CN102741338B - 包括分散的多峰表面改性纳米粒子的树脂体系 - Google Patents

包括分散的多峰表面改性纳米粒子的树脂体系 Download PDF

Info

Publication number
CN102741338B
CN102741338B CN201180007990.6A CN201180007990A CN102741338B CN 102741338 B CN102741338 B CN 102741338B CN 201180007990 A CN201180007990 A CN 201180007990A CN 102741338 B CN102741338 B CN 102741338B
Authority
CN
China
Prior art keywords
resin
nanoparticles
resin system
ratio
mode
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201180007990.6A
Other languages
English (en)
Chinese (zh)
Other versions
CN102741338A (zh
Inventor
克里斯廷·L·通霍斯特
温迪·L·汤普森
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
3M Innovative Properties Co
Original Assignee
3M Innovative Properties Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 3M Innovative Properties Co filed Critical 3M Innovative Properties Co
Publication of CN102741338A publication Critical patent/CN102741338A/zh
Application granted granted Critical
Publication of CN102741338B publication Critical patent/CN102741338B/zh
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
    • C08J5/005—Reinforced macromolecular compounds with nanosized materials, e.g. nanoparticles, nanofibres, nanotubes, nanowires, nanorods or nanolayered materials
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K9/00—Use of pretreated ingredients
    • C08K9/04—Ingredients treated with organic substances
    • C08K9/06—Ingredients treated with organic substances with silicon-containing compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C70/00—Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts
    • B29C70/04—Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts comprising reinforcements only, e.g. self-reinforcing plastics
    • B29C70/28—Shaping operations therefor
    • B29C70/30—Shaping by lay-up, i.e. applying fibres, tape or broadsheet on a mould, former or core; Shaping by spray-up, i.e. spraying of fibres on a mould, former or core
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C70/00—Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts
    • B29C70/04—Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts comprising reinforcements only, e.g. self-reinforcing plastics
    • B29C70/28—Shaping operations therefor
    • B29C70/40—Shaping or impregnating by compression not applied
    • B29C70/42—Shaping or impregnating by compression not applied for producing articles of definite length, i.e. discrete articles
    • B29C70/46—Shaping or impregnating by compression not applied for producing articles of definite length, i.e. discrete articles using matched moulds, e.g. for deforming sheet moulding compounds [SMC] or prepregs
    • B29C70/48—Shaping or impregnating by compression not applied for producing articles of definite length, i.e. discrete articles using matched moulds, e.g. for deforming sheet moulding compounds [SMC] or prepregs and impregnating the reinforcements in the closed mould, e.g. resin transfer moulding [RTM], e.g. by vacuum
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L101/00—Compositions of unspecified macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L63/00—Compositions of epoxy resins; Compositions of derivatives of epoxy resins
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/66—Additives characterised by particle size
    • C09D7/67—Particle size smaller than 100 nm
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/66—Additives characterised by particle size
    • C09D7/68—Particle size between 100-1000 nm
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2063/00—Use of EP, i.e. epoxy resins or derivatives thereof, as moulding material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2105/00—Condition, form or state of moulded material or of the material to be shaped
    • B29K2105/06—Condition, form or state of moulded material or of the material to be shaped containing reinforcements, fillers or inserts
    • B29K2105/16—Fillers
    • B29K2105/162—Nanoparticles
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2363/00—Characterised by the use of epoxy resins; Derivatives of epoxy resins
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K9/00—Use of pretreated ingredients
    • C08K9/02—Ingredients treated with inorganic substances

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Nanotechnology (AREA)
  • Organic Chemistry (AREA)
  • Composite Materials (AREA)
  • Health & Medical Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Manufacturing & Machinery (AREA)
  • General Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Physics & Mathematics (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
CN201180007990.6A 2010-02-11 2011-02-09 包括分散的多峰表面改性纳米粒子的树脂体系 Expired - Fee Related CN102741338B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US30340610P 2010-02-11 2010-02-11
US61/303,406 2010-02-11
PCT/US2011/024147 WO2011100289A1 (en) 2010-02-11 2011-02-09 Resin system comprising dispersed multimodal surface -modified nanoparticles

Publications (2)

Publication Number Publication Date
CN102741338A CN102741338A (zh) 2012-10-17
CN102741338B true CN102741338B (zh) 2015-04-15

Family

ID=43827146

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201180007990.6A Expired - Fee Related CN102741338B (zh) 2010-02-11 2011-02-09 包括分散的多峰表面改性纳米粒子的树脂体系

Country Status (8)

Country Link
US (2) US8871853B2 (enExample)
EP (1) EP2534199B1 (enExample)
JP (1) JP5798129B2 (enExample)
KR (1) KR101910202B1 (enExample)
CN (1) CN102741338B (enExample)
ES (1) ES2706398T3 (enExample)
PL (1) PL2534199T3 (enExample)
WO (1) WO2011100289A1 (enExample)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5861147A (en) 1997-06-09 1999-01-19 The Procter & Gamble Company Methods for controlling environmental odors on the body using compositions comprising uncomplexed cyclodextrins and perfume
WO2013130247A1 (en) 2012-02-28 2013-09-06 3M Innovative Properties Company Composition comprising surface modified high index nanoparticles suitable for optical coupling layer
DE102012205650A1 (de) * 2012-04-05 2013-10-10 Siemens Aktiengesellschaft Isolierstoff für rotierende Maschinen
WO2014099702A1 (en) 2012-12-21 2014-06-26 3M Innovative Properties Company Composition comprising particulate flow aid
US10422074B2 (en) * 2015-03-10 2019-09-24 Evonik Degussa Gmbh Carbon fibre fibre-sizing containing nanoparticles
JP2019532165A (ja) 2016-09-14 2019-11-07 スリーエム イノベイティブ プロパティズ カンパニー 速硬化性光学接着剤
WO2018085040A1 (en) 2016-11-07 2018-05-11 3M Innovative Properties Company Curable resin including nanoparticles including surface-bonded hydrophobically-modifying alkyl groups
WO2019070561A1 (en) * 2017-10-02 2019-04-11 Aleo Bme, Inc. ADHESIVES FOR WATER-BASED FABRICS
US11198263B2 (en) * 2018-03-22 2021-12-14 Rogers Corporation Melt processable thermoplastic composite comprising a multimodal dielectric filler
JP7032977B2 (ja) * 2018-03-30 2022-03-09 太陽インキ製造株式会社 硬化性樹脂組成物、ドライフィルム、硬化物、および、電子部品
WO2023136331A1 (ja) * 2022-01-13 2023-07-20 日産化学株式会社 粒度分布を有するシリカゾル及びその製造方法

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2003044099A1 (de) * 2001-11-23 2003-05-30 Deutsche Amphibolin-Werke Von Robert Murjahn Gmbh & Co. Kg Beschichtungsmasse enthaltend nanopartikel, verwendung der beschichtungsmasse und verfahren zur herstellung von beschichtungen
WO2009138471A1 (en) * 2008-05-14 2009-11-19 Dow Corning Corporation Process for reduction of friction

Family Cites Families (39)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2801185A (en) 1952-05-16 1957-07-30 Du Pont Silica hydrosol powder
NL199333A (enExample) 1955-07-30
US3018262A (en) 1957-05-01 1962-01-23 Shell Oil Co Curing polyepoxides with certain metal salts of inorganic acids
GB904177A (en) 1960-07-16 1962-08-22 Hans Joachim Zimmer Improvements in or relating to the production of phenolic resin moulding compositions
US3298998A (en) 1961-03-07 1967-01-17 Eastman Kodak Co Bisglycidyl ethers of bisphenols
FR1536946A (fr) 1967-02-28 1968-09-02 Rhodiaceta Nouveaux composés bis maléamiques
FR1555564A (fr) 1967-07-13 1969-01-31 Rhone Poulenc Sa Nouvelles résines thermostables dérivées de bis-imides d'acides dicarboxyliques non saturés
BE754723A (fr) 1969-08-12 1971-02-11 Rhone Poulenc Sa Procede de preparation de
CH586731A5 (enExample) 1973-11-05 1977-04-15 Ciba Geigy Ag
US4181752A (en) 1974-09-03 1980-01-01 Minnesota Mining And Manufacturing Company Acrylic-type pressure sensitive adhesives by means of ultraviolet radiation curing
CH615935A5 (enExample) 1975-06-19 1980-02-29 Ciba Geigy Ag
US4157360A (en) 1978-04-26 1979-06-05 Allied Chemical Corporation Thermoformable compositions comprising a crosslinked polycyanurate polymer and a thermoplastic polymer
US4329384A (en) 1980-02-14 1982-05-11 Minnesota Mining And Manufacturing Company Pressure-sensitive adhesive tape produced from photoactive mixture of acrylic monomers and polynuclear-chromophore-substituted halomethyl-2-triazine
US4330590A (en) 1980-02-14 1982-05-18 Minnesota Mining And Manufacturing Company Photoactive mixture of acrylic monomers and chromophore-substituted halomethyl-2-triazine
US4379201A (en) 1981-03-30 1983-04-05 Minnesota Mining And Manufacturing Company Multiacrylate cross-linking agents in pressure-sensitive photoadhesives
US4468497A (en) 1981-03-30 1984-08-28 Hitco Elastomer modified bis-maleimide resin
US4522958A (en) 1983-09-06 1985-06-11 Ppg Industries, Inc. High-solids coating composition for improved rheology control containing chemically modified inorganic microparticles
JPH08302121A (ja) * 1995-04-28 1996-11-19 Daicel Chem Ind Ltd スチレン重合体組成物
US6586483B2 (en) 2001-01-08 2003-07-01 3M Innovative Properties Company Foam including surface-modified nanoparticles
US6883908B2 (en) 2001-01-08 2005-04-26 3M Innovative Properties Company Methods and compositions for ink jet printing of pressure sensitive adhesive patterns or films on a wide range of substrates
US7514263B2 (en) 2001-04-02 2009-04-07 3M Innovative Properties Company Continuous process for the production of combinatorial libraries of materials
WO2003100214A1 (en) 2002-05-24 2003-12-04 3M Innovative Properties Company Use of surface-modified nanoparticles for oil recovery
DE10259460A1 (de) 2002-12-19 2004-07-01 Tesa Ag Transparente Acrylathaftklebemasse mit einem Füllstoff
EP1457509B1 (de) * 2003-03-11 2006-06-28 hanse chemie AG Polymere Epoxidharz-Zusammensetzung
US20060134362A1 (en) 2004-12-17 2006-06-22 3M Innovative Properties Company Optically clear pressure sensitive adhesive
US7264872B2 (en) * 2004-12-30 2007-09-04 3M Innovative Properties Company Durable high index nanocomposites for AR coatings
US7531595B2 (en) 2006-03-08 2009-05-12 3M Innovative Properties Company Pressure-sensitive adhesive containing silica nanoparticles
US7829188B2 (en) * 2006-04-03 2010-11-09 E.I. Du Pont De Nemours And Company Filled epoxy compositions
US20080153963A1 (en) * 2006-12-22 2008-06-26 3M Innovative Properties Company Method for making a dispersion
US7393901B1 (en) 2007-02-16 2008-07-01 3M Innovative Properties Company Acrylate adhesives containing silica nanoparticles crosslinked with polyfunctional aziridines
JP5132193B2 (ja) * 2007-06-02 2013-01-30 日揮触媒化成株式会社 多孔質シリカ粒子およびその製造方法
JP5453741B2 (ja) 2007-07-17 2014-03-26 日産自動車株式会社 ポリカーボネート樹脂組成物及びその製造方法
JP2011515569A (ja) 2008-03-28 2011-05-19 スリーエム イノベイティブ プロパティズ カンパニー 粒子の表面改質のための方法
CN102037066B (zh) 2008-03-28 2014-11-19 3M创新有限公司 填充树脂及制造填充树脂的方法
JP2009263542A (ja) 2008-04-25 2009-11-12 Three M Innovative Properties Co （メタ）アクリル系粘着性発泡体及びその製造方法
ES2690653T3 (es) 2008-06-16 2018-11-21 3M Innovative Properties Company Composiciones curables reforzadas
JP4524320B2 (ja) 2008-08-11 2010-08-18 日東電工株式会社 粘着剤組成物、粘着剤層、および粘着剤シート
EP2373727B1 (en) 2008-12-19 2014-01-22 3M Innovative Properties Company Nanocalcite composites
US9153354B2 (en) 2009-11-20 2015-10-06 3M Innovative Properties Company Compositions comprising conductive particles with surface-modified nanoparticles covalently attached thereto, and methods of making

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2003044099A1 (de) * 2001-11-23 2003-05-30 Deutsche Amphibolin-Werke Von Robert Murjahn Gmbh & Co. Kg Beschichtungsmasse enthaltend nanopartikel, verwendung der beschichtungsmasse und verfahren zur herstellung von beschichtungen
WO2009138471A1 (en) * 2008-05-14 2009-11-19 Dow Corning Corporation Process for reduction of friction

Also Published As

Publication number Publication date
WO2011100289A1 (en) 2011-08-18
JP5798129B2 (ja) 2015-10-21
KR20120134119A (ko) 2012-12-11
CN102741338A (zh) 2012-10-17
KR101910202B1 (ko) 2018-10-19
EP2534199B1 (en) 2019-01-16
US20120309870A1 (en) 2012-12-06
JP2013519756A (ja) 2013-05-30
US9718954B2 (en) 2017-08-01
PL2534199T3 (pl) 2019-04-30
ES2706398T3 (es) 2019-03-28
EP2534199A1 (en) 2012-12-19
US8871853B2 (en) 2014-10-28
US20150099833A1 (en) 2015-04-09

Similar Documents

Publication Publication Date Title
CN102741338B (zh) 包括分散的多峰表面改性纳米粒子的树脂体系
US10450444B2 (en) Nanocomposites containing spherical pyrogenic silica nanoparticles and composites, articles, and methods of making same
CN102119176B (zh) 配混纳米粒子和树脂的方法
EP3502054A1 (en) Functionalized graphene oxide curable formulations
CN102112536B (zh) 增韧可固化组合物
KR20170101254A (ko) 폴리머 조성물, 이의 제조 방법, 이의 용도 및 이를 포함하는 조성물

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20150415

Termination date: 20200209