CN102454226A - Wet paved/pre-paved polymer self-adhesive waterproofing rolled material and preparation method thereof - Google Patents
Wet paved/pre-paved polymer self-adhesive waterproofing rolled material and preparation method thereof Download PDFInfo
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- CN102454226A CN102454226A CN2010105293903A CN201010529390A CN102454226A CN 102454226 A CN102454226 A CN 102454226A CN 2010105293903 A CN2010105293903 A CN 2010105293903A CN 201010529390 A CN201010529390 A CN 201010529390A CN 102454226 A CN102454226 A CN 102454226A
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Abstract
The invention provides a wet paved/pre-paved polymer self-adhesive waterproofing rolled material which comprises a modified asphalt self-adhesive layer. The modified bitumen self-adhesive layer contains petroleum asphalt, modifier, softener, tackifier and filler. The wet paved/pre-paved polymer self-adhesive waterproofing rolled material which is prepared from the by taking a polymer resin layer as a base has a long use life, stable chemical properties and excellent waterproof effect, wherein the modified asphalt self-adhesive layer is prepared through single side or double side adhering.
Description
Technical field
The present invention relates to adhesive polymer waterproof roll of a kind of pre-spread/wet shop and preparation method thereof.
Background technology
Waterproof roll mainly is to be used for construction wall, roofing and tunnel, highway, subway, refuse landfill etc. to locate; Play a kind of flexible building material product that is curled into web-like of resisting extraneous rainwater, ground water seepage; Being connected as leakproof between engineering foundation and the building, is the first road barrier of whole engineering waterproofing, and whole engineering is played crucial effects; Can be divided into bituminous waterproofing material, modified-high polymer waterproof roll material and synthetic polymeric waterproofing material three major types asphalt water-proof coiled material asphalt water-proof coiled material according to its main waterproof composition material is after invading pitching on the basic tire (like body paper, fabric); The curled sheet waterproofing materials of processing at the isolated material of surperficial spreading powdery or sheet again, therefore, the traditional asphalt waterproofing materials is short application life; Poor chemical stability, and waterproof effect is undesirable.
Summary of the invention
The present invention aims to provide a kind of long service life, stable chemical performance, and the adhesive polymer waterproof roll of the pre-spread of good water-proof effect/wet shop, and for realizing the purpose of foregoing invention, the present invention adopts following technical scheme to solve:
The adhesive polymer waterproof roll of a kind of pre-spread/wet shop, the adhesive polymer waterproof roll of said pre-spread/wet shop comprises the modified bitumen self-adhesive layer, contains petroleum bitumen, modifier, softening agent, tackifier and filler in the said modified bitumen self-adhesive layer.
Preferably, said modifier is one or more of s-B-S (SBS), polypropylene (PP).
Preferably, said softening agent is second line of distillation oil, subtracts one or more of third fractional oil.
Preferably, stating tackifier is cycloparaffin resin.
Preferably, said filler is a French chalk.
Preferably, said modified bitumen self-adhesive layer prescription is (pressing mass fraction):
Petroleum bitumen 50-60;
Modifier 10-20;
Softening agent 5-15;
Tackifier 1-10;
Filler 10-20.
Preferably, said modified bitumen self-adhesive layer prescription is (pressing mass fraction):
Petroleum bitumen 54;
Modifier 15;
Softening agent 10;
Tackifier 5;
Filler 16.
Preferably; At least one side of said modified bitumen self-adhesive layer is equipped with polymer resin layer, and said polymer resin layer is one or more in blend ECB, polyvinylchloride and the high density polyethylene of ethylene-vinyl acetate copolymer EVA, ethene vinyl acetate and pitch.
Preferably, also be covered with barrier film outside the said polymer resin layer.
And the adhesive polymer waterproof roll preparation method of a kind of pre-spread/wet shop, may further comprise the steps:
In part petroleum bitumen, add modifier, softening agent and be warming up to 180 ℃-200 ℃, stirred 180 minutes, make modified materials;
Modified materials is squeezed into another sky agitator tank through colloid mill;
Add another kind of modifier (PP), filler in the modified materials in batches, every batch of interval 150 minutes, and continue to stir;
Add tackifier and keep 180 ℃, continue to stir with the residue asphalt temperature;
Modified bitumen is coated in polymer resin layer one or both sides with modified bitumen from sizing through immersion trough from sizing.
Can know that by such scheme the present invention is the tire base with the polymer resin layer, adhere to the modified bitumen self-adhesive layer of preparation through single or double and form pre-spread/wet adhesive polymer waterproof roll of spreading.Macromolecule resin has following advantage: it is superior, tasteless, pollution-free 1, to have long service life, weather-proof, ageing-resistant, waterproof, antiseptic property, and construction safety is easy, and the duration is short.2, protection against the tide, mildew-resistant, smooth abrasion-proof, induration are nontoxic.3, the chemicals erosion performance of coating acid and alkali resistance, salt and oils and anti-all kinds of solvents is strong, good anti-flammability is arranged, insulating properties.And the pitch self-adhesive layer of the adhesive polymer waterproof roll of pre-spread/wet shop can be that main construction body produces ion and exchanges with concrete, makes the two firm being bonded together, and forms gapless waterproof sealing system.
The specific embodiment
Below in conjunction with through embodiment the present invention being set forth, yet protection scope of the present invention is not only to be confined to following examples.The those of ordinary skill of affiliated technical field all can be realized the object of the invention according to content disclosed by the invention.
The adhesive polymer waterproof roll of pre-spread/wet shop, the adhesive polymer waterproof roll of said pre-spread/wet shop comprises the modified bitumen self-adhesive layer, contains petroleum bitumen, modifier, softening agent, tackifier and filler in the said modified bitumen self-adhesive layer.
Preferably, said modified bitumen self-adhesive layer prescription is (pressing mass fraction):
Petroleum bitumen 50-60;
Modifier 10-20;
Softening agent 5-15;
Tackifier 1-10;
Filler 10-20.
At least one side of said modified bitumen self-adhesive layer is equipped with polymer resin layer, and said polymer resin layer is one or more in blend ECB, polyvinylchloride and the high density polyethylene of ethylene-vinyl acetate copolymer EVA, ethene vinyl acetate and pitch.
Further, the polymer resin layer outside also is covered with barrier film.
Embodiment 1:
Get petroleum bitumen 25g, in petroleum bitumen, add 5g s-B-S (SBS) as modifier, second line of distillation oil 5g is as softening agent and be warming up to 180 ℃, stirs 180 minutes, makes modified materials;
Modified materials is squeezed into another sky agitator tank through colloid mill;
Add another kind of modifier polypropylene (PP) 2.5g in the modified materials, reach 300 purpose French chalk 5g, stir after 150 minutes, add modifier polypropylene (PP) 2.5g once more, reach 300 purpose French chalk 5g as filler as filler;
Add the 1g cycloparaffin resin and keep 180 ℃, continue to stir as tackifier and 25g asphalt temperature;
Modified bitumen is coated in ethylene-vinyl acetate copolymer (EVA resin) side with modified bitumen from sizing through immersion trough from sizing, processes the adhesive polymer waterproof roll of pre-spread/wet shop.
As the improvement of the foregoing description scheme, ethylene-vinyl acetate copolymer (EVA resin) outside also is covered with barrier film.
Embodiment 2:
Get petroleum bitumen 30g, in petroleum bitumen, add 10g s-B-S (SBS) as modifier, second line of distillation oil 10g is as softening agent and be warming up to 200 ℃, stirs 180 minutes, makes modified materials;
Modified materials is squeezed into another sky agitator tank through colloid mill;
Add another kind of modifier polypropylene (PP) 5g in the modified materials, reach 300 purpose French chalk 10g, stir after 150 minutes, add modifier polypropylene (PP) 5g once more, reach 300 purpose French chalk 10g as filler as filler;
Add the 10g cycloparaffin resin and keep 180 ℃, continue to stir as tackifier and 30g asphalt temperature;
Modified bitumen is coated in blend (ECB) side of ethene vinyl acetate and pitch with modified bitumen from sizing through immersion trough from sizing, processes the adhesive polymer waterproof roll of pre-spread/wet shop.
As the improvement of the foregoing description scheme, the blend of ethene vinyl acetate and pitch (ECB) outside also is covered with barrier film.
Embodiment 3:
Get petroleum bitumen 27g, in petroleum bitumen, add 7g s-B-S (SBS) as modifier, subtract third fractional oil 10g as softening agent and be warming up to 200 ℃, stirred 180 minutes, make modified materials;
Modified materials is squeezed into another sky agitator tank through colloid mill;
Add another kind of modifier polypropylene (PP) 4g in the modified materials, reach 300 purpose French chalk 8g, stir after 150 minutes, add modifier polypropylene (PP) 4g once more, reach 300 purpose French chalk 8g as filler as filler;
Add the 10g cycloparaffin resin and keep 180 ℃, continue to stir as tackifier and 27g asphalt temperature;
Modified bitumen is coated in the both sides of polyvinyl chloride (PVC) or high density polyethylene (HDPE) (HDPE) or both mixture with modified bitumen from sizing through immersion trough from sizing, processes the adhesive polymer waterproof roll of pre-spread/wet shop.
As the improvement of the foregoing description scheme, the outside of polyvinyl chloride (PVC) or high density polyethylene (HDPE) (HDPE) or both mixtures also is covered with barrier film.
More than the adhesive polymer waterproof roll of pre-spread provided by the present invention/wet shop has been carried out detailed introduction; Used concrete example among this paper principle of the present invention and embodiment are set forth, the explanation of above embodiment just is used for helping to understand method of the present invention and core concept thereof; Simultaneously, for one of ordinary skill in the art, according to thought of the present invention, the part that on the specific embodiment and range of application, all can change, in sum, this description should not be construed as limitation of the present invention.
Claims (10)
1. the adhesive polymer waterproof roll of a pre-spread/wet shop is characterized in that:
The adhesive polymer waterproof roll of said pre-spread/wet shop comprises the modified bitumen self-adhesive layer, contains petroleum bitumen, modifier, softening agent, tackifier and filler in the said modified bitumen self-adhesive layer.
2. the adhesive polymer waterproof roll of pre-spread as claimed in claim 1/wet shop is characterized in that:
Said modifier be s-B-S, polyacrylic one or more.
3. the adhesive polymer waterproof roll of pre-spread as claimed in claim 1/wet shop is characterized in that:
Said softening agent is second line of distillation oil, subtract one or more of third fractional oil.
4. the adhesive polymer waterproof roll of pre-spread as claimed in claim 1/wet shop is characterized in that:
Said tackifier are cycloparaffin resin.
5. the adhesive polymer waterproof roll of pre-spread as claimed in claim 1/wet shop is characterized in that:
Said filler is a French chalk.
6. the adhesive polymer waterproof roll of pre-spread as claimed in claim 1/wet shop is characterized in that said modified bitumen self-adhesive layer prescription is (pressing mass fraction):
Petroleum bitumen 50-60;
Modifier 10-20;
Softening agent 5-15;
Tackifier 1-10;
Filler 10-20.
7. the adhesive polymer waterproof roll of pre-spread as claimed in claim 6/wet shop is characterized in that said modified bitumen self-adhesive layer prescription is (pressing mass fraction):
Petroleum bitumen 54;
Modifier 15;
Softening agent 10;
Tackifier 5;
Filler 16.
8. the adhesive polymer waterproof roll of pre-spread as claimed in claim 1/wet shop is characterized in that:
At least one side of said modified bitumen self-adhesive layer is equipped with polymer resin layer; Said polymer resin layer is one or more in blend, polyvinyl chloride and the high density polyethylene (HDPE) of ethylene-vinyl acetate copolymer, ethene vinyl acetate and pitch.
9. the adhesive polymer waterproof roll of pre-spread as claimed in claim 8/wet shop is characterized in that:
The said polymer resin layer outside also is covered with barrier film.
10. the adhesive polymer waterproof roll preparation method of a pre-spread/wet shop is characterized in that may further comprise the steps:
In part petroleum bitumen, add modifier, softening agent and be warming up to 180 ℃-200 ℃, stirred 180 minutes, make modified materials;
Modified materials is squeezed into another sky agitator tank through colloid mill;
Add another kind of modifier (PP), filler in the modified materials in batches, every batch of interval 150 minutes, and continue to stir;
Add tackifier and keep 180 ℃, continue to stir with the residue asphalt temperature;
Modified bitumen is coated in polymer resin layer one or both sides with modified bitumen from sizing through immersion trough from sizing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010529390.3A CN102454226B (en) | 2010-10-29 | 2010-10-29 | High-polymer self-adhesion waterproof coiled material of a kind of pre-spread/wet paving and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010529390.3A CN102454226B (en) | 2010-10-29 | 2010-10-29 | High-polymer self-adhesion waterproof coiled material of a kind of pre-spread/wet paving and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102454226A true CN102454226A (en) | 2012-05-16 |
| CN102454226B CN102454226B (en) | 2016-04-20 |
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| CN201010529390.3A Expired - Fee Related CN102454226B (en) | 2010-10-29 | 2010-10-29 | High-polymer self-adhesion waterproof coiled material of a kind of pre-spread/wet paving and preparation method thereof |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103361980A (en) * | 2013-08-02 | 2013-10-23 | 南京道润交通科技有限公司 | Preparation method for self-adhesive polyester glass fabric and self-adhesive polyester glass fabric |
| CN103802380A (en) * | 2014-02-28 | 2014-05-21 | 北京东方雨虹防水技术股份有限公司 | Modified asphalt waterproof sheet material |
| CN104194719A (en) * | 2014-09-11 | 2014-12-10 | 惠州东方雨虹建筑材料有限责任公司 | Creeping self-adhesive asphalt water-proof coiled material and preparation method thereof |
| CN104830207A (en) * | 2015-05-28 | 2015-08-12 | 天津市禹红建筑防水材料有限公司 | Organic adhesive cover paint and application thereof in modified asphalt waterproof coils |
| CN104960267A (en) * | 2015-06-18 | 2015-10-07 | 四川蜀羊防水材料有限公司 | Modified asphalt waterproof coiled material |
| CN105885441A (en) * | 2016-04-20 | 2016-08-24 | 锦州东方雨虹建筑材料有限责任公司 | Modified asphalt for waterproof coiled material and preparation method of modified asphalt |
| CN106675409A (en) * | 2016-12-30 | 2017-05-17 | 上海东方雨虹防水技术有限责任公司 | Modified asphalt coating with saline-alkaline tolerance and root resistance and production method as well as waterproof roll and production method |
| CN107663380A (en) * | 2016-07-30 | 2018-02-06 | 甘肃西盟公路新材料科技有限公司 | A kind of bituminous composition and preparation method thereof |
| CN108116004A (en) * | 2016-11-29 | 2018-06-05 | 河北四正北方新型材料科技有限公司 | Band takes off the modified pitch base waterproof roll of membrane process |
| CN109695158A (en) * | 2017-10-23 | 2019-04-30 | 南京道之尊复合材料有限公司 | A kind of self-adhering type stress cloth |
| CN110016298A (en) * | 2019-04-16 | 2019-07-16 | 新疆北新路桥集团股份有限公司 | A kind of concrete road conserving material and its application |
| CN113059895A (en) * | 2021-05-08 | 2021-07-02 | 四川环图材料科技有限公司 | Preparation method of plant root puncture-resistant waterproof coiled material for planted roof |
| CN114672264A (en) * | 2022-04-06 | 2022-06-28 | 安徽省奥佳建材有限公司 | Elastic self-adhesive waterproof roll and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103361980A (en) * | 2013-08-02 | 2013-10-23 | 南京道润交通科技有限公司 | Preparation method for self-adhesive polyester glass fabric and self-adhesive polyester glass fabric |
| CN103361980B (en) * | 2013-08-02 | 2015-08-12 | 南京道润交通科技有限公司 | The preparation method of self-adhering type Fibergrass polyester mat and self-adhering type Fibergrass polyester mat |
| CN103802380A (en) * | 2014-02-28 | 2014-05-21 | 北京东方雨虹防水技术股份有限公司 | Modified asphalt waterproof sheet material |
| CN104194719A (en) * | 2014-09-11 | 2014-12-10 | 惠州东方雨虹建筑材料有限责任公司 | Creeping self-adhesive asphalt water-proof coiled material and preparation method thereof |
| CN104830207A (en) * | 2015-05-28 | 2015-08-12 | 天津市禹红建筑防水材料有限公司 | Organic adhesive cover paint and application thereof in modified asphalt waterproof coils |
| CN104960267A (en) * | 2015-06-18 | 2015-10-07 | 四川蜀羊防水材料有限公司 | Modified asphalt waterproof coiled material |
| CN110128841A (en) * | 2016-04-20 | 2019-08-16 | 锦州东方雨虹建筑材料有限责任公司 | A kind of modified pitch and preparation method thereof for waterproof roll |
| CN105885441A (en) * | 2016-04-20 | 2016-08-24 | 锦州东方雨虹建筑材料有限责任公司 | Modified asphalt for waterproof coiled material and preparation method of modified asphalt |
| CN110128840A (en) * | 2016-04-20 | 2019-08-16 | 锦州东方雨虹建筑材料有限责任公司 | A kind of modified pitch and preparation method thereof for waterproof roll |
| CN110128841B (en) * | 2016-04-20 | 2021-06-04 | 锦州东方雨虹建筑材料有限责任公司 | Modified asphalt for waterproof coiled material and preparation method thereof |
| CN110128840B (en) * | 2016-04-20 | 2021-07-30 | 锦州东方雨虹建筑材料有限责任公司 | Modified asphalt for waterproof coiled material and preparation method thereof |
| CN107663380A (en) * | 2016-07-30 | 2018-02-06 | 甘肃西盟公路新材料科技有限公司 | A kind of bituminous composition and preparation method thereof |
| CN108116004A (en) * | 2016-11-29 | 2018-06-05 | 河北四正北方新型材料科技有限公司 | Band takes off the modified pitch base waterproof roll of membrane process |
| CN106675409A (en) * | 2016-12-30 | 2017-05-17 | 上海东方雨虹防水技术有限责任公司 | Modified asphalt coating with saline-alkaline tolerance and root resistance and production method as well as waterproof roll and production method |
| CN109695158A (en) * | 2017-10-23 | 2019-04-30 | 南京道之尊复合材料有限公司 | A kind of self-adhering type stress cloth |
| CN109695158B (en) * | 2017-10-23 | 2021-09-28 | 南京道之尊复合材料有限公司 | Self-adhesive stress cloth |
| CN110016298A (en) * | 2019-04-16 | 2019-07-16 | 新疆北新路桥集团股份有限公司 | A kind of concrete road conserving material and its application |
| CN113059895A (en) * | 2021-05-08 | 2021-07-02 | 四川环图材料科技有限公司 | Preparation method of plant root puncture-resistant waterproof coiled material for planted roof |
| CN114672264A (en) * | 2022-04-06 | 2022-06-28 | 安徽省奥佳建材有限公司 | Elastic self-adhesive waterproof roll and preparation method thereof |
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|---|---|
| CN102454226B (en) | 2016-04-20 |
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