CN102849880A - 一种用于油田废弃物综合处理的方法 - Google Patents
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Abstract
本发明公开了一种用于油田废弃物综合处理的方法，其特点是它包括清洗分离、超声分离、调质脱稳、油水分离、离心分离、混拌固化、气浮选分离、吸附过滤、絮凝沉淀、氧化电解、深度净化和渗透过滤工艺步骤；使油田废弃物得以分类处理利用，使污油回收、固相达到油田污泥处理设计规范（SY/T6851-2012)排放标准或制作建材再次利用；液相经水处理后达到GB8978-1996污水综合排放标准。
Description
技术领域
本发明涉及油田废弃物的处理和利用技术，尤其是一种用于钻井废弃物综合处理的工艺技术。
背景技术
油田勘探、开发、钻井过程中产生大量由钻井岩屑、泥浆、污水、污油形成的混合物-钻井废弃物、含油废弃物，传统的处置方式是排放在井场的泥浆污水池中，按照池内就地处理办法进行固化处理，以减少其污染危害；由于泥浆污水储存池渗漏、溢池等存在长期的污染隐患；目前废弃钻井液处理产生的污泥已列入为危险废物，废物类别HW08，废物代码为071-002-08。面对更加严格的环保标准，油田废弃物的综合处理势在必行；现对油田废弃物的治理主要以固化为主，按目前的标准已不符合环保要求。
发明内容
本发明的目的是克服上述已有技术的不足，而提供一种用于油田废弃物综合处理的方法，主要解决现有的油田废弃物采用的固化处理不符合环保要求的问题。
本发明的技术方案是：一种用于油田废弃物综合处理的方法，其特殊之处在于它包括清洗分离、超声分离、调质脱稳、油水分离、离心分离、混拌固化、气浮选分离、吸附过滤、絮凝沉淀、氧化电解、深度净化和渗透过滤工艺步骤；
所述清洗分离，是将油田废弃物中的钻井废弃物回收后，首先进入清洗分离系统，在清洗分离系统内加水，混合后，加入分离剂，在罐内循环搅拌后，通过振动筛筛分的固相输送到混拌固化系统，固相在混拌固化系统内投入苦土粉、石灰、硫酸亚铁混合后，输出达到环保排放的固相物质；振动筛筛分的液相进入调质脱稳系统；
所述超声分离，是将油田废弃物中的含油废弃物回收后，首先与蒸汽混合，温度达到80℃后进入超声波固液分离系统，超声波固液分离系统悬浮液体输送到调质脱稳系统，超声波固液分离系统上浮的油输送到油水分离器；
所述调质脱稳，在调质脱稳系统内与加入200ppm的破乳剂，充分混合絮凝后，由离心泵输送到两相分离系统进行两相分离；
所述油水分离，超声分离分离出的油经油水分离器分离出的水进入调质脱稳系统，分离出的油进入三相分离系统；
所述离心分离，在两相分离系统的离心机的离心分离下，分离出的固相输送到混拌固化系统，分离出的液相泵送到气浮选分离系统；在三相分离系统，经三相离心机分离出的油输送到储油罐储存，分离出的水泵送到气浮选分离系统；
所述混拌固化，固相在混拌固化系统内投入苦土粉、石灰、硫酸亚铁混合后，输出达到环保排放的固相物质；
所述气浮选分离，进入气浮选分离系统的水中的浮油，在溶汽气浮装置下，装置气压0.4-0.6Mpa，油上浮，输送到三相分离系统；下部混合液输送到吸附过滤系统；
所述吸附过滤，进入吸附过滤系统内的水经其内部活性炭的吸附作用去除水中色度、ss，处理后的水输送到絮凝沉淀系统；
所述絮凝沉淀，水与在絮凝沉淀系统内加入浓度0.3%絮凝剂PAM，混合絮凝、沉淀后输送到氧化电解系统；
所述氧化电解，水在氧化电解系统内首先加酸经PH调节到3-4后，在高级氧化及铁碳微电解作用下去除水中的有机物，经氧化电解处理后的水输送到深度净化系统；
所述深度净化，水在深度净化系统内首先加入碱将PH调到6-7，去除水中ss、色度和TDM，经深度净化系统处理的水输送到渗透过滤系统；
所述渗透过滤，水在渗透过滤系统内在活性炭过滤、纤维过滤，进一步去除水的有机物、ss、色度等，使水达标排放。
其中，清洗分离步骤所述钻井废弃物与水的体积比1：3；所述分离剂为混合物体积的20%。
其中，超声分离步骤所述含油废弃物为含固浓度为20%的含油废水，超声系统的超声频率为25HZ。
其中，油水分离步骤采用卧螺离心机2000-g分离。
其中，混拌固化步骤所述的苦土粉、石灰、硫酸亚铁的重量比为2:1:1
本发明所述的一种用于油田废弃物综合处理的方法与已有技术相比具有突出的实质性特点和显著进步，解决油田区域钻井废弃物和含油废弃物的处理和利用问题，采用分离处理，做到水、泥砂、油分离，达标利用，处理量大，可规模化生产，降低系统治理成本，有效解决钻井废弃物及含油废弃物的污染问题，满足油田作业及环境保护的实际需求。
附图说明：
图1是本发明的流程示意图。
具体实施方式：
为了更好地理解与实施，下面结合附图详细说明本发明。
实施例1，参见图１，将油田废弃物中的钻井废弃物回收后，首先进入清洗分离系统，在清洗分离系统内与水1：3体积比混合后，加入混合物体积20%的分离剂，在罐内循环搅拌后，通过振动筛筛分的固相由振动筛下部的螺旋输送器输送到混拌固化系统，固相在混拌固化系统内与投入重量比2:1:1的苦土粉、石灰、硫酸亚铁混合，由下部皮带输送机输出具有一定强度的固相物质，可作为建材原料，经混拌固化的固相，经检测各项指标达到国家排放标准；振动筛筛分的液相进入下部缓存罐后，泵送至调质脱稳系统，在调质脱稳系统内与加入200ppm破乳剂充分混合絮凝后，由离心泵输送到两相离心分离系统，在卧螺离心机2000-g离心分离下，分离出的固相由螺旋输送器输送到混拌固化系统，分离出的液相泵送到气浮分离系统；
将油田废弃物中的含油废弃物回收后，油废弃物为含固浓度为20%的含油废水，首先与蒸汽混合温度达到80℃后进入超声波固液分离系统，超声系统的超声频率为25HZ，在超声波固液分离系统内经超声振动及空化作用下，超声波固液分离系统悬浮液体经下部螺杆泵输送到调质脱稳系统，上浮的油经抽吸器输送到浮油缓存罐后泵送到油水分离系统由油水分离机进行油水分离，分离出的水输送到调质脱稳系统，分离出的油泵送到三相离心分离系统；经三相离心机分离出的油输送到储油罐储存，待输送给甲方，分离出的水泵送到气浮选分离系统；
进入气浮选分离系统的水中的浮油，在溶汽气浮装置下（气压0.4-0.6Mpa），油上浮，通过撇油器及泵输送到三相分离系统；下部混合液泵送到过滤吸附系统；进入吸附过滤系统内的水经其内部活性炭的吸附作用去除水中色度、ss，处理后的水输送到絮凝沉淀系统；水与在絮凝沉淀系统内加入的浓度0.3%絮凝剂PAM，混合絮凝、沉淀后输送到氧化电解系统；水在氧化电解系统内首先加酸将PH调节到3-4后，常用的酸为盐酸或硫酸，在高级氧化及铁碳微电解作用下去除水中的有机物，经氧化电解处理后的水输送到深度净化系统；水在深度净化系统内首先入碱将PH调到6-7，常用的碱为氢氧化钠，通过深度净化作用，去除水中ss、色度和TDM，经深度净化系统处理的水输送到渗透过滤系统；水在渗透过滤系统内在活性炭过滤、纤维过滤，进一步去除水的有机物、ss、色度等，使水达标排放。
Claims (5)
1.一种用于油田废弃物综合处理的方法，其特征在于它包括清洗分离、超声分离、调质脱稳、油水分离、离心分离、混拌固化、气浮选分离、吸附过滤、絮凝沉淀、氧化电解、深度净化和渗透过滤工艺步骤；
所述清洗分离，是将油田废弃物中的钻井废弃物回收后，首先进入清洗分离系统，在清洗分离系统内加水，混合后，加入分离剂，在罐内循环搅拌后，通过振动筛筛分的固相输送到混拌固化系统，振动筛筛分的液相进入调质脱稳系统；
所述超声分离，是将油田废弃物中的含油废弃物回收后，首先与蒸汽混合，温度达到80℃后进入超声波固液分离系统，超声波固液分离系统悬浮液体输送到调质脱稳系统，超声波固液分离系统上浮的油输送到油水分离器；
所述调质脱稳，在调质脱稳系统内与加入200ppm的破乳剂，充分混合絮凝后，由离心泵输送到两相分离系统进行两相分离；
所述油水分离，超声分离分离出的油经油水分离器分离出的水进入调质脱稳系统，分离出的油进入三相分离系统；
所述离心分离，在两相分离系统的离心机的离心分离下，分离出的固相输送到混拌固化系统，分离出的液相泵送到气浮选分离系统；在三相分离系统，经三相离心机分离出的油输送到储油罐储存，分离出的水泵送到气浮选分离系统；
所述混拌固化，固相在混拌固化系统内投入苦土粉、石灰、硫酸亚铁混合后，输出达到环保排放的固相物质；
所述气浮选分离，进入气浮选分离系统的水中的浮油，在溶汽气浮装置下，装置气压0.4-0.6Mpa，油上浮，输送到三相分离系统；下部混合液输送到吸附过滤系统；
所述吸附过滤，进入吸附过滤系统内的水经其内部活性炭的吸附作用去除水中色度、ss，处理后的水输送到絮凝沉淀系统；
所述絮凝沉淀，水与在絮凝沉淀系统内加入浓度0.3%絮凝剂PAM，混合絮凝、沉淀后输送到氧化电解系统；
所述氧化电解，水在氧化电解系统内首先加酸经PH调节到3-4后，在高级氧化及铁碳微电解作用下去除水中的有机物，经氧化电解处理后的水输送到深度净化系统；
所述深度净化，水在深度净化系统内首先加入碱将PH调到6-7，去除水中ss、色度和TDM，经深度净化系统处理的水输送到渗透过滤系统；
所述渗透过滤，水在渗透过滤系统内在活性炭过滤、纤维过滤，进一步去除水的有机物、ss、色度等，使水达标排放。
2.根据权利要求1所述的一种用于油田废弃物综合处理的方法，其特征在于清洗分离步骤所述钻井废弃物与水的体积比1：3；所述分离剂为混合物体积的20%。
3.根据权利要求1所述的一种用于油田废弃物综合处理的方法，其特征在于超声分离步骤所述含油废弃物为含固浓度为20%的含油废水，超声系统的超声频率为25HZ。
4.根据权利要求1所述的一种用于油田废弃物综合处理的方法，其特征在于油水分离步骤采用卧螺离心机2000-g分离。
5.根据权利要求1所述的一种用于油田废弃物综合处理的方法，其特征在于混拌固化步骤所述的苦土粉、石灰、硫酸亚铁的重量比为2:1:1。
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