CN106974856A - Shampoo and its method prepared by a kind of utilization kudzuvine root starch waste water - Google Patents
Shampoo and its method prepared by a kind of utilization kudzuvine root starch waste water Download PDFInfo
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- CN106974856A CN106974856A CN201710177110.9A CN201710177110A CN106974856A CN 106974856 A CN106974856 A CN 106974856A CN 201710177110 A CN201710177110 A CN 201710177110A CN 106974856 A CN106974856 A CN 106974856A
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- kudzuvine root
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/008—Preparations for oily hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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Abstract
The invention discloses shampoo prepared by a kind of utilization kudzuvine root starch waste water, each material comprising following composition by weight:40 70 parts of kudzuvine root starch waste water, 48 parts of ammonium lactate, 36 parts of neopelex, 58 parts of N sodium lauroyl sarcosines, 37 parts of dimethyl silicone polymer, 10 15 parts of tetramethylenthanediol, 10 20 parts of allyl glycidyl ether, N, 38 parts of N diethyl acetoacetamides, 3,26 parts of 5 dimethyl, 1,2 cyclopentanedione, 9 15 parts of acrylate, 7 12 parts of menthyl acetate.The present invention carries out extraction modification by adding a variety of chemical compositions in kudzuvine root starch waste water, prepares with nourishing, oil-control, the shampoo of anti-dandruff function.
Description
Technical field
The invention belongs to shampoo field, shampoo and its method prepared by more particularly to a kind of utilization kudzuvine root starch waste water.
Background technology
Kudzu-vine root powder, also referred to as Pachyrhizua angulatus,《Compendium of Materia Medica》《Sheng Nong's herbal classic》、《Classified Materia Meidca》、《Huatuo's posthumous papers》、《China
Pharmacopeia》、《King of medicine pandect》、《Collected books handed down from ancient times》It is discussed in detail in big classical etc. the traditional Chinese medical science eight.Kudzu-vine root powder has edible, medicinal, spy
The purposes of different industrial three aspect, the root of kudzu vine includes 12% flavone compound, such as Puerarin, daizeol glycosides, peanut element battalion
Form point, also the mineral matter such as protein, amino acid, sugar and iron needed by human, calcium, copper, selenium, contained by the root of kudzu vine and Ge Ye
Flavones has a variety of definite health-care effects, and its clinical practice shows quick-acting and efficient rare characteristic.Kudzuvine root starch not only has uniqueness
Tempting local flavor, its mouthfeel and food therapy value are also superior.Particularly current environmental pollution, chemical contamination, even air are dirty
Dye, it is universal it is contaminated in the case of, people advocate pure natural, safely, effectively, and the food for having special health benefit is world's tide
Stream.It is rare invigorant suitable for people of all ages, the good reputation for having " ginseng in thousand ".Kudzu-vine root powder also has lipid-loweringing, decompression, fall fire, heat-clearing solution
The effects such as poison, rising Yang expelling pathogenic factors from muscles and skin, spasmolysis and analgesia, promoting eruption antidiarrheal, increase brain and coronal blood glucose, improvement brain microcirculation, be the high blood of preventing and treating
The important source material of the medicine of a variety of diseases such as pressure, high fat of blood, coronary heart diseases and angina pectoris, diabetes, cerebral thrombus, enterogastritis.In production
In root of kudzu vine technical process, its root of kudzu vine waste water largely discharged can then cause larger pollution, due to Pueraria lobota as handled not in time to environment
Containing some abundant nutritional ingredients in root waste water, while being also a kind of waste of the energy.Nervous, the state in nowadays energy resource
Family is advocated under economy, the overall background of Sustainable Development and Utilization, and waste, which is made full use of very, its realistic meaning.
The content of the invention
For drawbacks described above, the shampoo prepared it is an object of the invention to provide a kind of utilization kudzuvine root starch waste water and its method,
By adding a variety of chemical compositions in kudzuvine root starch waste water extraction modifications are carried out, prepare and washed with nourishing, oil-control, anti-dandruff function
Lotion.
The purpose of the present invention can be achieved through the following technical solutions:
Shampoo prepared by a kind of utilization kudzuvine root starch waste water, each material comprising following composition by weight:40-70 parts of kudzuvine root starch waste water, breast
Sour ammonium 4-8 parts, 3-6 parts of neopelex, 5-8 parts of N- sodium lauroyl sarcosines, 3-7 parts of dimethyl silicone polymer, four
10-15 parts of Propylene Glycol, 10-20 parts of allyl glycidyl ether, N, 3-8 parts of N- diethyl acetoacetamides, 3,5- diformazans
2-6 parts of base -1,2- cyclopentanediones, 9-15 parts of acrylate, 7-12 parts of menthyl acetate.
It is preferred that, 50-60 parts of the kudzuvine root starch waste water, 5-7 parts of ammonium lactate, 4-6 parts of neopelex, N- lauroyl
6-8 parts of sodium sarcosinate, 4-6 parts of dimethyl silicone polymer, 11-14 parts of tetramethylenthanediol, allyl glycidyl ether 12-16
Part, N, 4-7 parts of N- diethyl acetoacetamides, 3-5 parts of 3,5- dimethyl -1,2- cyclopentanediones, 11-14 parts of acrylate, second
Sour menthyl ester 9-11 parts.
It is preferred that, 55 parts of the kudzuvine root starch waste water, 6 parts of ammonium lactate, 5 parts of neopelex, N- Hamposyl Ls
7 parts of sodium, 5 parts of dimethyl silicone polymer, 12 parts of tetramethylenthanediol, 14 parts of allyl glycidyl ether, N, N- diethyl acetyl
6 parts of acetamide, 4 parts of 3,5- dimethyl -1,2- cyclopentanediones, 13 parts of acrylate, 10 parts of menthyl acetate.
A kind of method that utilization kudzuvine root starch waste water prepares shampoo, comprises the following steps:
S1:By 40-70 parts of kudzuvine root starch waste water, 4-8 parts of ammonium lactate, 3-6 parts of neopelex, N- sodium lauroyl sarcosines 5-
8 parts, 10-20 parts of allyl glycidyl ether add in reactors, be heated to after 60-80 DEG C, insulation reaction 5-15min, continue
Stirring reaction 15-20min;
S2:3-7 parts of dimethyl silicone polymer, 10-15 parts of tetramethylenthanediol, 9-15 parts of acrylate are added in step S1,
Mix after 10-20min, be warming up to 80-100 DEG C, insulation reaction 15-20min;
S3:7-12 parts of 2-6 parts of 3,5- dimethyl -1,2- cyclopentanediones and menthyl acetate are added in step S2, temperature is raised
To 100-120 DEG C, stirring reaction 20-30min;When reaction is cooled to 30-40 DEG C, N, N- diethyl acetoacetamides 3-8 are added
Part, arrest reaction 3-6h can obtain the shampoo after question response cooling.
It is preferred that, 75 DEG C, insulation reaction 10min, with speed 500-700r/min stirring reactions are heated in step S1
20min。
It is preferred that, it is warming up to 95 DEG C, insulation reaction 20min after mixing 15min in step S2.
It is preferred that, temperature is raised in step S3 to 110 DEG C, with speed 800-1000r/min stirring reaction 25min, reaction
It is cooled to 35 DEG C, arrest reaction 4.5h.
Compared with prior art, its advantage is the present invention:
The method that a kind of utilization kudzuvine root starch waste water of the present invention prepares shampoo, based on kudzuvine root starch waste water, matches somebody with somebody except adding to commonly use
Side is outer, is additionally added the things such as ammonium lactate, allyl glycidyl ether, dimethyl silicone polymer, 3,5- dimethyl -1,2- cyclopentanediones
Matter, fully extract, using the nutritional ingredient in kudzuvine root starch waste water, prepares and is washed with good nourishing, oil-control, anti-dandruff function
Lotion.The present invention efficiently solves the Utilizing question of kudzuvine root starch industrial wastewater, reduces the pollution to environment, improves energy utilization rate
With the economic benefit of enterprise.
Embodiment
The present invention is further illustrated with reference to embodiments.
Embodiment 1
S1:By 40 parts of kudzuvine root starch waste water, 4 parts of ammonium lactate, 3 parts of neopelex, 5 parts of N- sodium lauroyl sarcosines, allyl
10 parts of base glycidol ether is added in reactor, is heated to after 60 DEG C, insulation reaction 5min, continues to stir with speed 500r/min
React 15min;
S2:3 parts of dimethyl silicone polymer, 10 parts of tetramethylenthanediol, 9 parts of acrylate are added in step S1, mixed
After 10min, 80 DEG C, insulation reaction 15min are warming up to;
S3:7 parts of 2 parts of 3,5- dimethyl -1,2- cyclopentanedione and menthyl acetate are added in step S2, rise temperature to 100
DEG C, with speed 800r/min stirring reactions 20min;When reaction is cooled to 30 DEG C, addition N, 3 parts of N- diethyl acetoacetamides,
Arrest reaction 3h, the shampoo is can obtain after question response cooling.
Comparative example 1
S1:40 parts of kudzuvine root starch waste water, 3 parts of neopelex, 5 parts of N- sodium lauroyl sarcosines are added in reactor, plus
Heat is to 60 DEG C, after insulation reaction 5min, continues with speed 500r/min stirring reactions 15min;
S2:10 parts of tetramethylenthanediol, 9 parts of acrylate are added in step S1, mixes after 10min, is warming up to 80 DEG C,
Insulation reaction 15min;When reaction is cooled to 30 DEG C, N, 3 parts of N- diethyl acetoacetamides, arrest reaction 3h, question response are added
The shampoo is can obtain after cooling.
Embodiment 2
S1:By 70 parts of kudzuvine root starch waste water, 8 parts of ammonium lactate, 6 parts of neopelex, 8 parts of N- sodium lauroyl sarcosines, allyl
20 parts of base glycidol ether is added in reactor, is heated to after 80 DEG C, insulation reaction 15min, and continuation is stirred with speed 700r/min
Mix reaction 20min;
S2:7 parts of dimethyl silicone polymer, 15 parts of tetramethylenthanediol, 15 parts of acrylate are added in step S1, mixed
After 20min, 100 DEG C, insulation reaction 20min are warming up to;
S3:12 parts of 6 parts of 3,5- dimethyl -1,2- cyclopentanedione and menthyl acetate are added in step S2, rise temperature to 120
DEG C, with speed 1000r/min stirring reactions 30min;When reaction is cooled to 40 DEG C, addition N, 8 parts of N- diethyl acetoacetamides,
Arrest reaction 6h, the shampoo is can obtain after question response cooling.
Comparative example 2
S1:70 parts of kudzuvine root starch waste water, 6 parts of neopelex, 8 parts of N- sodium lauroyl sarcosines are added in reactor, plus
Heat is to 80 DEG C, after insulation reaction 15min, continues with speed 700r/min stirring reactions 20min;
S2:15 parts of tetramethylenthanediol, 15 parts of acrylate are added in step S1, mixes after 20min, is warming up to 100
DEG C, insulation reaction 20min;When reaction is cooled to 40 DEG C, N is added, 8 parts of N- diethyl acetoacetamides, arrest reaction 6h treats anti-
The shampoo is can obtain after should cooling down.
Embodiment 3
S1:By 50 parts of kudzuvine root starch waste water, 5 parts of ammonium lactate, 4 parts of neopelex, 6 parts of N- sodium lauroyl sarcosines, allyl
12 parts of base glycidol ether is added in reactor, is heated to after 65 DEG C, insulation reaction 10min, and continuation is stirred with speed 550r/min
Mix reaction 15min;
S2:4 parts of dimethyl silicone polymer, 11 parts of tetramethylenthanediol, 11 parts of acrylate are added in step S1, mixed
After 10min, 80 DEG C, insulation reaction 15min are warming up to;
S3:9 parts of 3 parts of 3,5- dimethyl -1,2- cyclopentanedione and menthyl acetate are added in step S2, rise temperature to 100
DEG C, with speed 850r/min stirring reactions 20min;When reaction is cooled to 30 DEG C, addition N, 4 parts of N- diethyl acetoacetamides,
Arrest reaction 3h, the shampoo is can obtain after question response cooling.
Embodiment 4
S1:By 60 parts of kudzuvine root starch waste water, 7 parts of ammonium lactate, 6 parts of neopelex, 8 parts of N- sodium lauroyl sarcosines, allyl
16 parts of base glycidol ether is added in reactor, is heated to after 75 DEG C, insulation reaction 15min, and continuation is stirred with speed 650r/min
Mix reaction 20min;
S2:6 parts of dimethyl silicone polymer, 14 parts of tetramethylenthanediol, 14 parts of acrylate are added in step S1, mixed
After 20min, 100 DEG C, insulation reaction 20min are warming up to;
S3:11 parts of 5 parts of 3,5- dimethyl -1,2- cyclopentanedione and menthyl acetate are added in step S2, rise temperature to 120
DEG C, with speed 1000r/min stirring reactions 30min;When reaction is cooled to 40 DEG C, addition N, 7 parts of N- diethyl acetoacetamides,
Arrest reaction 6h, the shampoo is can obtain after question response cooling.
Embodiment 5
S1:By 55 parts of kudzuvine root starch waste water, 6 parts of ammonium lactate, 5 parts of neopelex, 7 parts of N- sodium lauroyl sarcosines, allyl
14 parts of base glycidol ether is added in reactor, is heated to after 75 DEG C, insulation reaction 10min, and continuation is stirred with speed 600r/min
Mix reaction 20min;
S2:5 parts of dimethyl silicone polymer, 12 parts of tetramethylenthanediol, 13 parts of acrylate are added in step S1, mixed
After 15min, 95 DEG C, insulation reaction 20min are warming up to;
S3:10 parts of 4 parts of 3,5- dimethyl -1,2- cyclopentanedione and menthyl acetate are added in step S2, rise temperature to 110
DEG C, with speed 950r/min stirring reactions 25min;When reaction is cooled to 35 DEG C, addition N, 7 parts of N- diethyl acetoacetamides,
Arrest reaction 4.5h, the shampoo is can obtain after question response cooling.
The anti-dandruff and clean effect of shampoo obtained by the various embodiments described above and comparative example is investigated, it is as a result as follows:
Experiment | Inhibition zone diameter(mm) | Anti-dandruff effect | Soil removal efficiency(%) |
Embodiment 1 | 29.8 | Substantially | 95.1 |
Comparative example 1 | 7.8 | It is unobvious | 62.5 |
Embodiment 2 | 30.5 | Substantially | 96.7 |
Comparative example 2 | 8.7 | It is unobvious | 59.3 |
Embodiment 3 | 32.4 | Substantially | 97.2 |
Embodiment 4 | 33.7 | Substantially | 97.5 |
Embodiment 5 | 34.5 | Substantially | 98.1 |
The invention is not restricted to embodiment here, those skilled in the art do not depart from scope according to the announcement of the present invention
The improvement and modification made all should be within protection scope of the present invention.
Claims (7)
1. a kind of shampoo prepared by utilization kudzuvine root starch waste water, it is characterised in that each material comprising following composition by weight:Kudzuvine root starch gives up
40-70 parts of water, 4-8 parts of ammonium lactate, 3-6 parts of neopelex, 5-8 parts of N- sodium lauroyl sarcosines, poly dimethyl silicon
3-7 parts of oxygen alkane, 10-15 parts of tetramethylenthanediol, 10-20 parts of allyl glycidyl ether, N, N- diethyl acetoacetamides 3-8
Part, 2-6 parts of 3,5- dimethyl -1,2- cyclopentanediones, 9-15 parts of acrylate, 7-12 parts of menthyl acetate.
2. shampoo prepared by a kind of utilization kudzuvine root starch waste water according to claim 1, it is characterised in that the kudzuvine root starch waste water
50-60 parts, 5-7 parts of ammonium lactate, 4-6 parts of neopelex, 6-8 parts of N- sodium lauroyl sarcosines, polydimethylsiloxanes
4-6 parts of alkane, 11-14 parts of tetramethylenthanediol, 12-16 parts of allyl glycidyl ether, N, N- diethyl acetoacetamides 4-7
Part, 3-5 parts of 3,5- dimethyl -1,2- cyclopentanediones, 11-14 parts of acrylate, 9-11 parts of menthyl acetate.
3. shampoo prepared by a kind of utilization kudzuvine root starch waste water according to claim 2, it is characterised in that the kudzuvine root starch waste water
55 parts, 6 parts of ammonium lactate, 5 parts of neopelex, 7 parts of N- sodium lauroyl sarcosines, 5 parts of dimethyl silicone polymer, tetramethyl
12 parts of ethyl glycol, 14 parts of allyl glycidyl ether, N, 6 parts of N- diethyl acetoacetamides, 3,5- dimethyl -1,2- rings penta
4 parts of diketone, 13 parts of acrylate, 10 parts of menthyl acetate.
4. a kind of method that utilization kudzuvine root starch waste water prepares shampoo, it is characterised in that comprise the following steps:
S1:By 40-70 parts of kudzuvine root starch waste water, 4-8 parts of ammonium lactate, 3-6 parts of neopelex, N- sodium lauroyl sarcosines 5-
8 parts, 10-20 parts of allyl glycidyl ether add in reactors, be heated to after 60-80 DEG C, insulation reaction 5-15min, continue
Stirring reaction 15-20min;
S2:3-7 parts of dimethyl silicone polymer, 10-15 parts of tetramethylenthanediol, 9-15 parts of acrylate are added in step S1,
Mix after 10-20min, be warming up to 80-100 DEG C, insulation reaction 15-20min;
S3:7-12 parts of 2-6 parts of 3,5- dimethyl -1,2- cyclopentanediones and menthyl acetate are added in step S2, temperature is raised
To 100-120 DEG C, stirring reaction 20-30min;When reaction is cooled to 30-40 DEG C, N, N- diethyl acetoacetamides 3-8 are added
Part, arrest reaction 3-6h can obtain the shampoo after question response cooling.
5. the method that a kind of utilization kudzuvine root starch waste water according to claim 4 prepares shampoo, it is characterised in that in step S1
It is heated to 75 DEG C, insulation reaction 10min, with speed 500-700r/min stirring reactions 20min.
6. the method that a kind of utilization kudzuvine root starch waste water according to claim 4 prepares shampoo, it is characterised in that in step S2
95 DEG C, insulation reaction 20min are warming up to after mixing 15min.
7. the method that a kind of utilization kudzuvine root starch waste water according to claim 4 prepares shampoo, it is characterised in that in step S3
Temperature is raised to 110 DEG C, with speed 800-1000r/min stirring reaction 25min, reaction is cooled to 35 DEG C, arrest reaction 4.5h.
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CN201710177110.9A CN106974856A (en) | 2017-03-23 | 2017-03-23 | Shampoo and its method prepared by a kind of utilization kudzuvine root starch waste water |
PCT/CN2017/098523 WO2018171117A1 (en) | 2017-03-23 | 2017-08-22 | Shampoo prepared with kudzu powder waste water and method therefor |
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CN201710177110.9A CN106974856A (en) | 2017-03-23 | 2017-03-23 | Shampoo and its method prepared by a kind of utilization kudzuvine root starch waste water |
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CN201710177110.9A Withdrawn CN106974856A (en) | 2017-03-23 | 2017-03-23 | Shampoo and its method prepared by a kind of utilization kudzuvine root starch waste water |
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WO2018171117A1 (en) * | 2017-03-23 | 2018-09-27 | 苏州顶裕节能设备有限公司 | Shampoo prepared with kudzu powder waste water and method therefor |
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CN1176934C (en) * | 2001-07-11 | 2004-11-24 | 梅县梅雁生物工程研究所 | Process for extracitng puerarin from waste water from producing puerarin starch and increasing its yield |
KR20080011970A (en) * | 2006-08-01 | 2008-02-11 | (주)로다멘코스메딕스 | Compositions for prevention of hair loss or hair restoration containing extracts of pueraria plants |
CN102858319A (en) * | 2010-03-04 | 2013-01-02 | 株式会社爱茉莉太平洋 | Composition for preventing or treating poliosis or vitiligo comprising a pueraria genus plant extract or puerarin |
CN102451131A (en) * | 2010-11-01 | 2012-05-16 | 董根荣 | Chinese medicinal shampoo with blood pressure lowering function and preparation method thereof |
CN103169631B (en) * | 2011-12-22 | 2016-01-20 | 天津天狮生物发展有限公司 | A kind of submissive glossy shampoo and preparation method containing Chinese medicine composition |
CN102727658B (en) * | 2012-06-19 | 2013-12-04 | 北京华夏众芳生物科技有限公司 | Chinese herbal extract with anti-dropping and oil-controlling effects, preparation method and application thereof |
CN106974856A (en) * | 2017-03-23 | 2017-07-25 | 苏州顶裕节能设备有限公司 | Shampoo and its method prepared by a kind of utilization kudzuvine root starch waste water |
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2017
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WO2018171117A1 (en) * | 2017-03-23 | 2018-09-27 | 苏州顶裕节能设备有限公司 | Shampoo prepared with kudzu powder waste water and method therefor |
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