CN102503574B - Manufacture craft for pale yellowish green colored glaze of Ru porcelain - Google Patents
Manufacture craft for pale yellowish green colored glaze of Ru porcelain Download PDFInfo
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- CN102503574B CN102503574B CN2011103395907A CN201110339590A CN102503574B CN 102503574 B CN102503574 B CN 102503574B CN 2011103395907 A CN2011103395907 A CN 2011103395907A CN 201110339590 A CN201110339590 A CN 201110339590A CN 102503574 B CN102503574 B CN 102503574B
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Abstract
A manufacture craft for pale yellowish green colored glaze of Ru porcelain includes the steps of utilizing kaolin, melilite, black feldspar, white feldspar, quartz, calcite, potassium feldspar and zinc oxide as glaze raw materials, performing wet grinding with water after the green body raw materials are crushed and adjusting the moisture content of slurry into 58-60%; placing a wiped biscuit into glaze slurry for dipping; and placing the dipped biscuit into a furnace for firing in an oxidizing atmosphere and then for firing in a reduction atmosphere after the furnace temperature rises to 1058 DEG C, holding at the temperature of 1058 DEG C prior to that the temperature rises to 1245 DEG C, and holding for half an hour prior to firing off for cooling, so that the pale yellowish green colored glaze is prepared. In the technical scheme, all raw material components are firmly bonded, the body color of Ru porcelain teaware fired by the preparation method is pale yellowish green, and the Ru porcelain teaware is attractive in appearance.
Description
Technical field
The present invention relates to a kind of manufacture craft of your enamel, specifically a kind of manufacture craft of your porcelain pale yellowish green colored glaze.
Background technology
Your porcelain is one of China's five your name's porcelain, and its manufacturing process is once once lost, by technician's lucubrate, now resumes production.It is modelled after an antique as main that but your current porcelain making still be take, and also there is certain deficiency in its manufacture craft.Because of it, the craft died out and the fine technique was lost, calcines your porcelain always in conceptual phase, finds that after deliberation your enamel look rises former in pale yellowish green, and this glaze colours not only color and luster is pure, bright and not dazzling, is the main glaze colours of Song dynasty common cave.And at present to the research of your enamel look, physical chemistry form and burn till, the moulding process flow process clearly do not grasp its rule.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of manufacture craft of your porcelain pale yellowish green colored glaze, your the porcelain tea set burnt out, and the tire look is prase, good looking appearance.
The present invention solves the problems of the technologies described above adopted technical scheme to be: the manufacture craft of your porcelain pale yellowish green colored glaze, adopt wind scoop soil, melilith, black feldspar, white feldspar, quartz, calcite, potassium felspar sand and zinc oxide as the glaze raw material, the weight percent of each raw material add-on is: wind scoop soil 14-16%, melilith 16-18%, black feldspar 8-10%, white feldspar 17-20%, quartzy 17-19%, calcite 15-17%, potassium felspar sand 5-6%, zinc oxide 0.5-1.5%, and its preparation method is:
Step 1, by after described glaze raw material pulverizing, mix and to put into ball mill according to aforementioned proportion, add the water of mixing raw material gross weight 29-33%, start wet-milling 14-18 hour, cross 300 mesh sieves through the slip of wet-milling, after standing 24 hours, the water content of slip is adjusted into to 58-60%, standby;
Step 2, water are wiped base to biscuit, the glaze of step 1 being made according to clockwise or counterclockwise direction with waddy when wiping base is stirred, during stirring from the center of slip, and to circumference, move gradually, churning time is 20 minutes, after having stirred, biscuit after the wiping base is put into to the glaze slip, watered glaze at the biscuit outside surface, after watering glaze and completing, the finishing base substrate;
Step 3, the base substrate that step 2 is trimmed are put into kiln, in kiln, ventilate, and base substrate is fired in oxidizing atmosphere, control the firing temperature in kiln, make temperature evenly rise to 671 ℃ in 2 hours, then evenly be warming up to 887 ℃ in 1 hour, then be warming up to 1058 ℃ in 1 hour; Reduce the ventilation of kiln, make in stove to change into reducing atmosphere, base substrate is incubated and fires 30 minutes under the condition of 1058 ℃; then the speed with 1 ℃ of per minute heats up gradually, after being warming up to 1245 ℃, is incubated half an hour; cease fire, naturally cool to room temperature, complete making.
The invention has the beneficial effects as follows: select powder kind raw material in glaze, recall enamel germ, character according to individual raw material, heating curve by controlling firing temperature and the state of different firing atmospheres, variation etc., the pottery be fired into, surface journey prase, this glaze colours not only color and luster is pure, and bright and not dazzling.
Embodiment
The manufacture craft of your porcelain pale yellowish green colored glaze, adopt wind scoop soil, melilith, black feldspar, white feldspar, quartz, calcite, potassium felspar sand and zinc oxide as the glaze raw material, the weight percent of each raw material add-on is: wind scoop soil 14-16%, melilith 16-18%, black feldspar 8-10%, white feldspar 17-20%, quartzy 17-19%, calcite 15-17%, potassium felspar sand 5-6%, zinc oxide 0.5-1.5%, and its preparation method is:
Step 1, by after described glaze raw material pulverizing, mix and to put into ball mill according to aforementioned proportion, add the water of mixing raw material gross weight 29-33%, start wet-milling 14-18 hour, cross 300 mesh sieves through the slip of wet-milling, after standing 24 hours, the water content of slip is adjusted into to 58-60%, standby;
Step 2, water are wiped base to biscuit, the glaze of step 1 being made according to clockwise or counterclockwise direction with waddy when wiping base is stirred, during stirring from the center of slip, and to circumference, move gradually, churning time is 20 minutes, after having stirred, biscuit after the wiping base is put into to the glaze slip, watered glaze at the biscuit outside surface, after watering glaze and completing, the finishing base substrate;
Step 3, the base substrate that step 2 is trimmed are put into kiln, in kiln, ventilate, and base substrate is fired in oxidizing atmosphere, control the firing temperature in kiln, make temperature evenly rise to 671 ℃ in 2 hours, then evenly be warming up to 887 ℃ in 1 hour, then be warming up to 1058 ℃ in 1 hour; Reduce the ventilation of kiln, make in stove to change into reducing atmosphere, base substrate is incubated and fires 30 minutes under the condition of 1058 ℃; then the speed with 1 ℃ of per minute heats up gradually, after being warming up to 1245 ℃, is incubated half an hour; cease fire, naturally cool to room temperature, complete making.
In the present invention, potassium felspar sand used is the wind scoop feldspar.
In the present invention wind scoop used soil, wind scoop feldspar be porcelain fire in normally used common raw material, can on market, buy.Wherein, wind scoop soil, be a kind of kaolin, and the percentage composition of its major ingredient is Al
2O
338.9%, SiO
243.57%, Fe
2O
31.2%, CaO0.06%, MgO0.59%, K
2O0.91%, Na
2O0.17%, TiO
20.98%, other foreign matter content is 13.62%.At State Administration for Quality Supervision and Inspection and Quarantine's bulletin, 2004 No. 94 file is mentioned.The wind scoop feldspar, be wind scoop area feldspar, and the percentage composition of its major ingredient is Al
2O
313.43%, SiO
270.32%, Fe
2O
30.57%, CaO0.27%, MgO0.97%, K
2O5.81%, Na
2O3.47%, TiO
20.07%, other foreign matter content is 0.07%.
In making method of the present invention, for the raw material of selecting, not only the composition of blank raw material has considerable influence to the intensity of finished product, and the difference of glaze is mainly manifested in the impact on your porcelain outward appearance, therefore for the special requirement that have of glaze, adopt the special glaze adopted while firing your porcelain to get final product.In making processes, the method for repaired biscuit, wiping base all can be carried out according to ordinary process.The repaired biscuit main purpose is finishing mold surface, equating limit mouth burr etc.Wipe base and use soft and wet cloth wiping billet surface, stick with paste billet surface hair on the neck eye with pulp-water, and be beneficial to each adhering components.In sintering procedure, flame atmosphere when oxidizing atmosphere used is the oxygen supply abundance in the complete combustion of fuel situation, in this process, the interior air visibility of furnace chamber is good, can be observed shape of product.Reducing atmosphere is the oxygen supply deficiency, and the flame atmosphere in the non-complete combustion of fuel situation now produces a large amount of carbon monoxide, has reductive action, more muddy in furnace chamber, smudgy in this process.
In the deironing described in step 1 for utilizing the deironing of high-strength magnetic iron staff, the glaze slip with from high-strength bar magnet laminar flow mistake, calculated a deironing.
Original stirring is stirred by minipump, the mixing effect of minipump is poor, can not reach the effect of removing vacuum, in the stirring described in step 1, is in order to remove vacuum, when glaze just goes out to grind, need to manually to glaze slip, be stirred the ，Cong center with woodenware and start to stir clockwise or counterclockwise, and be moved to circumference gradually, slowly stir about 20 minutes and get final product, glaze is essential through removing vacuum operating before using, more standing 24 hours, after having placed, can use.
Embodiment 1
The manufacture craft of your porcelain pale yellowish green colored glaze, adopt wind scoop soil, melilith, black feldspar, white feldspar, quartz, calcite, potassium felspar sand and zinc oxide as the glaze raw material, the weight percent of each raw material add-on is: wind scoop soil 15%, melilith 17%, black feldspar 9%, white feldspar 19%, quartz 18%, calcite 16%, potassium felspar sand 5%, zinc oxide 1%, and its preparation method is:
Step 1, by after described glaze raw material pulverizing, mix and to put into ball mill according to aforementioned proportion, add the water of mixing raw material gross weight 29%, start wet-milling 14 hours, cross 300 mesh sieves through the slip of wet-milling, after standing 24 hours, the water content of slip is adjusted into to 60%, standby;
Step 2, water are wiped base to biscuit, the glaze of step 1 being made according to clockwise or counterclockwise direction with waddy when wiping base is stirred, during stirring from the center of slip, and to circumference, move gradually, churning time is 20 minutes, after having stirred, biscuit after the wiping base is put into to the glaze slip, watered glaze at the biscuit outside surface, after watering glaze and completing, the finishing base substrate;
Step 3, the base substrate that step 2 is trimmed are put into kiln, in kiln, ventilate, and base substrate is fired in oxidizing atmosphere, control the firing temperature in kiln, make temperature evenly rise to 671 ℃ in 2 hours, then evenly be warming up to 887 ℃ in 1 hour, then be warming up to 1058 ℃ in 1 hour; Reduce the ventilation of kiln, make in stove to change into reducing atmosphere, base substrate is incubated and fires 30 minutes under the condition of 1058 ℃; then the speed with 1 ℃ of per minute heats up gradually, after being warming up to 1245 ℃, is incubated half an hour; cease fire, naturally cool to room temperature, complete making.
Embodiment 2
The manufacture craft of your porcelain pale yellowish green colored glaze, adopt wind scoop soil, melilith, black feldspar, white feldspar, quartz, calcite, potassium felspar sand and zinc oxide as the glaze raw material, the weight percent of each raw material add-on is: wind scoop soil 16%, melilith 16%, black feldspar 8%, white feldspar 20%, quartz 19%, calcite 15%, potassium felspar sand 5%, zinc oxide 1%, and its preparation method is:
Step 1, by after described glaze raw material pulverizing, mix and to put into ball mill according to aforementioned proportion, add the water of mixing raw material gross weight 33%, start wet-milling 18 hours, cross 300 mesh sieves through the slip of wet-milling, after standing 24 hours, the water content of slip is adjusted into to 58%, standby;
Step 2, water are wiped base to biscuit, the glaze of step 1 being made according to clockwise or counterclockwise direction with waddy when wiping base is stirred, during stirring from the center of slip, and to circumference, move gradually, churning time is 20 minutes, after having stirred, biscuit after the wiping base is put into to the glaze slip, watered glaze at the biscuit outside surface, after watering glaze and completing, the finishing base substrate;
Step 3, the base substrate that step 2 is trimmed are put into kiln, in kiln, ventilate, and base substrate is fired in oxidizing atmosphere, control the firing temperature in kiln, make temperature evenly rise to 671 ℃ in 2 hours, then evenly be warming up to 887 ℃ in 1 hour, then be warming up to 1058 ℃ in 1 hour; Reduce the ventilation of kiln, make in stove to change into reducing atmosphere, base substrate is incubated and fires 30 minutes under the condition of 1058 ℃; then the speed with 1 ℃ of per minute heats up gradually, after being warming up to 1245 ℃, is incubated half an hour; cease fire, naturally cool to room temperature, complete making.
Embodiment 3
The manufacture craft of your porcelain pale yellowish green colored glaze, adopt wind scoop soil, melilith, black feldspar, white feldspar, quartz, calcite, potassium felspar sand and zinc oxide as the glaze raw material, the weight percent of each raw material add-on is: wind scoop soil 14%, melilith 18%, black feldspar 10%, white feldspar 17%, quartz 17%, calcite 17%, potassium felspar sand 6%, zinc oxide 1%, and its preparation method is:
Step 1, by after described glaze raw material pulverizing, mix and to put into ball mill according to aforementioned proportion, add the water of mixing raw material gross weight 30%, start wet-milling 16 hours, cross 300 mesh sieves through the slip of wet-milling, after standing 24 hours, the water content of slip is adjusted into to 60%, standby;
Step 2, water are wiped base to biscuit, the glaze of step 1 being made according to clockwise or counterclockwise direction with waddy when wiping base is stirred, during stirring from the center of slip, and to circumference, move gradually, churning time is 20 minutes, after having stirred, biscuit after the wiping base is put into to the glaze slip, watered glaze at the biscuit outside surface, after watering glaze and completing, the finishing base substrate;
Step 3, the base substrate that step 2 is trimmed are put into kiln, in kiln, ventilate, and base substrate is fired in oxidizing atmosphere, control the firing temperature in kiln, make temperature evenly rise to 671 ℃ in 2 hours, then evenly be warming up to 887 ℃ in 1 hour, then be warming up to 1058 ℃ in 1 hour; Reduce the ventilation of kiln, make in stove to change into reducing atmosphere, base substrate is incubated and fires 30 minutes under the condition of 1058 ℃; then the speed with 1 ℃ of per minute heats up gradually, after being warming up to 1245 ℃, is incubated half an hour; cease fire, naturally cool to room temperature, complete making.
The content that the present invention does not narrate is prior art.
Claims (1)
1. the manufacture craft of your porcelain pale yellowish green colored glaze, adopt wind scoop soil, melilith, black feldspar, white feldspar, quartz, calcite, potassium felspar sand and zinc oxide as the glaze raw material, it is characterized in that: the weight percent of each raw material add-on is: wind scoop soil 14-16%, melilith 16-18%, black feldspar 8-10%, white feldspar 17-20%, quartzy 17-19%, calcite 15-17%, potassium felspar sand 5-6%, zinc oxide 1%, and its preparation method is:
Step 1, by after described glaze raw material pulverizing, mix and to put into ball mill according to aforementioned proportion, add the water of mixing raw material gross weight 29-33%, start wet-milling 14-18 hour, cross 300 mesh sieves through the slip of wet-milling, after standing 24 hours, the water content of slip is adjusted into to 58-60%, standby;
Step 2, water are wiped base to biscuit, the glaze of step 1 being made according to clockwise or counterclockwise direction with waddy when wiping base is stirred, during stirring from the center of slip, and to circumference, move gradually, churning time is 20 minutes, after having stirred, biscuit after the wiping base is put into to the glaze slip, watered glaze at the biscuit outside surface, after watering glaze and completing, the finishing base substrate;
Step 3, the base substrate that step 2 is trimmed are put into kiln, in kiln, ventilate, and base substrate is fired in oxidizing atmosphere, control the firing temperature in kiln, make temperature evenly rise to 671 ℃ in 2 hours, then evenly be warming up to 887 ℃ in 1 hour, then be warming up to 1058 ℃ in 1 hour; Reduce the ventilation of kiln, make in stove to change into reducing atmosphere, biscuit is incubated and fires 30 minutes under the condition of 1058 ℃; then the speed with 1 ℃ of per minute heats up gradually, after being warming up to 1245 ℃, is incubated half an hour; cease fire, naturally cool to room temperature, complete making.
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| CN2011103395907A CN102503574B (en) | 2011-11-01 | 2011-11-01 | Manufacture craft for pale yellowish green colored glaze of Ru porcelain |
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| CN104211447B (en) * | 2014-09-10 | 2015-09-30 | 张天庆 | Your porcelain ceregat glaze a kind of, working method and your porcelain, method for cooking |
| CN104496416B (en) * | 2014-11-28 | 2016-08-24 | 冯艳琴 | The manufacture method of the transparent pea green starved glaze of your porcelain |
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| CN104843998B (en) * | 2015-03-30 | 2017-11-21 | 姚瑞平 | Your red glaze of your porcelain and its manufacture craft |
| CN108752050B (en) * | 2018-06-19 | 2020-12-15 | 张玉凤 | Ru porcelain tea dust glaze and preparation method thereof |
| CN109928728B (en) * | 2019-04-10 | 2021-11-30 | 王晟鸣 | Moon white glaze Ru porcelain and preparation method thereof |
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| CN111423120A (en) * | 2020-04-27 | 2020-07-17 | 许昌学院 | Preparation method of pine and cypress green ceramic glaze |
| CN113058497A (en) * | 2021-03-26 | 2021-07-02 | 龙泉市九龙青瓷有限公司 | Glaze debugging device and method |
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Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101058476A (en) * | 2007-03-27 | 2007-10-24 | 王振芳 | Antiseep glaze material and glair for Ruyao kiln package container and preparing method thereof |
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| JPH02102179A (en) * | 1988-10-05 | 1990-04-13 | Yamaka Toki Kk | Calcination of white porcelain |
| JP2742293B2 (en) * | 1989-04-25 | 1998-04-22 | 東陶機器株式会社 | Manufacturing method of decorative ceramics |
| CN101747089B (en) * | 2008-12-16 | 2012-01-25 | 郭秀贞 | Ru agate glaze and processing method and application thereof |
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| CN101058476A (en) * | 2007-03-27 | 2007-10-24 | 王振芳 | Antiseep glaze material and glair for Ruyao kiln package container and preparing method thereof |
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