CN102369960A - Solid fumigation disinfectant and preparation method thereof - Google Patents
Solid fumigation disinfectant and preparation method thereof Download PDFInfo
- Publication number
- CN102369960A CN102369960A CN2010102585242A CN201010258524A CN102369960A CN 102369960 A CN102369960 A CN 102369960A CN 2010102585242 A CN2010102585242 A CN 2010102585242A CN 201010258524 A CN201010258524 A CN 201010258524A CN 102369960 A CN102369960 A CN 102369960A
- Authority
- CN
- China
- Prior art keywords
- solid
- disinfectant
- paraformaldehyde
- raw material
- fumigating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000645 desinfectant Substances 0.000 title claims abstract description 39
- 239000007787 solid Substances 0.000 title claims abstract description 24
- 238000002360 preparation method Methods 0.000 title claims abstract description 7
- 238000003958 fumigation Methods 0.000 title abstract description 17
- 239000002994 raw material Substances 0.000 claims abstract description 19
- 229930040373 Paraformaldehyde Natural products 0.000 claims abstract description 17
- 229920002866 paraformaldehyde Polymers 0.000 claims abstract description 17
- 238000002485 combustion reaction Methods 0.000 claims abstract description 11
- YRIZYWQGELRKNT-UHFFFAOYSA-N 1,3,5-trichloro-1,3,5-triazinane-2,4,6-trione Chemical compound ClN1C(=O)N(Cl)C(=O)N(Cl)C1=O YRIZYWQGELRKNT-UHFFFAOYSA-N 0.000 claims description 18
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 18
- FSNCEEGOMTYXKY-JTQLQIEISA-N Lycoperodine 1 Natural products N1C2=CC=CC=C2C2=C1CN[C@H](C(=O)O)C2 FSNCEEGOMTYXKY-JTQLQIEISA-N 0.000 claims description 18
- 239000011734 sodium Substances 0.000 claims description 18
- 229910052708 sodium Inorganic materials 0.000 claims description 18
- 235000003092 Artemisia dracunculus Nutrition 0.000 claims description 11
- 240000001851 Artemisia dracunculus Species 0.000 claims description 11
- 241001647745 Banksia Species 0.000 claims description 10
- 235000002991 Coptis groenlandica Nutrition 0.000 claims description 10
- 244000247747 Coptis groenlandica Species 0.000 claims description 10
- 235000015489 Emblica officinalis Nutrition 0.000 claims description 10
- 241000220317 Rosa Species 0.000 claims description 10
- 244000277583 Terminalia catappa Species 0.000 claims description 10
- 235000011517 Terminalia chebula Nutrition 0.000 claims description 10
- 239000002671 adjuvant Substances 0.000 claims description 10
- 239000003795 chemical substances by application Substances 0.000 claims description 7
- 238000002156 mixing Methods 0.000 claims description 5
- 239000000126 substance Substances 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 15
- 244000144972 livestock Species 0.000 abstract description 9
- 230000000249 desinfective effect Effects 0.000 abstract 3
- 239000000779 smoke Substances 0.000 abstract 1
- XSXSKSKONCDOMZ-UHFFFAOYSA-N sodium;1,3,5-trichloro-1,3,5-triazinane-2,4,6-trione Chemical compound [Na+].ClN1C(=O)N(Cl)C(=O)N(Cl)C1=O XSXSKSKONCDOMZ-UHFFFAOYSA-N 0.000 abstract 1
- 238000004659 sterilization and disinfection Methods 0.000 description 16
- 244000144977 poultry Species 0.000 description 8
- 230000001954 sterilising effect Effects 0.000 description 8
- 238000000034 method Methods 0.000 description 7
- 239000007921 spray Substances 0.000 description 4
- 241000894006 Bacteria Species 0.000 description 3
- 230000003115 biocidal effect Effects 0.000 description 3
- 239000003814 drug Substances 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 238000005507 spraying Methods 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 230000000840 anti-viral effect Effects 0.000 description 2
- 239000000460 chlorine Substances 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- 201000010099 disease Diseases 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 230000002147 killing effect Effects 0.000 description 2
- 239000002075 main ingredient Substances 0.000 description 2
- 244000005700 microbiome Species 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000005070 sampling Methods 0.000 description 2
- 238000004062 sedimentation Methods 0.000 description 2
- 238000009423 ventilation Methods 0.000 description 2
- 241000193830 Bacillus <bacterium> Species 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 241000700605 Viruses Species 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 230000002155 anti-virotic effect Effects 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 210000004666 bacterial spore Anatomy 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000002316 fumigant Substances 0.000 description 1
- 230000000855 fungicidal effect Effects 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention belongs to the technical field of disinfectants and relates to a solid fumigation disinfectant and a preparation method thereof. The solid fumigation disinfectant consists of the following raw materials in percentage by weight: 30 to 60 percent of sodium trichloroisocyanurate, 5 to 10 percent of paraformaldehyde and the balance of combustion improver. The proper ratio range of each raw material is selected, so the solid fumigation disinfectant does not generate naked flame, can be combusted completely and generates a large amount of smoke during use to fulfill the completely disinfecting aim. The solid fumigation disinfectant is mainly used for disinfecting livestock houses in the field of animal husbandry and disinfects by an ignition and fumigation mode so as to achieve the effects of saving time and labor and disinfecting completely.
Description
Technical field
The invention belongs to the disinfectant technical field, relate to a kind of solid fumigating disinfectant and preparation method thereof.
Background technology
In the feeding process of livestock and poultry, usually receive the harm of various diseases, at present, disease preventing and treating takes place and spreads the most the most frequently used method, utilizes disinfectant to carry out comprehensive multi-level strict sterilization such as environment, apparatus exactly.Disinfectant commonly used is divided into chlorinated product, phenols, surfactant etc. by its Main Ingredients and Appearance, with regard to its type of service, has obtain solution to spray spraying, dry powder powder and fumigation etc.Wherein the chlorine-containing disinfectant fungicidal spectrum is wide; Can kill various microorganisms; Comprise bacterial spore that bacterial propagule, virus, fungi, tubercle bacillus and drag are the strongest etc., but it is unstable after water-soluble, is prone to its active ingredient of forfeiture; The effect of killing microorganisms is obviously weakened, cause Disinfection Effect significantly to descend.The great advantage that fumigation is compared with other measure is each corner that stifling medicine can be distributed to pouity dwelling place equably, and sterilization is not only thorough comprehensively, and the save trouble and labor.But present fumigant is because the defective on prescription, causes in when burning fully inadequately, and Disinfection Effect is also as one wishes not to the utmost, so fumigating disinfectant also needs further to optimize and perfect.
Summary of the invention
The object of the present invention is to provide good solid fumigating disinfectant of a kind of Disinfection Effect and preparation method thereof.
The present invention adopts following technical scheme:
A kind of solid fumigating disinfectant is made up of following raw materials by weight percent: the combustion adjuvant of TCCA sodium 30～60%, paraformaldehyde 5%～10% and surplus.
Form by following raw materials by weight percent: TCCA sodium 52.5%, paraformaldehyde 7.5% and combustion adjuvant 40%.
Said combustion adjuvant is made up of the raw material of following weight portion: 5～10 parts of 10～15 parts of tarragons, 5～15 parts of rhizoma atractylodis, 5～10 parts of myrobalans, 5～10 parts of the coptiss and the banksia rose.
The chemical formula of said paraformaldehyde is (CH
2O) n, n are 8～20.
The preparation method of solid fumigating disinfectant may further comprise the steps: get each raw material in proportion, each raw material was pulverized 80～100 mesh sieves respectively, then TCCA sodium is packaged as host separately, paraformaldehyde and combustion adjuvant mixing are packaged as secondary agent.
The present invention adopts TCCA sodium as main ingredient, and the available chlorine content of TCCA sodium is high, and sterilizing power is strong, and stabilization time is long, can long term storage, transportation, and convenient and safe low toxicity, pollution-free; Adopt paraformaldehyde and TCCA sodium to be used, this is because paraformaldehyde can play the effect that increases inflammability and fumigation, makes that the burning of solid fumigating disinfectant of the present invention is more thorough, and Disinfection Effect is more obvious; The present invention selects tarragon, rhizoma atractylodis, myrobalan, the coptis and banksia rose collocation as combustion adjuvant; Tarragon works the effect of igniting, and the volatile oil that the tarragon burning produces has antibiotic, antivirus action, and rhizoma atractylodis, myrobalan, the coptis and the banksia rose also have same purpose; Because of its antibiotic, antiviral kind difference; Be blended together use, can increase antibiotic, antiviral scope, combustion adjuvant not only has combustion-supporting effect; And the smog that burning produces also has the fumigation effect, strengthened the Disinfection Effect of fumigating disinfectant of the present invention simultaneously.
The present invention has selected the suitable proportion of each raw material just, just makes solid fumigating disinfectant of the present invention in use, neither produces naked light; Can thoroughly burn again; Produce a large amount of smog, reach the purpose of thorough disinfection, be mainly used in the sterilization of livestock-raising field livestock and poultry house; Carry out disinfection through lighting stifling mode, reach time saving and energy saving, the effect completely of sterilizing.
When solid fumigating disinfectant of the present invention uses host and secondary agent are mixed, light, make it produce smog; Every 500g solid fumigating disinfectant can be fumigated the 300-400 cubic meter; Confirm drug dose according to livestock and poultry houses space, require under no livestock and poultry situation, to use, airtight livestock and poultry give up fumigation more than 2 hours for well; Plant the egg fumigation and be no more than 30 minutes, open the door and window ventilation then.
Embodiment
Embodiment 1
The solid fumigating disinfectant, its composition is: TCCA sodium 52.5g, paraformaldehyde (CH
2O)
87.5g, tarragon 10g, rhizoma atractylodis 6g, myrobalan 8g, coptis 8g and banksia rose 8g.
Get each raw material in proportion, each raw material was pulverized 80 mesh sieves respectively, then TCCA sodium is packaged as host separately, paraformaldehyde, tarragon, rhizoma atractylodis, myrobalan, the coptis and banksia rose mixing are packaged as secondary agent.
Embodiment 2
The solid fumigating disinfectant, its composition is: TCCA sodium 30g, paraformaldehyde (CH
2O)
1610g, tarragon 15g, rhizoma atractylodis 15g, myrobalan 10g, coptis 10g and banksia rose 10g.
Get each raw material in proportion, each raw material was pulverized 100 mesh sieves respectively, then TCCA sodium is packaged as host separately, paraformaldehyde, tarragon, rhizoma atractylodis, myrobalan, the coptis and banksia rose mixing are packaged as secondary agent.
Embodiment 3
The solid fumigating disinfectant, its composition is: TCCA sodium 60g, paraformaldehyde (CH
2O)
205g, tarragon 12g, rhizoma atractylodis 8g, myrobalan 5g, coptis 5g and banksia rose 5g.
Get each raw material in proportion, each raw material was pulverized 90 mesh sieves respectively, then TCCA sodium is packaged as host separately, paraformaldehyde, tarragon, rhizoma atractylodis, myrobalan, the coptis and banksia rose mixing are packaged as secondary agent.
When the solid fumigating disinfectant of embodiment 1-3 uses host and secondary agent are mixed, light, make it produce smog; Every 500g solid fumigating disinfectant can be fumigated the 300-400 cubic meter; Confirm drug dose according to livestock and poultry houses space, require under no livestock and poultry situation, to use, airtight livestock and poultry give up fumigation more than 2 hours for well; Plant the egg fumigation and be no more than 30 minutes, open the door and window ventilation then.
Disinfection effect test
1, purpose is the Disinfection Effect of more different sterilization methods, uses fumigating disinfectant fumigation and the TCCA sodium pulvis spray disinfectant method of embodiment 1 to make an experiment.
2, method is measured airborne total number of bacteria with plate sedimentation, carries out air sterillization with fumigating disinfectant fumigation and the TCCA sodium pulvis spray disinfectant method of embodiment 1 respectively again.Select two identical room (15m of volume
3), earlier, handle post-sampling with fumigating disinfectant fumigation and the common pulvis TCCA sodium pulvis spray disinfectant method of embodiment 1 respectively again with the plate sedimentation preceding sampling that carries out disinfection.The result sees table 1.
Two kinds of air sterilization effect testing results of table 1
Testing result shows, 25 ℃ of indoor temperatures, under the situation of relative moisture 50%～70%, with fumigating disinfectant 1g/m of the present invention
3Degerming rate to airborne natural bacteria behind the sootiness 24h can reach more than 90%, and the degerming rate of pulvis spraying is lower than 90%, explains that fumigating disinfectant sootiness sterilization of the present invention has significant killing action than spraying to bacterium in the air.
Claims (5)
1. a solid fumigating disinfectant is characterized in that being made up of following raw materials by weight percent: the combustion adjuvant of TCCA sodium 30～60%, paraformaldehyde 5%～10% and surplus.
2. solid fumigating disinfectant as claimed in claim 1 is characterized in that being made up of following raw materials by weight percent: TCCA sodium 52.5%, paraformaldehyde 7.5% and combustion adjuvant 40%.
3. according to claim 1 or claim 2 solid fumigating disinfectant, it is characterized in that: said combustion adjuvant is made up of the raw material of following weight portion: 5～10 parts of 10～15 parts of tarragons, 5～15 parts of rhizoma atractylodis, 5～10 parts of myrobalans, 5～10 parts of the coptiss and the banksia rose.
4. solid fumigating disinfectant as claimed in claim 3 is characterized in that: the chemical formula of said paraformaldehyde is (CH
2O) n, n are 8～20.
5. the preparation method of the described solid fumigating disinfectant of claim 1; It is characterized in that may further comprise the steps: get each raw material in proportion; Each raw material was pulverized 80～100 mesh sieves respectively; Then TCCA sodium is packaged as host separately, paraformaldehyde and combustion adjuvant mixing are packaged as secondary agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201010258524 CN102369960B (en) | 2010-08-20 | 2010-08-20 | Solid fumigation disinfectant and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201010258524 CN102369960B (en) | 2010-08-20 | 2010-08-20 | Solid fumigation disinfectant and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102369960A true CN102369960A (en) | 2012-03-14 |
| CN102369960B CN102369960B (en) | 2013-10-02 |
Family
ID=45789594
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201010258524 Expired - Fee Related CN102369960B (en) | 2010-08-20 | 2010-08-20 | Solid fumigation disinfectant and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102369960B (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102631695A (en) * | 2012-03-31 | 2012-08-15 | 湖南宜章乐水养鸡专业合作社 | Henhouse sterilizing method |
| CN103444797A (en) * | 2013-08-15 | 2013-12-18 | 五河县畜牧兽医技术推广中心 | Disinfecting fumigant for animal building and preparation method of disinfecting fumigant |
| CN106913893A (en) * | 2017-03-06 | 2017-07-04 | 杨开山 | A kind of method to indoor environment fumigation |
| CN109674081A (en) * | 2018-12-25 | 2019-04-26 | 贵州省烟草科学研究院 | It is a kind of for prevent and treat baking phase tobacco leaf go rotten disease fumigant, preparation method and the usage |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1080473A (en) * | 1993-06-07 | 1994-01-12 | 山东农业大学 | Smudging sterilizing composite |
| CN1454476A (en) * | 2002-12-13 | 2003-11-12 | 国家农产品保鲜工程技术研究中心（天津） | Method of inhibiting rottenness during storage and production process of agricultural products |
| CN1505930A (en) * | 2002-12-13 | 2004-06-23 | 国家农产品保鲜工程技术研究中心(天津 | Smoke agent for sterilizing refrigeration house and processing workshop and its prepn process |
| CN101138339A (en) * | 2007-08-22 | 2008-03-12 | 浙江省农业科学院 | Fume smoking sanitizer for sericultural production and preparing method thereof |
| CN101273734A (en) * | 2008-02-01 | 2008-10-01 | 康可新 | Smokes applied in producing edible or medicinal fungi for sterilization |
-
2010
- 2010-08-20 CN CN 201010258524 patent/CN102369960B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1080473A (en) * | 1993-06-07 | 1994-01-12 | 山东农业大学 | Smudging sterilizing composite |
| CN1454476A (en) * | 2002-12-13 | 2003-11-12 | 国家农产品保鲜工程技术研究中心（天津） | Method of inhibiting rottenness during storage and production process of agricultural products |
| CN1505930A (en) * | 2002-12-13 | 2004-06-23 | 国家农产品保鲜工程技术研究中心(天津 | Smoke agent for sterilizing refrigeration house and processing workshop and its prepn process |
| CN101138339A (en) * | 2007-08-22 | 2008-03-12 | 浙江省农业科学院 | Fume smoking sanitizer for sericultural production and preparing method thereof |
| CN101273734A (en) * | 2008-02-01 | 2008-10-01 | 康可新 | Smokes applied in producing edible or medicinal fungi for sterilization |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102631695A (en) * | 2012-03-31 | 2012-08-15 | 湖南宜章乐水养鸡专业合作社 | Henhouse sterilizing method |
| CN103444797A (en) * | 2013-08-15 | 2013-12-18 | 五河县畜牧兽医技术推广中心 | Disinfecting fumigant for animal building and preparation method of disinfecting fumigant |
| CN106913893A (en) * | 2017-03-06 | 2017-07-04 | 杨开山 | A kind of method to indoor environment fumigation |
| CN109674081A (en) * | 2018-12-25 | 2019-04-26 | 贵州省烟草科学研究院 | It is a kind of for prevent and treat baking phase tobacco leaf go rotten disease fumigant, preparation method and the usage |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102369960B (en) | 2013-10-02 |
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