CN102793641A - Preparation method of beautyberry herbal mouth wash - Google Patents

Abstract

The invention discloses a preparation method of beautyberry herbal mouth wash. The preparation method comprises the following steps of: (1) holding medicinal materials such as beautyberry, honeysuckle, stevia rebaudianum, mulberry leaf and peppermint leaf in a cooking vacuum tank and adding water to cook for 2 hours to take the liquid medicine; (2) sieving the liquid medicine with gauze to remove residues and fading with active carbon to obtain liquid medicine for later use; (3) pouring pure water into a dried vacuum tank and then adding the liquid medicine extracted by the step (2) when heating to 60 DEG C; (4) continuously stirring mixture of the pure water and the liquid medicine of the step (3), raising temperature to 80 DEG C and adding essence and preservative; (5) continuously stirring mixture of the step (4), raising temperature to 85 DEG C and stopping; (6) pouring the mixed solution of the step (5) into a large container for storage, cooling to constant temperature and preparing to sub-package; (7) performing sampling inspection; (8) sub-packaging qualified products and marking the production date and the batch number on the outer packages; and (9) warehousing. The beautyberry herbal mouth wash has the effects of bacteriostasis, hemostasia, pain easing, inflammation diminishing, improvement on gum bleeding, gum swelling, oral ulcer, gingival atrophy and periodontitis and protection of teeth.

Description

The method for preparing of Callicarpa nudiflora draft collutory

Technical field

The present invention relates to a kind of method for preparing of Callicarpa nudiflora draft collutory.

Background technology

Callicarpa nudiflora (callicarpanudifloraHook.exArn) is Verenaceae (Verbenaceae) Callicarpa plant, and main product is a kind of Hainan authentic medicinal herbs in China Hainan, and also there is distribution in China Guangdong, Guangxi.Mainly be distributed in India, Vietnam and Malaysia abroad.Its root, leaf can be used as medicine, and antibacterial anti hemorrhagic is arranged, eliminating inflammation and expelling toxin, and dissipating blood stasis for subsidence of swelling, effects such as wind-expelling and dispelling dampness cure mainly diseases such as suppurative inflammation, acute infectious hepatitis, respiratory tract and digestive tract hemorrhage, wound hemorrhage, and burn and traumatic hemorrhage etc. are controlled in external.

Though what big problem the oral inflammation that gingival hemorrhage, oral ulcer, alimentary canal inflammation etc. cause, halitosis etc. are not, taking place often will be to causing no small puzzlement people's orthobiosis.At present, because people's life step is very fast, cause the oral inflammation odds very high, the crowd of generation is also very general.Therefore, how to reduce and avoid these troubles of bothering people's daily life often, it is just extremely urgent to the needs of healthy and high-quality life to satisfy the present stage people.

Summary of the invention

The method for preparing that the purpose of this invention is to provide a kind of Callicarpa nudiflora draft collutory; That the Callicarpa nudiflora draft collutory that this method for preparing obtains has is antibacterial, hemostasis, analgesia, antiinflammatory, improve gingival hemorrhage, gingival swelling and pain, oral ulcer, gingival atrophy, periodontitis, and characteristics such as take care of one's teeth.

To achieve these goals, technical scheme of the present invention is: a kind of method for preparing of Callicarpa nudiflora draft collutory is provided, may further comprise the steps:

(1) the material Callicarpa nudiflora 200～400kg that gets it filled, Flos Lonicerae 15～25 kg, Flos Chrysanthemi 15～25kg, Folium Mori 50～60kg, mentha leave 50～60 kg put into the steaming and decocting vacuum tank, add 2 hours taking liquids of water 5000 kg steaming and decoctings;

(2) medicinal liquid sieves with gauze and removes slag, and fades with active carbon then, and it is subsequent use to get medicinal liquid;

(3) pour in the exsiccant vacuum tank when heating to 60 ℃ behind the pure water and add the medicinal liquid that step (2) obtains, wherein the volume ratio of pure water and medicinal liquid is 7～9:1;

(4) pure water of continuous whipping step (3) and the amalgam of medicinal liquid add essence and antiseptic when being warming up to 80 ℃;

(5) amalgam of continuous whipping step (4) stops when being warming up to 85 ℃;

(6) pour the mixed liquor in the step (5) into bulk container interior storage to cooling off constant temperature preparation packing;

(7) sampling inspection;

What (8) be up to the standards carries out packing, outer package date of manufacture, lot number;

(9) warehouse-in.

That Callicarpa nudiflora draft collutory of the present invention has is antibacterial, hemostasis, analgesia, antiinflammatory, improve gingival hemorrhage, gingival swelling and pain, oral ulcer, gingival atrophy, periodontitis, takes care of one's teeth.

The specific embodiment

Embodiment 1150ml/ bottle

(1) the material Callicarpa nudiflora 200kg that gets it filled, Flos Lonicerae 15 kg, Flos Chrysanthemi 15 kg, Folium Mori 50 kg, mentha leave 50 kg put into the steaming and decocting vacuum tank, add 2 hours taking liquids of water 5000 kg steaming and decoctings;

(2) medicinal liquid sieves with gauze and removes slag, and fades with active carbon then, and it is subsequent use to get medicinal liquid;

(3) pour in the exsiccant vacuum tank and add the 18ml medicinal liquid that step (2) obtains when heating to 60 ℃ behind the pure water of 131.5ml;

(4) pure water of continuous whipping step (3) and the amalgam of medicinal liquid add 0.15ml essence and 0.35ml antiseptic when being warming up to 80 ℃;

(5) amalgam of continuous whipping step (4) stops when being warming up to 85 ℃;

(6) pour the mixed liquor in the step (5) into bulk container interior storage to cooling off constant temperature preparation packing;

(7) sampling inspection;

What (8) be up to the standards carries out packing, outer package date of manufacture, lot number; Ascertaining the reason of disqualified upon inspection, if antibacterial exceed standard get back to step (4) inspection, get back to step (3) inspection if medicinal liquid is underproof;

(9) warehouse-in.

Embodiment 2 1000ml/ bottles

(1) the material Callicarpa nudiflora 300kg that gets it filled, Flos Lonicerae 20 kg, Flos Chrysanthemi 20 kg, Folium Mori 55 kg, mentha leave 55 kg put into the steaming and decocting vacuum tank, add 2 hours taking liquids of water 5000 kg steaming and decoctings;

(2) medicinal liquid sieves with gauze and removes slag, and fades with active carbon then, and it is subsequent use to get medicinal liquid;

(3) pour in the exsiccant vacuum tank and add the 118ml medicinal liquid that step (2) is extracted when heating to 60 ℃ behind the pure water of 880ml;

(4) pure water of continuous whipping step (3) and the amalgam of medicinal liquid add 0.5ml essence and 1.5ml antiseptic when being warming up to 80 ℃;

(5) amalgam of continuous whipping step (4) stops when being warming up to 85 ℃;

(6) pour the mixed liquor in the step (5) into bulk container interior storage to cooling off constant temperature preparation packing;

(7) sampling inspection;

What (8) be up to the standards carries out packing, outer package date of manufacture, lot number; Ascertaining the reason of disqualified upon inspection, if antibacterial exceed standard get back to step (4) inspection, get back to step (3) inspection if medicinal liquid is underproof;

(9) warehouse-in.

With 100 artificial subjects of suffering from various oral diseases such as gingival hemorrhage, gingival swelling and pain, oral ulcer, gingival atrophy, periodontitis; Adopting for each person every day sooner or later adopts this collutory to gargle once; About a 10ml, after gargling 8-10 days, the experimenter gargles, and 85%-95% patient takes effect obviously behind the collutory of the present invention; 5%-6% patient takes effect generally, and 2%-3% patient shows improvement.Ten days is a course of treatment, connects to gargle 3-4 the course of treatment.

It below is the drug inspection statement of entrusting Hainan Pharmaceutical Factory Co., Ltd. to provide

Hainan Pharmaceutical Factory Co., Ltd.'s drug inspection account

Statement numbering: ZF120709

Above disclosedly be merely preferred embodiment of the present invention, can not limit the present invention's interest field certainly with this, the equivalent variations of therefore doing according to claim of the present invention still belongs to the scope that the present invention is contained.

Claims (1)

1. the method for preparing of a Callicarpa nudiflora draft collutory is characterized in that may further comprise the steps:

(1) the material Callicarpa nudiflora 200～400kg that gets it filled, Flos Lonicerae 15～25 kg, Flos Chrysanthemi 15～25kg, Folium Mori 50～60kg, mentha leave 50～60 kg put into the steaming and decocting vacuum tank, add 2 hours taking liquids of water 5000 kg steaming and decoctings;

(2) medicinal liquid sieves with gauze and removes slag, and fades with active carbon then, and it is subsequent use to get medicinal liquid;

(3) pour in the exsiccant vacuum tank when heating to 60 ℃ behind the pure water and add the medicinal liquid that step (2) obtains, wherein the volume ratio of pure water and medicinal liquid is 7～9:1;

(4) pure water of continuous whipping step (3) and the amalgam of medicinal liquid add essence and antiseptic when being warming up to 80 ℃;

(5) amalgam of continuous whipping step (4) stops when being warming up to 85 ℃;

(6) pour the mixed liquor in the step (5) into bulk container interior storage to cooling off constant temperature preparation packing;

(7) sampling inspection;

What (8) be up to the standards carries out packing, outer package date of manufacture, lot number;

(9) warehouse-in.