CN102727658B - Chinese herbal extract with anti-dropping and oil-controlling effects, preparation method and application thereof - Google Patents
Chinese herbal extract with anti-dropping and oil-controlling effects, preparation method and application thereof Download PDFInfo
- Publication number
- CN102727658B CN102727658B CN2012102099474A CN201210209947A CN102727658B CN 102727658 B CN102727658 B CN 102727658B CN 2012102099474 A CN2012102099474 A CN 2012102099474A CN 201210209947 A CN201210209947 A CN 201210209947A CN 102727658 B CN102727658 B CN 102727658B
- Authority
- CN
- China
- Prior art keywords
- weight portions
- chinese medicine
- parts
- preparation
- shampoo
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Images
Landscapes
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a Chinese herbal extract with anti-dropping and oil-controlling effects. Active components of the Chinese herbal extract are prepared from the following raw materials of: by weight, 10-20 parts of red sage root, 5-10 parts of Chinese angelica, 10-15 parts of sophora flavescens, 5-8 parts of Ligusticum wallichii, 5-8 parts of matrimony vine, 5-10 parts of pericarpium zanthoxyli, 4-8 parts of ligustrum lucidum, 10-15 parts of radix scrophulariae, 5-8 parts of bitter orange and 6-10 parts of root of kudzu vine. The Chinese herbal extract provided by the invention has good anti-dropping and oil-controlling effects. Its preparation method is simple. The product obtained is green and safe, has substantial efficacy, and is in favor of stimulating hair follicle, activating scalp cells and enhance blood circulation. The Chinese herbal extract itself has effects of invigorate blood circulation, promoting qi, preventing hair dropping and controlling oil, and especially has a better curative effect in allusion to seborrheic alopecia.
Description
Technical field
The present invention relates to a kind of Chinese medicine extract with anticreep control oil effect and preparation method thereof and application.
Background technology
Clinical common alopecia has two kinds of alopecia areata and seborrheic alopecia.Alopecia areata claims again circular alopecia, and the traditional Chinese medical science is called " alopecia areata ", " alopecia areata ", is a kind of speckle shape alopecia suddenly occurred, the lighter's alopecia in the form of sheets, but severe one alopecia totalis or alopecia universalis.It is relevant with autoimmune situation, heredity and Nervous and Mental Factors that pathogenic factor is thought.Seborrheic alopecia is called again androgenetic alopecia, it is one of modal alopecia reason, men and women's both sexes all have generation, in male colony, incidence rate is very high, androgenetic alopecia can occur in the time of 50 years old in 50% male, though along with the increase occurrence probability at the age 70% seborrheic alopecia no conscious sympton that rises, larger to alopecia people's psychological impact, and likely affecting its daily life along with growth in the living standard, people also more pay attention to alopeciaing therapeutic.
Chinese medicine is mainly Chinese medicine to be made to the tincture of hair growth promoting to the external treatment of alopecia, makes medicine directly act on affected part, and certain stimulation is played in part, thereby promote the blood circulation of local skin, improve trichotrophy, promote hair growth and drug absorption, through Transdermal absorption, also can produce general action.General initial effect shows as hair strengthening, stops alopecia or alopecia and reduces, and hair growth promoting, long hair occur subsequently, first bear the fine hair on birds or animals galley proof and send out, then gradually become terminal hair, or the fine hair on birds or animals galley proof is sent out blackening gradually, thick, hard, long.Separately scalp itch, dandruff, sebum are too much had to therapeutical effect in various degree.
Therefore, on safety, healthy health preserving basis, in conjunction with China's Traditional Chinese Medicine theory, according to monarch, minister, the Traditional Chinese Medicine Theory helping, make, prepare by compound recipe that to develop the anticreep hair care formulations with fine effect be the focus that those skilled in the art study.
Summary of the invention
The object of the invention is to propose a kind of Chinese medicine composition and application thereof with the oily effect of good anticreep hair care control.
Compositions with the oily effect of anticreep hair care control provided by the present invention, its active component is made by the former medicine of following portions by weight ratio:
Radix Salviae Miltiorrhizae 10～20 weight portions, Radix Angelicae Sinensis 5～10 weight portions, Radix Sophorae Flavescentis 10～15 weight portions, Rhizoma Chuanxiong 5～8 weight portions, Fructus Lycii 5～8 weight portions, Fructus Zanthoxyli 5～10 weight portions, Fructus Ligustri Lucidi 4～8 weight portions, Radix Scrophulariae 10～15 weight portions, Fructus Aurantii Immaturus 5～8 weight portions, Radix Puerariae 6～10 weight portions.
Its active component of described compositions is preferably made by the former medicine of following portions by weight ratio:
Radix Salviae Miltiorrhizae 20 weight portions, Radix Angelicae Sinensis 10 weight portions, Radix Sophorae Flavescentis 15 weight portions, Rhizoma Chuanxiong 8 weight portions, Fructus Lycii 5 weight portions, Fructus Zanthoxyli 5 weight portions, Fructus Ligustri Lucidi 4 weight portions, Radix Scrophulariae 10 weight portions, Fructus Aurantii Immaturus 8 weight portions, Radix Puerariae 10 weight portions.
The present invention also provides the above-mentioned preparation method with Chinese medicine composition of the oily effect of anticreep hair care control.The method, comprise the steps:
1) take each former medicine according to the described proportioning of claim 1 or 2, after former medicine is mixed, pulverizer is pulverized;
2) the former medicine of Chinese medicine after pulverizing in step 1) is joined in alcoholic solution, soak 1-2 hour;
3) agitating heating is extracted, and the extraction temperature is 65-75 ℃, extracts 2 hours;
4) room temperature staticly settles 2-4 hour, gets supernatant, and coarse filtration is centrifugal, gets supernatant, and the supernatant clarification is bright is light red;
5) supernatant step 4) obtained is placed in rotary evaporator and is concentrated, and removes ethanol, is condensed into rare extractum shape, obtains peony to the dark brown thick liquid, is Chinese medicine extract.
In described step 1), described pulverizing is that described former medicated powder is broken to granular size is 20 orders-60 orders; Described step 2) in, the concentration expressed in percentage by volume of described alcoholic solution is 90-95%, is preferably 95%, and the ratio of the former medicine of described Chinese medicine and alcoholic solution is 1g:(15-25) ml, be preferably 1g:20ml.
In described step (4), filter is that 100～200 mesh filter screens filter; 5000 rev/mins of centrifugal rotational speeds, the time is 10 minutes.
In described step (5), described concentrated temperature is 55 ℃～60 ℃, specifically can be 55 ℃ or 60 ℃.
The hair care formulations that the above-mentioned compositions with the oily effect of anticreep hair care control of take is active component also belongs to protection scope of the present invention.As tincture, shampoo or hair conditioner etc.
Wherein, described shampoo can be made by following component:
Laureth sulfuric ester ammonium 20%; Fatty monoethanol amide 1%; Lauroylamidopropyl betaine 4%; Guar hydroxypropyltrimonium chloride 0.2%; Disodiumedetate 0.1%; Cetearyl alcohol 0.5%; Dimethyl siloxane 2%; Above-mentioned Chinese medicine composition 1-2%; Methylchloroisothiazandnone or Methylisothiazolinone 0.1%; Ethylene glycol stearate or glycol distearate 2%; Surplus is water, and described % refers to the quality percentage composition.
The mass percent concentration in shampoo of above-mentioned Chinese medicine composition is preferably 1%.
The preparation method of above-mentioned shampoo, comprise the steps:
1) according to the component of above-mentioned shampoo, add 60 ℃ of stirrings of heating in part water to make material dissolution complete laureth sulfuric ester ammonium;
2) according to the component of above-mentioned shampoo, after fatty monoethanol amide, lauroylamidopropyl betaine, guar hydroxypropyltrimonium chloride, disodiumedetate are added in part water and stir, in the solution that adds step 1) to obtain, be heated to 80-85 ℃, homogenizing 3min, stir cooling; Add the Chinese medicine composition that in cetearyl alcohol, dimethyl siloxane and cocamido propyl betaine, claim 3-5 prepared by any one after cooling, stir evenly, after adding again methylchloroisothiazandnone or Methylisothiazolinone, ethylene glycol stearate or glycol distearate, supply water, mix and obtain shampoo.
Invention thinking of the present invention is: take the Chinese medical science theory as basis, take human hair health as aim, according to monarch, minister, the traditional Chinese medical science prescription thought helping, make, Chinese herbal medicine Radix Salviae Miltiorrhizae, Radix Angelicae Sinensis, Radix Sophorae Flavescentis, Rhizoma Chuanxiong, Fructus Lycii, Fructus Zanthoxyli, Fructus Ligustri Lucidi, Radix Scrophulariae, Fructus Aurantii Immaturus, Radix Puerariae are effectively combined, and take the prescription Chinese medicine extract as main functional additive, be aided with the formulated Chinese medicinal anti-hair loss shampoo of matrix components commonly used in shampoo.The natural gentleness of Chinese medicine treatment of the present invention, safe and non-stimulating, and very easily be absorbed by the skin, nourish transdermal, reach the effect that prevents alopecia, promotes hair growth and scalp control oil.
Beneficial effect of the present invention: Chinese medicine extract of the present invention has the oily effect of good anticreep hair care control, and preparation method is easy, the products obtained therefrom green safety, and effect is remarkable, is conducive to hair follicle stimulating, the activation scalp cells, and strengthen blood circulation.Chinese medicine extract itself has blood-activating and qi-promoting, prevents alopecia and controls oily effect, especially for seborrheic alopecia, better curative effect is arranged.
The accompanying drawing explanation
Fig. 1 is the routine clinical observation result of Chinese medicine shampoo hair growth 120 provided by the invention;
Fig. 2 is that Chinese medicine shampoo provided by the invention suppresses scalp fat secretion design sketch.
The specific embodiment
Embodiment 1, the present invention have the preparation of the Chinese medicine extract of anticreep control oil effect
1) take each crude drug according to following proportioning:
Radix Salviae Miltiorrhizae 20g, Radix Angelicae Sinensis 10g, Radix Sophorae Flavescentis 15g, Rhizoma Chuanxiong 8g, Fructus Lycii 5g, Fructus Zanthoxyli 5g, Fructus Ligustri Lucidi 4g, Radix Scrophulariae 10g, Fructus Aurantii Immaturus 8g, Radix Puerariae 10g;
2) after Chinese medicine mixes, pulverizer is pulverized, and is crushed to 20 orders-60 order.
3) Chinese medicine after pulverizing is joined in the alcoholic solution that concentration expressed in percentage by volume is 95%, the ratio of Chinese medicine and alcoholic solution is 1g:20ml, soaks 1 hour.
4) agitating heating is extracted, and extracting temperature is 75 ℃, extracts 2h.
5) room temperature staticly settles 4 hours, gets supernatant, 100 mesh filter screen coarse filtrations, and 5000 rev/mins, centrifugal 10 minutes, get supernatant, the supernatant clarification is bright is light red.
6) supernatant step 5) obtained is placed in rotary evaporator and is concentrated, and removes ethanol, is condensed into rare extractum shape, and for peony, to the dark brown thick liquid, density is 1.10-1.30.The density calculation method is: Chinese medicine extract density=quality (g)/volume (ml).
The preparation of embodiment 2 Chinese medicine extract of the present invention
1) take each crude drug according to following proportioning:
Radix Salviae Miltiorrhizae 10g, Radix Angelicae Sinensis 5g, Radix Sophorae Flavescentis 10g, Rhizoma Chuanxiong 5g, Fructus Lycii 8g, Fructus Zanthoxyli 10g, Fructus Ligustri Lucidi 8g, Radix Scrophulariae 15g, Fructus Aurantii Immaturus 8g, Radix Puerariae 5g;
2) after Chinese medicine mixes, pulverizer is pulverized.Be crushed to 20 orders-60 order.
3) Chinese medicine after pulverizing is joined in the alcoholic solution that concentration expressed in percentage by volume is 90%, the ratio of Chinese medicine and alcoholic solution is 1g:15ml, soaks 2 hours;
4) agitating heating is extracted, and extracting temperature is 70 ℃.Extract 2h.
Room temperature staticly settles 2 hours, gets supernatant, 150 mesh filter screen coarse filtrations, 5000 rev/mins centrifugal 10 minutes, get supernatant, supernatant clarification is bright is light red.
6) supernatant step 5) obtained is placed in rotary evaporator and is concentrated, and removes ethanol, is condensed into rare extractum shape, and for peony, to the dark brown thick liquid, density is 1.10-1.30; The density calculation method is: Chinese medicine extract density=quality (g)/volume (ml).
The preparation of embodiment 3 Chinese medicine extract of the present invention
1) take each crude drug according to following proportioning:
Radix Salviae Miltiorrhizae 15g, Radix Angelicae Sinensis 8g, Radix Sophorae Flavescentis 12g, Rhizoma Chuanxiong 7g, Fructus Lycii 6g, Fructus Zanthoxyli 8g, Fructus Ligustri Lucidi 6g, Radix Scrophulariae 12g, Fructus Aurantii Immaturus 6g, Radix Puerariae 8g;
2) after Chinese medicine mixes, pulverizer is pulverized.Be crushed to 20 orders-60 order.
3) Chinese medicine after pulverizing is joined in the alcoholic solution that concentration expressed in percentage by volume is 95%, the ratio of Chinese medicine and alcoholic solution is 1g:25ml, soaks 2 hours;
4) agitating heating is extracted, and extracting temperature is 65 ℃.Extract 2h.
5) room temperature staticly settles 3 hours, gets supernatant, 200 mesh filter screen coarse filtrations, 5000 rev/mins centrifugal 10 minutes, get supernatant, supernatant clarification is bright is light red.
Supernatant is placed in rotary evaporator and is concentrated, and removes ethanol, is condensed into rare extractum shape, and for peony, to the dark brown thick liquid, density is 1.10-1.30; The density calculation method is: Chinese medicine extract density=quality (g)/volume (ml).
The preparation of the shampoo that embodiment 4, the Chinese medicine extract of the present invention of take are active component
Raw material components according to table 1 prepares shampoo, and concrete steps are as described below:
1), according to the component of the A in table 1, B, C, D phase, be mixed into respectively the mixture of A, B, C, D phase.
2) A being added to 60 ℃ of stirrings of heating in part water makes material dissolution complete;
3) B is added in remainder water after stirring add A mutually in, be heated to 80-85 ℃, homogenizing 3min, stir cooling.Add the C phase after cooling, stir evenly, then add the D phase, mix rear the acquisition respectively and take the shampoo that the Chinese medicine extract of embodiment 1, embodiment 2 or embodiment 3 is active component.
The raw material components of table 1. shampoo
Shampoo clinical experiment and result that embodiment 5, the Chinese medicine extract of the present invention of take are active component
One, the routine clinical observation of Chinese medicine shampoo hair growth 120 provided by the invention
Experiment purpose: choose seborrheic alopecia crowd (men and women does not limit), respectively (it is identical with number of times with matched group (trying out commercially available shampoo) trial method that trial edition invention Chinese medicine ingredients shampoo be take the shampoo (preparation method of shampoo as described in Example 4) that the Chinese medicine extract of embodiment 1, embodiment 2 or embodiment 3 is active component to the contrived experiment group.Method: hair is drenched, with the shampoo of monobasic coin-size, be placed on rubbing foaming on hand, then be put on hair and start to crumple hair, if feel not have wash clean, then wash by the method for front, consumption is half of front, after once with referring to the abdominal massage scalp, with clear water, rinse.General two days once.
Observe " alopecia situation ", " scalp fat secretion situation ", " the anti-dandruff situation " of two groups of crowds before and after on probation, analyze Chinese medicine ingredients prepared by the present invention shampoo anticreep and control oily effect.
Experimentation: experimental group crowd age 18-60 one full year of life, the men and women does not limit, and takes the form that enters at random group to carry out.Case load 120, wherein experimental group is 80 examples, matched group is 40 examples.The shampoo that the Chinese medicine extract of embodiment 1, embodiment 2 or embodiment 3 of take is active component is on probation to above-mentioned experiment crowd successively, all establishes matched group at every turn.
Evaluation criterion: by patient's readme impression, human experimentation and naked eyes visual experiment.Effectively: during hair washing, the amount of losing hair reduces, the hair quality hardening, and the scalp fat secretion reduces.It is fine and better effectively being divided into two grades, finely for the alopecia amount, uses front remarkable minimizing, and the scalp greasy feeling alleviates greatly, and the dandruff greatly reduces; Preferably alopecia amount reduces before using to some extent, and the scalp greasy feeling alleviates, and the dandruff reduces to some extent.Not obvious: before and after using, sensation is without significant change.Poor: as after use, not to be any change.
Result is as described in table 2-table 7, and result shows to take shampoo that the Chinese medicine extract of embodiment 1, embodiment 2 or embodiment 3 is active component at Anti-hair loss and controls oily effective percentage all more than 80%.
Table 2. be take the shampoo trial effect statistical table that the Chinese medicine extract of embodiment 1 is active component
| Effect/evaluation (test group) | Fine | Better | Not obvious | Poor | Do not know | Effective percentage |
| The Anti-hair loss situation | 32 | 40 | 8 | 0 | 0 | 90% |
| Control oily situation | 39 | 31 | 10 | 0 | 0 | 87.5% |
| Control oily persistency | 36 | 31 | 13 | 0 | 0 | 83.75% |
| Anti-dandruff situation | 29 | 27 | 22 | 2 | 0 | 70% |
Table 3. contrast shampoo trial effect statistical table
| Effect/evaluation (matched group) | Fine | Better | Not obvious | Poor | Do not know | Effective percentage |
| The Anti-hair loss situation | 8 | 13 | 16 | 3 | 0 | 52.5% |
| Control oily situation | 6 | 16 | 15 | 3 | 0 | 55% |
| Control oily persistency | 2 | 10 | 19 | 6 | 0 | 30% |
| Anti-dandruff situation | 6 | 18 | 12 | 6 | 0 | 60% |
Table 4. be take the shampoo trial effect statistical table that the Chinese medicine extract of embodiment 2 is active component
| Effect/evaluation (test group) | Fine | Better | Not obvious | Poor | Do not know | Effective percentage |
| The |
30 | 39 | 11 | 0 | 0 | 86.25% |
| Control oily situation | 41 | 30 | 9 | 0 | 0 | 88.75% |
| Control |
35 | 30 | 15 | 0 | 0 | 81.25% |
| Anti-dandruff situation | 28 | 30 | 20 | 2 | 0 | 72.5% |
Table 5. contrast shampoo trial effect statistical table
| Effect/evaluation (matched group) | Fine | Better | Not obvious | Poor | Do not know | Effective percentage |
| The Anti-hair loss situation | 9 | 15 | 15 | 1 | 0 | 56% |
| Control oily situation | 10 | 16 | 12 | 2 | 0 | 65% |
| Control oily persistency | 3 | 12 | 20 | 5 | 0 | 37.5% |
| Anti-dandruff situation | 8 | 18 | 12 | 2 | 0 | 65% |
Table 6. be take the shampoo trial effect statistical table that the Chinese medicine extract of embodiment 3 is active component
| Effect/evaluation (test group) | Fine | Better | Not obvious | Poor | Do not know | Effective percentage |
| The Anti-hair loss situation | 32 | 39 | 9 | 0 | 0 | 88.75% |
| Control oily situation | 42 | 28 | 10 | 0 | 0 | 87.5% |
| Control oily persistency | 36 | 32 | 12 | 0 | 0 | 85% |
| Anti-dandruff situation | 26 | 31 | 21 | 2 | 0 | 71.25% |
Table 7. contrast shampoo trial effect statistical table
| Effect/evaluation (matched group) | Fine | Better | Not obvious | Poor | Do not know | Effective percentage |
| The Anti-hair loss situation | 10 | 16 | 14 | 0 | 0 | 65% |
| Control oily situation | 8 | 15 | 11 | 2 | 0 | 57.5% |
| Control |
5 | 12 | 13 | 5 | 0 | 42.5% |
| Anti-dandruff situation | 9 | 16 | 13 | 2 | 0 | 62.5% |
Two, Chinese medicine shampoo provided by the invention suppresses scalp fat secretion effect test
1, experimental principle
Human experimentation, choose the seborrheic alopecia crowd as the experimenter, and test subject is used the variation of Chinese medicine shampoo front and back leather point haze wax fat content, thereby determine the oily effect of control.
2, experimental apparatus and sample
Experimental apparatus: skin oil and fat tester
3, experiment crowd
The experimenter amounts to 40 people.Concrete sex composition and age structure are determined at random; Result is not found untoward reaction.
4, experimental technique
Take the form that enters at random group to carry out, and select the tested zone of experimenter's scalp.Each 20 people of sample sets and matched group; Sample component sample 1 and sample 2, wherein sample 1 is for take the shampoo (preparation method is shown in embodiment 4) that the Chinese medicine extract of embodiment 1 preparation is active fraction preparation, sample 2 is for take the shampoo (preparation method is shown in embodiment 4) that the Chinese medicine extract of embodiment 2 preparations is active fraction preparation, sample 3 is for take the shampoo (preparation method is shown in embodiment 4) that the Chinese medicine extract of embodiment 3 preparations is active fraction preparation, and sample 4 is commercially available shampoo.Matched group is not add drug extract still according to the method for embodiment 4, to add the shampoo of other component.
The technical staff uses the skin oil and fat tester
3-5 time, test test position, average, the blank value of data acquisition for the first time.
Test position the experimenter and use sample, and test the fat content at tested position.
The experimenter, using continuously sample after 1,2,4 hours, uses the skin oil and fat tester by the technical staff
Measure 3-5 time, average.
The experimenter, using sample the 7th day, the 14th day, the 21st day, the 28th day continuously, uses the skin oil and fat tester by the technical staff
Measure 3-5 time, average.
The numerical value that statistics records, adopt averaging method, analyzing skin fat secretion Changing Pattern and persistency.
Five, experimental result
The fat content variation was reflected in test period, Experimental Area fat content change with time.Its value is larger, and fat content is larger, otherwise fat content is less.
Each time point oil content (T after fat content difference (Δ T)=use product
hOil content (T before)-use product
0).
Table 8. is used the difference between shampoo of the present invention back haze wax fat content and initial value
From can find out in table 8, after sample 1, sample 2, sample 3 and sample 4 are used, the difference of fat content is always lower than blank group, with respect to sample 4, sample 1, sample 2, sample 3 differences are relatively little, show that sample 1, sample 2, sample 3 press down the fat more remarkable effect.
As can be seen from Figure 2, along with the prolongation of time, the effect that Chinese medicine shampoo (sample 1, sample 2 and sample 3) suppresses the scalp fat secretion is more obvious.This is also consistent with the human body test, and in tested crowd, the obvious person of control oil, obviously feel that scalp is dry, and the secretion oil quantity greatly reduces.
Claims (13)
1. one kind has the compositions that the anticreep hair care is controlled oily effect, and its active component is made by the former medicine of following portions by weight ratio:
Radix Salviae Miltiorrhizae 10～20 weight portions, Radix Angelicae Sinensis 5～10 weight portions, Radix Sophorae Flavescentis 10～15 weight portions, Rhizoma Chuanxiong 5～8 weight portions, Fructus Lycii 5～8 weight portions, Fructus Zanthoxyli 5～10 weight portions, Fructus Ligustri Lucidi 4～8 weight portions, Radix Scrophulariae 10～15 weight portions, Fructus Aurantii Immaturus 5～8 weight portions, Radix Puerariae 6～10 weight portions.
2. compositions according to claim 1, its active component of described compositions is made by the former medicine of following portions by weight ratio:
Radix Salviae Miltiorrhizae 20 weight portions, Radix Angelicae Sinensis 10 weight portions, Radix Sophorae Flavescentis 15 weight portions, Rhizoma Chuanxiong 8 weight portions, Fructus Lycii 5 weight portions, Fructus Zanthoxyli 5 weight portions, Fructus Ligustri Lucidi 4 weight portions, Radix Scrophulariae 10 weight portions, Fructus Aurantii Immaturus 8 weight portions, Radix Puerariae 10 weight portions.
3. the preparation method with Chinese medicine extract of the oily effect of anticreep hair care control, comprise the steps:
1) take each former medicine according to the described proportioning of claim 1 or 2, after former medicine is mixed, pulverizer is pulverized;
2) the former medicine of Chinese medicine after pulverizing in step 1) is joined in alcoholic solution, soak 1-2 hour;
3) agitating heating is extracted, and the extraction temperature is 65-75 ℃, extracts 2 hours;
4) room temperature staticly settles 2-4 hour, gets supernatant, filters, centrifugal, gets supernatant;
5) supernatant step 4) obtained is placed in rotary evaporator and is concentrated, and removes ethanol, is condensed into rare extractum shape, obtains peony to the dark brown thick liquid,, be Chinese medicine extract.
4. method according to claim 3 is characterized in that: in described step 1), described pulverizing is that described former medicated powder is broken to granular size is 20 orders-60 orders; Described step 2) in, the concentration expressed in percentage by volume of described alcoholic solution is 90-95%, and the ratio of the former medicine of described Chinese medicine and alcoholic solution is 1g:(15-25) ml.
5. method according to claim 4, it is characterized in that: described step 2), the concentration expressed in percentage by volume of described alcoholic solution is 95%, and the ratio of the former medicine of described Chinese medicine and alcoholic solution is 1g:20ml.
6. according to the described method of claim 4 or 5, it is characterized in that: in described step (4), filtering is that 100～200 mesh filter screens filter; 5000 rev/mins of centrifugal rotational speeds, the time is 10 minutes; In described step (5), described concentrated temperature is 55 ℃～60 ℃.
7. method according to claim 6, it is characterized in that: in described step (5), described concentrated temperature is 55 ℃ or 60 ℃.
8. the hair care formulations that the described compositions with the oily effect of anticreep hair care control of the claim 1 or 2 of take is active component.
9. preparation according to claim 8, it is characterized in that: described preparation is tincture, shampoo or hair conditioner.
10. preparation according to claim 9, it is characterized in that: described shampoo is made by following component:
Laureth sulfuric ester ammonium 20%; Fatty monoethanol amide 1%; Lauroylamidopropyl betaine 4%; Guar hydroxypropyltrimonium chloride 0.2%; Disodiumedetate 0.1%; Cetearyl alcohol 0.5%; Dimethyl siloxane 2%; The Chinese medicine extract 1-2% that in claim 3-7 prepared by any one, methylchloroisothiazandnone or Methylisothiazolinone 0.1%; Ethylene glycol stearate or glycol distearate 2%; Surplus is water, and described " % " refers to the quality percentage composition.
11. preparation according to claim 10 is characterized in that: the mass percent concentration of described Chinese medicine extract is 1%.
12. the preparation method of a shampoo, comprise the steps:
1), according to the described component of claim 10 or 11, add 60 ℃ of stirrings of heating in part water to make material dissolution complete laureth sulfuric ester ammonium;
2) according to the described component of claim 10 or 11, after fatty monoethanol amide, lauroylamidopropyl betaine, guar hydroxypropyltrimonium chloride, disodiumedetate are added in remainder water and stir, in the solution that adds step 1) to obtain, be heated to 80-85 ℃, homogenizing 3min, stir cooling; Add the Chinese medicine extract that in cetearyl alcohol, dimethyl siloxane and cocamido propyl betaine, claim 3-5 prepared by any one after cooling, stir evenly, after adding again methylchloroisothiazandnone or Methylisothiazolinone, ethylene glycol stearate or glycol distearate, mix and obtain shampoo.
13. the described compositions of claim 1 or 2 has the application in the hair care formulations of the oily effect of anticreep hair care control in preparation.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012102099474A CN102727658B (en) | 2012-06-19 | 2012-06-19 | Chinese herbal extract with anti-dropping and oil-controlling effects, preparation method and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012102099474A CN102727658B (en) | 2012-06-19 | 2012-06-19 | Chinese herbal extract with anti-dropping and oil-controlling effects, preparation method and application thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102727658A CN102727658A (en) | 2012-10-17 |
| CN102727658B true CN102727658B (en) | 2013-12-04 |
Family
ID=46984422
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2012102099474A Active CN102727658B (en) | 2012-06-19 | 2012-06-19 | Chinese herbal extract with anti-dropping and oil-controlling effects, preparation method and application thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102727658B (en) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103432227B (en) * | 2013-08-23 | 2015-07-29 | 广州市天吻娇颜化妆品有限公司 | Anti-hair loss Chinese herb compound of antagonism expression of androgen receptor and preparation method thereof |
| CN104188847A (en) * | 2014-08-07 | 2014-12-10 | 兰晶 | Non-silicone-oil plant anti-allergic shampoo |
| CN106974856A (en) * | 2017-03-23 | 2017-07-25 | 苏州顶裕节能设备有限公司 | Shampoo and its method prepared by a kind of utilization kudzuvine root starch waste water |
| CN107898703A (en) * | 2017-12-20 | 2018-04-13 | 杨新三 | A kind of Chinese medicine shampoo |
| CN111956587B (en) * | 2020-09-16 | 2021-05-04 | 孙开军 | Black-hair and bright-hair shampoo and preparation method thereof |
| CN114732847A (en) * | 2022-04-19 | 2022-07-12 | 赵鸿斌 | Oil-control anti-alopecia composition, oil-control anti-alopecia product and preparation method thereof |
| CN115531273A (en) * | 2022-11-02 | 2022-12-30 | 广州恒宁生物科技有限公司 | Traditional Chinese medicine composition for removing oil from hair and shampoo thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1819816A (en) * | 2005-04-11 | 2006-08-16 | 孟悦华 | Chinese medicinal preparation for removing dandruff and production thereof |
-
2012
- 2012-06-19 CN CN2012102099474A patent/CN102727658B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN102727658A (en) | 2012-10-17 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102727658B (en) | Chinese herbal extract with anti-dropping and oil-controlling effects, preparation method and application thereof | |
| US9005595B2 (en) | Chinese medicine hair-blackening preparation and formula and preparation method therefor | |
| CN103655383B (en) | Chinese medicinal herb extract and preparation method and application thereof | |
| CN102614102B (en) | Dandruff-removing medicinal composition and preparation method thereof | |
| CN102038626B (en) | Traditional Chinese medicinal hair-restoring and anti-alopecia shampoo and preparation method thereof | |
| US9180087B2 (en) | Chinese medicine hair-regrowth preparation and formula and preparation method therefor | |
| CN103784358A (en) | Shampoo | |
| CN108743729A (en) | A kind of herb composition that treating alopecia seborrheica and nanometer hair nourishing liquid | |
| CN102018771A (en) | Hair anti-dropping medical pilatory | |
| CN104107375A (en) | Traditional Chinese medicinal composition for nourishing and solidifying hair, as well as preparation method and application of traditional Chinese medicinal composition | |
| CN102895401A (en) | Germinal traditional Chinese medicine and preparation method thereof | |
| CN100337667C (en) | Chinese medicinal preparation for treating alopecin and early wbiteness of beard and hair | |
| CN101804188B (en) | Composition for controlling atrichia and manufacture method thereof | |
| CN104606118A (en) | Plant liquid shampoo for nourishing scalp hairs and preventing hair loss and white hairs and preparation method for plant liquid shampoo | |
| CN104055817A (en) | Composition with sedative effect and atomization preparation thereof | |
| CN115006336B (en) | Plant shampoo capable of preventing hair loss, strengthening hair, removing dandruff and relieving itching and preparation method thereof | |
| CN106474447A (en) | A kind of antagonism head infection, compositionss of antipruritic anticreep and its preparation method and application | |
| CN106038393A (en) | Hair regeneration care liquid and preparation method thereof | |
| CN103735443A (en) | Alopecia-resistant smoothing shampoo and preparation method thereof | |
| CN109172608B (en) | A kind of Chinese medicine composition that can improve sleep quality | |
| CN106880800A (en) | With Chinese medicine composition for educating hair effect and its preparation method and application | |
| CN106668685A (en) | Traditional Chinese medicine head massage paste | |
| CN101485875A (en) | Medicament composing prescription for preventing and treating alopecia and preparation method thereof | |
| CN1116022C (en) | Shampoo | |
| CN101380380A (en) | Traditional Chinese medicine for treating seborrheic baldness and its preparation method |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20160324 Address after: 101200, No. 3, M2-5 District, Hing Valley Economic Development Zone, Pinggu District, Beijing Patentee after: Beijing Orient Miao Sen bio tech ltd Address before: 100037 Beijing City, Haidian District, office building No. 21 room 1017 Patentee before: Beijing Huaxia Zhongfang Biological Technology Co.,Ltd. |