CN102754728B - Blueberry, black fungus and carrot composite jelly and preparation method thereof - Google Patents

Blueberry, black fungus and carrot composite jelly and preparation method thereof Download PDF

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CN102754728B
CN102754728B CN 201210266056 CN201210266056A CN102754728B CN 102754728 B CN102754728 B CN 102754728B CN 201210266056 CN201210266056 CN 201210266056 CN 201210266056 A CN201210266056 A CN 201210266056A CN 102754728 B CN102754728 B CN 102754728B
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carrot
blueberry
black fungus
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water
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CN102754728A (en
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陈福存
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Great Khingan Xing'an Organic Food Co Ltd
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Great Khingan Xing'an Organic Food Co Ltd
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Abstract

The invention provides blueberry, black fungus and carrot composite jelly and a preparation method thereof, relates to composite jelly and a preparation method thereof, and aims at solving the problems of poor taste, complicated preparation process and high cost of the existing lead removing functional food. The jelly is prepared from blueberry juice, black fungus, carrot, gelatin, pectin, sodium alginate, white granulated sugar, high fructose corn syrup, nitric acid and water. The preparation method comprises the following steps: 1, weighing the blueberry juice, the black fungus, the carrot, the gelatin, the pectin, the sodium alginate, the white granulated sugar, the high fructose corn syrup, the nitric acid and the water in a mass percentage; 2, cooking; 3, decocting; 4, standing; 5, pouring a mold and forming; and 6, drying to obtain the blueberry, black fungus and carrot composite jelly. The jelly is fruit and vegetable jelly with a function of promoting lead removal, and the preparation method is applied to the blueberry industry.

Description

A kind of blueberry, black fungus, the compound soft sweets of carrot and preparation method thereof
Technical field
The present invention relates to a kind of compound soft sweets and preparation method thereof.
Background technology
Along with the fast development of China's modern industry and Modern Traffic industry, the environment lead contamination is on the rise.Lead is a kind of pewter metal, belong to nondegradable environmental contaminants, in environment, can accumulate for a long time, mainly advance people's human body by food, soil, water and air per os, part is accumulated in human body, cause the infringement of system such as human nerve, hematopoiesis, immunity, digestion, growth and each organ aspect of human body to some extent, more seriously lead loss is hindered brain functions such as infant's cognition and neurobehavioral, influence growth and intelligence development.Particularly children ' s lead poisoning is worldwide popular, has caused social concerns.Science Times report China big industrialization city has 85% children to surpass lead poisoning standard 100 μ g/L at present, is in asymptomatic sub-clinical state.Lead how to get rid of body accumulation becomes the focus of concern.
Lead can directly be absorbed in vivo, is distributed in blood, soft tissue (as kidney, marrow, dried dirty, brain) and the mineralized tissue (bone and tooth).The lead content that enters human circulation through food intake mainly depends on plumbous chemistry and the form of physics, and organism physiological property at that time, for example nutrition condition [calcium in the human body, iron, zinc, vitamin (mainly be VC, VB), the level of fat and protein) and age etc.Lead enters to be drained behind the human body extremely slowly, and bone plumbous about 20 years of biological half-life, plumbous biological half-life is longer in the cortex bone.Even the environment lead concentration is down to below the permissible value, long-term a small amount of plumbous institute that absorbs causes that the cumulative bad infringement also is difficult to avoid, so by reducing the plumbous prevention of environment lead poisoning the human body infringement is still disliked not enough merely.
Functional food is historical later China's development, and lead-expelling function food just begins to research and develop in recent years.Existing lead-expelling function food is because preparation cost is high and complex process and price is higher, and mouthfeel is general, is not easy to be accepted by masses.How developing a kind of popular, food economic, that have lead-expelling function, is the thing that needs to be resolved hurrily.
Summary of the invention
The objective of the invention is to solve that existing lead-expelling function food mouthfeel is poor, complicated process of preparation and the high problem of cost, and provide a kind of blueberry, black fungus, the compound soft sweets of carrot and preparation method thereof.
Blueberry, black fungus, the compound soft sweets of carrot are to be prepared from by 12.5 ~ 22.5 portions of white granulated sugars, 7 ~ 15 parts of HFCSs, 40 ~ 50 parts of water, 8 ~ 16 parts of gelatin, 0.6 ~ 1.4 part of pectin, 0.2 ~ 0.6 part of sodium alginate, 0.5 ~ 2.5 part of citric acid, 6 ~ 14 parts of blueberry juice, 1 ~ 5 portion of carrot juice, 0.6 ~ 1.4 portion of black fungus and 0.005 ~ 0.025 part of vitamin C by mass fraction.
The preparation method of above-mentioned blueberry, black fungus, the compound soft sweets of carrot is to carry out according to the following steps:
One, blueberry, carrot juice are produced: take by weighing the rotten blueberry of nothing and really carry out squeezing the juice after flowing water cleans, it is standby to obtain blueberry juice; Choosing does not have the carrot of rotting, and cleans, and is cut into piece then and squeezes the juice, and it is standby to obtain carrot juice;
Two, the preparation of black fungus piece: get dried black fungus and place 40~50 ℃ of water to soak 15~20min, remove the base of a fruit then, clean, dry surface moisture, stripping and slicing;
Three, take by weighing raw material: take by weighing 0.005 ~ 0.025 part of 0.6 ~ 1.4 part of the black fungus of 1 ~ 5 part of 6 ~ 14 parts in blueberry juice, carrot juice, step 2 preparation of 12.5 ~ 22.5 parts of white granulated sugars, 7 ~ 15 parts of HFCSs, 40 ~ 50 parts in water, 8 ~ 16 parts in gelatin, 0.6 ~ 1.4 part of pectin, 0.2 ~ 0.6 part of sodium alginate, 0.5 ~ 2.5 part of citric acid, step 1 preparation and vitamin C by mass fraction; The white granulated sugar that takes by weighing is divided into three parts of X, Y and Z, and white granulated sugar X: white granulated sugar Y: the mass ratio of white granulated sugar Z is (3 ~ 11): (3 ~ 7): (2 ~ 6); Be four parts of A, B, C and D with the moisture that takes by weighing, water A: water B: water C: the mass ratio of water D is (2 ~ 10): (16 ~ 32): (3 ~ 7): (10 ~ 30);
Four, infusion: white granulated sugar X, HFCS and water A that step 3 is taken by weighing put into the container mixing, and being heated to temperature is 115 ℃~125 ℃, continues infusion 10 ~ 20min again after all dissolving, and obtains syrup;
Five, the gelatin that step 3 is taken by weighing adds water among the B, heats in container, and being heated to temperature is 45 ~ 55 ℃, and gelatin is all dissolved, and is cooled to room temperature then, obtains frozen glue;
Six, pectin, white granulated sugar Y and the water C that takes by weighing in the step 3 put into the container mixing, being heated to temperature is 80 ~ 90 ℃, and pectin is dissolved fully, mixes with syrup in the step 3 then, obtains mixing molasses L;
Seven, sodium alginate and the white granulated sugar Z that takes by weighing in the step 3 put into the container mixing, add water D after, be that water-bath joins temperature then and is among 70 ~ 80 ℃ the mixing molasses L to dissolving in 70 ℃ the water bath in temperature, obtain mixing molasses M behind the mixing;
Eight, the temperature of mixing molasses M is down to 60~70 ℃, add the frozen glue that step 4 obtains then, after stirring 5 ~ 15min all dissolves frozen glue, add citric acid, blueberry juice, carrot juice, auricularia auriculajudae piece and vitamin C that step 3 takes by weighing again, after mixing, obtain mixing molasses N;
Nine, adding mass fraction in the mixing molasses N is 5% CaCl 2Solution pours in the template then, leaves standstill gel to the room temperature, obtains gel piece, wherein mixing molasses N and CaCl 2Volume ratio be 100:0.6;
Ten, the gel piece that step 9 is obtained is dry 40~60min under 30~40 ℃ the condition in temperature, obtains blueberry, black fungus, the compound soft sweets of carrot.
Utilization of the present invention has the strong anti-oxidation activity and is added in the candy with the blueberry, black fungus, carrot, pectin and the vitamin C that the promote lead-expelling function major function raw material as soft sweets, selected gelatin, pectin, sodium alginate as gel, the fruits and vegetables soft sweets of preparing mouthfeel, excellent flavor, having the promotion lead-expelling function and have no side effect, compound soft sweets quality softness, the mouthfeel frankness of the present invention preparation, blueberry fragrance is arranged, sense of taste is pure and sweet and sour taste, be easy to be accepted by masses especially children.The primary raw material of the lead-expelling function food that the inventive method is produced is natural food, and cost is lower, and production technology is simple, production, with short production cycle easily.
The specific embodiment:
The specific embodiment one: present embodiment is that a kind of blueberry, black fungus, the compound soft sweets of carrot are to be prepared from by 12.5 ~ 22.5 portions of white granulated sugars, 7 ~ 15 parts of HFCSs, 40 ~ 50 parts of water, 8 ~ 16 parts of gelatin, 0.6 ~ 1.4 part of pectin, 0.2 ~ 0.6 part of sodium alginate, 0.5 ~ 2.5 part of citric acid, 6 ~ 14 parts of blueberry juice, 1 ~ 5 portion of carrot juice, 0.6 ~ 1.4 portion of black fungus and 0.005 ~ 0.025 part of vitamin C by mass fraction.
The present embodiment utilization has the strong anti-oxidation activity and is added in the candy with the blueberry, black fungus, carrot, pectin and the vitamin C that the promote lead-expelling function major function raw material as soft sweets, selected gelatin, pectin, sodium alginate as gel, the fruits and vegetables soft sweets of preparing mouthfeel, excellent flavor, having the promotion lead-expelling function and have no side effect.Fruits and vegetables soft sweets quality softness, the mouthfeel frankness of present embodiment preparation, blueberry fragrance is arranged, sense of taste is pure and sweet and sour taste, be easy to be accepted by masses especially children.
The specific embodiment two: what present embodiment and the specific embodiment one were different is: blueberry, black fungus, the compound soft sweets of carrot are to be prepared from by 16 portions of white granulated sugars, 13 parts of HFCSs, 46 parts of water, 12 parts of gelatin, 0.6 part of pectin, 0.25 part of sodium alginate, 1 part of citric acid, 8 parts of blueberry juice, 2 portions of carrot juices, 1 portion of black fungus and 0.015 part of vitamin C by mass fraction.Other is identical with the specific embodiment one.
The specific embodiment three: the preparation method of a kind of blueberry, black fungus, the compound soft sweets of carrot, the preparation method who it is characterized in that blueberry, black fungus, the compound soft sweets of carrot carries out according to the following steps:
One, blueberry, carrot juice are produced: take by weighing the rotten blueberry of nothing and really carry out squeezing the juice after flowing water cleans, it is standby to obtain blueberry juice; Choosing does not have the carrot of rotting, and cleans, and is cut into piece then and squeezes the juice, and it is standby to obtain carrot juice;
Two, the preparation of black fungus piece: get dried black fungus and place 40~50 ℃ of water to soak 15~20min, remove the base of a fruit then, clean, dry surface moisture, stripping and slicing;
Three, take by weighing raw material: take by weighing 0.005 ~ 0.025 part of 0.6 ~ 1.4 part of the black fungus of 1 ~ 5 part of 6 ~ 14 parts in blueberry juice, carrot juice, step 2 preparation of 12.5 ~ 22.5 parts of white granulated sugars, 7 ~ 15 parts of HFCSs, 40 ~ 50 parts in water, 8 ~ 16 parts in gelatin, 0.6 ~ 1.4 part of pectin, 0.2 ~ 0.6 part of sodium alginate, 0.5 ~ 2.5 part of citric acid, step 1 preparation and vitamin C by mass fraction; The white granulated sugar that takes by weighing is divided into three parts of X, Y and Z, and white granulated sugar X: white granulated sugar Y: the mass ratio of white granulated sugar Z is (3 ~ 11): (3 ~ 7): (2 ~ 6); Be four parts of A, B, C and D with the moisture that takes by weighing, water A: water B: water C: the mass ratio of water D is (2 ~ 10): (16 ~ 32): (3 ~ 7): (10 ~ 30);
Four, infusion: white granulated sugar X, HFCS and water A that step 3 is taken by weighing put into the container mixing, and being heated to temperature is 115 ℃~125 ℃, continues infusion 10 ~ 20min again after all dissolving, and obtains syrup;
Five, the gelatin that step 3 is taken by weighing adds water among the B, heats in container, and being heated to temperature is 45 ~ 55 ℃, and gelatin is all dissolved, and is cooled to room temperature then, obtains frozen glue;
Six, pectin, white granulated sugar Y and the water C that takes by weighing in the step 3 put into the container mixing, being heated to temperature is 80 ~ 90 ℃, and pectin is dissolved fully, mixes with syrup in the step 3 then, obtains mixing molasses L;
Seven, sodium alginate and the white granulated sugar Z that takes by weighing in the step 3 put into the container mixing, add water D after, be that water-bath joins temperature then and is among 70 ~ 80 ℃ the mixing molasses L to dissolving in 70 ℃ the water bath in temperature, obtain mixing molasses M behind the mixing;
Eight, the temperature of mixing molasses M is down to 60~70 ℃, add the frozen glue that step 4 obtains then, after stirring 5 ~ 15min all dissolves frozen glue, add citric acid, blueberry juice, carrot juice, auricularia auriculajudae piece and vitamin C that step 3 takes by weighing again, after mixing, obtain mixing molasses N;
Nine, adding mass fraction in the mixing molasses N is 5% CaCl 2Solution pours in the template then, leaves standstill gel to the room temperature, obtains gel piece, wherein mixing molasses N and CaCl 2Volume ratio be 100:0.6;
Ten, the gel piece that step 9 is obtained is dry 40~60min under 30~40 ℃ the condition in temperature, obtains blueberry, black fungus, the compound soft sweets of carrot.
The primary raw material of the lead-expelling function food of the lead-expelling function food production that present embodiment is produced is natural food, and cost is lower, and production technology is simple, production, with short production cycle easily.
The specific embodiment four: what present embodiment and the specific embodiment three were different is: step 3 is described to take by weighing 0.015 part of 16 parts of white granulated sugars, 13 parts of HFCSs, 46 parts in water, 12 parts in gelatin, 0.6 part of pectin, 0.25 part of sodium alginate, 1 part of citric acid, 8 parts in blueberry juice, 2 parts of carrot juices, 1 part of black fungus and vitamin C by mass fraction.Other is identical with the specific embodiment three.
The specific embodiment five: what present embodiment was different with the specific embodiment three or four is: step 4 described heat time heating time is 15min, and being heated to temperature is 120 ℃.Other is identical with the specific embodiment three or four.
The specific embodiment six: what present embodiment was different with one of specific embodiment three to five is: the described temperature that is heated to of step 5 is 50 ℃.Other are identical with one of specific embodiment three to five.
The specific embodiment seven: what present embodiment was different with one of specific embodiment three to six is: the described temperature that is heated to of step 6 is 85 ℃.Other are identical with one of specific embodiment three to six.
The specific embodiment eight: what present embodiment was different with one of specific embodiment three to seven is: the described mixing time of step 8 is 15min.Other are identical with one of specific embodiment three to seven.
The specific embodiment nine: what present embodiment was different with one of specific embodiment three to eight is: the described baking temperature of step 10 is 30 ℃, and be 60min drying time.Other are identical with one of specific embodiment three to eight.
By following verification experimental verification effect of the present invention:
The preparation method of test 1, blueberry, black fungus, the compound soft sweets of carrot:
The preparation method of a kind of blueberry of this test, black fungus, the compound soft sweets of carrot is undertaken by following steps:
One, blueberry, carrot juice are produced: take by weighing the rotten blueberry of nothing and really carry out squeezing the juice after flowing water cleans, it is standby to obtain blueberry juice; Choosing does not have the carrot of rotting, and cleans, and is cut into piece then and squeezes the juice, and it is standby to obtain carrot juice;
Two, the preparation of black fungus piece: get dried black fungus and place 40~50 ℃ of water to soak 15~20min, remove the base of a fruit then, clean, spread out then in desktop, dry surface moisture, stripping and slicing;
Three, take by weighing raw material: take by weighing 0.015 part of 16 parts of white granulated sugars, 13 parts of HFCSs, 46 parts in water, 12 parts in gelatin, 0.6 part of pectin, 0.25 part of sodium alginate, 1 part of citric acid, 8 parts in blueberry juice, 2 parts of carrot juices, 1 part of black fungus and vitamin C by mass fraction;
Four, infusion: 10.5 portions of white granulated sugars, 13 parts of HFCSs and 2.5 parts of water that step 3 takes by weighing are put into the container mixing, and being heated to temperature is 115 ℃~125 ℃, continues infusion 10 ~ 20min again after all dissolving, and obtains syrup.
Five, the mass ratio by gelatin and water is that 1:2 adds the gelatin that step 3 takes by weighing in 24 parts of water, heats in container, and being heated to temperature is 45 ~ 55 ℃, and gelatin is all dissolved, and is cooled to room temperature then, obtains frozen glue;
Six, the 0.6 part of pectin that takes by weighing in the step 3,3 portions of white granulated sugars and 6 parts of water are put into the container mixing, being heated to temperature is 85 ℃, and pectin is dissolved fully, mixes with syrup in the step 3 then, obtains mixing molasses L;
Seven, 0.25 part of sodium alginate and 2.5 portions of white granulated sugars of taking by weighing in the step 3 are put into the container mixing, after adding 12.5 parts of water, be that water-bath joins temperature then and is among 70 ~ 80 ℃ the mixing molasses L to dissolving in 70 ℃ the water bath in temperature, obtain mixing molasses M behind the mixing;
Eight, the temperature of mixing molasses M is down to 60~70 ℃, add the frozen glue that step 4 obtains then, after stirring 15min all dissolves frozen glue, add citric acid, blueberry juice, carrot juice, auricularia auriculajudae piece and vitamin C that step 3 takes by weighing again, after mixing, obtain mixing molasses N;
Nine, the adding mass fraction is 5% CaCl 2, pour into then in the template, leave standstill gel to the room temperature, obtain gel piece, wherein mixing molasses N and CaCl 2Volume ratio be 100:0.6;
Ten, the gel piece that step 7 is obtained is dry 60min under 30 ℃ the condition in temperature, obtains blueberry, black fungus, the compound soft sweets of carrot.
The blueberry of this test one, black fungus and carrot are the commercially available prod.There is the composition of personnel appraise group of sensory evaluation experience that the compound soft sweets of blueberry, black fungus, carrot that obtain are carried out appraise by 10, organoleptic quality to product is carried out overall merit, and product appearance is regular, and size evenly, glossiness redness, the black fungus unanimity that is evenly distributed; Has the distinctive flavour of blueberry and fragrance, free from extraneous odour; The sweet acid of sugar body is suitable, and agreeable to the taste chewiness, elasticity and toughness are arranged; Transparence, sugar-free is separated out, and is smooth neat, the visible impurity of no naked eyes.The blueberry of this test 1, black fungus and carrot are the commercially available prod.
The physical and chemical index of the blueberry of this test preparation, black fungus, the compound soft sweets of carrot is as follows:
Solid content 〉=75%; Moisture≤24%; Reduced sugar 35%~40%; Copper (Cu)≤10mg/kg; Plumbous (pb)≤1.0mg/kg; Total arsenic (in As)≤0.5mg/kg.
The microbiological indicator of the blueberry of this test preparation, black fungus, the compound soft sweets of carrot is as follows:
Total plate count≤1000CFU/g, coliform≤90MPN/100g, pathogenic bacteria (salmonella, Shigella, staphylococcus aureus) must not detect.
The test 2, to testing the animal experiment that 1 soft sweets that obtain carry out the lead discharging effect
Experimental condition:
Select for use Male Kunming strain mice to be divided into blank group, model control group, low dosage feeding group (1g/kg.bw at random, quite 2.45 times of the human body recommended amounts), middle dosage feeding group (2g/kg.bw, quite 4.90 times of the human body recommended amounts), high dose feeding group (4g/kg.bw, quite 9.80 times of the human body recommended amounts) 5 groups, 12 every group; Wherein the body weight of Male Kunming strain mice is 18~22g, available from central laboratory of Harbin Pharmaceutical General Factory.
Test method:
Adopt the plumbous animal model of preventative height.Except the blank group is freely drunk the deionized water, all the other four groups equal freely drinking contain 0.1% acetate trihydrate lead [Pb (CH 3COO) 23H 2O] deionized water solution (Pb 2+Concentration is 546.2mg/L), change liquid weekly 1~2 time.Basic, normal, high dosage group gives given the test agent by last dosage setting respectively simultaneously and irritates stomach, and blank group and model control group are irritated stomach and given the equal-volume deionized water, continuously 30d.After last was irritated stomach 24h, about eyeball blood sampling 1.00g, disconnected neck was put to death mouse, gets liver 0.20g, a side femur, with the red fuming nitric acid (RFNA) of 3:1 (v/v): the perchloric acid hot digestion, measure blood lead, liver lead, femur lead content with graphite furnace atomic absorption spectrometry.Measure omnidistance freeze-drying blood lead, zinc, the copper standard substance that uses national standard material center to produce and carry out quality control, per 12 sample measuring space reference materials once.
Result of the test:
(1) blueberry, black fungus, the compound soft sweets of carrot are to the influence of mouse body weight
Table 1 blueberry, black fungus, carrot lead discharging health care soft sweet to the influence of mouse body weight (X ± SD, n=12)
Figure BDA00001949298600061
By table 1 as seen, there was no significant difference (P>0.05) between initial body weight, whole opisthosoma weigh between each dosage group and the control group.Be that blueberry, black fungus, carrot lead discharging health care soft sweet do not have the conspicuousness influence to rat body weight.
(2) blueberry, black fungus, the compound soft sweets of carrot are to mouse blood lead and the plumbous influence of tissue
Blueberry, black fungus, the compound soft sweets of carrot see Table 2 and table 3 to mouse blood lead and the plumbous influence of tissue.Blood lead in the his-and-hers watches 2, liver lead, femur lead content carry out homogeneity test of variance, find heterogeneity of variance, therefore above-mentioned data are carried out number conversion, data in must table 3, homogeneity test of variance shows that variance is neat, adopt one-way analysis of variance totally to compare, find between blood lead, liver lead, plumbous each group of femur overall more variant (the P value is O, 000).Further carry out comparing in twos of a plurality of dosage groups and model control group mean with the Dunnett method, find that three dosage group blood leads, liver lead content all significantly are lower than model control group, and the bone lead content is not made significant difference.
Table 2 blood lead and organize plumbous measurement result (X ± SD)
Table 3 blood lead and organize lead content logarithm conversion value
Figure BDA00001949298600072
Test 2 results and show that per os gives mouse blueberry, black fungus, the compound soft sweets 1.0g/kgbw of carrot, 2.0g/kgbw, 4.Og/kgbw(and is equivalent to 2.45,4.90,9.80 times of human body recommended amounts respectively) 30d, three dosage all can significantly reduce the plumbous and hepatic tissue lead of mouse whole blood, and mouse bone lead content does not make significant difference.By the promotion lead-expelling function criterion in " health food check and assessment technique standard ", blueberry, black fungus, carrot lead discharging health care soft sweet have the promotion lead-expelling function to animal.
The test 3, to test 1 soft sweets that obtain carry out the lead discharging effect human trial
Experimental condition:
Being tried into the person has plumbous contact history, and Pb-B is 25~50 years old professional population more than 200 μ g/L.Get rid of experimenter's standard: suffer from systemic disease persons such as cardiovascular, liver, kidney and hemopoietic system; Gestation and women breast-feeding their children; Take the article relevant with being tried function in a short time, have influence on the judgement person to the result; Withdraw given the test agent or add other medicines midway, can't judge the experimenter that effect or data are incomplete.
Test method:
Counter point between own control and group is adopted in this test, and satisfactory 104 examples are subjected to the examination adult, is divided into blueberry, black fungus, carrot compound soft sweets test-meal group and blank group, test-meal group 52 examples, control group 52 examples randomly according to blood lead, lead in urine level.The compound soft sweets test-meal of blueberry, black fungus, carrot is formed edible certain kind of berries people's every day, black fungus, the compound soft sweets of carrot 2 times, and each 10g continues 30d.Control group does not apply any processing factor, and two groups are normal diet, and does not change eating habit at ordinary times.
Before the test all are tried to be grown up and carried out conventional physical examination and necessary laboratory examination.Comprise general situation such as spirit, sleep, diet, stool and urine, blood pressure, blood, routine urianlysis, liver, kidney function test, Abdominal B type ultrasonography, Chest X-rays, Electrocardioscopy (every index in pretest inspection once), the mensuration of urine calcium, urine zinc (is measured before the test-meal respectively and 10d, 20d, 30d urine calcium, urine zinc after the test-meal, three measurement results after the merging test-meal are carried out statistical analysis).
The record cardinal symptom before and after the test-meal of being tried to be grown up, the main symptoms such as dizziness, insomnia, weakness of limbs of observing, by light (1 minute), in (2 minutes), weigh (3 minutes) and add up integration respectively; Gather before test-meal front and back blood and the test-meal and the 24h urine specimen of test-meal 10d, 2Od and 30d, measure blood lead, lead content in urine.Total lead in urine is three lead in urine measured value sums.
Result of the test:
(1) two group is subjected to the preceding every index of examination adult test-meal test
Situation relatively as table 4 test-meal test was last
Figure BDA00001949298600081
Two groups are subjected to the preceding every index of examination adult test-meal test to see Table 4.As shown in Table 4, two groups are subjected to the preceding every index no significant difference of examination adult test-meal test, have comparativity.
(2) security is observed:
Blood routine examination result before and after the table 5 test-meal test (X ± S)
Figure BDA00001949298600091
Laboratory examination result (X scholar S) before and after the table 6 test-meal test
Figure BDA00001949298600092
Total urine calcium discharge rate compares (mg/L, X scholar S) before and after the table 7 test-meal test
Example number (people) Urine calcium before the test Test back total urine calcium
The test-meal group 52 263.4 the scholar 102.1 761.7 soil 190.8
Control group 52 275.9 the scholar 113.3 787.8 the scholar 195.9
P value (between group) - 0.5558 0.4929
Total urine zinc discharge rate compares (mg/L, X scholar S) before and after the table 8 test-meal test
Example number (people) Urine calcium before the test Test back total urine calcium
The test-meal group 52 0.54 soil 0.22 1.77 the scholar 0.63
Control group 52 0.56 the scholar 0.30 1.67 the scholar 0.60
P value (between group) - 0.6991 0.4091
From table 5, table 6 as seen, routine blood test, blood pressure, heart rate, liver function, the renal function of testing back test-meal group and control group checked that each index does not have obvious change, check result is all in range of normal value.Harmful effect is not also found in routine urinalysis, Abdominal B type ultrasonography, Chest X-rays, Electrocardioscopy.By table 7, table 8 as seen, after the test-meal test, the test-meal group is always urinated calcium, is always urinated zinc discharge rate and control group relatively, no significant difference (P>0.05).Illustrate that black fungus, carrot lead discharging health care soft sweet are harmless to health.
(3) effect is observed:
Clinical symptoms integration situations of change (X scholar S) before and after the table 9 test-meal group test-meal test
Example number (people) Before the test-meal After the test-meal P value (self)
Dizzy 52 1.63 the scholar 0.71 1.27 soil 0.45 ** 0.000
Insomnia 52 1.48 the scholar O.64 1.25 the scholar 0.44 ** O.000
Weakness of limbs 52 1.54 the scholar 0.67 1.39 the scholar 0.53 * 0.018
Annotate: *For with test-meal before relatively, P<0.01; *For comparing P<0.05 with control group.
Clinical symptoms integration situations of change (X scholar S) before and after the table 10 control group test-meal test
Example number (people) Before the test-meal After the test-meal P value (self)
Dizzy 52 1.69 the scholar 0.67 1.67 soil 0.68 0.883
Insomnia 52 1.50 the scholar O.67 1.50 the scholar 0.64 1.000
Weakness of limbs 52 1.56 the scholar 0.72 1.56 the scholar 0.70 0.159
10d lead in urine discharge rate compares (μ g/L, X scholar S) before and after the table 11 test-meal test
Example number (people) Before the test-meal After the test-meal P value (self)
The test-meal group 52 177.4 the scholar 88.3 192.4 soil 93.7 0.307
Control group 52 195.0 the scholar 92.5 193.3 the scholar 90.9 O.901
P value (between group) - 0.3233 0.9064
20d lead in urine discharge rate compares (μ g/L, X scholar S) before and after the table 12 test-meal test
Example number (people) Before the test-meal After the test-meal P value (self)
The test-meal group 52 177.4 the scholar 88.3 229.6 soil 93.7 **# 0.000
Control group 52 195.0 the scholar 92.5 194.0 the scholar 83.5 O.793
P value (between group) - 0.3233 0.0419
Annotate: *For with test-meal before relatively, P<0.01; #For comparing P<0.05 with control group.
30d lead in urine discharge rate compares (μ g/L, X scholar S) before and after the table 13 test-meal test
Example number (people) Before the test-meal After the test-meal P value (self)
The test-meal group 52 177.4 the scholar 88.3 237.4 soil 90.2 **# 0.000
Control group 52 195.0 the scholar 92.5 197.6 the scholar 78.2 O.612
P value (between group) - 0.3233 0.0180
Annotate: *For with test-meal before relatively, P<0.01; #For comparing P<0.05 with control group.
Total lead in urine discharge rate compares (μ g/L, X scholar S) before and after the table 14 test-meal test
Figure BDA00001949298600111
Can obviously reduce the clinical symptoms integration of test-meal group by the visible blueberry of table 9, table 10, black fungus, the compound soft sweets of carrot, difference has conspicuousness (P<0.05 or P<0.01).By table 11, table 12, table 13, table 14 as seen, after the test-meal, self compare with test is preceding, 20d, 30d are subjected to examination adult lead in urine discharge rate obviously to increase (P<0.01), relatively, lead in urine discharge rate difference has conspicuousness (P<0.05) between 20d, 30d test-meal group and control group group.
By test 2 as can be known, blueberry, black fungus, the compound soft sweets of carrot can obviously reduce the clinical symptoms integration of test-meal group, and test-meal group self compares before and after the test-meal, and difference has conspicuousness (P<0.05 or P<0.01); 20d, 3Od lead in urine discharge rate are apparently higher than control group after edible blueberry, black fungus, the compound soft sweets composition of the carrot people test-meal, relatively reach test-meal group self between 20d, 30d test-meal group and control group group relatively, lead in urine is discharged difference conspicuousness (P<0.05 or P<0.01); Test-meal group and control group routine blood test, blood pressure, heart rate, liver function, renal function index do not have obvious change after the checkout facility, and all in range of normal value, harmful effect is not also found in routine urinalysis, Abdominal B type ultrasonography, Chest X-rays, Electrocardioscopy to check result; The test-meal group is always urinated calcium, is always urinated zinc discharge rate and control group relatively, and difference does not have conspicuousness (P>0.05).Prompting black fungus, carrot lead discharging health care soft sweet have obvious promotion lead-eliminating effect, and harmless to experimenter's health.

Claims (9)

1. a blueberry, black fungus, the compound soft sweets of carrot is characterized in that blueberry, black fungus, the compound soft sweets of carrot are to be prepared from by 12.5 ~ 22.5 portions of white granulated sugars, 7 ~ 15 parts of HFCSs, 40 ~ 50 parts of water, 8 ~ 16 parts of gelatin, 0.6 ~ 1.4 part of pectin, 0.2 ~ 0.6 part of sodium alginate, 0.5 ~ 2.5 part of citric acid, 6 ~ 14 parts of blueberry juice, 1 ~ 5 portion of carrot juice, 0.6 ~ 1.4 portion of black fungus and 0.005 ~ 0.025 part of vitamin C by mass fraction.
2. a kind of blueberry according to claim 1, black fungus, the compound soft sweets of carrot is characterized in that blueberry, black fungus, the compound soft sweets of carrot are to be prepared from by 16 portions of white granulated sugars, 13 parts of HFCSs, 46 parts of water, 12 parts of gelatin, 0.6 part of pectin, 0.25 part of sodium alginate, 1 part of citric acid, 8 parts of blueberry juice, 2 portions of carrot juices, 1 portion of black fungus and 0.015 part of vitamin C by mass fraction.
3. the preparation method of a kind of blueberry, black fungus, the compound soft sweets of carrot according to claim 1, the preparation method who it is characterized in that blueberry, black fungus, the compound soft sweets of carrot carries out according to the following steps:
One, blueberry, carrot juice are produced: take by weighing the rotten blueberry of nothing and really carry out squeezing the juice after flowing water cleans, it is standby to obtain blueberry juice; Choosing does not have the carrot of rotting, and cleans, and is cut into piece then and squeezes the juice, and it is standby to obtain carrot juice;
Two, the preparation of black fungus piece: get dried black fungus and place 40~50 ℃ of water to soak 15~20min, remove the base of a fruit then, clean, dry surface moisture, stripping and slicing;
Three, take by weighing raw material: take by weighing 0.005 ~ 0.025 part of 0.6 ~ 1.4 part of the black fungus of 1 ~ 5 part of 6 ~ 14 parts in blueberry juice, carrot juice, step 2 preparation of 12.5 ~ 22.5 parts of white granulated sugars, 7 ~ 15 parts of HFCSs, 40 ~ 50 parts in water, 8 ~ 16 parts in gelatin, 0.6 ~ 1.4 part of pectin, 0.2 ~ 0.6 part of sodium alginate, 0.5 ~ 2.5 part of citric acid, step 1 preparation and vitamin C by mass fraction; The white granulated sugar that takes by weighing is divided into three parts of X, Y and Z, and white granulated sugar X: white granulated sugar Y: the mass ratio of white granulated sugar Z is (3 ~ 11): (3 ~ 7): (2 ~ 6); Be four parts of A, B, C and D with the moisture that takes by weighing, water A: water B: water C: the mass ratio of water D is (2 ~ 10): (16 ~ 32): (3 ~ 7): (10 ~ 30);
Four, infusion: white granulated sugar X, HFCS and water A that step 3 is taken by weighing put into the container mixing, and being heated to temperature is 115 ℃~125 ℃, continues infusion 10 ~ 20min again after all dissolving, and obtains syrup;
Five, the gelatin that step 3 is taken by weighing adds water among the B, heats in container, and being heated to temperature is 45 ~ 55 ℃, and gelatin is all dissolved, and is cooled to room temperature then, obtains frozen glue;
Six, pectin, white granulated sugar Y and the water C that takes by weighing in the step 3 put into the container mixing, being heated to temperature is 80 ~ 90 ℃, and pectin is dissolved fully, mixes with syrup in the step 4 then, obtains mixing molasses L;
Seven, sodium alginate and the white granulated sugar Z that takes by weighing in the step 3 put into the container mixing, add water D after, be that water-bath joins temperature then and is among 70 ~ 80 ℃ the mixing molasses L to dissolving in 70 ℃ the water bath in temperature, obtain mixing molasses M behind the mixing;
Eight, the temperature of mixing molasses M is down to 60~70 ℃, add the frozen glue that step 5 obtains then, after stirring 5 ~ 15min all dissolves frozen glue, add citric acid, blueberry juice, carrot juice, auricularia auriculajudae piece and vitamin C that step 3 takes by weighing again, after mixing, obtain mixing molasses N;
Nine, adding mass fraction in the mixing molasses N is 5% CaCl 2Solution pours in the template then, leaves standstill gel to the room temperature, obtains gel piece, wherein mixing molasses N and CaCl 2Volume ratio be 100:0.6;
Ten, the gel piece that step 9 is obtained is dry 40~60min under 30~40 ℃ the condition in temperature, obtains blueberry, black fungus, the compound soft sweets of carrot.
4. the preparation method of a kind of blueberry according to claim 3, black fungus, the compound soft sweets of carrot is characterized in that in the step 3 taking by weighing 0.015 part of 16 parts of white granulated sugars, 13 parts of HFCSs, 46 parts in water, 12 parts in gelatin, 0.6 part of pectin, 0.25 part of sodium alginate, 1 part of citric acid, 8 parts in blueberry juice, 2 parts of carrot juices, 1 part of black fungus and vitamin C by mass fraction.
5. according to the preparation method of claim 3 or 4 described a kind of blueberries, black fungus, the compound soft sweets of carrot, it is characterized in that be 15min heat time heating time in the step 4, being heated to temperature is 120 ℃.
6. the preparation method of a kind of blueberry according to claim 5, black fungus, the compound soft sweets of carrot, it is characterized in that being heated in the step 5 temperature is 50 ℃.
7. the preparation method of a kind of blueberry according to claim 6, black fungus, the compound soft sweets of carrot, it is characterized in that being heated in the step 6 temperature is 85 ℃.
8. the preparation method of a kind of blueberry according to claim 7, black fungus, the compound soft sweets of carrot is characterized in that mixing time is 15min in the step 8.
9. the preparation method of a kind of blueberry according to claim 8, black fungus, the compound soft sweets of carrot is characterized in that baking temperature is 30 ℃ in the step 10, and be 60min drying time.
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