CN102583376A - 纳米TiC粉末及其制备方法和应用 - Google Patents
纳米TiC粉末及其制备方法和应用 Download PDFInfo
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- CN102583376A CN102583376A CN2012100671810A CN201210067181A CN102583376A CN 102583376 A CN102583376 A CN 102583376A CN 2012100671810 A CN2012100671810 A CN 2012100671810A CN 201210067181 A CN201210067181 A CN 201210067181A CN 102583376 A CN102583376 A CN 102583376A
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- tic powder
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- 239000000843 powder Substances 0.000 title claims abstract description 67
- 238000002360 preparation method Methods 0.000 title claims abstract description 22
- MTPVUVINMAGMJL-UHFFFAOYSA-N trimethyl(1,1,2,2,2-pentafluoroethyl)silane Chemical compound C[Si](C)(C)C(F)(F)C(F)(F)F MTPVUVINMAGMJL-UHFFFAOYSA-N 0.000 title abstract description 49
- 238000005245 sintering Methods 0.000 claims abstract description 30
- 229930006000 Sucrose Natural products 0.000 claims abstract description 23
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims abstract description 23
- 239000002245 particle Substances 0.000 claims abstract description 16
- YHWCPXVTRSHPNY-UHFFFAOYSA-N butan-1-olate;titanium(4+) Chemical compound [Ti+4].CCCC[O-].CCCC[O-].CCCC[O-].CCCC[O-] YHWCPXVTRSHPNY-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000003960 organic solvent Substances 0.000 claims abstract description 12
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract description 11
- 238000006243 chemical reaction Methods 0.000 claims abstract description 7
- 238000001035 drying Methods 0.000 claims abstract description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical group CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 24
- 239000005720 sucrose Substances 0.000 claims description 22
- 230000032683 aging Effects 0.000 claims description 10
- 239000008367 deionised water Substances 0.000 claims description 8
- 229910021641 deionized water Inorganic materials 0.000 claims description 8
- 239000000463 material Substances 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 229960000583 acetic acid Drugs 0.000 claims description 4
- 230000029087 digestion Effects 0.000 claims description 2
- 230000035484 reaction time Effects 0.000 claims description 2
- 238000003756 stirring Methods 0.000 abstract description 6
- 235000011194 food seasoning agent Nutrition 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 abstract 1
- 229960004793 sucrose Drugs 0.000 abstract 1
- 239000002253 acid Substances 0.000 description 10
- 238000000034 method Methods 0.000 description 9
- 239000002994 raw material Substances 0.000 description 6
- 238000001514 detection method Methods 0.000 description 5
- 238000005303 weighing Methods 0.000 description 5
- 238000005520 cutting process Methods 0.000 description 3
- 239000007921 spray Substances 0.000 description 3
- 230000003245 working effect Effects 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 239000000919 ceramic Substances 0.000 description 2
- 238000005229 chemical vapour deposition Methods 0.000 description 2
- 208000012839 conversion disease Diseases 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 230000001105 regulatory effect Effects 0.000 description 2
- 238000003980 solgel method Methods 0.000 description 2
- 239000010936 titanium Substances 0.000 description 2
- 229910052719 titanium Inorganic materials 0.000 description 2
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 2
- 229910010413 TiO 2 Inorganic materials 0.000 description 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 239000003082 abrasive agent Substances 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000006229 carbon black Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000012797 qualification Methods 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
- 239000011378 shotcrete Substances 0.000 description 1
- 230000035882 stress Effects 0.000 description 1
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- Ceramic Products (AREA)
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Compositions Of Oxide Ceramics (AREA)
Abstract
Description
Claims (9)
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CN201210067181.0A CN102583376B (zh) | 2012-03-15 | 2012-03-15 | 纳米TiC粉末及其制备方法和应用 |
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CN201210067181.0A CN102583376B (zh) | 2012-03-15 | 2012-03-15 | 纳米TiC粉末及其制备方法和应用 |
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CN102583376A true CN102583376A (zh) | 2012-07-18 |
CN102583376B CN102583376B (zh) | 2014-07-30 |
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Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102876094A (zh) * | 2012-10-19 | 2013-01-16 | 广西梧州港德硬质合金制造有限公司 | 一种硬质合金烧结防粘涂料 |
CN103265032A (zh) * | 2013-06-16 | 2013-08-28 | 桂林理工大学 | 以TiOSO4和季戊四醇分别为钛源和碳源制备TiC粉体的方法 |
CN103274409A (zh) * | 2013-06-01 | 2013-09-04 | 桂林理工大学 | 以TiOSO4和酚醛树脂分别为钛源和碳源制备超细TiC粉体的方法 |
CN103274411A (zh) * | 2013-06-16 | 2013-09-04 | 桂林理工大学 | 以TiOSO4和蔗糖分别为钛源和碳源制备TiC粉体的方法 |
CN103274412A (zh) * | 2013-06-16 | 2013-09-04 | 桂林理工大学 | 以钛酸四丁酯和酚醛树脂分别为钛源和碳源制备TiC粉体的方法 |
CN103332691A (zh) * | 2013-06-25 | 2013-10-02 | 桂林理工大学 | 以钛酸四丁酯和蔗糖分别为钛源和碳源制备TiC粉体的方法 |
CN103435355A (zh) * | 2013-08-28 | 2013-12-11 | 桂林理工大学 | 以钛酸四丁酯和蔗糖分别为钛源和碳源制备TiCN粉体的方法 |
CN104626679A (zh) * | 2015-02-15 | 2015-05-20 | 珠海拾比佰彩图板股份有限公司 | 一种覆膜铝板及其制备方法 |
CN109133062A (zh) * | 2018-10-10 | 2019-01-04 | 西南交通大学 | 一种超稳定Ti3C2悬浮液的制备方法 |
CN109956750A (zh) * | 2019-03-28 | 2019-07-02 | 西北工业大学 | 碱金属热电转换器多孔碳化钛电极材料的制备方法 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101367669A (zh) * | 2008-09-27 | 2009-02-18 | 武汉科技大学 | 含B4C-C复合粉体和纳米TiC粉体的低碳镁碳砖及其制备方法 |
CN101486462A (zh) * | 2009-02-23 | 2009-07-22 | 潍坊学院 | 一种碳化钛微粉的制备方法 |
CN101565183A (zh) * | 2009-05-31 | 2009-10-28 | 四川大学 | 表面修饰高能球磨法分散纳米TiC粉体 |
CN101891192A (zh) * | 2010-07-02 | 2010-11-24 | 山东大学 | 一种固相反应合成碳化物纳米粉体的方法 |
-
2012
- 2012-03-15 CN CN201210067181.0A patent/CN102583376B/zh active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101367669A (zh) * | 2008-09-27 | 2009-02-18 | 武汉科技大学 | 含B4C-C复合粉体和纳米TiC粉体的低碳镁碳砖及其制备方法 |
CN101486462A (zh) * | 2009-02-23 | 2009-07-22 | 潍坊学院 | 一种碳化钛微粉的制备方法 |
CN101565183A (zh) * | 2009-05-31 | 2009-10-28 | 四川大学 | 表面修饰高能球磨法分散纳米TiC粉体 |
CN101891192A (zh) * | 2010-07-02 | 2010-11-24 | 山东大学 | 一种固相反应合成碳化物纳米粉体的方法 |
Non-Patent Citations (1)
Title |
---|
CHENG GUO,ET.AL: "Fabrication of hierarchical porous carbide-derived carbons by chlorination of mesoporous titanium carbides", 《新型炭材料》, vol. 24, no. 3, 30 September 2009 (2009-09-30) * |
Cited By (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102876094B (zh) * | 2012-10-19 | 2015-04-01 | 广西梧州港德硬质合金制造有限公司 | 一种硬质合金烧结防粘涂料 |
CN102876094A (zh) * | 2012-10-19 | 2013-01-16 | 广西梧州港德硬质合金制造有限公司 | 一种硬质合金烧结防粘涂料 |
CN103274409A (zh) * | 2013-06-01 | 2013-09-04 | 桂林理工大学 | 以TiOSO4和酚醛树脂分别为钛源和碳源制备超细TiC粉体的方法 |
CN103265032A (zh) * | 2013-06-16 | 2013-08-28 | 桂林理工大学 | 以TiOSO4和季戊四醇分别为钛源和碳源制备TiC粉体的方法 |
CN103274411A (zh) * | 2013-06-16 | 2013-09-04 | 桂林理工大学 | 以TiOSO4和蔗糖分别为钛源和碳源制备TiC粉体的方法 |
CN103274412A (zh) * | 2013-06-16 | 2013-09-04 | 桂林理工大学 | 以钛酸四丁酯和酚醛树脂分别为钛源和碳源制备TiC粉体的方法 |
CN103332691A (zh) * | 2013-06-25 | 2013-10-02 | 桂林理工大学 | 以钛酸四丁酯和蔗糖分别为钛源和碳源制备TiC粉体的方法 |
CN103435355A (zh) * | 2013-08-28 | 2013-12-11 | 桂林理工大学 | 以钛酸四丁酯和蔗糖分别为钛源和碳源制备TiCN粉体的方法 |
CN104626679A (zh) * | 2015-02-15 | 2015-05-20 | 珠海拾比佰彩图板股份有限公司 | 一种覆膜铝板及其制备方法 |
CN104626679B (zh) * | 2015-02-15 | 2016-05-18 | 珠海拾比佰彩图板股份有限公司 | 一种覆膜铝板及其制备方法 |
CN109133062A (zh) * | 2018-10-10 | 2019-01-04 | 西南交通大学 | 一种超稳定Ti3C2悬浮液的制备方法 |
CN109133062B (zh) * | 2018-10-10 | 2021-10-01 | 西南交通大学 | 一种超稳定Ti3C2悬浮液的制备方法 |
CN109956750A (zh) * | 2019-03-28 | 2019-07-02 | 西北工业大学 | 碱金属热电转换器多孔碳化钛电极材料的制备方法 |
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CN102583376B (zh) | 2014-07-30 |
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Denomination of invention: Nano titanium carbide (TiC) powder and preparation method and application thereof Effective date of registration: 20181012 Granted publication date: 20140730 Pledgee: Huarong Bank of Xiangjiang Limited by Share Ltd. 51 Zhuzhou branch Pledgor: ZHUZHOU JINGGONG CEMENTED CARBIDE Co.,Ltd. Registration number: 2018980000175 |
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Date of cancellation: 20190906 Granted publication date: 20140730 Pledgee: Huarong Bank of Xiangjiang Limited by Share Ltd. 51 Zhuzhou branch Pledgor: ZHUZHOU JINGGONG CEMENTED CARBIDE Co.,Ltd. Registration number: 2018980000175 |
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Denomination of invention: Nano titanium carbide (TiC) powder and preparation method and application thereof Effective date of registration: 20191101 Granted publication date: 20140730 Pledgee: Huarong Bank of Xiangjiang Limited by Share Ltd. 51 Zhuzhou branch Pledgor: ZHUZHOU JINGGONG CEMENTED CARBIDE Co.,Ltd. Registration number: Y2019980000370 |
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Date of cancellation: 20210422 Granted publication date: 20140730 Pledgee: Huarong Bank of Xiangjiang Limited by Share Ltd. 51 Zhuzhou branch Pledgor: ZHUZHOU JINGGONG CEMENTED CARBIDE Co.,Ltd. Registration number: Y2019980000370 |
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Denomination of invention: Nano tic powder and its preparation method and Application Effective date of registration: 20211123 Granted publication date: 20140730 Pledgee: Huarong Bank of Xiangjiang Limited by Share Ltd. 51 Zhuzhou branch Pledgor: ZHUZHOU JINGGONG CEMENTED CARBIDE Co.,Ltd. Registration number: Y2021980013080 |
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Date of cancellation: 20221027 Granted publication date: 20140730 Pledgee: Huarong Bank of Xiangjiang Limited by Share Ltd. 51 Zhuzhou branch Pledgor: ZHUZHOU JINGGONG CEMENTED CARBIDE Co.,Ltd. Registration number: Y2021980013080 |