CN102198078B - Foaming facial cleanser containing traditional Chinese medicines and preparation method thereof - Google Patents

Foaming facial cleanser containing traditional Chinese medicines and preparation method thereof Download PDF

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Publication number
CN102198078B
CN102198078B CN201110134081.0A CN201110134081A CN102198078B CN 102198078 B CN102198078 B CN 102198078B CN 201110134081 A CN201110134081 A CN 201110134081A CN 102198078 B CN102198078 B CN 102198078B
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chinese medicine
surfactant
cleansing milk
extract
preparation
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CN102198078A (en
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刘谋盛
陈邈
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Kunming University of Science and Technology
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Kunming University of Science and Technology
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Abstract

A foaming facial cleanser containing traditional Chinese medicines and a preparation method thereof belong to the field of cleaning cosmetics. The formula of the facial cleanser comprises the following components: anionic surfactant, non-ionic surfactant, zwitterionic surfactant, cationic surfactant, fatty acid, lanolin, humectant, de-ionized water, traditional Chinese medicine extracts, preservative and essence, wherein the traditional Chinese medicine extracts are made of licorice, radix angelicae, goldthread root, fructus cnidii, rhizome typhoon, Scutellaria baicalensis, dittany bark, Ligusticum wallichii, asarum, Poria cocos, bitter apricot kernel, white atractylodes rhizome, radix polygonati officinalis and musk. The traditional Chinese medicine extracts are uniformly distributed in the base materials so as to form a stable emulsion system. The foaming facial cleanser not only realizes the decontamination function, but also has the advantages of good moisturizing effect, no stimulus and abundant and delicate foam, is mild for use, and has the obvious effects of acne removal, fungus resistance and skin whitening, thereby achieving the purpose of skin care and beautification.

Description

A kind of foam type cleansing milk containing Chinese medicine and preparation method thereof
Technical field
The present invention relates to clean class cosmetic field, especially a kind of Chinese medicine cleansing milk with acne-removal function.Belong to clean class cosmetic field.
Background technology
Chinese medicine cleansing milk is in the market also existing a variety of, but the Chinese herbal medicine kind often wherein containing is single or only have a few, if the patent No. is CN1103779A, CN101439010, CN1927158A etc., Chinese medicine additional proportion is also very little, and effect is single and not remarkable, and the trend of cosmetics is exactly back to nature, the cleansing milk effect of adding after Chinese herbal medicine and natural plants melon and fruit is distinguished, have national characters, so natural Chinese medicinal herb cleansing milk fully develops talents, market prospect is wide.Yet adding of a small amount of Chinese medicine, will cause the inapparent drawback of effect, and too much can cause the unstable of system adding of Chinese medicine, so Chinese medicine adds the research of technique to become the key of Chinese medicine cleansing milk Development Techniques.
Summary of the invention
The object of the invention is to the technical problem existing in present Chinese herbal medicine facial cleanser, invent the certain technique of a kind of employing, add a certain proportion of natural Chinese medicines extract in cleansing milk substrate, when making it have anti-acne, antifungal, white-skinned face function, can make again drug distribution even, form stable emulsification system.
Another object of the present invention is to provide the preparation technology of this kind of Chinese herbal medicine facial cleanser of preparation.
Object of the present invention realizes by such method: a kind of foam type cleansing milk containing Chinese medicine, the mass fraction % that it is characterized in that forming the component formula of this cleansing milk is: anion surfactant 10~25%, non-ionic surface active agent 2~5%, zwitterionic surfactant 2~5%, cationic surfactant 3~8%, fatty acid 0.5~5%, lanoline 0.5~5%, wetting agent 0.5~20%, deionized water 45~65%, Chinese medicine extract 3~8%, then add appropriate antiseptic and appropriate essence.
Described anion surfactant is selected from one or more in polyoxyethylenated alcohol sodium sulfate, sodium lauryl sulphate, ammonium lauryl sulfate; Described non-ionic surface active agent is selected from one or more in coconut oil fatty acid monoethanolamide, cocoanut fatty acid diethanolamide.
Described zwitterionic surfactant is selected from one or more in cocamido propyl betaine, dodecyldimethylammonium hydroxide inner salt, alkyl dimethyl amine-oxides.
Described cationic surfactant is selected from one or more in dodecayl dimethyl amine oxide, dodecyl dimethyl benzyl ammonium chloride, triethanolamine; Described fatty acid is selected from one or more in dodecoic acid, tetradecylic acid, hexadecylic acid, stearic acid.
Described wetting agent is at least one in polyhydric alcohol, pyrrolidone sodium carboxylate, lactic acid and sodium lactate, collagen protein, aminoacid, hyaluronic acid of glycerol, propylene glycol, 1,3 butylene glycol, polyethylene glycols.
The serve as reasons crude drug of following weight portion of described Chinese medicine extract is made: Radix Glycyrrhizae 10~40, the Radix Angelicae Dahuricae 4~18, Rhizoma Coptidis 3~15, Fructus Cnidii 5~20, Rhizoma Typhonii 4~18, Radix Scutellariae 3~15, Cortex Dictamni 5~16, Rhizoma Chuanxiong 4~15, Herba Asari 5~20, Poria 5~15, Semen Armeniacae Amarum 3~10, the Rhizoma Atractylodis Macrocephalae 5~20, Rhizoma Polygonati Odorati 5~20, Moschus 5~15.
Described Chinese medicine extract, its preparation method is that after alcohol reflux, spraying is dry, step is as follows:
(1) take each raw material of Chinese medicine medicine of described weight portion, pulverize, cross 40 mesh sieves;
(2) by 5~10 times of each raw material of Chinese medicine medicine weight portions, get 75~95% ethanol, soak 0.5~5h, 40~75 ℃ of reflux, extract, 1~3h;
(3) filter, then get 5%~9% ethanol, reflux, extract, 1~3h by 5~10 times of filtering residue parts by weight;
(4) filter the rear two kinds of filtrates that merge, obtain Chinese medicine alcohol extract, put shady place and save backup;
(5) the spray-dried Chinese medicine dry powder that obtains of Chinese medicine alcohol extract.
A preparation method for the foam type cleansing milk of Chinese medicine, its preparation method comprises the steps:
1) in deionized water, add the components such as anion surfactant, non-ionic surface active agent, cationic surfactant, zwitterionic surfactant, wetting agent, 60~85 ℃, shearing force is 500~800rpm, stirring and evenly mixing 0.2~1h;
2) lanoline and 60~85 ℃ of heated and stirred of fatty acid are mixed;
3) (2) gains are slowly added in (1) gains, 60~85 ℃, shearing force is 500~800rpm, stirring and evenly mixing 0.2~1h;
4) be cooled to 50~65 ℃, in (3) gains, add Chinese medicine dry powder, continue to stir 10~50min;
5) continue to be cooled to 40~50 ℃, add appropriate essence, antiseptic, stir 0.2~1h;
6) step (5) gains are evacuated to finished pot, obtain product.
Its Chinese medicine add method to comprise directly joining method or grind well with wetting agent after add again two kinds of modes.
The present invention's test shows, by specifically adding mode, Chinese herbal medicine is combined with cleansing milk substrate, not only make drug distribution even, form stable emulsification system, and can obtain more significant drug effect, application example also shows to comprise in the present invention Chinese medicine compound and makes this cleansing milk have multiple efficacies and effect is remarkable.
Advantage of the present invention and effect are: not only realized the dirt-removing functions of cleansing milk, moistening effect is good, gentle, non-stimulated, and foam is abundant fine and smooth, and has obvious anti-acne, whitening, antifungal efficacy, skin-protecting face nursing.
The specific embodiment
By specific embodiment given below and typical Application Example, can further be well understood to the present invention, but they not limitation of the invention.
The mass fraction (%) that forms the component formula of this cleansing milk of the present invention is: anion surfactant 10~25, non-ionic surface active agent 2~5, zwitterionic surfactant 2~5, cationic surfactant 3~8, fatty acid 0.5~5, lanoline 0.5~5, wetting agent 0.5~20, deionized water 45~65, Chinese medicine extract 3~8, antiseptic, essence (in right amount).
Its preparation method comprises the steps:
(1) in deionized water, add the components such as anion surfactant, non-ionic surface active agent, cationic surfactant, zwitterionic surfactant, wetting agent, 60~85 ℃, shearing force is 500~800rpm, stirring and evenly mixing 0.2~1h;
(2) lanoline and 60~85 ℃ of heated and stirred of fatty acid are mixed;
(3) (2) gains are slowly added in (1) gains, 60~85 ℃, shearing force is 500~800rpm, stirring and evenly mixing 0.2~1h;
(4) be cooled to 50~65 ℃, in (3) gains, add Chinese medicine dry powder, continue to stir 10~50min;
(5) continue to be cooled to 40~50 ℃, add appropriate essence, antiseptic, stir 0.2~1h;
Step (5) gains are evacuated to finished pot, obtain product.
Embodiment 1
(1) in deionized water 53.5g, add polyoxyethylenated alcohol sodium sulfate 10.0g, sodium lauryl sulphate 2.5g, cocoanut fatty acid diethanolamide 4.0g, cocamido propyl betaine 5.0g, dodecayl dimethyl amine oxide 4.0g and glycerol 10.0g, 70 ℃, shearing force is 750rpm, stirring and evenly mixing 0.5h;
(2), by lanoline 1.0g and stearic acid 2.0g, 70 ℃ of heated and stirred mix;
(3) (2) gains are slowly added in (1) gains, 70 ℃, shearing force is 700rpm, stirring and evenly mixing 0.5h;
(4) be cooled to 55 ℃, in (3) gains, add Chinese medicine dry powder 8.0g, continue to stir 20min;
(5) continue to be cooled to 45 ℃, add appropriate essence, antiseptic, stir 0.5h;
(6) step (5) gains are evacuated to finished pot, obtain product.
Embodiment 2
(1) in deionized water 45.0g, add polyoxyethylenated alcohol sodium sulfate 15.0g, sodium lauryl sulphate 3g, cocoanut fatty acid diethanolamide 3.0g, cocamido propyl betaine 3.0g, dodecayl dimethyl amine oxide 4.0g and glycerol 10.0g, 70 ℃, shearing force is 700rpm, stirring and evenly mixing 0.8h;
(2), by lanoline 2.0g and stearic acid 1.0g, 70 ℃ of heated and stirred mix;
(3) (2) gains are slowly added in (1) gains, 65 ℃, shearing force is 650rpm rpm, stirring and evenly mixing 0.8h;
(4) be cooled to 50 ℃, in (3) gains, add Chinese medicine dry powder 5.0g, continue to stir 30min;
(5) continue to be cooled to 40 ℃, add appropriate essence, antiseptic, stir 0.8h;
(6) step (5) gains are evacuated to finished pot, obtain product.
Embodiment 3
(1) in deionized water 65.0g, add polyoxyethylenated alcohol sodium sulfate 15.0g, sodium lauryl sulphate 2.5g, cocoanut fatty acid diethanolamide 3.0g, cocamido propyl betaine 3.0g, dodecayl dimethyl amine oxide 5.0g and glycerol 15.0g, 60 ℃, shearing force is 800rpm, stirring and evenly mixing 0.6h;
(2), by lanoline 1.5g and stearic acid 1.5g, 60 ℃ of heated and stirred mix;
(3) (2) gains are slowly added in (1) gains, 60 ℃, shearing force is 800rpm, stirring and evenly mixing 0.6h;
(4) be cooled to 60 ℃, in (3) gains, add Chinese medicine dry powder 4.0g, continue to stir 40min;
(5) continue to be cooled to 50 ℃, add appropriate essence, antiseptic, stir 0.6h;
(6) step (5) gains are evacuated to finished pot, obtain product.
Application Example 1
Object of study: oiliness skin quality, acne are compared with severe one, 15 examples.
Using method: sooner or later use every day each once, use continuously 3 weeks.
Experimental result: cure 7 examples, effective 5 examples, responder's 3 examples.
Application Example 2
Object of study: dryness skin quality, pruritus patient, 10 examples.
Using method: sooner or later use every day each once, use continuously 4 weeks.
Experimental result: sensation moistening effect is good, cures 7 examples, sensation is general, slightly effective 3 examples.
Application Example 3
Object of study: neutral skin quality person's 30 examples.
Using method: sooner or later use every day each once, use continuously 2 weeks
Experimental result: feel comfortable person's 24 examples, sensation general person 6 examples.

Claims (7)

1. the foam type cleansing milk containing Chinese medicine, the mass fraction % that it is characterized in that forming the component formula of this cleansing milk is: anion surfactant 10~25%, non-ionic surface active agent 2~5%, zwitterionic surfactant 2~5%, cationic surfactant 3~8%, fatty acid 0.5~5%, lanoline 0.5~5%, wetting agent 0.5~20%, deionized water 45~65%, Chinese medicine extract 3~8%, then add appropriate antiseptic and appropriate essence
The serve as reasons crude drug of following weight portion of described Chinese medicine extract is made: Radix Glycyrrhizae 10~40, the Radix Angelicae Dahuricae 4~18, Rhizoma Coptidis 3~15, Fructus Cnidii 5~20, Rhizoma Typhonii 4~18, Radix Scutellariae 3~15, Cortex Dictamni 5~16, Rhizoma Chuanxiong 4~15, Herba Asari 5~20, Poria 5~15, Semen Armeniacae Amarum 3~10, the Rhizoma Atractylodis Macrocephalae 5~20, Rhizoma Polygonati Odorati 5~20, Moschus 5~15;
Described Chinese medicine extract, its preparation method is that after alcohol reflux, spraying is dry, step is as follows:
(1) take each raw material of Chinese medicine medicine of weight portion, pulverize, cross 40 mesh sieves;
(2) by 5~10 times of each raw material of Chinese medicine medicine weight portions, get 75~95% ethanol, soak 0.5~5h, 40~75 ℃ of reflux, extract, 1~3h;
(3) filter, then get 5%~9% ethanol, reflux, extract, 1~3h by 5~10 times of filtering residue parts by weight;
(4) filter the rear two kinds of filtrates that merge, obtain Chinese medicine alcohol extract, put shady place and save backup;
(5) the spray-dried Chinese medicine dry powder that obtains of Chinese medicine alcohol extract.
2. the foam type cleansing milk containing Chinese medicine according to claim 1, is characterized in that described anion surfactant is selected from one or more in polyoxyethylenated alcohol sodium sulfate, sodium lauryl sulphate, ammonium lauryl sulfate; Described non-ionic surface active agent is selected from one or more in coconut oil fatty acid monoethanolamide, cocoanut fatty acid diethanolamide.
3. the foam type cleansing milk containing Chinese medicine according to claim 1, is characterized in that described zwitterionic surfactant is selected from one or more in cocamido propyl betaine, dodecyldimethylammonium hydroxide inner salt, alkyl dimethyl amine-oxides.
4. the foam type cleansing milk containing Chinese medicine according to claim 1, is characterized in that described cationic surfactant is selected from one or more in dodecayl dimethyl amine oxide, dodecyl dimethyl benzyl ammonium chloride, triethanolamine; Described fatty acid is selected from one or more in dodecoic acid, tetradecylic acid, hexadecylic acid, stearic acid.
5. the foam type cleansing milk containing Chinese medicine according to claim 1, it is characterized in that described wetting agent is at least one in glycerol, propylene glycol, 1,3 butylene glycol, Polyethylene Glycol, pyrrolidone sodium carboxylate, lactic acid and sodium lactate, collagen protein, aminoacid, hyaluronic acid.
6. the preparation method of the foam type cleansing milk containing Chinese medicine according to claim 1, is characterized in that preparation method comprises the steps:
1) in deionized water, add anion surfactant, non-ionic surface active agent, cationic surfactant, zwitterionic surfactant, wetting agent component, 60~85 ℃, shearing force is 500~800rpm, stirring and evenly mixing 0.2~1h;
2) lanoline and 60~85 ℃ of heated and stirred of fatty acid are mixed;
3) (2) gains are slowly added in (1) gains, 60~85 ℃, shearing force is 500~800rpm, stirring and evenly mixing 0.2~1h;
4) be cooled to 50~65 ℃, in (3) gains, add Chinese medicine dry powder, continue to stir 10~50min;
5) continue to be cooled to 40~50 ℃, add appropriate essence, antiseptic, stir 0.2~1h;
6) step (5) gains are evacuated to finished pot, obtain product.
7. the preparation method of the foam type cleansing milk containing Chinese medicine according to claim 6, is characterized in that wherein in step (4), Chinese medicine dry powder directly adds.
CN201110134081.0A 2011-05-23 2011-05-23 Foaming facial cleanser containing traditional Chinese medicines and preparation method thereof Expired - Fee Related CN102198078B (en)

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CN104546608A (en) * 2014-12-26 2015-04-29 刘三猫 Composition for preparing facial cleaner and facial cleaner
CN104546610B (en) * 2015-01-09 2018-04-13 湖南新金浩茶油股份有限公司 A kind of anti-aging facial cleanser and preparation method thereof
CN105030620A (en) * 2015-08-28 2015-11-11 青岛海之源智能技术有限公司 Moisturizing and acne removing facial cleanser and preparing method thereof
CN105147562A (en) * 2015-09-30 2015-12-16 青岛海之源智能技术有限公司 Gentle couperose-skin-removal facial cleanser and preparation method thereof
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