CN102746063B - Fruit-tree wound-healing agent - Google Patents
Fruit-tree wound-healing agent Download PDFInfo
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- CN102746063B CN102746063B CN201210233776.9A CN201210233776A CN102746063B CN 102746063 B CN102746063 B CN 102746063B CN 201210233776 A CN201210233776 A CN 201210233776A CN 102746063 B CN102746063 B CN 102746063B
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- wounds
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- healing agent
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- 239000003357 wound healing promoting agent Substances 0.000 title claims abstract description 12
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 7
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 7
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims abstract description 7
- 235000010234 sodium benzoate Nutrition 0.000 claims abstract description 7
- 239000004299 sodium benzoate Substances 0.000 claims abstract description 7
- 229940051841 polyoxyethylene ether Drugs 0.000 claims abstract description 6
- 229920000056 polyoxyethylene ether Polymers 0.000 claims abstract description 6
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 5
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 5
- 229910021538 borax Inorganic materials 0.000 claims abstract description 5
- 239000004202 carbamide Substances 0.000 claims abstract description 5
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 claims abstract description 5
- 235000003891 ferrous sulphate Nutrition 0.000 claims abstract description 5
- 239000011790 ferrous sulphate Substances 0.000 claims abstract description 5
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 claims abstract description 5
- 229910000359 iron(II) sulfate Inorganic materials 0.000 claims abstract description 5
- 229910000402 monopotassium phosphate Inorganic materials 0.000 claims abstract description 5
- 235000019796 monopotassium phosphate Nutrition 0.000 claims abstract description 5
- 239000011734 sodium Substances 0.000 claims abstract description 5
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 5
- 239000004328 sodium tetraborate Substances 0.000 claims abstract description 5
- 235000010339 sodium tetraborate Nutrition 0.000 claims abstract description 5
- 229910000365 copper sulfate Inorganic materials 0.000 claims abstract description 3
- 239000013078 crystal Substances 0.000 claims abstract description 3
- 239000002994 raw material Substances 0.000 claims abstract description 3
- 230000029663 wound healing Effects 0.000 claims description 10
- 239000010949 copper Substances 0.000 claims description 9
- 239000003795 chemical substances by application Substances 0.000 claims description 6
- 230000000536 complexating effect Effects 0.000 claims description 6
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 claims description 5
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 claims description 5
- 230000000149 penetrating effect Effects 0.000 claims description 5
- -1 0.3 part Substances 0.000 claims description 4
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 4
- 229910052802 copper Inorganic materials 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 4
- PJNZPQUBCPKICU-UHFFFAOYSA-N phosphoric acid;potassium Chemical compound [K].OP(O)(O)=O PJNZPQUBCPKICU-UHFFFAOYSA-N 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 claims description 2
- MPYDICYHUNOOFV-UHFFFAOYSA-N disodium azane Chemical compound N.N.[Na+].[Na+] MPYDICYHUNOOFV-UHFFFAOYSA-N 0.000 claims description 2
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 claims 3
- 244000052616 bacterial pathogen Species 0.000 claims 1
- 235000013877 carbamide Nutrition 0.000 claims 1
- 206010052428 Wound Diseases 0.000 abstract description 15
- 208000027418 Wounds and injury Diseases 0.000 abstract description 15
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 abstract description 7
- 201000010099 disease Diseases 0.000 abstract description 6
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 abstract description 6
- 206010020649 Hyperkeratosis Diseases 0.000 abstract description 5
- 230000032823 cell division Effects 0.000 abstract description 5
- 239000002023 wood Substances 0.000 abstract description 5
- 238000005336 cracking Methods 0.000 abstract description 4
- 238000001704 evaporation Methods 0.000 abstract description 4
- 230000008020 evaporation Effects 0.000 abstract description 4
- 208000015181 infectious disease Diseases 0.000 abstract description 4
- 230000001737 promoting effect Effects 0.000 abstract description 3
- 238000013138 pruning Methods 0.000 abstract description 2
- 229960001484 edetic acid Drugs 0.000 abstract 2
- USVMJSALORZVDV-UHFFFAOYSA-N 6-(gamma,gamma-dimethylallylamino)purine riboside Natural products C1=NC=2C(NCC=C(C)C)=NC=NC=2N1C1OC(CO)C(O)C1O USVMJSALORZVDV-UHFFFAOYSA-N 0.000 abstract 1
- 241000894006 Bacteria Species 0.000 abstract 1
- USVMJSALORZVDV-SDBHATRESA-N N(6)-(Delta(2)-isopentenyl)adenosine Chemical compound C1=NC=2C(NCC=C(C)C)=NC=NC=2N1[C@@H]1O[C@H](CO)[C@@H](O)[C@H]1O USVMJSALORZVDV-SDBHATRESA-N 0.000 abstract 1
- 230000009286 beneficial effect Effects 0.000 abstract 1
- 238000009395 breeding Methods 0.000 abstract 1
- 230000001488 breeding effect Effects 0.000 abstract 1
- UQHKFADEQIVWID-UHFFFAOYSA-N cytokinin Natural products C1=NC=2C(NCC=C(CO)C)=NC=NC=2N1C1CC(O)C(CO)O1 UQHKFADEQIVWID-UHFFFAOYSA-N 0.000 abstract 1
- 239000004062 cytokinin Substances 0.000 abstract 1
- 230000035876 healing Effects 0.000 abstract 1
- GNSKLFRGEWLPPA-UHFFFAOYSA-M potassium dihydrogen phosphate Chemical compound [K+].OP(O)([O-])=O GNSKLFRGEWLPPA-UHFFFAOYSA-M 0.000 abstract 1
- LWIHDJKSTIGBAC-UHFFFAOYSA-K potassium phosphate Substances [K+].[K+].[K+].[O-]P([O-])([O-])=O LWIHDJKSTIGBAC-UHFFFAOYSA-K 0.000 abstract 1
- 230000004936 stimulating effect Effects 0.000 abstract 1
- 238000005406 washing Methods 0.000 abstract 1
- QJZYHAIUNVAGQP-UHFFFAOYSA-N 3-nitrobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid Chemical compound C1C2C=CC1C(C(=O)O)C2(C(O)=O)[N+]([O-])=O QJZYHAIUNVAGQP-UHFFFAOYSA-N 0.000 description 6
- 239000004021 humic acid Substances 0.000 description 6
- 238000000034 method Methods 0.000 description 6
- 244000052769 pathogen Species 0.000 description 6
- 230000001717 pathogenic effect Effects 0.000 description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- JPVYNHNXODAKFH-UHFFFAOYSA-N Cu2+ Chemical compound [Cu+2] JPVYNHNXODAKFH-UHFFFAOYSA-N 0.000 description 3
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 3
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 3
- 206010039509 Scab Diseases 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 230000003628 erosive effect Effects 0.000 description 3
- 229940071106 ethylenediaminetetraacetate Drugs 0.000 description 3
- 239000011591 potassium Substances 0.000 description 3
- 229910052700 potassium Inorganic materials 0.000 description 3
- 210000001082 somatic cell Anatomy 0.000 description 3
- 102000004190 Enzymes Human genes 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 2
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 2
- 210000000170 cell membrane Anatomy 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 229910052750 molybdenum Inorganic materials 0.000 description 2
- 239000011733 molybdenum Substances 0.000 description 2
- 230000001954 sterilising effect Effects 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 241000675108 Citrus tangerina Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 102000018697 Membrane Proteins Human genes 0.000 description 1
- 108010052285 Membrane Proteins Proteins 0.000 description 1
- 235000006040 Prunus persica var persica Nutrition 0.000 description 1
- 240000006413 Prunus persica var. persica Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000000740 bleeding effect Effects 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 210000004027 cell Anatomy 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 229910001431 copper ion Inorganic materials 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 208000010801 foot rot Diseases 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 230000034659 glycolysis Effects 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 230000003204 osmotic effect Effects 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 231100000572 poisoning Toxicity 0.000 description 1
- 230000000607 poisoning effect Effects 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000007790 scraping Methods 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000010148 water-pollination Effects 0.000 description 1
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The invention discloses a fruit-tree wound-healing agent, which is characterized by being prepared from the following raw-material components: 25 parts of sodium humate (the mass percentage is 50 percent), 0.6 part of copper sulfate crystal, 0.3 part of urea, 0.25 part of monopotassium phosphate, 0.05 part of ferrous sulfate, 0.05 part of borax, 0.2 part of EDTA (Ethylene Diamine Tetraacetic Acid), 1.2 parts of polyvinyl alcohol, 0.3 part of sodium benzoate, 0.3 part of penetrant JFC (fatty alcohol-polyoxyethylene ether), 0.1 part of plant cytokinin (isopentenyl adenosine) and 71.7 parts of water. The fruit-tree wound-healing agent is mainly used for better healing the tree-body wounds of fruit trees caused by pruning wounds, sawing wounds, girding wounds and diseases, can be used for effectively protecting the wounds and stopping the infection of harmful bacteria after being smeared. The fruit-tree wound-healing agent has the beneficial effects of reducing the evaporation of the water, stimulating tree-body cell division to form calluses and rapidly grow new bark, promoting the wounds to be rapidly healed and preventing naked xylems from cracking and breeding wood rots due to rainwater washing at the same time.
Description
Technical field
The invention belongs to agricultural technology field, be specifically related to a kind of fruit tree wound healing agent, for promoting the protectant of fruit tree branch bar wound healing.
Background technology
Fruit tree tree body owing to rotting, the tree body wound that causes of the disease such as dry rot, gummosis or because of the needs of pruning, all to cut artificially some every year and leave larger wound compared with thick branch.This technology is new and effective fruit tree wound healing agent; being mainly used in fruit tree heals better because of the tree body wound that clip, saw kerf, band girdle mouth and disease cause; after smearing, can effectively protect wound, stop infection process; reduce moisture evaporation; stimulate tree somatic cell division form callus and grow rapidly new skin; promote wound healing, also can prevent exposed xylem cracking simultaneously and grow wood rot because of rain drop erosion.
Summary of the invention
The object of this invention is to provide the wound healing of a kind of promotion fruit tree branch bar; effectively protect wound, stop infection process; reduce moisture evaporation; stimulate tree somatic cell division form callus and grow rapidly new skin; promote wound healing, also can prevent exposed xylem cracking simultaneously and grow the fruit tree wound healing agent of wood rot because of rain drop erosion.
The present invention is achieved through the following technical solutions, described a kind of fruit tree wound healing agent and preparation method thereof, mainly by the raw material of following weight composition, made: 25 parts of the sodium humates that mass fraction is 50%, 0.6 part of copper sulfate crystal, 0.3 part, urea, 0.25 part of potassium dihydrogen phosphate, 0.05 part, ferrous sulfate, 0.05 part of borax, 0.2 part of disodium ethylene diamine tetraacetate (EDTA), 1.2 parts of polyvinyl alcohol, 0.3 part of Sodium Benzoate, 0.3 part of penetrating agent JFC (fatty alcohol-polyoxyethylene ether), 0.1 part of phytocytomine (IPA), 71.7 parts, water.Preparing process: (1) first strengthens tree vigo(u)r by EDTA (b diammonium disodium edta) complexing and promotes the macro-and microelements such as the potassium of fruit tree scab wound healing ability, iron, molybdenum; (2) by humic acid and bivalent cupric ion complex reaction, form the copper humate with sterilizing function again; (3) with alcohol, phytocytomine (IPA) is dissolved; (4) water dissolves Sodium Benzoate; (5) with hot water, polyvinyl alcohol is dissolved; Finally (1), (2), (3), (4) added successively in (5) and constantly stir, the pH value that finally adds penetrating agent JFC (fatty alcohol-polyoxyethylene ether) and adjust solution is 8-9, makes liquid become viscoloid character.
Proportioning principle: humic acid in this technical products (R-COOH) is a kind of complexity fragrance polymer composite with hydroxyl and carboxyl, the existence of the active group that they are a large amount of has determined that humic acid has the special natures such as hydrophily, ion exchangeable, complexing and adsorption capacity and physiologically active, bivalent cupric ion has poisoning ability to pathogens such as rot, ring spot, dry rot, root rot, oranges and tangerines foot rot, peach gummosis, is mainly Cu
2+with having an effect it is lost activity containing SH enzyme on pathogen cell membrane, simultaneously Cu
2+also, with pathogen surface of cell membrane hydrogen, calcium, magnesium, the exchange of potassium plasma, pathogen cell membrane protein is solidified, a part of copper ion of while also can enter in pathogen cell is thoroughly obstructed the glycolysis of pathogen endocellular sugar with some enzyme decohesion enzymic activity.Utilize the complexing of humic acid itself and strengthen biomembranous permeability, making humic acid and Cu
2+the copper humate that complexing forms, has strengthened Cu on the one hand
2+osmotic absorption, the effect that fruit tree wound is prevented and cured diseases strengthens greatly, has also strengthened callus ability and the antibacterial ability of fruit tree simultaneously; On the other hand, due to humic acid and Cu
2+complexing has formed the copper humate complex compound of rock-steady structure, becomes colloidal nature, steady quality; For improving crop disease-resistant ability, strengthen tree vigo(u)r and promoting scab wound healing ability, in proportioning, increased the macro-and microelements of the promotion fruit tree wound healings such as potassium, iron, molybdenum, increased the short bark growing plants basic element of cell division; After adding polyvinyl alcohol and bleeding agent that product is used, at fruit tree wound, form very thin biomembrane and increase the osmosis of medicine, can preventing rain wash, nutrient loss, improve sterilization, the rotten ability of disease-resistant, anti-exposed xylem wood; Add Sodium Benzoate and can prevent that protectant from depositing going mouldy of process etc.
Using method: skin 1 centimeters of should first becoming better around fruit tree wound scab with cutter during operation cuts diseased tissues, requires the neat stubble of otch fusiformis not stay dead angle, and the sick skin of scraping has exposed skin, then liquid is evenly filled to affected part with hairbrush.
A kind of fruit tree wound healing agent; there is the wound healing of the fruit tree branch of promotion bar; effectively protect wound, stop infection process; reduce moisture evaporation; stimulate tree somatic cell division form callus and grow rapidly new skin; promote wound healing, also can prevent exposed xylem cracking simultaneously and grow the advantage of wood rot because of rain drop erosion.
Embodiment
The production 1000Kg product of take is example:
The first step: with the water-soluble solution disodium ethylene diamine tetraacetate of 100Kg (EDTA) 2Kg, then add potassium dihydrogen phosphate 2.5Kg, urea 3Kg, ferrous sulfate 0.5Kg, borax 0.5Kg to dissolve;
Second step: the sodium humate 250Kg that is 50% with the water-soluble solution mass fraction of 250Kg, then add copper sulphate 6Kg stirring and dissolving;
The 3rd step: 1Kg phytocytomine (IPA) is dissolved with 250ml alcohol;
The 4th step: after 12Kg polyvinyl alcohol being dissolved with 150Kg hot water, 3Kg Sodium Benzoate is added, then add 217Kg water; First three solution of being made into respectively of step is added and wherein stirs 30 minutes;
The 5th step: 3Kg penetrating agent JFC (fatty alcohol-polyoxyethylene ether) is added, and the pH value of adjusting solution is in 8-9 scope, makes liquid become colloidal nature, metering filling is finished product after chemical examination.
Claims (2)
1. a fruit tree wound healing agent, it is characterized in that by the raw material of following component formulated, 25 parts of the sodium humates that mass fraction is 50%, 0.6 part of copper sulfate crystal, 0.3 part, urea, 0.25 part of potassium dihydrogen phosphate, 0.05 part, ferrous sulfate, 0.05 part of borax, 0.2 part of disodium ethylene diamine tetraacetate (EDTA-2Na), 1.2 parts of polyvinyl alcohol, 0.3 part of Sodium Benzoate, 0.3 part of penetrating agent JFC (fatty alcohol-polyoxyethylene ether), 0.1 part of IPA, 71.7 parts, water.
2. a kind of fruit tree wound healing agent according to claim 1, is characterized in that first potassium dihydrogen phosphate, ferrous sulfate, urea, the borax that is promoted fruit tree wound healing by b diammonium disodium edta (EDTA-2Na) complexing; (2) by sodium humate and copper sulphate complex reaction, form and there is the copper humate that kills rotten pathogenic bacteria function again; (3) water dissolves Sodium Benzoate; (4) with alcohol, will promote fissional IPA to dissolve; (5) with hot water, polyvinyl alcohol is dissolved; Finally (1), (2), (3), (4) added successively in (5) and constantly stir, the pH value that finally adds penetrating agent JFC (fatty alcohol-polyoxyethylene ether) and adjust solution is 8-9, makes liquid become viscoloid character.
Priority Applications (1)
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CN201210233776.9A CN102746063B (en) | 2012-06-26 | 2012-06-26 | Fruit-tree wound-healing agent |
Applications Claiming Priority (1)
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CN201210233776.9A CN102746063B (en) | 2012-06-26 | 2012-06-26 | Fruit-tree wound-healing agent |
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CN102746063A CN102746063A (en) | 2012-10-24 |
CN102746063B true CN102746063B (en) | 2014-07-16 |
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CN106608762A (en) * | 2016-12-19 | 2017-05-03 | 广西金神农生态农业科技开发有限公司 | Planting method for Citrus grandis |
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CN107079927A (en) * | 2017-06-22 | 2017-08-22 | 和县赭洛山茶叶种植专业合作社 | A kind of plant sprout connects wound healing agent and preparation method thereof |
CN107279142A (en) * | 2017-06-23 | 2017-10-24 | 合肥市风达农业有限责任公司 | One planting fruit-trees wound healing protective agent and preparation method thereof |
CN108576052A (en) * | 2018-05-25 | 2018-09-28 | 钱万琦 | A kind of preparation method of fruit tree wound healing agent |
CN109588183B (en) * | 2018-11-26 | 2023-10-03 | 中国林业科学研究院热带林业实验中心 | Pruning method for wood-saving-free cultivation |
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CN1593154A (en) * | 2004-07-13 | 2005-03-16 | 田忠科 | Copper humate agricultural chemicals bactericide for prevention and cure of fruit tree branch disease |
CN101161075A (en) * | 2007-11-27 | 2008-04-16 | 李开森 | Fruit tree wound healing protective agent |
CN101731242A (en) * | 2009-12-22 | 2010-06-16 | 李开森 | Fruit tree wound healing protective agent and preparation method thereof |
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2012
- 2012-06-26 CN CN201210233776.9A patent/CN102746063B/en not_active Expired - Fee Related
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1593154A (en) * | 2004-07-13 | 2005-03-16 | 田忠科 | Copper humate agricultural chemicals bactericide for prevention and cure of fruit tree branch disease |
CN101161075A (en) * | 2007-11-27 | 2008-04-16 | 李开森 | Fruit tree wound healing protective agent |
CN101731242A (en) * | 2009-12-22 | 2010-06-16 | 李开森 | Fruit tree wound healing protective agent and preparation method thereof |
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