CN102807781A - Paint cleaning agent and preparation method thereof - Google Patents

Paint cleaning agent and preparation method thereof Download PDF

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Publication number
CN102807781A
CN102807781A CN2012103051839A CN201210305183A CN102807781A CN 102807781 A CN102807781 A CN 102807781A CN 2012103051839 A CN2012103051839 A CN 2012103051839A CN 201210305183 A CN201210305183 A CN 201210305183A CN 102807781 A CN102807781 A CN 102807781A
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China
Prior art keywords
out system
clean
fatty acid
acid ester
ethyl acetate
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Application number
CN2012103051839A
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Chinese (zh)
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CN102807781B (en
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刘杰
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Individual
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Individual
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Priority to CN201210305183.9A priority Critical patent/CN102807781B/en
Publication of CN102807781A publication Critical patent/CN102807781A/en
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Publication of CN102807781B publication Critical patent/CN102807781B/en
Expired - Fee Related legal-status Critical Current
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Abstract

The invention relates to a cleaning agent, in particular to a paint cleaning agent which is strong, powerful, economical, high-efficient, energy-saving, environment-friendly, novel and concentrated and a preparation method thereof. The paint cleaning agent is prepared by the following raw materials by weight percent: 15 to 25 percent of dimethoxy dipropylene glycol, 25 to 40 percent of N-methylpyrrolidine, 5 to 8 percent of ethanolamine, 20 to 30 percent of ethyl acetate, 5 to 10 percent of fatty acid ester, 15 to 25 percent of dimethyl ketone and 0.2 percent of fruity essence.

Description

A kind of paint clean-out system and preparation method thereof
Technical field
The present invention relates to a kind of clean-out system, especially a kind of safety brute force, economical and efficient, energy-conserving and environment-protective, novel spissated paint clean-out system and preparation method thereof.
Background technology
The illegal small advertisement sponsor of Chinese city, forever firm for making its small advertisement, also be retained on the buildingss such as city body of wall, road, lighting standard.Use the firm paint of bonding ten minutes to spray.Remove the big chronic disease that the paint spraying advertisement has become the Chinese city management.
China generally adopts the improvement method of paint, coating covering for a long time, and the one, can not thoroughly remove, the 2nd, cause secondary pollution.Therefore be badly in need of inventing that a kind of removing power is strong, safety and environmental protection, novel spissated green painting clean-out system come beautifying urban environment thoroughly to solve the city management chronic disease.
Summary of the invention
The present invention is directed to a kind of technical problem of above-mentioned paint proposition safe brute force, economical and efficient, energy-conserving and environment-protective, novel spissated paint clean-out system and preparation method thereof are provided.
This paint clean-out system is to carry out hybrid reaction through dipropylene glycol dme, N-Methyl pyrrolidone, ethanol ammonia, ethyl acetate, fatty acid ester, dimethyl ketone and fruital essential oil with the ratio of following quality percentage composition to process:
Dipropylene glycol dme 15-25%;
N-Methyl pyrrolidone 25-40%;
Ethanol ammonia 5-8%;
Ethyl acetate 20-30%;
Fatty acid ester 5-10%;
Dimethyl ketone 15-25%;
Fruital essential oil 0.2%.
Preferably, this clean-out system is to be to be carried out hybrid reaction by 20% dipropylene glycol dme, 25% N-Methyl pyrrolidone, 5.8% ethanol ammonia, 22% ethyl acetate, 7% fatty acid ester, 20% dimethyl ketone, 0.2% fruital essential oil and processed by massfraction by said clean-out system.
Preferably, the nanometer Margarita powder that also adds 0.01-0.05% in the said paint clean-out system.
The present invention also provides a kind of method for preparing above-mentioned paint clean-out system, and it comprises the steps:
The first step takes by weighing dipropylene glycol dme, N-Methyl pyrrolidone, ethanol ammonia, 22% ethyl acetate, fatty acid ester, dimethyl ketone, fruital essential oil in proportion and packs in the airtight mixing vessel, under 30-40 ℃ of normal pressure, mixes one hour;
Second step added nanometer Margarita powder again, and stirring reaction is 30 minutes under the environmental stress of 2-5MPa, after mixing, carries out forming product behind the filtration, purification.
This technical scheme compared with prior art has following beneficial effect:
The cleansing power of this clean-out system is strong, noresidue, safety economy, energy-conserving and environment-protective, novel concentrating, and is used for the removal fully that matrix (being generally crust) is coated paint, does not damage stromal surface.Add the part green solvent and the micro-nano green factor, make clean-out system environmental protection more, more efficient, dissolve peeling painting, coating more fast, wetting, emulsification, cleaning function are stronger, and stability is better, more helps the antiredeposition of dirt.
Specific embodiment
This paint clean-out system provided by the present invention, it is processed with the mixed reaction of following quality percentage composition through dipropylene glycol dme, N-Methyl pyrrolidone, ethanol ammonia, ethyl acetate, fatty acid ester, dimethyl ketone and fruital essential oil:
Dipropylene glycol dme 15-25%; N-Methyl pyrrolidone 25-40%; Ethanol ammonia 5-8%; Ethyl acetate 20-30%; Fatty acid ester 5-10%; Dimethyl ketone 15-25%; Fruital essential oil 0.2%.
Wherein, fatty ester is that propylene glycol fatty acid ester is by lipid acid and 1,2 one Ucar 35 esterification reaction and get, and products therefrom is the mixture of monoesters and dibasic acid esters, can obtain the Ucar 35 mono fatty acid ester through short-path distillation again; Parts such as the flower of fruital essential oil through the plant of fruit fragrance, leaf, root, skin, stem, branch, fruit, seed; The oily mater that take to distill, method such as squeezing, extraction, absorption makes with characteristic perfume; In order to prolong its work-ing life; Let its effect keep for a long time; The long-acting natural phant lasting agent with sustained release performance that can also prepare through advanced person's high molecular nanometer microencapsulation technology at present, just industrial essence, the mask agent of using always in a kind of heavy chemicals field.
Below with the preparation 100KG the paint clean-out system specify this paint clean-out system provided by the present invention with and concrete preparation method.
Embodiment 1:
The fruital essential oil of dimethyl ketone and 0.2KG that takes by weighing fatty acid ester, the 20KG of ethyl acetate, the 7KG of ethanol ammonia, the 22KG of N-Methyl pyrrolidone, the 5.8KG of dipropylene glycol dme, the 25KG of 20KG is respectively packed in the airtight mixing vessel; Utilization mixing tank or similar variable-ratio machine (having suitable general the mixing and kneading operation of thruster) stirred one hour under 30 ℃ of normal pressures; Add then and contain the 0.005Kg nanometer Margarita powder; Stirring reaction is 30 minutes under the environmental stress of 2MPa, carries out filtration, purification formation product after 2 hours until mixing the back quiescent setting.
Embodiment 2:
The fruital essential oil of dimethyl ketone 0.4KG that takes by weighing fatty acid ester, the 30KG of ethyl acetate, the 10KG of ethanol ammonia, the 40KG of N-Methyl pyrrolidone, the 15.6KG of dipropylene glycol dme, the 54KG of 50KG is respectively packed in the airtight mixing vessel; Utilization mixing tank or similar variable-ratio machine (having suitable general the mixing and kneading operation of thruster) stirred one hour under 40 ℃ of normal pressures; Add then and contain the 0.005Kg nanometer Margarita powder; Stirring reaction is 30 minutes under the environmental stress of 5MPa, carries out filtration, purification formation product after 2 hours until mixing the back quiescent setting.
Method of use in the face of this paint clean-out system describes down:
This paint clean-out system adopts special-purpose aerosol jar splendid attire; Spray gun is cleaned apart from cleaning thing 10-15CM scope internal spraying; Stop 5-7 at scavenger surface and permeate decomposition second, wipe residual dirt with wet towel then, clean as new scavenger surface will come into view; Run into the dirty seal of obstinate serious color and will prolong and soak the reaction times and can prove effective, can add the place, slit and extend shower nozzle and clean.
Above disclosedly be merely some preferred embodiments of the present invention, can not limit the present invention's interest field certainly with this, the equivalent variations of therefore doing according to claim of the present invention still belongs to the scope that the present invention is contained.

Claims (4)

1. one kind is painted clean-out system, and it carries out hybrid reaction through dipropylene glycol dme, N-Methyl pyrrolidone, ethanol ammonia, ethyl acetate, fatty acid ester, dimethyl ketone and fruital essential oil with the ratio of following quality percentage composition and processes:
Dipropylene glycol dme 15-25%;
N-Methyl pyrrolidone 25-40%;
Ethanol ammonia 5-8%;
Ethyl acetate 20-30%;
Fatty acid ester 5-10%;
Dimethyl ketone 15-25%;
Fruital essential oil 0.2%.
2. paint clean-out system as claimed in claim 1; It is characterized in that it is to be carried out hybrid reaction by 20% dipropylene glycol dme, 25% N-Methyl pyrrolidone, 5.8% ethanol ammonia, 22% ethyl acetate, 7% fatty acid ester, 20% dimethyl ketone, 0.2% fruital essential oil and processed by massfraction by said clean-out system.
3. paint clean-out system as claimed in claim 1 is characterized in that, also adds the nanometer Margarita powder of 0.01-0.05% in the said paint clean-out system.
4. method for preparing like the said paint clean-out system of claim 3, it comprises the steps:
The first step takes by weighing dipropylene glycol dme, N-Methyl pyrrolidone, ethanol ammonia, 22% ethyl acetate, fatty acid ester, dimethyl ketone, fruital essential oil in proportion and packs in the airtight mixing vessel, under 30-40 ℃ of normal pressure, mixes one hour;
Second step added nanometer Margarita powder again, and stirring reaction is 30 minutes under the environmental stress of 2-5MPa, after mixing, carries out forming product behind the filtration, purification.
CN201210305183.9A 2012-08-24 2012-08-24 Preparation method of paint cleaning agent Expired - Fee Related CN102807781B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201210305183.9A CN102807781B (en) 2012-08-24 2012-08-24 Preparation method of paint cleaning agent

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201210305183.9A CN102807781B (en) 2012-08-24 2012-08-24 Preparation method of paint cleaning agent

Publications (2)

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CN102807781A true CN102807781A (en) 2012-12-05
CN102807781B CN102807781B (en) 2014-12-10

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105331178A (en) * 2015-12-03 2016-02-17 关勇河 Cleaning agent and preparing method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2001064549A (en) * 1999-08-27 2001-03-13 Shinzen:Kk Method for peeling transfer image
US20060234890A1 (en) * 2005-04-15 2006-10-19 Ecolab Inc. Stripping floor finishes using composition that thickens following dilution with water
CN1944547A (en) * 2006-10-11 2007-04-11 中国化工建设总公司常州涂料化工研究院 Paint remover and its preparing method and using method
CN101319105A (en) * 2008-07-18 2008-12-10 东南大学 Paint stripper of oil emulsion-in-water

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2001064549A (en) * 1999-08-27 2001-03-13 Shinzen:Kk Method for peeling transfer image
US20060234890A1 (en) * 2005-04-15 2006-10-19 Ecolab Inc. Stripping floor finishes using composition that thickens following dilution with water
CN1944547A (en) * 2006-10-11 2007-04-11 中国化工建设总公司常州涂料化工研究院 Paint remover and its preparing method and using method
CN101319105A (en) * 2008-07-18 2008-12-10 东南大学 Paint stripper of oil emulsion-in-water

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
刘杰: "一种新型无毒脱漆剂的研究", 《四川化工》, vol. 15, no. 3, 31 March 2012 (2012-03-31), pages 4 - 6 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105331178A (en) * 2015-12-03 2016-02-17 关勇河 Cleaning agent and preparing method thereof

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Granted publication date: 20141210

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CF01 Termination of patent right due to non-payment of annual fee