CN102641307A - Ganoderma lucidum granule and preparation method thereof - Google Patents
Ganoderma lucidum granule and preparation method thereof Download PDFInfo
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- CN102641307A CN102641307A CN2012101545603A CN201210154560A CN102641307A CN 102641307 A CN102641307 A CN 102641307A CN 2012101545603 A CN2012101545603 A CN 2012101545603A CN 201210154560 A CN201210154560 A CN 201210154560A CN 102641307 A CN102641307 A CN 102641307A
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Abstract
The invention discloses a ganoderma lucidum granule and a preparation method thereof, and belongs to the field of ganoderma lucidum processing. The preparation method comprises the steps of grinding residues after alcohol extraction of a ganoderma lucidum fruit body, adding cellulase, belta-glucanase and protease for enzymolysis, heating for enzyme inactivation and concentration to obtain paste, adding an auxiliary material and a wetting agent in the paste, uniformly mixing, and then granulating, drying and finishing, thus obtaining the ganoderma lucidum granule. Cellulase, belta-glucanase and protease are utilized for enzymolysis, the problem of low utilization rate of ganoderma lucidum in the traditional technology is solved and the utilization rate of ganoderma lucidum is improved remarkably; and through enzymolysis of different enzymes, ingredients in the ganoderma lucidum, which cannot be easily absorbed by human bodies, become products which can be easily absorbed by human bodies, the releasing of active ingredients and the product quality are improved, therefore the ganoderma lucidum granule and the preparation method therefore have remarkable economical and social benefits.
Description
Technical field
The invention belongs to the Ganoderma manufacture field, more specifically relate to a kind of glossy ganoderma particle and preparation method thereof.
Background technology
That Ganoderma just is considered to since ancient times is lucky, rich and honour, fine, the life-prolonging symbol, and the title of " Herba mesonae chinensis ", " Ganoderma " is arranged, chinese tradition medical science for a long time a direct-view Ganoderma be strengthening by means of tonics, consolidate set upright, the precious Chinese herbal medicine of life lengthening.365 kinds of Chinese medicines of record are divided into the upper, middle and lower three products, in 120 kinds of top grade Chinese medicines in China's the most ancient existing Chinese medicine ancient books and records Shennong's Herbal; Ganoderma is arranged and is higher than Radix Ginseng, is medicine-feeding, and according to the form and the color of Ganoderma class Ganoderma is divided into six sesames; Think Ganoderma " pacify smart soul, increase wisdom, the beneficial motive; hard muscles and bones, good color, for a long time food is made light of one's life by commiting suicide not oldly, and the angle prolongs life ".Say that Ganoderma is " medicine of going up very much " in " Chinese force in pass ", " and eat it, the day after tomorrow and always ".Put down in writing in the Compendium of Material Medica that the famous medical scholar's Li Shizhen (1518-1593 A.D.) of the Ming Dynasty is write: " Ganoderma bitter in the mouth, flat, nontoxic, the beneficial motive is invigorated blood circulation, and goes into heart hyperemia; help the heart to fill arteries and veins, calm the nerves, lung benefiting gas, tonifying liver gas, invigorating middle warmer; increase wisdom, good color, sharp joint, hard muscles and bones ... " now; Ganoderma was formally recorded by the Pharmacopoeia of the People's Republic of China in 2000 as medicine, and it is again the new resource food of health ministry approval simultaneously, has no side effect, can medicine-food two-purpose." U.S.'s medical herbs pharmacopeia and treatment summary (American Herbal Pharmacopoeia and Therapeutic Compendium) " also recorded Ganoderma.
Summary of the invention
The objective of the invention is to a kind of glossy ganoderma particle and preparation method thereof; Utilize cellulase, 1,4 beta-glucanase and protease hydrolyzed, solved because of the low problem of traditional handicraft Ganoderma utilization rate, feasible utilization to Ganoderma is improved significantly; And zymolysis through different enzymes; Become human body to be prone to the product that absorbs the composition enzymolysis that is difficult in the Ganoderma being absorbed by the body, improve when effective ingredient discharges and also improved product quality, have remarkable economical and social benefit.
For realizing above-mentioned purpose, the present invention adopts following technical scheme:
A kind of method for preparing of glossy ganoderma particle, the Ganoderma sporophore defective material after alcohol extraction adds cellulase, 1,4 beta-glucanase and protease and carries out enzymolysis through pulverizing; With concentrated, the paste that obtains adds adjuvant and wetting agent through the intensification enzyme denaturing; Mix homogeneously is through granulating drying; Granulate promptly gets described glossy ganoderma particle.
The defective material of Ganoderma sporophore after alcohol extraction is through pulverizing, and fineness is at the 60-120 order; Add cellulase, 1,4 beta-glucanase and protease and carry out enzymolysis, enzymolysis degree >=90%.
The parts by weight of the used enzyme of enzymolysis are: 25～75 parts of cellulase, 25～75 parts of 1,4 beta-glucanases, proteinase-10 .1～45 part; The proportion that enzyme accounts for acetic acid-sodium acetate buffer solution is 0.03～1.0 ﹪; Hydrolysis temperature is 25～50 ℃, and enzymolysis time is 0.5～10 hour, and mixing speed is 20～120rpm.
Enzyme-removal temperature is 90～100 ℃, and the enzyme denaturing time is 20～30min.
The adjuvant that adds is a glossy ganoderma ultra-fine powder, and addition is 0.5-5 a times of paste quality.
The wetting agent that adds is a high concentration ethanol solution, and concentration is more than 95%, and addition is 15～65% of a paste quality.
Paste, adjuvant and wetting agent are put into blender stirred 30-150 minute, temperature is controlled at 20-60 ℃, makes its mix homogeneously, processes ointment; Granulate through mesh screen, fineness of the particles is the 10-60 order.
Baking temperature is 30-70 ℃, and drying time, 3-18h was degree below the control moisture to 2%; Through 65 mesh sieve granulate, space temperature is controlled to be 18-26 ℃, and humidity is 20-50%.
The glossy ganoderma particle that a kind of aforesaid method for preparing makes.
Beneficial effect of the present invention:
(1) to adopt cellulase, 1,4 beta-glucanase, protease mixed enzyme be to come enzymolysis through the Ganoderma sporophore of alcohol extraction residue defective material in the present invention, makes the Ganoderma utilization ratio of raw materials is significantly improved, and improved economic benefit.
(2) be that enzymolysis makes that the release of the effective ingredient in the Ganoderma is more thorough with cellulase, 1,4 beta-glucanase, protease mixed enzyme, the product of enzymolysis more is prone to be absorbed by the body and utilize, and has strengthened the quality of product.
(3) cellulose is difficult for directly being absorbed by human body, uses the cellulase degradation cellulose, makes that the effective ingredient in the cellulose is discharged fully, and is easier to absorption by human body.
(4) taking convenience of granule in routine work, also can improve immunity and resisting fatigue during study, and owing to be dissolved in the aqueous solution, big with the contact area of human body, absorb soon, produce effects is rapid, and is convenient, quick.
(5) also can improve the immunity of self by the edible glossy ganoderma granule for some patients that can only eat slop, accelerate resume speed, improve the health care of product, enlarge the colony of consumption.
The specific embodiment
The addition of adjuvant is 0.5～5 times of major ingredient in the glossy ganoderma particle.
The machining process route of glossy ganoderma particle is: Ganoderma sporophore is enzymolysis → concentrate drying → paste Ganoderma vigor composition → addings adjuvant and as the high concentration ethanol → mix homogeneously → granulation → drying of the sieving → granulate that sieves → finished product examination of wetting agent through alcohol extraction remaining defective material → cellulase, 1,4 beta-glucanase, protease mixed enzyme.
Procedure of processing comprises: choose the remaining defective material of Ganoderma sporophore through alcohol extraction, fineness is 60～120 orders, is enzymolysis with cellulase, 1,4 beta-glucanase, protease mixed enzyme; Enzymolysis degree >=90%, the product of enzymolysis through intensification enzyme denaturing and filtration under diminished pressure, pressure is-0.03～-0.10Mpa; Concentrate through 70～100 ℃, concentration time is 1～5 hour, is concentrated into 1 ∕, 3～1 ∕ 10; Product and the adjuvant and the wetting agent that obtain paste enzymolysis product enzymolysis are put into blender and are stirred, and mixing time is 30～150 minutes, makes its mix homogeneously; Granulate through mesh screen, fineness of the particles is 10～60 orders.Then through super-dry, baking temperature is 30～70 ℃, drying time 3～18h, dried granule is crossed sieve (65 order) granulate once more No. four, promptly gets glossy ganoderma particle.
The remarkable advantage of these article is: cellulose can not directly be absorbed by human body, is enzymolysis with cellulase, 1,4 beta-glucanase, protease mixed enzyme, makes that the effective ingredient in the cellulose is discharged fully, and is easier to absorption by human body.Since be dissolved in the aqueous solution, big with the contact area of human body, absorbing soon, produce effects is rapid.Also can improve the immunity of self by the edible glossy ganoderma granule for some patients that can only eat slop, accelerate resume speed, improve the health care of product, enlarge the colony of consumption.
Below be several embodiments of the present invention, further specify the present invention, but the present invention is not limited only to this.
Embodiment 1
The addition of adjuvant is 0.5 times of major ingredient in the glossy ganoderma particle.
The machining process route of glossy ganoderma particle is: Ganoderma sporophore is enzymolysis → concentrate drying → paste Ganoderma vigor composition → addings adjuvant and as the high concentration ethanol → mix homogeneously → granulation → drying of the sieving → granulate that sieves → finished product examination of wetting agent through alcohol extraction remaining defective material → cellulase, 1,4 beta-glucanase, protease mixed enzyme.
Procedure of processing comprises: choose the residue defective material through the Ganoderma sporophore of alcohol extraction, fineness is 60 orders, is enzymolysis with cellulase, 1,4 beta-glucanase, protease mixed enzyme; Enzymolysis degree >=90%, through intensification enzyme denaturing and filtration under diminished pressure, pressure is-0.03Mpa the product of enzymolysis; Concentrate through 70 ℃, concentration time is 1 hour, is concentrated into 1 ∕ 3; The product of enzymolysis and adjuvant and wetting agent are put into blender and are stirred, and mixing time is 30 minutes, make its mix homogeneously; Granulate through mesh screen, fineness of the particles is 10 orders.Then through super-dry, baking temperature is 30 ℃, drying time 3h, dried granule is crossed sieve (65 order) granulate once more No. four, promptly gets glossy ganoderma particle.
Embodiment 2
The addition of adjuvant is 3.5 times of major ingredient in the glossy ganoderma particle.
The machining process route of glossy ganoderma particle is: Ganoderma sporophore is enzymolysis → concentrate drying → paste Ganoderma vigor composition → addings adjuvant and as the high concentration ethanol → mix homogeneously → granulation → drying of the sieving → granulate that sieves → finished product examination of wetting agent through alcohol extraction remaining defective material → cellulase, 1,4 beta-glucanase, protease mixed enzyme.
Procedure of processing comprises: choose the residue defective material through the Ganoderma sporophore of alcohol extraction, fineness is 100 orders, is enzymolysis with cellulase, 1,4 beta-glucanase, protease mixed enzyme; Enzymolysis degree >=90%, through intensification enzyme denaturing and filtration under diminished pressure, pressure is-0.06Mpa the product of enzymolysis; Concentrate through 80 ℃, concentration time is 35 hours, is concentrated into 1 ∕ 7; The product of enzymolysis and adjuvant and wetting agent are put into blender and are stirred, and mixing time is 90 minutes, make its mix homogeneously; Granulate through mesh screen, fineness of the particles is 40 orders.Then through super-dry, baking temperature is 50 ℃, drying time 9h, dried granule is crossed sieve (65 order) granulate once more No. four, promptly gets glossy ganoderma particle.
Embodiment 3
The addition of adjuvant is 5 times of major ingredient in the glossy ganoderma particle.
The machining process route of glossy ganoderma particle is: Ganoderma sporophore is enzymolysis → concentrate paste Ganoderma vigor composition → addings adjuvant and as the high concentration ethanol → mix homogeneously → granulation → drying of the sieving → granulate that sieves → finished product examination of wetting agent through alcohol extraction remaining defective material → cellulase, 1,4 beta-glucanase, protease mixed enzyme.
Procedure of processing comprises: choose through the remaining Ganoderma sporophore defective material of alcohol extraction, fineness is 120 orders, is enzymolysis with cellulase, 1,4 beta-glucanase, protease mixed enzyme; Enzymolysis degree >=90%, through intensification enzyme denaturing and filtration under diminished pressure, pressure is-0.10Mpa the product of enzymolysis; Concentrate through 100 ℃, concentration time is 5 hours, is concentrated into 1 ∕ 10; The product of enzymolysis and adjuvant and wetting agent are put into blender and are stirred, and mixing time is 150 minutes, make its mix homogeneously; Granulate through mesh screen, fineness of the particles is 60 orders.Then through super-dry, baking temperature is 70 ℃, drying time 18h, dried granule is crossed sieve (65 order) granulate once more No. four, promptly gets glossy ganoderma particle.
The above is merely preferred embodiment of the present invention, and all equalizations of doing according to claim of the present invention change and modify, and all should belong to covering scope of the present invention.
Claims (9)
1. the method for preparing of a glossy ganoderma particle is characterized in that: the defective material of Ganoderma sporophore after alcohol extraction adds cellulase, 1,4 beta-glucanase and protease and carries out enzymolysis through pulverizing; With concentrated, the paste that obtains adds adjuvant and wetting agent through the intensification enzyme denaturing; Mix homogeneously is through granulating drying; Granulate promptly gets described glossy ganoderma particle.
2. the method for preparing of glossy ganoderma particle according to claim 1 is characterized in that: the defective material of Ganoderma sporophore after alcohol extraction is through pulverizing, and fineness is at the 60-120 order; Add cellulase, 1,4 beta-glucanase and protease and carry out enzymolysis, enzymolysis degree >=90%.
3. the method for preparing of glossy ganoderma particle according to claim 1, it is characterized in that: the parts by weight of the used enzyme of enzymolysis are: 25～75 parts of cellulase, 25～75 parts of 1,4 beta-glucanases, proteinase-10 .1～45 part; The proportion that enzyme accounts for acetic acid-sodium acetate buffer solution is 0.03～1.0 ﹪; Hydrolysis temperature is 25～50 ℃, and enzymolysis time is 0.5～10 hour, and mixing speed is 20～120rpm.
4. the method for preparing of glossy ganoderma particle according to claim 1, it is characterized in that: enzyme-removal temperature is 90～100 ℃, the enzyme denaturing time is 20～30min.
5. the method for preparing of glossy ganoderma particle according to claim 1, it is characterized in that: the adjuvant of adding is a glossy ganoderma ultra-fine powder, addition be the paste quality 0.5-5 doubly.
6. the method for preparing of glossy ganoderma particle according to claim 1, it is characterized in that: the wetting agent of adding is a high concentration ethanol solution, and concentration is more than 95%, and addition is 15～65% of a paste quality.
7. the method for preparing of glossy ganoderma particle according to claim 1 is characterized in that: paste, adjuvant and wetting agent are put into blender stirred 30-150 minute, temperature is controlled at 20-60 ℃, makes its mix homogeneously, processes ointment; Granulate through mesh screen, fineness of the particles is the 10-60 order.
8. the method for preparing of glossy ganoderma particle according to claim 1, it is characterized in that: baking temperature is 30-70 ℃, drying time, 3-18h was degree below the control moisture to 2%; Through 65 mesh sieve granulate, space temperature is controlled to be 18-26 ℃, and humidity is 20-50%.
9. glossy ganoderma particle that method for preparing as claimed in claim 1 makes.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105995966A (en) * | 2016-06-20 | 2016-10-12 | 张勇 | Preparation method of enzymolysis ganoderma lucidum powder |
| CN113678921A (en) * | 2021-08-27 | 2021-11-23 | 武平县营林公司 | Superfine grinding enzymolysis production process of purple lucid ganoderma instant tea |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105995966A (en) * | 2016-06-20 | 2016-10-12 | 张勇 | Preparation method of enzymolysis ganoderma lucidum powder |
| CN113678921A (en) * | 2021-08-27 | 2021-11-23 | 武平县营林公司 | Superfine grinding enzymolysis production process of purple lucid ganoderma instant tea |
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| CN102641307B (en) | 2014-03-19 |
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