80-100 ℃.
7. The method for preparing the automobile finish protective wax according to claim 5, wherein the heating rate in the step (1) is 5-10 ℃/min.
8. The preparation method of the automobile paint protection wax as claimed in claim 5, wherein the stirring speed of the disperser in the step (1) is 300-500 r/min.
9. The preparation method of the automobile paint protection wax as claimed in claim 5, wherein the stirring speed of the disperser in the step (2) is 200-400 r/min.
10. The method for preparing the automobile paint protection wax as claimed in claim 5, wherein the rotation speed of the homogenizer in the step (3) is 1500-2500 r/min.
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| Application Number | Priority Date | Filing Date | Title |
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| CN202010105447.0A CN111234710A (en) | 2020-02-20 | 2020-02-20 | Automobile paint surface protective wax and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202010105447.0A CN111234710A (en) | 2020-02-20 | 2020-02-20 | Automobile paint surface protective wax and preparation method thereof |
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| CN202010105447.0A Pending CN111234710A (en) | 2020-02-20 | 2020-02-20 | Automobile paint surface protective wax and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114806399A (en) * | 2022-04-28 | 2022-07-29 | 广东优贝科技股份有限公司 | Automobile paint surface glaze and preparation method thereof |
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| CN102876238A (en) * | 2012-09-18 | 2013-01-16 | 江苏雪豹日化有限公司 | High-performance nutritious waterproof shoe cream and preparation method thereof |
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| CN106957533A (en) * | 2017-05-03 | 2017-07-18 | 吴子良 | A kind of paraffin wax emulsions and preparation method thereof |
| CN107384219A (en) * | 2017-08-10 | 2017-11-24 | 中国科学院长春应用化学研究所 | A kind of automobile finish polishing agent and preparation method thereof |
| CN107523224A (en) * | 2016-06-17 | 2017-12-29 | 中国石油化工股份有限公司 | The method for producing wax polish |
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2020
- 2020-02-20 CN CN202010105447.0A patent/CN111234710A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102876238A (en) * | 2012-09-18 | 2013-01-16 | 江苏雪豹日化有限公司 | High-performance nutritious waterproof shoe cream and preparation method thereof |
| CN105086566A (en) * | 2015-08-05 | 2015-11-25 | 广州赫厉狮森汽车用品有限公司 | Water-based environment-friendly automotive paint surface repairing wax and preparing method thereof |
| CN107523224A (en) * | 2016-06-17 | 2017-12-29 | 中国石油化工股份有限公司 | The method for producing wax polish |
| CN106957533A (en) * | 2017-05-03 | 2017-07-18 | 吴子良 | A kind of paraffin wax emulsions and preparation method thereof |
| CN107384219A (en) * | 2017-08-10 | 2017-11-24 | 中国科学院长春应用化学研究所 | A kind of automobile finish polishing agent and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN114806399A (en) * | 2022-04-28 | 2022-07-29 | 广东优贝科技股份有限公司 | Automobile paint surface glaze and preparation method thereof |
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Application publication date: 20200605 |