CN105535590A - Traditional Chinese medicinal mouthwash for treating gingival bleeding and preparation method of traditional Chinese medicinal mouthwash - Google Patents

Traditional Chinese medicinal mouthwash for treating gingival bleeding and preparation method of traditional Chinese medicinal mouthwash Download PDF

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CN105535590A
CN105535590A CN201510995023.5A CN201510995023A CN105535590A CN 105535590 A CN105535590 A CN 105535590A CN 201510995023 A CN201510995023 A CN 201510995023A CN 105535590 A CN105535590 A CN 105535590A
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folium
chinese medicine
parts
schreib
traditional chinese
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张敏
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/88—Liliopsida (monocotyledons)
    • A61K36/899—Poaceae or Gramineae (Grass family), e.g. bamboo, corn or sugar cane
    • A—HUMAN NECESSITIES
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    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A—HUMAN NECESSITIES
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    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/21—Amaranthaceae (Amaranth family), e.g. pigweed, rockwort or globe amaranth
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
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    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/44—Ebenaceae (Ebony family), e.g. persimmon
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    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
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    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/70—Polygonaceae (Buckwheat family), e.g. spineflower or dock
    • A61K36/704—Polygonum, e.g. knotweed
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    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/71—Ranunculaceae (Buttercup family), e.g. larkspur, hepatica, hydrastis, columbine or goldenseal
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    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/76—Salicaceae (Willow family), e.g. poplar
    • A—HUMAN NECESSITIES
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    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/77—Sapindaceae (Soapberry family), e.g. lychee or soapberry
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    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/85—Verbenaceae (Verbena family)
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    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/87—Vitaceae or Ampelidaceae (Vine or Grape family), e.g. wine grapes, muscadine or peppervine
    • A—HUMAN NECESSITIES
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    • A61K36/898—Orchidaceae (Orchid family)
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    • A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/30—Macromolecular organic or inorganic compounds, e.g. inorganic polyphosphates
    • A61K47/36—Polysaccharides; Derivatives thereof, e.g. gums, starch, alginate, dextrin, hyaluronic acid, chitosan, inulin, agar or pectin
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    • A61K9/00—Medicinal preparations characterised by special physical form
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    • A61K9/0053—Mouth and digestive tract, i.e. intraoral and peroral administration
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    • A61K2236/30—Extraction of the material
    • A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
    • A61K2236/333—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
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    • A61K2236/50—Methods involving additional extraction steps
    • A61K2236/53—Liquid-solid separation, e.g. centrifugation, sedimentation or crystallization

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Abstract

The invention relates to a traditional Chinese medicinal composition, in particular to a traditional Chinese medicinal mouthwash for treating gingival bleeding and a preparation method of the traditional Chinese medicinal mouthwash. The preparation method comprises the following steps of grinding and crushing Chinese soapberry fruit, folium ilicis cornutae, herba alternantherae, cardamine hirsute, persimmon leaf, Japanese cayratia herb, narrowleaf screwtree root, salix leaf, digitaria ischaemum, taiwan beautyberry leaf and herba pyrola, adding the mixture into a container of which the volume is 50 to 70 times the volume of the mixture; introducing water vapor with the temperature of 285 to 300DEG C and the pressure of 8 to 10MPa; treating for 3 to 5 minutes, then immediately placing the treated traditional Chinese medicinal powder into ethanol with the concentration of 80 to 85 percent, wherein the ratio of materials is 1: (6-8); stirring at the ultrasonic temperature of 55 to 58DEG C for 14 to 16 minutes; stirring at the ultrasonic temperature of 115 to 120DEG C for 50 to 80s, filtering to remove residues, and obtaining filtrate; adding guar gum of which the weight is 3 to 5 percent of that of the filtrate, uniformly stirring, sealing and canning.

Description

A kind of Chinese medicine gargle for the treatment of gingival hemorrhage and preparation method thereof
Technical field
The present invention relates to a kind of Chinese medicine composition, be specifically related to a kind of Chinese medicine gargle for the treatment of gingival hemorrhage and preparation method thereof.
Background technology
Gingival hemorrhage is one of department of stomatology common sympton, and what refer to that gingiva is idiopathic or cause due to minimal irritation bleeds on a small quantity.The lighter show as only sucking, brush teeth, when chewing harder food in saliva with the blood streak, severe one is when gingiva is subject to minimal irritation and hemorrhage more even hematostaxis, the development of periodontal disease is hidden very much, Silent Neuritis progress in early days, but periodontal disease can not spontaneous recovery, when by the time there is the symptom such as pain, swelling, much more to belong to late period, early stage gingivitis is treated not in time, periodontal ligament is attacked, support that the alveolar bone of tooth is destroyed and absorb, also there will be halitosis, gingiva pyorrhea, even can cause loosening and coming off of tooth.
Summary of the invention
The object of the present invention is to provide a kind of Chinese medicine gargle for the treatment of gingival hemorrhage and preparation method thereof.
Technical solution of the present invention is as follows, a kind of Chinese medicine gargle for the treatment of gingival hemorrhage and preparation method thereof, is made up of according to weight fraction following component:
Fructus Sapindi Mukouossi 3-5 part, Folium Ilicis Cornutae 10-12 part, Alternanthera sessilis (L.) DC. 10-15, Hairy Bittercress 15-20 part, Folium Kaki 1-3 part, Herba Cayatiae Japonicae 4-7 part, Radix Helicteris 1-2 part, Folium Salicis Babylonicae 5-8 part, part, Digitaria ischaemum (Schreib.) Schreib. Ex Mubl. 1-3 part, Folium Callicarpae Formosanae 5-7 part, Herba pyrolae japonicae 8-12 part.
By Fructus Sapindi Mukouossi, Folium Ilicis Cornutae, Alternanthera sessilis (L.) DC., Hairy Bittercress, Folium Kaki, Herba Cayatiae Japonicae, Radix Helicteris, Folium Salicis Babylonicae, Digitaria ischaemum (Schreib.) Schreib. Ex Mubl., Folium Callicarpae Formosanae, Herba pyrolae japonicae is ground to 80-100 order, obtain Chinese medicine powder, Chinese medicine powder is put into the container of its 50-70 times volume, passing into temperature is 285-300 DEG C, pressure is the steam of 8-10MPa, process after 3-5 minute, Chinese medicine powder after process is put into the ethanol that concentration is 80-85% immediately, material ratio is 1:6 ~ 8, 14-16 minute is stirred by the stir speed (S.S.) of 300-350r/min at ultrasonic temperature is 55-58 DEG C, 50-80s is stirred by the stir speed (S.S.) of 300-350r/min at ultrasonic temperature is 115-120 DEG C, filter and remove residue, obtain filtrate, the guar gum of filtrate weight 3%-5% is added in filtrate, stir, sealing tinning.
In side of the present invention, Fructus Sapindi Mukouossi, Folium Salicis Babylonicae, Alternanthera sessilis (L.) DC. synergism has clearing away heat and cooling blood, effect of detumescence and drawing out poison, Folium Ilicis Cornutae, Folium Kaki, Folium Callicarpae Formosanae is collaborative have antibacterial, effect of antiinflammatory, Herba Cayatiae Japonicae, Digitaria ischaemum (Schreib.) Schreib. Ex Mubl., Radix Helicteris, Herba pyrolae japonicae synergism, there is hemostasis, promoting tissue regeneration by removing blood stasis, effect of nourishing the liver and kidney, each raw material is by reasonable component compatibility, synergism, to halitosis, gingival hemorrhage, periodontal tissue's pathological changes such as gingival swelling and pain have significant therapeutic effect, manufacture method is simple, easy to use, collutory can effectively rest on gingiva place, reach thorough sterilization, the effect of antiinflammatory, life-time service can be repaired and rebuild alveolar bone, eliminate periodontal disease, set up new dental bed basis, firm tooth.
Detailed description of the invention
Embodiment 1, a kind of Chinese medicine gargle for the treatment of gingival hemorrhage, by Fructus Sapindi Mukouossi 3 parts, Folium Ilicis Cornutae 10 parts, Alternanthera sessilis (L.) DC. 10, Hairy Bittercress 15 parts, Folium Kaki 1 part, Herba Cayatiae Japonicae 4 parts, Radix Helicteris 1 part, Folium Salicis Babylonicae 5 parts, part, Digitaria ischaemum (Schreib.) Schreib. Ex Mubl. 1 part, Folium Callicarpae Formosanae 5 parts, Herba pyrolae japonicae 8 parts, by Fructus Sapindi Mukouossi, Folium Ilicis Cornutae, Alternanthera sessilis (L.) DC., Hairy Bittercress, Folium Kaki, Herba Cayatiae Japonicae, Radix Helicteris, Folium Salicis Babylonicae, Digitaria ischaemum (Schreib.) Schreib. Ex Mubl., Folium Callicarpae Formosanae, Herba pyrolae japonicae is ground to 80 orders, obtain Chinese medicine powder, Chinese medicine powder is put into the container of its 50 times of volumes, passing into temperature is 285 DEG C, pressure is the steam of 8MPa, process after 3 minutes, Chinese medicine powder after process is put into the ethanol that concentration is 80% immediately, material ratio is 1:6, 14 minutes are stirred by the stir speed (S.S.) of 300r/min at ultrasonic temperature is 55 DEG C, 50s is stirred by the stir speed (S.S.) of 300r/min at ultrasonic temperature is 115 DEG C, filter and remove residue, obtain filtrate, the guar gum of filtrate weight 3% is added in filtrate, stir, sealing tinning.
Embodiment 2, a kind of Chinese medicine gargle for the treatment of gingival hemorrhage, by Fructus Sapindi Mukouossi 5 parts, Folium Ilicis Cornutae 12 parts, Alternanthera sessilis (L.) DC. 15, Hairy Bittercress 20 parts, Folium Kaki 3 parts, Herba Cayatiae Japonicae 7 parts, Radix Helicteris 2 parts, Folium Salicis Babylonicae 8 parts, Digitaria ischaemum (Schreib.) Schreib. Ex Mubl. 3 parts, Folium Callicarpae Formosanae 7 parts, Herba pyrolae japonicae 12 parts, by Fructus Sapindi Mukouossi, Folium Ilicis Cornutae, Alternanthera sessilis (L.) DC., Hairy Bittercress, Folium Kaki, Herba Cayatiae Japonicae, Radix Helicteris, Folium Salicis Babylonicae, Digitaria ischaemum (Schreib.) Schreib. Ex Mubl., Folium Callicarpae Formosanae, Herba pyrolae japonicae is ground to 100 orders, obtain Chinese medicine powder, Chinese medicine powder is put into the container of its 70 times of volumes, passing into temperature is 300 DEG C, pressure is the steam of 10MPa, process after 5 minutes, Chinese medicine powder after process is put into the ethanol that concentration is 85% immediately, material ratio is 1:8, 16 minutes are stirred by the stir speed (S.S.) of 350r/min at ultrasonic temperature is 58 DEG C, 80s is stirred by the stir speed (S.S.) of 350r/min at ultrasonic temperature is 120 DEG C, filter and remove residue, obtain filtrate, the guar gum of filtrate weight 5% is added in filtrate, stir, sealing tinning.
Collutory therapeutic effect of the present invention is set forth further below by way of concrete case.
Case 1, money, man, 32;
Main suit: gingival hemorrhage 3 years when patient brushes teeth, occasionally has spontaneous hemorrhage, brushes teeth every day 2 times, oral cavity free from extraneous odour.
Check: poor oral hygiene, gingiva color is red, and matter is soft, rear odontoseisis, periodontal pyorrhea, gingival recession.
Treatment: gargle with clear water after meal, then adopt collutory of the present invention to rinse, rinse three every day, continuous flushing is after seven days, and gingiva is no longer hemorrhage, and halitosis disappears, continuous flushing, after one month, checks further, gingiva pinkiness, glossy, matter is tough and tensile, and suggestion patient can adopt collutory of the present invention to gargle (generally once a day) for a long time, to ensure gingiva and dental health, follow up a case by regular visits to 1 year, without recurrence, gingiva meets health standards.
Case 2, Zhang, man, 40 years old;
Main suit: lower anterior teeth gingival hemorrhage 1 month;
Check: see that lower labial teeth has dental calculus, swelling and aching of gum.
Treatment: gargle with clear water after meal, then adopt collutory of the present invention to rinse, rinse three every day, continuous flushing is after seven days, and gingiva is no longer hemorrhage, and swelling disappears, continuous flushing, after 30 days, checks further, gingiva pinkiness, glossy, matter is tough and tensile, and dental calculus is thin out, suggestion patient can adopt collutory of the present invention to gargle (generally once a day) for a long time, to ensure gingiva and dental health, follows up a case by regular visits to half a year, without recurrence, dental calculus disappears, and gingiva meets health standards.
Case 3, Zhu, female, 25 years old;
, there is halitosis in main suit: hemorrhage when gingiva is brushed teeth often in this year, and nearly January, lower labial teeth place had pyorrhea to go out.
Check: red swelling of gingiva, gently leans out blood, and deep periodontal pocket is about in 4-5mm pus.
Treatment: gargle with clear water after meal, then adopt collutory of the present invention to rinse, rinse three every day, continuous flushing is after 15 days, and gingiva is no longer hemorrhage, and red and swollen halitosis disappears, gingiva is pyorrhea no longer, and continuous flushing, after 30 days, checks further, gingiva pinkiness, glossy, matter is tough and tensile, suggestion patient can adopt collutory of the present invention to gargle (generally once a day) for a long time, to ensure gingiva and dental health, follows up a case by regular visits to 1 year, without recurrence, gingiva meets health standards.
Case 4, grandson, female, 20 years old;
Main suit: lower-left tooth has the cavity several years, without sense of discomfort, because chewing hard object, there is pain in tooth, and serious gradually, and pain came to go to a doctor after 3 days;
Check: lower-left 6 dental caries loosen, root tip is red and swollen, lays one's hand on pain, left surface buccal edema, body temperature 38 degree;
Treatment: gargle with clear water after meal, adopt collutory of the present invention to rinse again, rinse three every day, continuous flushing is after three days, tooth is pain no longer, facial edema disappears, and temperature recovery is normal, continuous flushing 7 days, root redness disappears, continuous flushing, after 2 months, checks further, gingiva pinkiness, glossy, matter is tough and tensile, and tooth recovers normal, and suggestion patient can adopt collutory of the present invention to gargle (generally once a day) for a long time, to ensure gingiva and dental health, follow up a case by regular visits to 1 year, without recurrence, gingiva meets health standards.
Case 5, Wang, man, 42 years old;
Main suit: lower labial teeth brush teeth and laboratory rodent chow easily hemorrhage, continue about 1 one months;
Check: lower incisor cervical region tartar 1 degree deposition, gingiva hyperemia is rubescent, and quality is soft, and edge is thick blunt, and gum nipple circle is blunt, and loose face light, gingival sulcus gently leans out blood.
Treatment: gargle with clear water after meal, collutory of the present invention is adopted to rinse again, rinse three every day, continuous flushing is after five days, and gingiva is no longer hemorrhage, continuous flushing 10 days, root hyperemia disappears, and continuous flushing is after 2 months, and dental calculus disappears, further inspection, gingiva pinkiness, glossy, matter is tough and tensile, tooth recovers normal, suggestion patient can adopt collutory of the present invention to gargle (generally once a day) for a long time, to ensure gingiva and dental health, follows up a case by regular visits to 3 months, without recurrence, gingiva meets health standards.

Claims (4)

1. treat a Chinese medicine gargle for gingival hemorrhage, it is characterized in that, described collutory is made up of the raw material of Chinese medicine of following parts by weight:
Fructus Sapindi Mukouossi 3-5 part, Folium Ilicis Cornutae 10-12 part, Alternanthera sessilis (L.) DC. 10-15, Hairy Bittercress 15-20 part, Folium Kaki 1-3 part, Herba Cayatiae Japonicae 4-7 part, Radix Helicteris 1-2 part, Folium Salicis Babylonicae 5-8 part, part, Digitaria ischaemum (Schreib.) Schreib. Ex Mubl. 1-3 part, Folium Callicarpae Formosanae 5-7 part, Herba pyrolae japonicae 8-12 part.
2. a kind of Chinese medicine gargle for the treatment of gingival hemorrhage according to claim 1, it is characterized in that, described collutory is made up of the raw material of Chinese medicine of following parts by weight:
Fructus Sapindi Mukouossi 4 parts, Folium Ilicis Cornutae 11 parts, Alternanthera sessilis (L.) DC. 12, Hairy Bittercress 18 parts, Folium Kaki 2 parts, Herba Cayatiae Japonicae 6 parts, Radix Helicteris 1.4 parts, Folium Salicis Babylonicae 6 parts, part, Digitaria ischaemum (Schreib.) Schreib. Ex Mubl. 2 parts, Folium Callicarpae Formosanae 6 parts, Herba pyrolae japonicae 10 parts.
3. the manufacture method of the Chinese medicine gargle of a treatment gingival hemorrhage according to claim 1, it is characterized in that, described collutory is when making, by Fructus Sapindi Mukouossi, Folium Ilicis Cornutae, Alternanthera sessilis (L.) DC., Hairy Bittercress, Folium Kaki, Herba Cayatiae Japonicae, Radix Helicteris, Folium Salicis Babylonicae, Digitaria ischaemum (Schreib.) Schreib. Ex Mubl., Folium Callicarpae Formosanae, Herba pyrolae japonicae is ground to 80-100 order, obtain Chinese medicine powder, Chinese medicine powder is put into the container of its 50-70 times volume, passing into temperature is 285-300 DEG C, pressure is the steam of 8-10MPa, process after 3-5 minute, Chinese medicine powder after process is put into the ethanol that concentration is 80-85% immediately, material ratio is 1:6 ~ 8, 14-16 minute is stirred by the stir speed (S.S.) of 300-350r/min at ultrasonic temperature is 55-58 DEG C, 50-80s is stirred by the stir speed (S.S.) of 300-350r/min at ultrasonic temperature is 115-120 DEG C, filter and remove residue, obtain filtrate, the guar gum of filtrate weight 3%-5% is added in filtrate, stir, sealing tinning.
4. a kind of manufacture method for the treatment of the Chinese medicine gargle of gingival hemorrhage according to claim 3, it is characterized in that, described collutory is when making, by Fructus Sapindi Mukouossi, Folium Ilicis Cornutae, Alternanthera sessilis (L.) DC., Hairy Bittercress, Folium Kaki, Herba Cayatiae Japonicae, Radix Helicteris, Folium Salicis Babylonicae, Digitaria ischaemum (Schreib.) Schreib. Ex Mubl., Folium Callicarpae Formosanae, Herba pyrolae japonicae is ground to 90 orders, obtain Chinese medicine powder, Chinese medicine powder is put into the container of its 60 times of volumes, passing into temperature is 290 DEG C, pressure is the steam of 9MPa, process after 4 minutes, Chinese medicine powder after process is put into the ethanol that concentration is 83% immediately, material ratio is 1:7, 15 minutes are stirred by the stir speed (S.S.) of 320r/min at ultrasonic temperature is 57 DEG C, 70s is stirred by the stir speed (S.S.) of 330r/min at ultrasonic temperature is 117 DEG C, filter and remove residue, obtain filtrate, the guar gum of filtrate weight 4% is added in filtrate, stir, sealing tinning.
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* Cited by examiner, † Cited by third party
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