CN105086566A - Water-based environment-friendly automotive paint surface repairing wax and preparing method thereof - Google Patents
Water-based environment-friendly automotive paint surface repairing wax and preparing method thereof Download PDFInfo
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- CN105086566A CN105086566A CN201510472907.2A CN201510472907A CN105086566A CN 105086566 A CN105086566 A CN 105086566A CN 201510472907 A CN201510472907 A CN 201510472907A CN 105086566 A CN105086566 A CN 105086566A
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Abstract
The invention relates to repairing wax and a preparing method, in particular to water-based environment-friendly automotive paint surface repairing wax and a preparing method thereof. The water-based environment-friendly automotive paint surface repairing wax has the decontaminating, glazing and protecting effects of traditional automotive wax, can repair or fill tiny scratches and cracks of an automotive paint surface as the repairing wax contains unique micro-nano polishing powder, and has good functions of removing the scratches and filling the paint surface, and the comprehensive performance of the automotive wax is further improved; in addition, as the main solvent component is deionized water, and the repairing wax only contains a small amount of environment-friendly solvent, in the construction process, solvent volatilization hardly causes pollution to air environment, the preparing technology includes simple steps and is easy to operate, and production cost is low.
Description
Technical field
The present invention relates to a kind of reparation wax and preparation method, be specifically related to a kind of aqueous environment protection automobile finish and repair wax and preparation method thereof.
Background technology
Traditional car wax is formed primarily of wax, silicone oil and solvent, and such wax contains volatile noxious solvent composition, and in the process of spraying operation, solvent is volatile to environment, is not suitable for routine use.Simultaneously; such car wax is mainly effect that automobile finish brings decontamination, glazing and protection; the function of repair problems such as the cuts of automobile finish, filling is more weak; in addition; to automobile finish gloss and guard time shorter; need often to carry out waxing protection to car surface, the demand of people can not be met.
Summary of the invention
The present invention's first object provides a kind of aqueous environment protection automobile finish to repair wax for the deficiencies in the prior art; possess the over-all propertieies such as decontamination, glazing, protection, scratch removal and lacquer painting filling; in addition; its primary solvent composition is deionized water; only containing a small amount of environment-friendly type solvent; thus this wax is in construction process, and the volatilization of solvent pollutes air ambient hardly.
Another object of the present invention provides a kind of aqueous environment protection automobile finish to repair the preparation method of wax for the deficiencies in the prior art, and processing step is simple to operation, and production cost is low.
In order to realize above object, the invention provides following technical scheme:
A kind of aqueous environment protection automobile finish repairs wax, comprises the component of following weight part:
Environment-friendly type aliphatic solvents 5-20 part
Acid montanin wax 1-10 part
Dimethyl silicone oil 1-10 part
Tensio-active agent 1-5 part
Polyvalent alcohol 1-5 part
Polishing powder 5-20 part
Thickening material 1-5 part
Sanitas 0.1-1 part
Pigment 0.01-0.1 part
Deionized water 30-70 part.
As preferably, described aqueous environment protection automobile finish repairs the component that wax comprises following weight part:
Environment-friendly type aliphatic solvents 5-15 part
Acid montanin wax 1-5 part
Dimethyl silicone oil 1-5 part
Tensio-active agent 1-3 part
Polyvalent alcohol 1-3 part
Polishing powder 5-15 part
Thickening material 1-3 part
Sanitas 0.1-0.5 part
Pigment 0.01-0.05 part
Deionized water 30-50 part.
Preferred as another, described aqueous environment protection automobile finish repairs the component that wax comprises following weight part:
Environment-friendly type aliphatic solvents 15-20 part
Acid montanin wax 5-10 part
Dimethyl silicone oil 5-10 part
Tensio-active agent 3-5 part
Polyvalent alcohol 3-5 part
Polishing powder 15-20 part
Thickening material 3-5 part
Sanitas 0.5-1 part
Pigment 0.05-0.1 part
Deionized water 50-70 part.
Wherein, described environment-friendly type aliphatic solvents is any one or the two or more mixture in tasteless kerosene D40, tasteless kerosene D60, Isopars L.
Wherein, described acid montanin wax is any one or the two or more mixture in Ke Laien S wax, Ke Laien LP wax, Ke Laien OP wax.
Wherein, described dimethyl silicone oil is any one or the two or more mixture in DOW CORNING PMX-200 silicone oil 100cs, DOW CORNING PMX-200 silicone oil 350cs, DOW CORNING PMX-200 silicone oil 1000cs, DOW CORNING PMX-200 silicone oil 12500cs.
Wherein, described tensio-active agent is any one or the two or more mixture in GP200, A165, tween/this dish composite emulsifying system, oleic acid/morpholine composite emulsifying system.
Wherein, described polyvalent alcohol is any one or two or more mixtures in ethylene glycol, propylene glycol, glycerol, and described polishing powder is any one or two or more mixtures in kaolin, diatomite, quartz sand.
Wherein, described thickening material is inorganic or organic thickening agent, and described sanitas is Sodium Benzoate, potassium sorbate or KF-88, and described pigment is water-soluble bloom or water-soluble rouge and powder.
Aqueous environment protection automobile finish repairs a preparation method for wax, comprises the following steps:
(1) take by weight and aliphatic solvents, acid montanin wax, dimethyl silicone oil are put in oil cauldron, under the condition constantly stirred, being warming up to 80-95 DEG C, treating that material dissolution is complete transparent liquid, constant temperature 5-30 minute;
(2) by weight deionized water, tensio-active agent, polyvalent alcohol, polishing powder are joined in emulsification pot, be heated to 70-90 DEG C while stirring, constant temperature 5-30 minute;
(3) high-speed mixing equipment of emulsification pot is started, material in oil cauldron was extracted in emulsification pot at 2-10 minute, 10-60 minute is reacted at 60-90 DEG C, then 60-80 DEG C is cooled to, add thickening material, sanitas, pigment, continue high-speed stirring 2-10 minute, get product after the assay was approved.
Compared with prior art, the beneficial effect that the present invention has is: aqueous environment protection automobile finish of the present invention repairs wax, its primary solvent composition is deionized water, only containing a small amount of environment-friendly type solvent, thus this wax is in construction process, the volatilization of solvent pollutes air ambient hardly, and its step of preparation process is simple to operation, and production cost is low.In addition; the present invention not only has decontamination that traditional vehicle wax possesses, the effect such as glazing and protection; include unique micro-nano polishing powder; can the fine scratches of automobile finish and crack be repaired or be filled; possesses the effect of good removal cut and filling lacquer painting; the further over-all properties expanding simoniz.
Embodiment
Below in conjunction with specific embodiment, the present invention is described in further detail, but any limitation of the invention do not formed.
Embodiment 1.
The aqueous environment protection automobile finish of the present embodiment repairs wax, comprises the component of following weight part:
Environment-friendly type aliphatic solvents 5 parts, acid montanin wax 1 part, dimethyl silicone oil 1 part, 1 part, tensio-active agent, polyvalent alcohol 1 part, polishing powder 5 parts, thickening material 1 part, sanitas 0.1 part, pigment 0.01 part, deionized water 30 parts.
The aqueous environment protection automobile finish of the present embodiment repairs the preparation method of wax, comprises the following steps:
(1) take successively by weight and aliphatic solvents 5 parts, acid montanin wax 1 part, dimethyl silicone oil 1 part are put in oil cauldron, under the condition constantly stirred, being warming up to 80 DEG C, treating that material dissolution is complete transparent liquid, constant temperature 5 minutes;
(2) by weight deionized water 30 parts, 1 part, tensio-active agent, polyvalent alcohol 1 part, polishing powder 5 parts are joined in emulsification pot, be heated to 70 DEG C while stirring, constant temperature 5 minutes;
(3) start the high-speed mixing equipment of emulsification pot, the material in oil cauldron was extracted in emulsification pot at 2 minutes, react 10 minutes at 60 DEG C, then 60 DEG C are cooled to, add thickening material 1 part, sanitas 0.1 part, pigment 0.01 part, continue high-speed stirring 2 minutes, get product after the assay was approved.
Embodiment 2.
The aqueous environment protection automobile finish of the present embodiment repairs wax, comprises the component of following weight part:
Environment-friendly type aliphatic solvents 20 parts, acid montanin wax 10 parts, dimethyl silicone oil 10 parts, 5 parts, tensio-active agent, polyvalent alcohol 5 parts, polishing powder 20 parts, thickening material 5 parts, sanitas 1 part, pigment 0.1 part, deionized water 70 parts.
The aqueous environment protection automobile finish of the present embodiment repairs the preparation method of wax, comprises the following steps:
(1) take successively by weight and aliphatic solvents 20 parts, acid montanin wax 10 parts, dimethyl silicone oil 10 parts are put in oil cauldron, under the condition constantly stirred, being warming up to 95 DEG C, treating that material dissolution is complete transparent liquid, constant temperature 30 minutes;
(2) by weight deionized water 70 parts, 5 parts, tensio-active agent, polyvalent alcohol 5 parts, polishing powder 20 parts are joined in emulsification pot, be heated to 90 DEG C while stirring, constant temperature 30 minutes;
(3) start the high-speed mixing equipment of emulsification pot, the material in oil cauldron was extracted in emulsification pot at 10 minutes, react 60 minutes at 90 DEG C, then 80 DEG C are cooled to, add thickening material 5 parts, sanitas 1 part, pigment 0.1 part, continue high-speed stirring 10 minutes, get product after the assay was approved.
Embodiment 3.
The aqueous environment protection automobile finish of the present embodiment repairs wax, comprises the component of following weight part:
Environment-friendly type aliphatic solvents 15 parts, acid montanin wax 5 parts, dimethyl silicone oil 5 parts, 3 parts, tensio-active agent, polyvalent alcohol 3 parts, polishing powder 15 parts, thickening material 3 parts, sanitas 0.5 part, pigment 0.05 part, deionized water 50 parts.
The aqueous environment protection automobile finish of the present embodiment repairs the preparation method of wax, comprises the following steps:
(1) take successively by weight and aliphatic solvents 15 parts, acid montanin wax 5 parts, dimethyl silicone oil 5 parts are put in oil cauldron, under the condition constantly stirred, being warming up to 90 DEG C, treating that material dissolution is complete transparent liquid, constant temperature 15 minutes;
(2) by weight deionized water 50 parts, 3 parts, tensio-active agent, polyvalent alcohol 3 parts, polishing powder 15 parts are joined in emulsification pot, be heated to 70 DEG C while stirring, constant temperature 15 minutes;
(3) high-speed mixing equipment of emulsification pot is started, material in oil cauldron was extracted in emulsification pot at 5 minutes, react 40 minutes at 70 DEG C, then 70 DEG C are cooled to, add thickening material 3 parts, sanitas 0.5 part, pigment 0.05 part, continue high-speed stirring 10 minutes, get product after the assay was approved.
Embodiment 4.
The aqueous environment protection automobile finish of the present embodiment repairs wax, comprises the component of following weight part:
Environment-friendly type aliphatic solvents 20 parts, acid montanin wax 5 parts, dimethyl silicone oil 5 parts, 2 parts, tensio-active agent, polyvalent alcohol 5 parts, polishing powder 10 parts, thickening material 2 parts, sanitas 1 part, pigment 0.1 part, deionized water 49.9 parts.
The aqueous environment protection automobile finish of the present embodiment repairs the preparation method of wax, comprises the following steps:
(1) take successively by weight and aliphatic solvents 20 parts, acid montanin wax 5 parts, dimethyl silicone oil 5 parts are put in oil cauldron, under the condition constantly stirred, being warming up to 85 DEG C, treating that material dissolution is complete transparent liquid, constant temperature 10 minutes;
(2) by weight deionized water 49.9 parts, 2 parts, tensio-active agent, polyvalent alcohol 5 parts, polishing powder 10 parts are joined in emulsification pot, be heated to 75 DEG C while stirring, constant temperature 5 minutes;
(3) start the high-speed mixing equipment of emulsification pot, the material in oil cauldron was extracted in emulsification pot at 5 minutes, react 30 minutes at 80 DEG C, then 70 DEG C are cooled to, add thickening material 2 parts, sanitas 1 part, pigment 0.1 part, continue high-speed stirring 5 minutes, get product after the assay was approved.
Embodiment 5.
The aqueous environment protection automobile finish of the present embodiment repairs wax, comprises the component of following weight part:
Environment-friendly type aliphatic solvents 15 parts, acid montanin wax 6 parts, dimethyl silicone oil 4 parts, 2 parts, tensio-active agent, polyvalent alcohol 5 parts, polishing powder 15 parts, thickening material 4 parts, sanitas 1 part, pigment 0.1 part, deionized water 47.9 parts.
The aqueous environment protection automobile finish of the present embodiment repairs the preparation method of wax, comprises the following steps:
(1) take successively by weight and aliphatic solvents 15 parts, acid montanin wax 6 parts, dimethyl silicone oil 4 parts are put in oil cauldron, under the condition constantly stirred, being warming up to 90 DEG C, treating that material dissolution is complete transparent liquid, constant temperature 10 minutes;
(2) by weight deionized water 47.9 parts, 2 parts, tensio-active agent, polyvalent alcohol 5 parts, polishing powder 15 parts are joined in emulsification pot, be heated to 80 DEG C while stirring, constant temperature 5 minutes;
(3) start the high-speed mixing equipment of emulsification pot, the material in oil cauldron was extracted in emulsification pot at 3 minutes, react 40 minutes at 80 DEG C, then 65 DEG C are cooled to, add thickening material 4 parts, sanitas 1 part, pigment 0.1 part, continue high-speed stirring 5 minutes, get product after the assay was approved.
Embodiment 6.
The aqueous environment protection automobile finish of the present embodiment repairs wax, comprises the component of following weight part:
Environment-friendly type aliphatic solvents 12 parts, acid montanin wax 7 parts, dimethyl silicone oil 6 parts, 2 parts, tensio-active agent, polyvalent alcohol 5 parts, polishing powder 10 parts, thickening material 2 parts, sanitas 1 part, pigment 0.1 part, deionized water 54.9 parts.
The aqueous environment protection automobile finish of the present embodiment repairs the preparation method of wax, comprises the following steps:
(1) take successively by weight and aliphatic solvents 12 parts, acid montanin wax 7 parts, dimethyl silicone oil 6 parts are put in oil cauldron, under the condition constantly stirred, being warming up to 80 DEG C, treating that material dissolution is complete transparent liquid, constant temperature 15 minutes;
(2) by weight deionized water 54.9 parts, 2 parts, tensio-active agent, polyvalent alcohol 5 parts, polishing powder 10 parts are joined in emulsification pot, be heated to 80 DEG C while stirring, constant temperature 5 minutes;
(3) start the high-speed mixing equipment of emulsification pot, the material in oil cauldron was extracted in emulsification pot at 5 minutes, react 30 minutes at 80 DEG C, then 70 DEG C are cooled to, add thickening material 2 parts, sanitas 1 part, pigment 0.1 part, continue high-speed stirring 5 minutes, get product after the assay was approved.
Embodiment 7.
The aqueous environment protection automobile finish of the present embodiment repairs wax, comprises the component of following weight part:
Environment-friendly type aliphatic solvents 10 parts, acid montanin wax 8 parts, dimethyl silicone oil 7 parts, 2 parts, tensio-active agent, polyvalent alcohol 3 parts, polishing powder 15 parts, thickening material 4 parts, sanitas 1 part, pigment 0.1 part, deionized water 49.9 parts.
The aqueous environment protection automobile finish of the present embodiment repairs the preparation method of wax, comprises the following steps:
(1) take successively by weight and aliphatic solvents 10 parts, acid montanin wax 8 parts, dimethyl silicone oil 7 parts are put in oil cauldron, under the condition constantly stirred, being warming up to 90 DEG C, treating that material dissolution is complete transparent liquid, constant temperature 5 minutes;
(2) by weight deionized water 49.9 parts, 2 parts, tensio-active agent, polyvalent alcohol 3 parts, polishing powder 15 parts are joined in emulsification pot, be heated to 80 DEG C while stirring, constant temperature 5 minutes;
(3) start the high-speed mixing equipment of emulsification pot, the material in oil cauldron was extracted in emulsification pot at 5 minutes, react 25 minutes at 85 DEG C, then 65 DEG C are cooled to, add thickening material 4 parts, sanitas 1 part, pigment 0.1 part, continue high-speed stirring 5 minutes, get product after the assay was approved.
The functional parameter that the aqueous environment protection automobile finish that the present invention obtains repairs wax is as shown in the table:
| Interventions Requested | Index |
| Outward appearance | Uniform and smooth body of paste |
| Smell | Original wax taste |
| Color | Golden yellow |
| Glossiness | Increase by more than 12 |
| Hydrophobicity (contact angle) | Be greater than 100 ° |
| Detersive power | By force |
| Scratch removal | Fine scratches can be repaired |
| Lacquer painting fillibility | Microscopic spaces can be filled |
| Automotive Paint Film Properties is affected | Nothing |
The invention provides a kind of aqueous environment protection automobile finish and repair wax, the primary solvent composition of this wax is deionized water, and only containing a small amount of environment-friendly type solvent, thus this wax is in construction process, and the volatilization of solvent pollutes air ambient hardly.In addition, this automobile finish is repaired wax and has been possessed the over-all propertieies such as decontamination, glazing, protection, scratch removal and lacquer painting filling, for car detailing maintenance market provides the product of a excellent performance, has the wide market space.
Above content is in conjunction with concrete preferred implementation further description made for the present invention, can not assert that specific embodiment of the invention is confined to these explanations.It should be pointed out that for those skilled in the art, under the prerequisite not departing from the technology of the present invention principle, can also make some improvement and modification, these all should be considered as protection scope of the present invention.
Claims (10)
1. aqueous environment protection automobile finish repairs a wax, it is characterized in that: the component comprising following weight part:
Environment-friendly type aliphatic solvents 5-20 part
Acid montanin wax 1-10 part
Dimethyl silicone oil 1-10 part
Tensio-active agent 1-5 part
Polyvalent alcohol 1-5 part
Polishing powder 5-20 part
Thickening material 1-5 part
Sanitas 0.1-1 part
Pigment 0.01-0.1 part
Deionized water 30-70 part.
2. aqueous environment protection automobile finish according to claim 1 repairs wax, it is characterized in that: the component comprising following weight part:
Environment-friendly type aliphatic solvents 5-15 part
Acid montanin wax 1-5 part
Dimethyl silicone oil 1-5 part
Tensio-active agent 1-3 part
Polyvalent alcohol 1-3 part
Polishing powder 5-15 part
Thickening material 1-3 part
Sanitas 0.1-0.5 part
Pigment 0.01-0.05 part
Deionized water 30-50 part.
3. aqueous environment protection automobile finish according to claim 1 repairs wax, it is characterized in that: the component comprising following weight part:
Environment-friendly type aliphatic solvents 15-20 part
Acid montanin wax 5-10 part
Dimethyl silicone oil 5-10 part
Tensio-active agent 3-5 part
Polyvalent alcohol 3-5 part
Polishing powder 15-20 part
Thickening material 3-5 part
Sanitas 0.5-1 part
Pigment 0.05-0.1 part
Deionized water 50-70 part.
4. aqueous environment protection automobile finish according to claim 1-3 any one repairs wax, it is characterized in that: described environment-friendly type aliphatic solvents is any one or two or more mixtures in tasteless kerosene D40, tasteless kerosene D60, Isopars L.
5. aqueous environment protection automobile finish according to claim 1-3 any one repairs wax, it is characterized in that: described acid montanin wax is any one or two or more mixtures in Ke Laien S wax, Ke Laien LP wax, Ke Laien OP wax.
6. aqueous environment protection automobile finish according to claim 1-3 any one repairs wax, it is characterized in that: described dimethyl silicone oil is any one or two or more mixtures in DOW CORNING PMX-200 silicone oil 100cs, DOW CORNING PMX-200 silicone oil 350cs, DOW CORNING PMX-200 silicone oil 1000cs, DOW CORNING PMX-200 silicone oil 12500cs.
7. aqueous environment protection automobile finish according to claim 1-3 any one repairs wax, it is characterized in that: described tensio-active agent is any one or two or more mixtures in GP200, A165, tween/this dish composite emulsifying system, oleic acid/morpholine composite emulsifying system.
8. the aqueous environment protection automobile finish according to claim 1-3 any one repairs wax, it is characterized in that: described polyvalent alcohol is any one or two or more mixtures in ethylene glycol, propylene glycol, glycerol, described polishing powder is any one or two or more mixtures in kaolin, diatomite, quartz sand.
9. the aqueous environment protection automobile finish according to claim 1-3 any one repairs wax, it is characterized in that: described thickening material is inorganic or organic thickening agent, described sanitas is Sodium Benzoate, potassium sorbate or KF-88, and described pigment is water-soluble bloom or water-soluble rouge and powder.
10. the aqueous environment protection automobile finish described in claim 1-3 any one repairs the preparation method of wax, it is characterized in that: comprise the following steps:
(1) take by weight and aliphatic solvents, acid montanin wax, dimethyl silicone oil are put in oil cauldron, under the condition constantly stirred, being warming up to 80-95 DEG C, treating that material dissolution is complete transparent liquid, constant temperature 5-30 minute;
(2) by weight deionized water, tensio-active agent, polyvalent alcohol, polishing powder are joined in emulsification pot, be heated to 70-90 DEG C while stirring, constant temperature 5-30 minute;
(3) high-speed mixing equipment of emulsification pot is started, material in oil cauldron was extracted in emulsification pot at 2-10 minute, 10-60 minute is reacted at 60-90 DEG C, then 60-80 DEG C is cooled to, add thickening material, sanitas, pigment, continue high-speed stirring 2-10 minute, get product after the assay was approved.
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| CN201510472907.2A CN105086566A (en) | 2015-08-05 | 2015-08-05 | Water-based environment-friendly automotive paint surface repairing wax and preparing method thereof |
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| CN201510472907.2A CN105086566A (en) | 2015-08-05 | 2015-08-05 | Water-based environment-friendly automotive paint surface repairing wax and preparing method thereof |
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| CN106893552A (en) * | 2015-12-17 | 2017-06-27 | 辽宁法库陶瓷工程技术研究中心 | A kind of aqueous three-in-one automobile grinding agent and preparation method |
| CN107227115A (en) * | 2016-03-23 | 2017-10-03 | 江阴樱花梦家庭用品有限公司 | A kind of sprayability liquid car Wax composition and preparation method thereof |
| CN108774594A (en) * | 2018-06-30 | 2018-11-09 | 江南大学 | A kind of selfreparing detergent and preparation method thereof |
| CN109852258A (en) * | 2017-11-30 | 2019-06-07 | 菏泽海诺知识产权服务有限公司 | A kind of decontamination wax and preparation method thereof |
| CN111234710A (en) * | 2020-02-20 | 2020-06-05 | 广州赫厉狮森汽车用品有限公司 | Automobile paint surface protective wax and preparation method thereof |
| CN113698872A (en) * | 2021-08-27 | 2021-11-26 | 广州赫厉狮森汽车用品有限公司 | Water-based environment-friendly automobile paint repair wax and preparation method thereof |
| CN114437877A (en) * | 2022-01-18 | 2022-05-06 | 江西瑞思博新材料有限公司 | Automobile hub oil stain cleaning agent and preparation method thereof |
| CN114806399A (en) * | 2022-04-28 | 2022-07-29 | 广东优贝科技股份有限公司 | Automobile paint surface glaze and preparation method thereof |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106893552A (en) * | 2015-12-17 | 2017-06-27 | 辽宁法库陶瓷工程技术研究中心 | A kind of aqueous three-in-one automobile grinding agent and preparation method |
| CN107227115A (en) * | 2016-03-23 | 2017-10-03 | 江阴樱花梦家庭用品有限公司 | A kind of sprayability liquid car Wax composition and preparation method thereof |
| CN109852258A (en) * | 2017-11-30 | 2019-06-07 | 菏泽海诺知识产权服务有限公司 | A kind of decontamination wax and preparation method thereof |
| CN108774594A (en) * | 2018-06-30 | 2018-11-09 | 江南大学 | A kind of selfreparing detergent and preparation method thereof |
| CN111234710A (en) * | 2020-02-20 | 2020-06-05 | 广州赫厉狮森汽车用品有限公司 | Automobile paint surface protective wax and preparation method thereof |
| CN113698872A (en) * | 2021-08-27 | 2021-11-26 | 广州赫厉狮森汽车用品有限公司 | Water-based environment-friendly automobile paint repair wax and preparation method thereof |
| CN114437877A (en) * | 2022-01-18 | 2022-05-06 | 江西瑞思博新材料有限公司 | Automobile hub oil stain cleaning agent and preparation method thereof |
| CN114806399A (en) * | 2022-04-28 | 2022-07-29 | 广东优贝科技股份有限公司 | Automobile paint surface glaze and preparation method thereof |
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Application publication date: 20151125 |