CN102228410B - Skin-care composite facial mask fluid and preparation method thereof - Google Patents
Skin-care composite facial mask fluid and preparation method thereof Download PDFInfo
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Abstract
A preparation method of a skin-care composite facial mask fluid is disclosed. Main raw materials include konjac glucomannan, k-carrageenan, isolated soybean protein, collagen, propolis and vitamin E. The preparation method comprises the preparation of konjac glucomannan sol, the preparation of compound protein solution, the preparation of k-carrageenan solution and the preparation of sucrose fatty acid ester diluent, and compound and blending of all the materials. The konjac glucomannan is a natural biological polymeric membrane material having excellent performance, and has excellent performances such as water sucking property, moisture preservation property, membrane formation property, gelation property, degradability and the like. Through the physical mixing of the konjac glucomannan with the k-carrageenan and the isolated soybean protein, the thermal properties and the mechanical properties of the membrane can be improved; and through formulation, a non-toxic, efficient and good-performance skin-care facial mask fluid is formed. The konjac glucomannan has a unique property of being liquid at a temperature below 10 DEG C and being naturally formed into a membrane at the normal temperature; therefore, the skin-care composite facial mask fluid is applied to face and a membrane can be naturally formed. The skin-care composite facial mask fluid of the invention is colourless and transparent, convenient for use, and non-toxic and safe.
Description
Technical field
The present invention relates to a kind of facial mask liquid and preparation method thereof, be specifically related to compound facial mask liquid of a kind of skin protection and preparation method thereof.
Background technology
Contain the raising of some harmful materials and people opposite film quality demand in view of part in the cosmetics in the market; In recent years; The research of various facial film new products receives much attention; The quantity of facial film and kind all have very big development, and 3 stages have mainly been experienced in the facial film development: (1) powdery, mud shape or cream pack; (2) mask type nutrient face-pack; (3) papery facial film.Before two stage facial film need consumer to carry out certain operation, the latter half facial film poor ductility, can not be well and face paste with, and cost an arm and a leg, energy-conservation inadequately.Improving constantly of Along with people's quality of life, the butcher,baker,and the candlestick maker often makes and applies some make up, because cosmetics in the market contain the disadvantageous chemical constituent of skin mostly, therefore, the facial mask liquid of probing into a kind of protecting skin is imperative.Facial mask liquid of the present invention is used before cosmetic can play isolation, and protective action can prevent chemical substance intrusion skin, and its effective ingredient has effects such as moist, nutrition to skin simultaneously.
It is the method that functional mass prepares collagen wet-retaining face mask with the collagen protein that the article " development of collagen wet-retaining face mask " of the Shu Zibin that " Sichuan Teachers University journal " 2008 the 31st the 6th phases of volume deliver etc. has been introduced a kind of; Carry out the contrast of performance of keeping humidity to adding the wetting agent front and back; Draw the optimum formula of preparation collagen wet-retaining face mask: 0.1g pours beaker into collagen protein; Add wetting agent lactic acid 2.0mL then; Starch 0.1g, cross-linking agent glutaraldehyde 3.0mL stirs under room temperature; Add then stirred for transparent thick carboxymethylcellulose sodium solution 9.0g in 40 ℃ continue to stir complex liquid; Pour complex liquid into die for molding; Bleed with vacuum pump, in baking oven, take off film behind 60 ℃ of freeze-day with constant temperature 6h, promptly get collagen wet-retaining face mask.Though that the method has is nontoxic, pollution-free, preserve moisture, the cost performance advantages of higher, in the preparation, stir often, time ratio more for a long time, not energy-conservation, use protection skin before costing an arm and a leg, can not being used to make up.
Application number is 03151161.9 patent of invention " a kind of solid phase cosmetic film " (applying date: 2005.03.30) introduced a kind of solid phase cosmetic film; It contain by lining material be positioned at by on the lining material or among the skin care activity composition; Described skin care activity composition constitutes immobilised complex with macromolecular material; This complex contains 0.01%-20% skin care activity composition and 10%-99% macromolecular material, by anhydrous complex gross weight.The useful effect of this solid phase cosmetic film part is helped protecting for a long time the activity of effective ingredient in the cosmetic film, but can not prevent the infringement of chemical substance to skin by immobilization, and advantages such as tool is energy-conservation, and is cheap not.
Summary of the invention
The objective of the invention is to utilize Rhizoma amorphophalli glucomannan being in a liquid state below 10 ℃, and under the room temperature, can film forming naturally peculiar property, provide a kind of can the compound facial mask liquid of film forming naturally skin protection and preparation method thereof.
The method for preparing of the compound facial mask liquid of skin protection of the present invention is characterized in that operating procedure is following:
(1) preparation of konjak portuguese gansu polyose sugar sol: get the 100.0mL sterilized water; The Rhizoma amorphophalli glucomannan that adds 0.3g-0.5g; Adopt blender under 40 ℃ of-50 ℃ of conditions, to stir 30.0 min, after leaving standstill swelling 1h-2h under 40 ℃ of-50 ℃ of conditions, be cooled to and be not higher than 10 ℃ with the speed of 75.0 r/min; Make the konjak portuguese gansu polyose sugar sol, subsequent use;
(2) preparation of compound protein solution: get soybean protein isolate 0.5g-0.75g; Collagen protein 0.1g-0.2g is dissolved in the 100.0mL sterilized water; In 70 ℃ of-80 ℃ of water-baths, stir 30.0min with the speed of 75.0r/min, it is fully dissolved after, under 40 ℃ of-50 ℃ of conditions, leave standstill swelling 1h-2h; Make compound protein solution, subsequent use;
(3) preparation of kappa-carrageenan solution: get the 100.0mL sterilized water; Add the 0.45g-0.75g kappa-carrageenan, the rotating speed with 75.0r/min in 70 ℃ of-80 ℃ of water-baths stirs 30.0min to fully dissolving, under 40 ℃ of-50 ℃ of conditions, leaves standstill swelling 1h-2h; Make kappa-carrageenan solution, subsequent use;
(4) preparation of sucrose fatty acid ester diluent: get the 100.0mL sterilized water; Add the 0.2g-0.5g sucrose fatty acid ester; In 70 ℃ of-80 ℃ of water-baths, dissolve to abundant; And add 0.1g-0.4g paraffin and be stirred to abundant dissolving with the rotating speed of 75.0r/min, add sterilized water with solution dilution to 500mL, the sucrose fatty acid ester diluent;
(5) preparation of the compound facial mask liquid of skin protection: the kappa-carrageenan solution that the konjak portuguese gansu polyose sugar sol that step (1) is made, the compound protein solution that step (2) makes and step (3) make mixes, and the rotating speed with 75.0r/min under 40 ℃ of-50 ℃ of conditions stirs 30.0min; Add the sucrose fatty acid ester diluent that step (4) makes, with the rotating speed stirring 5min of 75.0r/min; Be cooled to and be not higher than 10 ℃, add 2.0mL-3.0mL wetting agent lactic acid, 0.6g-0.9g vitamin E, 0.3g-0.5g propolis, and stir, regulate pH to 10.0 with the HCl of 1.0mol/L or the NaOH of 1.0 mol/L, must the compound facial mask liquid of skin protection.
The compound facial mask liquid of skin protection is coated on the face can the nature film forming.The compound facial mask liquid water white transparency of skin protection, easy to use, non-toxic and safe.
The method for preparing of the compound facial mask liquid of skin protection of the present invention has avoided general compound facial film need the glue of preparation be dried the filming technology of film forming complicacy and the shortcoming of higher cost.The raw material that uses is the Rhizoma amorphophalli glucomannan that contains in the Renewable resource plant Rhizoma amorphophalli, and it is a kind of natural biological macromolecule member material of function admirable, has good suction, preserves moisture, performance such as film forming, gel, degradability.Through the physical blending of Rhizoma amorphophalli glucomannan and kappa-carrageenan and soybean protein isolate, nontoxic to improve the thermal characteristics and the mechanicalness of film through composite formation, the efficient and good facial treatment mask liquid of performance.
The specific embodiment
In order fully to disclose compound facial mask liquid of skin protection of the present invention and preparation method thereof, explain below in conjunction with embodiment.
Embodiment: the method for preparing of the compound facial mask liquid of a kind of skin protection, concrete operations are following:
(1) gets the 100.0ml sterilized water, add the 0.3g Rhizoma amorphophalli glucomannan, adopt blender to stir 30.0min down in 45.0 ℃ of constant temperatures with the speed of 75.0r/min; After keeping 40 ℃-50 ℃ of temperature to leave standstill swelling 2.0h; Be cooled to 8 ℃, make the konjak portuguese gansu polyose sugar sol, subsequent use;
(2) 0.5g soybean separation protein Pseudobulbus Bletillae (Rhizoma Bletillae) 0.2g collagen protein is dissolved in the 100ml sterilized water, in 75 ℃ of water-baths, stirs 30.0min with 75.0r/min, it is fully dissolved after, under 45 ℃ of constant temperatures, leave standstill swelling 2.0h, make compound protein solution, subsequent use;
(3) get the 100ml sterilized water, add the 0.5g kappa-carrageenan, the rotating speed stirring 30.0min with 75.0r/min in 75 ℃ of water-baths makes its dissolving, and swelling 2.0h under 45 ℃ of constant temperatures makes kappa-carrageenan solution, and is subsequent use;
(4) get the 100mL sterilized water; Adding 0.25g sucrose fatty acid ester dissolves to abundant in 75.0 ℃ of stirred in water bath, and adds the rotating speed stirring 10.0min of 0.3g paraffin with 75.0r/min; The adding sterilized water to 500mL, makes the sucrose fatty acid ester diluent with above-mentioned solution dilution;
(5) the kappa-carrageenan solution that compound protein solution that the konjak portuguese gansu polyose sugar sol that step (1) is made, step (2) make and step (3) make mixes; Rotating speed with 75.0r/min under 40 ℃ of-50 ℃ of conditions stirs 30.0min, adds the sucrose-fatty ester solution that step (4) makes again, with the rotating speed stirring 5min of 75.0r/min; Be cooled to 7 ℃ then; Add 2.0mL wetting agent lactic acid, 0.7g vitamin E, 0.3g propolis, and stir, regulate pH to 10.0 with the HCl of 1.0mol/L or the NaOH of 1.0mol/L; Make the compound facial mask liquid of skin protection, preserve in not being higher than under 10 ℃ the condition.
The facial treatment mask liquid coated that makes of utilization the method in the people on the face, the advantage that having can natural at normal temperatures film forming, structural behaviour is stable.This facial treatment mask liquid is used for being applied to facial film forming before the cosmetic, has functions such as certain protection, nourishing, moistening skin.In addition, can also be applied to aspects such as biological medicine, daily-use chemical industry, be widely used.
Claims (3)
1. the method for preparing of the compound facial mask liquid of skin protection is characterized in that operating procedure is following:
(1) preparation of konjak portuguese gansu polyose sugar sol: get the 100.0mL sterilized water; The Rhizoma amorphophalli glucomannan that adds 0.3g-0.5g; Adopt blender under 40 ℃ of-50 ℃ of conditions, to stir 30.0 min, after leaving standstill swelling 1h-2h under 40 ℃ of-50 ℃ of conditions, be cooled to and be not higher than 10 ℃ with the speed of 75.0 r/min; Make the konjak portuguese gansu polyose sugar sol, subsequent use;
(2) preparation of compound protein solution: get soybean protein isolate 0.5g-0.75g; Collagen protein 0.1g-0.2g is dissolved in the 100.0mL sterilized water; In 70 ℃ of-80 ℃ of water-baths, stir 30.0min with the speed of 75.0r/min, it is fully dissolved after, under 40 ℃ of-50 ℃ of conditions, leave standstill swelling 1h-2h; Make compound protein solution, subsequent use;
(3) preparation of kappa-carrageenan solution: get the 100.0mL sterilized water; Add the 0.45g-0.75g kappa-carrageenan, the rotating speed with 75.0r/min in 70 ℃ of-80 ℃ of water-baths stirs 30.0min to fully dissolving, under 40 ℃ of-50 ℃ of conditions, leaves standstill swelling 1h-2h; Make kappa-carrageenan solution, subsequent use;
(4) preparation of sucrose fatty acid ester diluent: get the 100.0mL sterilized water; Add the 0.2g-0.5g sucrose fatty acid ester; In 70 ℃ of-80 ℃ of water-baths, dissolve to abundant; And add 0.1g-0.4g paraffin and be stirred to abundant dissolving with the rotating speed of 75.0r/min, add sterilized water with solution dilution to 500mL, the sucrose fatty acid ester diluent;
(5) preparation of the compound facial mask liquid of skin protection: the kappa-carrageenan solution that the konjak portuguese gansu polyose sugar sol that step (1) is made, the compound protein solution that step (2) makes and step (3) make mixes, and the rotating speed with 75.0r/min under 40 ℃ of-50 ℃ of conditions stirs 30.0min; Add the sucrose fatty acid ester diluent that step (4) makes, with the rotating speed stirring 5min of 75.0r/min; Be cooled to and be not higher than 10 ℃, add 2.0mL-3.0mL wetting agent lactic acid, 0.6g-0.9g vitamin E, 0.3g-0.5g propolis, and stir, get final product with the HCl of 1.0mol/L or the NaOH adjusting pH to 10.0 of 1.0 mol/L.
2. the method for preparing of the compound facial mask liquid of a kind of skin protection according to claim 1 is characterized in that operating procedure is following:
(1) gets the 100.0ml sterilized water, add the 0.3g Rhizoma amorphophalli glucomannan, adopt blender to stir 30.0min down in 45.0 ℃ of constant temperatures with the speed of 75.0r/min; After keeping 40 ℃-50 ℃ of temperature to leave standstill swelling 2.0h; Be cooled to 8 ℃, make the konjak portuguese gansu polyose sugar sol, subsequent use;
(2) 0.5g soybean separation protein Pseudobulbus Bletillae (Rhizoma Bletillae) 0.2g collagen protein is dissolved in the 100ml sterilized water, in 75 ℃ of water-baths, stirs 30.0min with 75.0r/min, it is fully dissolved after, under 45 ℃ of constant temperatures, leave standstill swelling 2.0h, make compound protein solution, subsequent use;
(3) get the 100ml sterilized water, add the 0.5g kappa-carrageenan, the rotating speed stirring 30.0min with 75.0r/min in 75 ℃ of water-baths makes its dissolving, and swelling 2.0h under 45 ℃ of constant temperatures makes kappa-carrageenan solution, and is subsequent use;
(4) get the 100mL sterilized water; Adding 0.25g sucrose fatty acid ester dissolves to abundant in 75.0 ℃ of stirred in water bath, and adds the rotating speed stirring 10.0min of 0.3g paraffin with 75.0r/min; The adding sterilized water to 500mL, makes the sucrose fatty acid ester diluent with above-mentioned solution dilution;
(5) the kappa-carrageenan solution that compound protein solution that the konjak portuguese gansu polyose sugar sol that step (1) is made, step (2) make and step (3) make mixes; Rotating speed with 75.0r/min under 40 ℃ of-50 ℃ of conditions stirs 30.0min; Add the sucrose-fatty ester solution that step (4) makes again; Rotating speed with 75.0r/min stirs 5min, is cooled to 7 ℃ then, adds 2.0mL wetting agent lactic acid, 0.7g vitamin E, 0.3g propolis; And stir, get final product with the HCl of 1.0mol/L or the NaOH adjusting pH to 10.0 of 1.0mol/L.
3. press the compound facial mask liquid of skin protection of the method preparation of claim 1 or 2.
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| CN102696940A (en) * | 2012-03-16 | 2012-10-03 | 桑植县溇水大鲵生物科技有限公司 | Detox beauty capsule of giant salamander and production method thereof |
| CN103845228B (en) * | 2013-07-08 | 2016-04-20 | 重庆大学 | A kind of method preparing skin-friendly compound protein mask |
| CN103405350B (en) * | 2013-07-16 | 2015-04-01 | 福建农林大学 | Granular glucomannan moisturizing mask and preparation method thereof |
| CN103432008B (en) * | 2013-08-30 | 2014-08-20 | 湖北一致魔芋生物科技有限公司 | Formed konjak mask and preparation method thereof |
| CN104473861A (en) * | 2015-01-19 | 2015-04-01 | 陈夏风 | Purple yam facial mask and preparing method of purple yam facial mask |
| CN105054565B (en) * | 2015-07-03 | 2018-05-08 | 福建农林大学 | Konjaku glucomannan double-edged eyelid patch and preparation method thereof |
| BR102015031933B1 (en) * | 2015-12-18 | 2021-05-25 | Universidade Estadual De Campinas - Unicamp | process for obtaining asymmetric membranes, membranes thus obtained and use |
| CN109316433B (en) * | 2018-12-05 | 2021-08-27 | 邯郸学院 | Skin care mask capable of reducing heavy metal pollution |
| CN110123701A (en) * | 2019-06-15 | 2019-08-16 | 福建农林大学 | A kind of konjaku glucomannan facial cleanser |
| CN110496081B (en) * | 2019-09-24 | 2021-06-04 | 肇庆学院 | Natural plant moisturizing and skin-tendering mask paste and preparation method thereof |
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| CN1568933A (en) * | 2004-04-29 | 2005-01-26 | 尚治国 | Crystalline beauty treatment mask and preparation method thereof |
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