CN102719033A - Ceiling decorative soft film material and production process thereof - Google Patents
Ceiling decorative soft film material and production process thereof Download PDFInfo
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- CN102719033A CN102719033A CN2012101860754A CN201210186075A CN102719033A CN 102719033 A CN102719033 A CN 102719033A CN 2012101860754 A CN2012101860754 A CN 2012101860754A CN 201210186075 A CN201210186075 A CN 201210186075A CN 102719033 A CN102719033 A CN 102719033A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/001—Combinations of extrusion moulding with other shaping operations
- B29C48/0022—Combinations of extrusion moulding with other shaping operations combined with cutting
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/03—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor characterised by the shape of the extruded material at extrusion
- B29C48/07—Flat, e.g. panels
- B29C48/08—Flat, e.g. panels flexible, e.g. films
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/25—Component parts, details or accessories; Auxiliary operations
- B29C48/92—Measuring, controlling or regulating
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C2948/00—Indexing scheme relating to extrusion moulding
- B29C2948/92—Measuring, controlling or regulating
- B29C2948/92504—Controlled parameter
- B29C2948/92704—Temperature
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C2948/00—Indexing scheme relating to extrusion moulding
- B29C2948/92—Measuring, controlling or regulating
- B29C2948/92819—Location or phase of control
- B29C2948/92857—Extrusion unit
- B29C2948/92876—Feeding, melting, plasticising or pumping zones, e.g. the melt itself
- B29C2948/92895—Barrel or housing
Abstract
The invention relates to a ceiling decorative soft film material and a production process thereof. The ceiling decorative soft film material is prepared by 100 parts of imported PVC(polyvinyl chloride) prepared by the ethylene method, 30-50 parts of plasticizers, 3-6 parts of epoxidized soybean oil, 3-6 parts of barium and zinc liquid stabilizers, 0.5-1.5 parts of barium and zinc powder stabilizers, 0-10 parts of activated nano-calcium, 0.3-20 parts of nano-level rutile titanium powder, 2-8 parts of nano-level antimony trioxide and 0.01-15 parts of color fabrics. The production process includes primary brightening and secondary brightening, wherein the primary brightening includes steps of preparing, mixing, plasticizing, filtering, shaping, embossing, cold-cutting, trimming and winding, and the secondary brightening includes steps of fitting, secondary embossing, secondary cold-cutting, secondary trimming and secondary winding. Raw materials, equipment, technology and the like are all taken into consideration in the production process, and thus the production process has novel design and is reasonable. The ceiling decorative soft film material produced by the production process has performances such as high surface brightness and few surface crystal points, and the glossiness thereof is equal to or larger than 90 degrees when tested at the reflection angle of 60 degrees.
Description
Technical field
The invention belongs to the building and ornament materials production technical field, particularly relate to a kind of smallpox and decorate soft film material, relate to the preparation method that this smallpox is decorated soft film material simultaneously.
Background technology
The smallpox soft film material is a kind of novel equivalent material of smallpox sheet material in the house decorative material.This material is firstly appeared the Switzerland in 19th-century, and 60 years with after the Fr is taken the house ornamentation market that is generalized to Europe and America after Lan Dekeer further improves.This novel finishing material and finishing mode by feat of the performance of excellence and construction and moulding easily, in short time more than ten years, become the most noticeable decoration type materials in place such as Chinese large-sized stadiums, hotel, meeting and exhibition center rapidly.Especially on 2010 Shanghai World's Fair that are the theme with " city let life finer ", obtain the most successful application and favorable comment.The principal feature of this material: (1) optics: translucent effect is soft, more saves the energy than traditional material.(2) can print: can air brushing and the various colour images of printing at this material surface.(3) be prone to moulding: can be according to the random moulding of various creative designs.(4) waterproof, antibiotic: waterproof and dampproof surface is not tied water and is revealed under general moist environment, can resist and prevent mikrobe (as mouldy bacterium) grow on its surface.(5) acoustic efficiency: can effectively improve the indoor tone quality effect, be ideal sound isolating decorative material.(6) low-carbon (LC), lightweight: material is light, volume is little, the construction convenient disassembly; And can be recycled.It is collection fashion and be useful for finishing material all over the body that smallpox is decorated mantle, receives liking and praising highly of upholstery planner deeply.At present, the most dependence on import of smallpox soft film material of having relatively high expectations on the decoration market both at home and abroad, the same type of material of domestic production is compared also existence than big distance with international like product on physical and chemical indexes.Break through existing weaponry and equipment, technology and technologic bottleneck, develop the smallpox of international similar level and decorate soft film material, become the new direction that the field of new development is decorated by China.
Summary of the invention
The present invention overcomes the deficiency that prior art exists, and has proposed a kind of smallpox and has decorated soft film material and preparation method thereof.Product smallpox of the present invention is decorated soft film material and is had good physical and chemical performance index, and the light of product is brighter, and mute light is muter.
The technical scheme that technical solution problem of the present invention is taked is:
First aspect, a kind of smallpox is decorated soft film material, is raw material with ethylene process PVC, and adding softening agent, VT 18, barium zinc stabilizer, Namigai, white titanium pigment, fire retardant and painting cloth also is prepared from; It is characterized in that its prescription is counted with weight part:
| Import ethylene process PVC | 100 parts, |
| Softening agent | 30-50 part, |
| Epoxy soybean oil | 3-6 part, |
| Liquid barium zinc stabilizer | 3-6 part, |
| Powder barium zinc stabilizer | 0.5-1.5 part, |
| The activation Namigai | 0-10 part, |
| The nm-class rutile white titanium pigment of chlorination preparation | 0.3-20 part, |
| The nano level flame retardant Antimony Trioxide: 99.5Min | 2-8 part, |
| Painting cloth | 0.01-15 part; |
Measure its surface gloss >=90o with the 60o reflection angle.
As a kind of preferred; Said softening agent is DOP or DINP, and said painting cloth is one or more in ultramarine painting cloth, whitening agent painting cloth, permanent violet painting cloth, the blue or green blue painting cloth of phthalein, the dark green painting cloth of phthalein, carbon black painting cloth, the red cloth of two (rubigan)-1.4-diketopyrrolo-pyrrole and the medium chrome yellow medium yellow painting cloth.
Second aspect; Described a kind of smallpox is decorated the preparation method of soft film material; Comprise a blast and secondary blast; A said blast comprises prescription, mixing, plasticizing, filtration, moulding, embossing, cold cut, cutting edge and rolling step, and said secondary blast comprises applying, secondary embossing, secondary cold cut, secondary cutting edge and secondary rolling step; It is characterized in that: wherein,
A blast:
⑴ prescription, in weight part:
| Import ethylene process PVC | 100 parts, |
| Softening agent | 30-50 part, |
| Epoxy soybean oil | 3-6 part, |
| Liquid barium zinc stabilizer | 3-6 part, |
| Powder barium zinc stabilizer | 0.5-1.5 part, |
| The activation Namigai | 0-10 part, |
| The nm-class rutile white titanium pigment of chlorination preparation | 0.3-20 part, |
| The nano level flame retardant Antimony Trioxide: 99.5Min | 2-8 part, |
| Painting cloth | 0.01-15 part; |
⑵ mix: the raw material of the step of will filling a prescription ⑴ is put into impeller and is stirred, and controlled temperature is 90-130 ℃, churning time 300-450s; Put into the cold stirrer stirring of low speed then and be cooled to 80-100 ℃;
⑶ plasticizing: through the planetary extruder extrusion plasticizing, the control extruder temperature is 160-200 ℃ with mixing step ⑵ gained compound; Move to two rolling turbines then and further plastify, 190-230 ℃ of turbine temperature rolled in control;
⑷ filter: after plasticizing step ⑶ fully plastified, again through the filter impurity screening, filtering the mesh number was the 60-120 order, and controlled temperature is 170-210 ℃;
⑸ moulding: get into the four-roll calender calendering formation then, controlled temperature is 170-210 ℃;
⑹ embossing, cold cut, cutting edge and rolling: the PVC film that is obtained by forming step ⑸ carries out embossing; Cold cut then, cutting edge and rolling;
The secondary blast:
⑺ fit: a blast rolling step gained PVC film as counterdie and facial mask, is got into rigging machine and fits; During applying; Counterdie is preheated to 90-130 ℃, and the minute surface of film simultaneously touch on the minute surface wheel and the minute surface of film does not contact rubber wheel, simultaneously facial mask is preheated to 90-130 ℃; The minute surface of film simultaneously touch on the minute surface wheel and the minute surface of film does not contact rubber wheel; And send into simultaneously the compacting rubber wheel with two membranes to pasting, promptly counterdie minute surface and facial mask minute surface are fitted relatively, laminate pressure 30-70kg;
⑻ secondary compacting, secondary cold cut, secondary cutting edge and secondary rolling: after applying step ⑺ fits, promptly carry out the secondary compacting, secondary pressing pressure 30-70kg; Carry out secondary cold cut, secondary cutting edge and secondary rolling then.
As a kind of preferred; Said softening agent is DOP or DINP, and said painting cloth is one or more in ultramarine painting cloth, whitening agent painting cloth, permanent violet painting cloth, the blue or green blue painting cloth of phthalein, the dark green painting cloth of phthalein, carbon black painting cloth, the red cloth of two (rubigan)-1.4-diketopyrrolo-pyrrole and the medium chrome yellow medium yellow painting cloth.
The present invention starts with from many-sides such as raw material, equipment and technologies, through many-sided innovative design and research trial, and final the achieving success.
Aspect the raw and auxiliary material selection:
1. PVC: adopt import ethylene process PVC, impurity is few, and fish eyes is few, good heat resistance, and differences between batches are little, and surface brightness is high.
2. white titanium pigment: adopt the nm-class rutile titanium valve of chlorination preparation, particle distribution is even, and fineness is thinner, good dispersivity; It is few to show as product impurity, and brilliant point is few, and brightness is high.
3. fire retardant: adopt nano level flame retardant, fineness is good, is uniformly dispersed, and flame retardant effect is good, and brightness effects is good.
4. pigment: adopt the pigment that grinds and be processed into painting cloth through three rollers, dispersed good, solved the problem that is prone to produce vitta and scenery with hills and waters line in the toner course of processing that adopts.
Aspect equipment: what kind of plasticizing equipment of employing is most important for plasticizing effect, and planetary extruder is with respect to ten thousand horsepowers, and it is big to PVC compound plastifying shearing force, and the upset uniformity coefficient is high, and plasticizing effect is good.The present invention selects for use planetary extruder as the plastifying nucleus equipment, and is abundant, even to the plasticizing of PVC compound; Make product brightness brighter, mute degree is muter, and quality is better.
At process aspect: adopt brightly, protect bright effect in the face of pasting.The PVC calendered film that blast forming step obtains is after the embossing step is by rubber wheel and minute surface wheel embossing; Film simultaneously is bright, and one side is made mute, and bright (being minute surface) of batching caudacoria is against mute face; Mute destruction can be produced in the face of bright, the secondary blast need be carried out usually.And the mute face of film leans on minute surface to take turns in the traditional secondary blast technology applying step, and the bright face of film receives the destruction of suppressing rubber wheel and the surface brightness that has reduced film.The present invention adopts the novel process of secondary blast, and in the applying step, the bright face of film touch the minute surface wheel, and the bright face of film is not run into rubber wheel in the whole flow process, and brightness is not damaged, and the brightness of taking turns the caudacoria surface of heating through minute surface obtains reduction and blast; And paste bright the facing of two membranes, bright (being minute surface) of batching caudacoria plays a protective role to bright face against bright.
Smallpox decoration soft film material preparation method of the present invention takes all factors into consideration from raw material, equipment and technology aspects, through innovative design, and research trial, technology is rationally advanced; The smallpox of preparation is decorated soft film material, has the surface brightness height, measures glossiness >=90o with the 60o reflection angle, and the brilliant point in surface is few, is close with external high-end product.
Description of drawings
Fig. 1 is preparing method's technological process of production figure of the present invention.
Embodiment
Embodiment 1: a kind of smallpox is decorated the prescription of soft film material, in weight part:
| Import ethylene process PVC | 100 parts, |
| DOP (DOP) | 43 parts, |
| Epoxy soybean oil | 3 parts, |
| Liquid barium zinc stabilizer | 5 parts, |
| Powder barium zinc stabilizer | 1.0 part, |
| The activation Namigai | 3 parts, |
| The nm-class rutile white titanium pigment of chlorination preparation | 18 parts, |
| The nano level flame retardant Antimony Trioxide: 99.5Min | 5 parts, |
| The ultramarine painting cloth | 0.01 part, |
| The whitening agent painting cloth | 0.02 part. |
Embodiment 2: another kind of smallpox is decorated the prescription of soft film material, in weight part:
| Import ethylene process PVC | 100 parts, |
| DOP (DOP) | 43 parts, |
| Epoxy soybean oil | 3 parts, |
| Liquid barium zinc stabilizer | 5 parts, |
| Powder barium zinc stabilizer | 1.0 part, |
| The activation Namigai | 3 parts, |
| The nm-class rutile white titanium pigment of chlorination preparation | 18 parts, |
| The nano level flame retardant Antimony Trioxide: 99.5Min | 5 parts, |
| The permanent violet painting cloth | 0.2 part, |
| The red cloth of two (rubigan)-1.4-diketopyrrolo-pyrroles | 0.6 part. |
Embodiment 3: another smallpox is decorated the prescription of soft film material, in weight part:
| Import ethylene process PVC | 100 parts, |
| DOP (DOP) | 43 parts, |
| Epoxy soybean oil | 3 parts, |
| Liquid barium zinc stabilizer | 5 parts, |
| Powder barium zinc stabilizer | 1.0 part, |
| The activation Namigai | 3 parts, |
| The nm-class rutile white titanium pigment of chlorination preparation | 18 parts, |
| The nano level flame retardant Antimony Trioxide: 99.5Min | 5 parts, |
| The dark green painting cloth of phthalein | 0.2 part, |
| The blue or green blue painting cloth of phthalein | 0.5 part. |
Embodiment 4: another smallpox is decorated the prescription of soft film material, in weight part:
| Import ethylene process PVC | 100 parts, |
| DOP (DOP) | 43 parts, |
| Epoxy soybean oil | 3 parts, |
| Liquid barium zinc stabilizer | 5 parts, |
| Powder barium zinc stabilizer | 1.0 part, |
| The activation Namigai | 3 parts, |
| The nm-class rutile white titanium pigment of chlorination preparation | 18 parts, |
| The nano level flame retardant Antimony Trioxide: 99.5Min | 5 parts, |
| The carbon black painting cloth | 0.1 part, |
| The medium chrome yellow medium yellow painting cloth | 2.0 part. |
Embodiment 5: another smallpox is decorated the prescription of soft film material, in weight part:
| Import ethylene process PVC | 100 parts, |
| DINP (DINP) | 45 parts, |
| Epoxy soybean oil | 3 parts, |
| Liquid barium zinc stabilizer | 5 parts, |
| Powder barium zinc stabilizer | 1.0 part, |
| The activation Namigai | 3 parts, |
| The nm-class rutile white titanium pigment of chlorination preparation | 18 parts, |
| The nano level flame retardant Antimony Trioxide: 99.5Min | 5 parts, |
| The carbon black painting cloth | 0.1 part, |
| The medium chrome yellow medium yellow painting cloth | 2.0 part. |
Embodiment 6: a kind of smallpox is decorated the preparation method of soft film material:
The raw material of embodiment 1 prescription is put into impeller in weight part stir, controlled temperature is 120 ℃, churning time 400s; Put into the cold stirrer stirring of low speed subsequently and be cooled to 90 ℃; Drop into the planetary extruder extrusion plasticizing then, the control extruder temperature is 190 ℃; And then move to two rolling turbines and further plastify, 220 ℃ of turbine temperature are rolled in control; Through the filter impurity screening, filtering the mesh number is 100 orders again, and controlled temperature is 200 ℃; Get into the four-roll calender calendering formation then, controlled temperature is 190 ℃, and through embossing, cold cut, cutting edge, rolling.Resulting PVC film is as counterdie and facial mask; Fit at rigging machine, counterdie is preheated to 120 ℃, the minute surface of film simultaneously touch on the minute surface wheel and the minute surface of film does not contact rubber wheel (with bright effect of protective membrane); Simultaneously facial mask is preheated to 120 ℃; The minute surface of film touch simultaneously that minute surface wheel is gone up and the minute surface of film does not contact rubber wheel (with bright effect of protective membrane), send into simultaneously again the compacting rubber wheel with two membranes to pasting laminate pressure 50kg; Carry out cold cut, cutting edge, rolling once more.Get product.
Embodiment 6: another kind of smallpox is decorated the preparation method of soft film material:
The raw material of embodiment 3 prescriptions is put into impeller in weight part stir, controlled temperature is 115 ℃, churning time 410s; Put into the cold stirrer stirring of low speed subsequently and be cooled to 95 ℃; Drop into the planetary extruder extrusion plasticizing then, the control extruder temperature is 195 ℃; And then move to two rolling turbines and further plastify, 225 ℃ of turbine temperature are rolled in control; Through the filter impurity screening, filtering the mesh number is 80 orders again, and controlled temperature is 205 ℃; Get into the four-roll calender calendering formation then, controlled temperature is 195 ℃, and through embossing, cold cut, cutting edge, rolling.Resulting PVC film is as counterdie and facial mask; Fit at rigging machine, counterdie is preheated to 115 ℃, the minute surface of film simultaneously touch on the minute surface wheel and the minute surface of film does not contact rubber wheel (with bright effect of protective membrane); Simultaneously facial mask is preheated to 115 ℃; The minute surface of film touch simultaneously that minute surface wheel is gone up and the minute surface of film does not contact rubber wheel (with bright effect of protective membrane), send into simultaneously again the compacting rubber wheel with two membranes to pasting laminate pressure 60kg; Carry out cold cut, cutting edge, rolling once more.Get product.
Claims (4)
1. a smallpox is decorated soft film material, is raw material with ethylene process PVC, and adding softening agent, VT 18, barium zinc stabilizer, Namigai, white titanium pigment, fire retardant and painting cloth also is prepared from; It is characterized in that its prescription is counted with weight part:
Measure its surface gloss >=90o with the 60o reflection angle.
2. smallpox according to claim 1 is decorated soft film material; It is characterized in that; Said softening agent is DOP or DINP, and said painting cloth is one or more in ultramarine painting cloth, whitening agent painting cloth, permanent violet painting cloth, the blue or green blue painting cloth of phthalein, the dark green painting cloth of phthalein, carbon black painting cloth, the red cloth of two (rubigan)-1.4-diketopyrrolo-pyrrole and the medium chrome yellow medium yellow painting cloth.
3. a kind of smallpox according to claim 1 is decorated the preparation method of soft film material; Comprise a blast and secondary blast; A said blast comprises prescription, mixing, plasticizing, filtration, moulding, embossing, cold cut, cutting edge and rolling step, and said secondary blast comprises applying, secondary embossing, secondary cold cut, secondary cutting edge and secondary rolling step; It is characterized in that: wherein,
A blast:
⑴ prescription, in weight part:
⑵ mix: the raw material of the step of will filling a prescription ⑴ is put into impeller and is stirred, and controlled temperature is 90-130 ℃, churning time 300-450s; Put into the cold stirrer stirring of low speed then and be cooled to 80-100 ℃;
⑶ plasticizing: through the planetary extruder extrusion plasticizing, the control extruder temperature is 160-200 ℃ with mixing step ⑵ gained compound; Move to two rolling turbines then and further plastify, 190-230 ℃ of turbine temperature rolled in control;
⑷ filter: after plasticizing step ⑶ fully plastified, again through the filter impurity screening, filtering the mesh number was the 60-120 order, and controlled temperature is 170-210 ℃;
⑸ moulding: get into the four-roll calender calendering formation then, controlled temperature is 170-210 ℃;
⑹ embossing, cold cut, cutting edge and rolling: the PVC film that is obtained by forming step ⑸ carries out embossing; Cold cut then, cutting edge and rolling;
The secondary blast:
⑺ fit: a blast rolling step gained PVC film as counterdie and facial mask, is got into rigging machine and fits; During applying; Counterdie is preheated to 90-130 ℃; The minute surface of film touch simultaneously that minute surface wheel is gone up and the minute surface of film does not contact rubber wheel, simultaneously facial mask is preheated to 90-130 ℃, and the minute surface of film touch simultaneously that the minute surface wheel is gone up and the minute surface of film does not contact rubber wheel; And send into simultaneously compacting wheel with counterdie and facial mask two membranes to subsides, laminate pressure 30-70kg;
⑻ secondary compacting, secondary cold cut, secondary cutting edge and secondary rolling: after applying step ⑺ fits, promptly carry out the secondary compacting, secondary pressing pressure 30-70kg; Carry out secondary cold cut, secondary cutting edge and secondary rolling then.
4. a kind of smallpox according to claim 3 is decorated the preparation method of soft film material; It is characterized in that; Said softening agent is DOP or DINP, and said painting cloth is one or more in ultramarine painting cloth, whitening agent painting cloth, permanent violet painting cloth, the blue or green blue painting cloth of phthalein, the dark green painting cloth of phthalein, carbon black painting cloth, the red cloth of two (rubigan)-1.4-diketopyrrolo-pyrrole and the medium chrome yellow medium yellow painting cloth.
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| CN114350081A (en) * | 2021-12-22 | 2022-04-15 | 江苏新丰之星膜材料有限公司 | Formula for producing decorative film |
| CN115109354A (en) * | 2022-07-25 | 2022-09-27 | 保定帝鹏实业有限公司 | PVC ceiling film product containing glass beads and preparation method thereof |
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| CN103059463A (en) * | 2012-12-25 | 2013-04-24 | 杭州弘泽新材料有限公司 | Ceiling membrane and producing method thereof |
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| CN103724886B (en) * | 2014-01-26 | 2016-03-30 | 东莞市悠悠美居家居制造有限公司 | transparent embossing table mat |
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| CN108164870A (en) * | 2017-12-25 | 2018-06-15 | 上海永冠众诚新材料科技（集团）股份有限公司 | A kind of air-conditioning band film and preparation method thereof |
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| CN113943466A (en) * | 2021-10-25 | 2022-01-18 | 江苏新丰之星膜材料有限公司 | Formula for producing middle-layer film in decorative film |
| CN114350081A (en) * | 2021-12-22 | 2022-04-15 | 江苏新丰之星膜材料有限公司 | Formula for producing decorative film |
| CN114085475A (en) * | 2021-12-31 | 2022-02-25 | 江苏新丰之星膜材料有限公司 | Formula for producing novel decorative middle layer film |
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Application publication date: 20121010 |