CN107320358A - A kind of Ai Xiang mildy wash and preparation method thereof - Google Patents
A kind of Ai Xiang mildy wash and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/733—Alginic acid; Salts thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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Abstract
The invention discloses a kind of Ai Xiang mildy wash, it is made up of the raw material of following weight parts：Sodium alginate 0.3 1, thickening emulsion 10 15, hexadecanoic acid 57, isopropanol 46, catalyst 0.01 0.02, soda 34, lauric acid amide of ethanol 0.6 1, lemon 12, folium artemisiae argyi 12, dispersant 0.8 1, methylisothiazolinone 0.1 0.2, triterpenoid saponin 0.08 0.1, radix glycyrrhizae 23, honeysuckle 13, the mildy wash formula of the present invention is reasonable, uniform and stable property is good, service life is long, applicability to various skin is good, allergic phenomena is not easily caused, security is good.
Description
Technical field
The invention belongs to cosmetic field, and in particular to a kind of Ai Xiang mildy wash and preparation method thereof.
Background technology
In general, mildy wash is made up of compositions such as oil phase thing, aqueous-phase material, surfactant, NMF, nutritional agents
Liquiform product.Wherein butyrous mildy wash contains oil-phase component, it is adaptable to which Dry is used;Crystal clear product not oil-containing
Phase constituent, such as formula conditioning is appropriate, can meet most consumers and use.Surfactant has wetting, divided in mildy wash
Scattered, foaming, decontamination, emulsification five effect greatly, are the chief active things of face cleaning product.In addition, according to the similar principle that mixes, washing one's face
Cheng Zhong, can borrow oil phase thing to dissolve the dirty and unnecessary grease of facial oil-soluble fat;By means of water miscible on its aqueous-phase material dissolving face
Sweat stain dirt；
Currently in order to meeting the different hobbies of people, various mildy wash arise at the historic moment, but presently commercially available mildy wash
Feature is more single, and the applicability to different skin is poor, and some meetings cause the phenomenons such as allergy；Folium artemisiae argyi it is outer to bacillus anthracis,
Alpha-hemolytic streptococcus, B- Streptococcus hemolyticus, corynebacterium diphtheriae, bacillus pseudodiphthericus, lung diplococcoid, staphylococcus aureus, lemon
10 kinds of gram-positive Aeromonas bacterias such as color staphylococcus, staphylococcus aureus, hay bacillus all have antibacterial action, to burn wound
Bacterium also there is good inhibition, and folium artemisiae argyi can antiallergy, safety non-toxic has delicate fragrance, therefore the purpose of the present invention
Exactly study that a kind of antiallergy, antibacterial, whitening, moisture retention be good, multi-functional mildy wash with Ai Xiang.
The content of the invention
It is an object of the invention to study, a kind of antiallergy, antibacterial, whitening, moisture retention be good, Multifunctional washing with Ai Xiang
There is provided a kind of Ai Xiang mildy wash and preparation method thereof for face milk.
To achieve the above object, the present invention uses following technical scheme：
A kind of Ai Xiang mildy wash, it is made up of the raw material of following weight parts：
Sodium alginate 0.3-1, thickening emulsion 10-15, hexadecanoic acid 5-7, isopropanol 4-6, catalyst 0.01-0.02, soda 3-
4th, lauric acid amide of ethanol 0.6-1, lemon 1-2, folium artemisiae argyi 1-2, dispersant 0.8-1, methylisothiazolinone 0.1-
0.2nd, triterpenoid saponin 0.08-0.1, radix glycyrrhizae 2-3, honeysuckle 1-3.
Described catalyst is the sulfuric acid that concentration is 96-98%.
Described dispersant is one kind in sorbitan monostearate, lauryl sodium sulfate or is two kinds of mixing
Thing, when for mixture, sorbitan monostearate, the weight ratio of lauryl sodium sulfate are 3-4:1.
Described thickening emulsion is made up of the raw material of following weight parts：
Xanthans 3-4, pentaerythrite 8-10, Cocoamidopropyl betaine 0.08-0.1, aloe 2-3, Semen Coicis 1-2.
The preparation method of described thickening emulsion comprises the following steps：
（1）Semen Coicis is taken, in the deionized water for being added to 60-70 times of its weight, boiling is heated to, keeps boiling 16-20 minutes, mistake
Filter, xanthans is added in filtrate, is stirred, latex solution is obtained；
（2）Pentaerythrite is taken, in the deionized water for being added to 10-15 times of its weight, is stirred, aloe is added, at 60-70 DEG C
Lower insulated and stirred 1-2 hours, filtering, filtrate is mixed with above-mentioned latex solution, adds Cocoamidopropyl betaine, is stirred to normal
Temperature, obtains the thickening emulsion.
A kind of preparation method of Ai Xiang mildy wash, comprises the following steps：
（1）In extracting liquorice, honeysuckle, folium artemisiae argyi mixing, the absolute ethyl alcohol for being added to 20-30 times of compound weight, at 65-70 DEG C
Insulated and stirred 1-2 hours, filtering, obtains extract solution；
（2）Methylisothiazolinone is taken, is added in isopropanol, is stirred, alcoholic solution is obtained；
（3）Triterpenoid saponin is taken, in the deionized water for being added to 10-15 times of its weight, is stirred, hexadecanoic acid, feeding is added
Into reactor, mixed with above-mentioned alcoholic solution, regulation temperature of reaction kettle is 90-95 DEG C, be added dropwise after catalyst, completion of dropping and be incubated
Stirring 2-3 hours, discharging, obtains esterification dispersion liquid；
（4）Thickening emulsion, dispersant are taken, in the deionized water for being added to 100-140 times of compound weight, is stirred,
Dispersion liquid must be thickened；
（5）Said extracted liquid, esterification dispersion liquid mixing are taken, stirs, adds soda, insulated and stirred 1-2 is small at 50-60 DEG C
When, ethanol is distilled off, adds above-mentioned thickening dispersion liquid, stirs, mixed with remaining each raw material, 1600-2000 revs/min is stirred
Mix 30-40 minutes, produce the Ai Xiang mildy wash.
Advantages of the present invention：
Triterpenoid saponin：It is dissolved in water more, colloidal solution can be generated after shaking, and have foam of the persistence like soap solution, with bright
It is aobvious it is impervious go out, the effect of anti-inflammatory, anti-hemostasis, the normal permeability of capillary can be recovered；
Folium artemisiae argyi：Outside to bacillus anthracis, Alpha-hemolytic streptococcus, B- Streptococcus hemolyticus, corynebacterium diphtheriae, bacillus pseudodiphthericus, the double balls of lung class
10 kinds of gram-positive Aeromonas bacterias such as bacterium, staphylococcus aureus, Staphylococcus citreus, staphylococcus aureus, hay bacillus
All have antibacterial action, also there is good inhibition to the bacterium of burn wound, and folium artemisiae argyi can antiallergy, safety non-toxic,
There is delicate fragrance；
Honeysuckle：Has inhibitory action to typhoid bacillus, shigella flexneri, staphylococcus aureus and Pseudomonas aeruginosa；
Aloe：With sterilization anti-inflammatory, the effect of beauty is moistened, aloe polysaccharide and vitamin have good battalion to the skin of human body
Foster, moist, whitening effect, especially youth maiden most worried acne, aloe are offseted except acne have good effect；
Triterpenoid saponin is distributed in the hexadecanoic acid aqueous solution by the present invention, and methylisothiazolinone is distributed into aqueous isopropanol
In, by the way that under the catalytic action of the concentrated sulfuric acid, hexadecanoic acid, isopropanol are carried out into esterification, obtained esterified material has very
Good dispersion effect, can promote active principle to the permeability of skin, strengthen the resistance of body, while playing more preferable U.S.
In vain, soft effect；
The mildy wash formula of the present invention is reasonable, and uniform and stable property is good, and service life is long, and the applicability to various skin is good, is difficult
Allergic phenomena is caused, security is good.
Embodiment
Embodiment 1
A kind of Ai Xiang mildy wash, it is made up of the raw material of following weight parts：
Sodium alginate 0.3, thickening emulsion 10, hexadecanoic acid 5, isopropanol 4, catalyst 0.01, soda 3, coconut oil diethanol acyl
Amine 0.6, lemon 1, folium artemisiae argyi 1, dispersant 0.8, methylisothiazolinone 0.1, triterpenoid saponin 0.08, radix glycyrrhizae 2, honeysuckle 1.
Described catalyst is the sulfuric acid that concentration is 96%.
Described dispersant is sorbitan monostearate.
Described thickening emulsion is made up of the raw material of following weight parts：
Xanthans 3, pentaerythrite 8, Cocoamidopropyl betaine 0.08, aloe 2, Semen Coicis 1.
The preparation method of described thickening emulsion comprises the following steps：
（1）Semen Coicis is taken, in the deionized water for being added to 60 times of its weight, boiling is heated to, keeps boiling 16 minutes, filter,
Xanthans is added in filtrate, is stirred, latex solution is obtained；
（2）Pentaerythrite is taken, in the deionized water for being added to 10 times of its weight, is stirred, aloe is added, is incubated at 60 DEG C
Stirring 1 hour, filtering, filtrate is mixed with above-mentioned latex solution, adds Cocoamidopropyl betaine, is stirred to normal temperature, is obtained institute
State thickening emulsion.
A kind of preparation method of Ai Xiang mildy wash, comprises the following steps：
（1）In extracting liquorice, honeysuckle, folium artemisiae argyi mixing, the absolute ethyl alcohol for being added to 20 times of compound weight, it is incubated and stirs at 65 DEG C
Mix 1 hour, filter, obtain extract solution；
（2）Methylisothiazolinone is taken, is added in isopropanol, is stirred, alcoholic solution is obtained；
（3）Triterpenoid saponin is taken, in the deionized water for being added to 10 times of its weight, is stirred, hexadecanoic acid is added, is sent to anti-
Answer in kettle, mixed with above-mentioned alcoholic solution, regulation temperature of reaction kettle is 90 DEG C, insulated and stirred 2 after catalyst, completion of dropping is added dropwise small
When, discharging obtains esterification dispersion liquid；
（4）Thickening emulsion, dispersant are taken, in the deionized water for being added to 100 times of compound weight, stirs, must increase
Thick dispersion liquid；
（5）Said extracted liquid, esterification dispersion liquid mixing are taken, is stirred, soda is added, insulated and stirred 1 hour at 50 DEG C is steamed
Ethanol is removed in distillation, is added above-mentioned thickening dispersion liquid, is stirred, mixed with remaining each raw material, and 1600 revs/min are stirred 30 minutes,
Produce the Ai Xiang mildy wash.
Embodiment 2
A kind of Ai Xiang mildy wash, it is made up of the raw material of following weight parts：
Sodium alginate 1, thickening emulsion 15, hexadecanoic acid 7, isopropanol 6, catalyst 0.02, soda 4, lauric acid amide of ethanol
1st, lemon 2, folium artemisiae argyi 2, dispersant 1, methylisothiazolinone 0.2, triterpenoid saponin 0.1, radix glycyrrhizae 3, honeysuckle 3.
Described catalyst is the sulfuric acid that concentration is 98%.
Described dispersant is lauryl sodium sulfate.
Described thickening emulsion is made up of the raw material of following weight parts：
Xanthans 4, pentaerythrite 10, Cocoamidopropyl betaine 0.1, aloe 3, Semen Coicis 2.
The preparation method of described thickening emulsion comprises the following steps：
（1）Semen Coicis is taken, in the deionized water for being added to 70 times of its weight, boiling is heated to, keeps boiling 20 minutes, filter,
Xanthans is added in filtrate, is stirred, latex solution is obtained；
（2）Pentaerythrite is taken, in the deionized water for being added to 15 times of its weight, is stirred, aloe is added, is incubated at 70 DEG C
Stirring 2 hours, filtering, filtrate is mixed with above-mentioned latex solution, adds Cocoamidopropyl betaine, is stirred to normal temperature, is obtained institute
State thickening emulsion.
A kind of preparation method of Ai Xiang mildy wash, comprises the following steps：
（1）In extracting liquorice, honeysuckle, folium artemisiae argyi mixing, the absolute ethyl alcohol for being added to 30 times of compound weight, it is incubated and stirs at 70 DEG C
Mix 2 hours, filter, obtain extract solution；
（2）Methylisothiazolinone is taken, is added in isopropanol, is stirred, alcoholic solution is obtained；
（3）Triterpenoid saponin is taken, in the deionized water for being added to 15 times of its weight, is stirred, hexadecanoic acid is added, is sent to anti-
Answer in kettle, mixed with above-mentioned alcoholic solution, regulation temperature of reaction kettle is 95 DEG C, insulated and stirred 3 after catalyst, completion of dropping is added dropwise small
When, discharging obtains esterification dispersion liquid；
（4）Thickening emulsion, dispersant are taken, in the deionized water for being added to 140 times of compound weight, stirs, must increase
Thick dispersion liquid；
（5）Said extracted liquid, esterification dispersion liquid mixing are taken, is stirred, soda is added, insulated and stirred 2 hours at 60 DEG C are steamed
Ethanol is removed in distillation, is added above-mentioned thickening dispersion liquid, is stirred, mixed with remaining each raw material, and 2000 revs/min are stirred 40 minutes,
Produce the Ai Xiang mildy wash.
Performance test：
50 subjects are sought, man 15, female 25, using the mildy wash of the present invention, once in the morning and once at night, adheres at age 16-50 Sui
Using 30 days, subject represented the salubrious non-greasy of face, can effectively clean dirt, and skin is more soft fine and smooth, not
Appearance local skin is bad to wait allergic reaction.
Claims (6)
1. a kind of Ai Xiang mildy wash, it is characterised in that it is made up of the raw material of following weight parts：
Sodium alginate 0.3-1, thickening emulsion 10-15, hexadecanoic acid 5-7, isopropanol 4-6, catalyst 0.01-0.02, soda 3-
4th, lauric acid amide of ethanol 0.6-1, lemon 1-2, folium artemisiae argyi 1-2, dispersant 0.8-1, methylisothiazolinone 0.1-
0.2nd, triterpenoid saponin 0.08-0.1, radix glycyrrhizae 2-3, honeysuckle 1-3.
2. a kind of Ai Xiang mildy wash according to claim 1, it is characterised in that described catalyst is that concentration is 96-98%
Sulfuric acid.
3. a kind of Ai Xiang mildy wash according to claim 1, it is characterised in that described dispersant is that sorb is smooth single stearic
One kind in acid esters, lauryl sodium sulfate is two kinds of mixture, when for mixture, sorbitan monostearate, ten
The weight ratio of sodium dialkyl sulfate is 3-4:1.
4. a kind of Ai Xiang mildy wash according to claim 1, it is characterised in that described thickening emulsion is by following weight
The raw material composition of part：
Xanthans 3-4, pentaerythrite 8-10, Cocoamidopropyl betaine 0.08-0.1, aloe 2-3, Semen Coicis 1-2.
5. a kind of Ai Xiang mildy wash according to claim 4, it is characterised in that the preparation method bag of described thickening emulsion
Include following steps：
（1）Semen Coicis is taken, in the deionized water for being added to 60-70 times of its weight, boiling is heated to, keeps boiling 16-20 minutes, mistake
Filter, xanthans is added in filtrate, is stirred, latex solution is obtained；
（2）Pentaerythrite is taken, in the deionized water for being added to 10-15 times of its weight, is stirred, aloe is added, at 60-70 DEG C
Lower insulated and stirred 1-2 hours, filtering, filtrate is mixed with above-mentioned latex solution, adds Cocoamidopropyl betaine, is stirred to normal
Temperature, obtains the thickening emulsion.
6. a kind of preparation method of Ai Xiang mildy wash as claimed in claim 1, it is characterised in that comprise the following steps：
（1）In extracting liquorice, honeysuckle, folium artemisiae argyi mixing, the absolute ethyl alcohol for being added to 20-30 times of compound weight, at 65-70 DEG C
Insulated and stirred 1-2 hours, filtering, obtains extract solution；
（2）Methylisothiazolinone is taken, is added in isopropanol, is stirred, alcoholic solution is obtained；
（3）Triterpenoid saponin is taken, in the deionized water for being added to 10-15 times of its weight, is stirred, hexadecanoic acid, feeding is added
Into reactor, mixed with above-mentioned alcoholic solution, regulation temperature of reaction kettle is 90-95 DEG C, be added dropwise after catalyst, completion of dropping and be incubated
Stirring 2-3 hours, discharging, obtains esterification dispersion liquid；
（4）Thickening emulsion, dispersant are taken, in the deionized water for being added to 100-140 times of compound weight, is stirred,
Dispersion liquid must be thickened；
（5）Said extracted liquid, esterification dispersion liquid mixing are taken, stirs, adds soda, insulated and stirred 1-2 is small at 50-60 DEG C
When, ethanol is distilled off, adds above-mentioned thickening dispersion liquid, stirs, mixed with remaining each raw material, 1600-2000 revs/min is stirred
Mix 30-40 minutes, produce the Ai Xiang mildy wash.
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Cited By (3)
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| CN108721164A (en) * | 2018-07-04 | 2018-11-02 | 徐姣姣 | A kind of facial cleanser and preparation method thereof that wrinkle effect is good |
| CN109276501A (en) * | 2018-11-16 | 2019-01-29 | 安徽迎春草生物科技有限公司 | Careless facial cleanser of the anti-radiation winter jasmine of one kind and preparation method thereof |
| CN111840185A (en) * | 2020-08-27 | 2020-10-30 | 刘克武 | Chinese medicinal wormwood face wash |
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| CN108721164A (en) * | 2018-07-04 | 2018-11-02 | 徐姣姣 | A kind of facial cleanser and preparation method thereof that wrinkle effect is good |
| CN109276501A (en) * | 2018-11-16 | 2019-01-29 | 安徽迎春草生物科技有限公司 | Careless facial cleanser of the anti-radiation winter jasmine of one kind and preparation method thereof |
| CN111840185A (en) * | 2020-08-27 | 2020-10-30 | 刘克武 | Chinese medicinal wormwood face wash |
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