CN102173953B - Selenium-containing fruit stem smear for fruits and vegetables and preparation method thereof as well as method for improving content of selenium in fruits and vegetables - Google Patents
Selenium-containing fruit stem smear for fruits and vegetables and preparation method thereof as well as method for improving content of selenium in fruits and vegetables Download PDFInfo
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Abstract
The invention belongs to the technical fields of selenium-containing fruit stem smears for fruits and vegetables, preparation processes and use methods thereof and discloses a selenium-containing fruit stem smear for f fruits and vegetables as well as a preparation process and a use method thereof. The selenium-containing smear is characterized by comprising the following materials by weight: 100kg of refined wool oil, 6.5-13 kg of refined food-grade compound amino acid powder, 0.06-0.6 kg of pure selenium contained in selenite or selenic acid and 10-13.5 kg of water. The materials are chelated and homogeneized, so that the selenium-containing fruit stem smear for fruits and vegetables can be attached to the fruit stems for a long term and can not be taken away by wind and rain; since theselenium element is directly absorbed by fruits without being consumed by other parts of plants, absorption rate is improved so that the fruits and vegetables which have stems contain high selenium contents; and the preparation method and use method are convenient for operation and are beneficial to popularization.
Description
Technical field
The invention belongs to fruits and vegetables smears, preparation technology and using method technical field, relate to concretely a kind of method that contains selenium fruits and vegetables carpopodium smears, preparation technology and improve the fruits and vegetables Se content.
Background technology
The endemic that causes because selenium lacks in China involves northeast to more than ten province and municipality in southwest.The Keshan disease of having found and Kaschin-Beck disease and lack selenium substantial connection is arranged.Keshan disease mostly occur grow the childhood, take 2-6 years old as common, also see simultaneously Women of Childbearing Age.Enlarging arrhythmia cordis, tachycardia appear or crosses the slow heart that reaches in the main heart of invading, and causes at last heart failure, cardiogenic shock.The Kaschin-Beck disease major lesions is cartilage cell's degeneration necrosis of epiphysis, and amyotrophy affects bone growth and development, and morbidity is also take the teenager as many.A kind of patient who medically is called " muscle syndrome " is also found in the area of low selenium in soil, shows as myalgia, walks weak.For improving the intake of people's selenium, people improve the content of selenium in fruit or the vegetables.
The method that improves for Se content in the fruits and vegetables at present is that inorganic fertilizer is mixed with in potassium selenate, sodium selenate or the ammonium selenate one or more, the main employing has following two kinds of fertilization modes: one, soil applies method, there is following shortcoming in the method: 1, the selenium element easily with soil in the element generation antagonism such as calcium, sulphur, magnesium or be adsorbed fixedly become not by the state of plant absorbing, thereby the reduction absorption ratio; 2, in the situation that the soil drought plant can't absorb, in the situation that waterlogging caused by excessive rain easily is leached again the following soil of root, root system can't reach, and can't absorb; Its two, foliage-spray, there is following shortcoming in the method: 1, the Se content of plant own is high, and the fruit Se content is low, because selenium is not the necessary nutritive element of plant, to the excessive selenium element that applies, easily causes the plant underproduction; 2, air dried weather absorption ratio is low, and the rainy day easily by the rainwater leaching loss, 3, absorb from blade, distribute through the transportation of rhizome branch again, at last in the fruit seldom, cause the waste of selenium element.
Summary of the invention
First technical problem that the present invention solves just provides that a kind of Se content is high, easy operating, absorption ratio are high contains selenium fruits and vegetables carpopodium smears.
For solving the problems of the technologies described above, the technical scheme that contains selenium fruits and vegetables carpopodium smears that the present invention proposes is: the material that includes following weight portion:
The refined wool fat double centner;
Purified diet level composite aminophenol powder 6.5---13 kilograms;
Be converted to pure selenium content 0.06---0.6 kilogram selenite;
Water 10---13.5 kilograms.
Its additional technical feature is:
The material that also comprises following weight portion:
90% gibberellin 1.14---1.26 kilograms, naphthoxyacetic acid 0.26---0.52 kilogram;
Described selenite is sodium selenite, and weight is 0.13---1.3 kilograms;
Described selenite is potassium selenite, and weight is 0.16---1.6 kilograms.
Second technical problem that the present invention solves just provides a kind of preparation technology who contains selenium fruits and vegetables carpopodium smears.
For solving the problems of the technologies described above, the technical scheme that the present invention proposes is:
This technique comprises the following steps:
The first step is selected materials,
Weight ratio according to each raw material takes by weighing raw material;
Second step dissolves purified diet level composite aminophenol powder,
Water is added in the first reactor, adds again purified diet level composite aminophenol powder, be stirred to it and dissolve, be heated to 80 ℃---90 ℃;
The 3rd step, chelating,
In the first reactor, add selenite, stir and maintain the temperature at 89 ℃---91 ℃, the time, making it abundant chelating became chelating attitude amino acid selenium liquid at 6-8 hour;
The 4th step, refined wool fat is mixed with chelating attitude amino acid selenium liquid,
Refined wool fat is packed in the second reactor into heat fused to 80 ℃---90 ℃, and chelating attitude amino acid selenium liquid joined in this second reactor, and stir;
The 5th step, homogeneous in homogenizer
Refined wool fat and chelating attitude amino acid selenium liquid mixture that the 4th step was obtained are cooled to 45 ℃---and 55 ℃, import in the homogenizer, carry out homogeneous;
The 6th step, can
To be cooled to through the mixture behind the homogeneous 40 ℃---45 ℃, become inner wrapping with the paste pouring machine can, naturally cool to after the can below 38 ℃ and get final product.
Its additional technical feature is:
The method also comprises the following steps:
90% gibberellin and naphthoxyacetic acid are crushed to the above mixing of 1000 orders with micronizer, then add in the homogenizer in the 5th step, with refined wool fat and chelating attitude amino acid selenium liquid mixture, homogeneous in homogenizer.
The 3rd technical problem that the present invention solves just provides a kind of above-mentioned method that contains selenium fruits and vegetables carpopodium smears Effective Raise fruits and vegetables Se content of utilizing.
For solving the problems of the technologies described above, the technical scheme that the present invention proposes is:
The method comprises the following steps:
The first step: smear
After fruit or vegetables bear fruit, smear a week with coating brush at the carpopodium place of fruit or vegetables, every gram contains containing selenium fruits and vegetables carpopodium smears and can smearing 10 of selenium 0.05%---50 carpopodiums;
Second step is plucked
During the fruits and vegetables results, cut off the part of carpopodium band smears with scissors, then frame up.
Its additional technical feature is:
Described fruit is apple, and every gram contains containing selenium fruits and vegetables carpopodium smears and can smearing 40 of selenium 0.05%---50 carpopodiums;
Described vegetables are eggplant, and every gram contains containing selenium fruits and vegetables carpopodium smears and can smearing 10-15 carpopodiums of selenium 0.05%.
The method that contains selenium fruits and vegetables carpopodium smears, preparation technology and improve the fruits and vegetables Se content provided by the invention, comparing with prior art has the following advantages: one, owing to including the material of following weight portion: the refined wool fat double centner; Purified diet level composite aminophenol powder 6.5---13 kilograms; Be converted to pure selenium content 0.06---0.6 kilogram selenite or selenic acid; Water 10---13.5 kilograms, and through chelating and homogeneous, so that containing selenium fruits and vegetables carpopodium smears, this can be attached to for a long time on the carpopodium, can be because wind and weather come off, the selenium element is directly absorbed by fruit without other positions of plant, improved absorption ratio, so that high with Se content in the fruit of carpopodium fruits and vegetables, and easy to operate, be beneficial to popularization.
Embodiment
The below is described further the method that contains selenium fruits and vegetables carpopodium smears, preparation technology and raising fruits and vegetables Se content proposed by the invention.
The technical scheme that contains selenium fruits and vegetables carpopodium smears that the present invention proposes is: the material that includes following weight portion:
The refined wool fat double centner;
Purified diet level composite aminophenol powder 6.5---13 kilograms;
Be converted to pure selenium content 0.06---0.6 kilogram selenite;
Water 10---13.5 kilograms.
Selenite can be sodium selenite, potassium selenite, can also be selenous acid ammonia, as long as selenium content reaches weight.
According to need of production, can also in containing selenium fruits and vegetables carpopodium smears, add 90% gibberellin 1.14---1.26 kilograms, naphthoxyacetic acid 0.26---0.52 kilogram.
Embodiment 1
The first step is selected materials
Take by weighing the refined wool fat double centner, 6.5 kilograms of purified diet level composite aminophenol powders, 0.13 kilogram of sodium selenite, 10 kilograms in water,
Second step dissolves purified diet level composite aminophenol powder,
Water is added in the first reactor, add again purified diet level composite aminophenol powder, be stirred to it and dissolve, be heated to 80 ℃;
The 3rd step, chelating,
Add selenite in the first reactor, stir and maintain the temperature at 89 ℃, the time, making it abundant chelating became chelating attitude amino acid selenium liquid at 6 hours;
The 4th step, refined wool fat is mixed with chelating attitude amino acid selenium liquid,
Refined wool fat is packed in the second reactor, heat fused to 80 ℃, and chelating attitude amino acid selenium liquid joined in this second reactor, and stir;
The 5th step, homogeneous in homogenizer
Refined wool fat and chelating attitude amino acid selenium liquid mixture that the 4th step was obtained are cooled to 45 ℃, import in the homogenizer, carry out homogeneous;
The 6th step, can
To be cooled to through the mixture behind the homogeneous 40 ℃, become inner wrapping with the paste pouring machine can, and naturally cool to after the can below 38 ℃ and get final product.
Embodiment 2
The first step is selected materials
Take by weighing the refined wool fat double centner, 13 kilograms of purified diet level composite aminophenol powders, 1.3 kilograms of sodium selenites, 13.5 kilograms in water,
Second step dissolves purified diet level composite aminophenol powder,
Water is added in the first reactor, add again purified diet level composite aminophenol powder, be stirred to it and dissolve, be heated to 90 ℃;
The 3rd step, chelating,
Add selenite in the first reactor, stir and maintain the temperature at 91 ℃, the time, making it abundant chelating became chelating attitude amino acid selenium liquid at 8 hours;
The 4th step, refined wool fat is mixed with chelating attitude amino acid selenium liquid,
Refined wool fat is packed in the second reactor, heat fused to 90 ℃, and chelating attitude amino acid selenium liquid joined in this second reactor, and stir;
The 5th step, homogeneous in homogenizer
Refined wool fat and chelating attitude amino acid selenium liquid mixture that the 4th step was obtained are cooled to 55 ℃, import in the homogenizer, carry out homogeneous;
The 6th step, can
To be cooled to through the mixture behind the homogeneous 45 ℃, become inner wrapping with the paste pouring machine can, and naturally cool to after the can below 38 ℃ and get final product.
Embodiment 3
The first step is selected materials
Take by weighing the refined wool fat double centner, 13 kilograms of purified diet level composite aminophenol powders, 0.16 kilogram of potassium selenite, 12.5 kilograms in water, 1.14 kilograms of 90% gibberellin, 0.26 kilogram of naphthoxyacetic acid;
Second step dissolves purified diet level composite aminophenol powder,
Water is added in the first reactor, add again purified diet level composite aminophenol powder, be stirred to it and dissolve, be heated to 85 ℃;
The 3rd step, chelating,
Add selenite in the first reactor, stir and maintain the temperature at 90 ℃, the time, making it abundant chelating became chelating attitude amino acid selenium liquid at 7 hours;
The 4th step, refined wool fat is mixed with chelating attitude amino acid selenium liquid,
Refined wool fat is packed in the second reactor, heat fused to 90 ℃, and chelating attitude amino acid selenium liquid joined in this second reactor, and stir;
The 5th step, homogeneous in homogenizer
Refined wool fat and chelating attitude amino acid selenium liquid mixture that the 4th step was obtained are cooled to 50 ℃, import in the homogenizer, then 90% gibberellin and naphthoxyacetic acid are crushed in the 1100 order mixings adding homogenizer with micronizer, carry out homogeneous;
The 6th step, can
To be cooled to through the mixture behind the homogeneous 42 ℃, become inner wrapping with the paste pouring machine can, and naturally cool to after the can below 38 ℃ and get final product.
Embodiment 4
The first step is selected materials
Take by weighing the refined wool fat double centner, 8 kilograms of purified diet level composite aminophenol powders, 1.6 kilograms of potassium selenites, 11.5 kilograms in water, 1.26 kilograms of 90% gibberellin, 0.52 kilogram of naphthoxyacetic acid;
Second step dissolves purified diet level composite aminophenol powder,
Water is added in the first reactor, add again purified diet level composite aminophenol powder, be stirred to it and dissolve, be heated to 87 ℃;
The 3rd step, chelating,
Add selenite in the first reactor, stir and maintain the temperature at 90 ℃, the time, making it abundant chelating became chelating attitude amino acid selenium liquid at 6.5 hours;
The 4th step, refined wool fat is mixed with chelating attitude amino acid selenium liquid,
Refined wool fat is packed in the second reactor, heat fused to 85 ℃, and chelating attitude amino acid selenium liquid joined in this second reactor, and stir;
The 5th step, homogeneous in homogenizer
Refined wool fat and chelating attitude amino acid selenium liquid mixture that the 4th step was obtained are cooled to 52 ℃, import in the homogenizer, then 90% gibberellin and naphthoxyacetic acid are crushed in the 1000 order mixings adding homogenizer with micronizer, carry out homogeneous;
The 6th step, can
To be cooled to through the mixture behind the homogeneous 43 ℃, become inner wrapping with the paste pouring machine can, and naturally cool to after the can below 38 ℃ and get final product.
Embodiment 5
The first step is selected materials
Take by weighing the refined wool fat double centner, 8 kilograms of purified diet level composite aminophenol powders, 0.11 kilogram of selenic acid, 11.5 kilograms in water, 1.20 kilograms of 90% gibberellin, 0.32 kilogram of naphthoxyacetic acid;
Second step dissolves purified diet level composite aminophenol powder,
Water is added in the first reactor, add again purified diet level composite aminophenol powder, be stirred to it and dissolve, be heated to 85 ℃;
The 3rd step, chelating,
Add selenite in the first reactor, stir and maintain the temperature at 90 ℃, the time, making it abundant chelating became chelating attitude amino acid selenium liquid at 7 hours;
The 4th step, refined wool fat is mixed with chelating attitude amino acid selenium liquid,
Refined wool fat is packed in the second reactor, heat fused to 88 ℃, and chelating attitude amino acid selenium liquid joined in this second reactor, and stir;
The 5th step, homogeneous in homogenizer
Refined wool fat and chelating attitude amino acid selenium liquid mixture that the 4th step was obtained are cooled to 51 ℃, import in the homogenizer, then 90% gibberellin and naphthoxyacetic acid are crushed in the 1300 order mixings adding homogenizer with micronizer, carry out homogeneous;
The 6th step, can
To be cooled to through the mixture behind the homogeneous 44 ℃, become inner wrapping with the paste pouring machine can, and naturally cool to after the can below 38 ℃ and get final product.
Embodiment 6
The first step is selected materials
Take by weighing the refined wool fat double centner, 8 kilograms of purified diet level composite aminophenol powders, 1.1 kilograms of selenic acids, 11.5 kilograms in water, 1.20 kilograms of 90% gibberellin, 0.32 kilogram of naphthoxyacetic acid;
Second step dissolves purified diet level composite aminophenol powder,
Water is added in the first reactor, add again purified diet level composite aminophenol powder, be stirred to it and dissolve, be heated to 82 ℃;
The 3rd step, chelating,
Add selenite in the first reactor, stir and maintain the temperature at 91 ℃, the time, making it abundant chelating became chelating attitude amino acid selenium liquid at 7.5 hours;
The 4th step, refined wool fat is mixed with chelating attitude amino acid selenium liquid,
Refined wool fat is packed in the second reactor, heat fused to 82 ℃, and chelating attitude amino acid selenium liquid joined in this second reactor, and stir;
The 5th step, homogeneous in homogenizer
Refined wool fat and chelating attitude amino acid selenium liquid mixture that the 4th step was obtained are cooled to 48 ℃, import in the homogenizer, then 90% gibberellin and naphthoxyacetic acid are crushed in the 1300 order mixings adding homogenizer with micronizer, carry out homogeneous;
The 6th step, can
To be cooled to through the mixture behind the homogeneous 44 ℃, become inner wrapping with the paste pouring machine can, and naturally cool to after the can below 38 ℃ and get final product.
The method that improves the fruits and vegetables Se content comprises the following steps:
The first step: smear
After fruit or vegetables bear fruit, smear a week with coating brush at the carpopodium place of fruit or vegetables, every gram contains containing selenium fruits and vegetables carpopodium smears and can smearing 10 of selenium 0.05%---50 carpopodiums;
Second step is plucked
During the fruits and vegetables results, cut off the part of carpopodium band smears with scissors, then frame up.
The method is applicable to the long fruit tree that carpopodium arranged and melon dish etc., such as apple, pears, peach, oranges and tangerines, watermelon, eggplant etc.
According to fruit size and breeding time length determine amount of application: general fruit growth period 20---25 days, the absorption conversion ratio of selenium is 30%---33%, fruit growth period 30---50 days, the absorption conversion ratio of selenium is 40%---45%, and fruit growth period 50---70 days, the absorption conversion ratio of selenium was 60%---65%, fruit growth period 75---100 days, the absorption conversion ratio of selenium is 75%---more than 85%, 120 day, the absorption conversion ratio of selenium is 90%---and 95%.And then the size that grows up to the consequence type according to fruit is determined amount of application in conjunction with above absorption ratio value for referencial use.As Fuji apple fruit breeding time more than 160 days, be 90-95% with reference to absorption ratio, fruit grows up to rear general fruit and heavily is the 200-300 gram, producing selenium content such as target is 20---the selenium-enriched apple of 50 microgram/kilograms, in the situation that soil lacks selenium, general selenium content is 0.2 when not adding selenium---0.9 microgram/kilogram, each apple should be mended selenium 4-10 microgram, contain selenium fruits and vegetables carpopodium smears in the middle and upper part of each apple carpopodium with 20 milligrams of selenium contents 0.05% and smear a circle before the surely really rear bagging of Fuji apple, namely the selenium fruits and vegetables carpopodium smears that contains of every gram selenium content 0.05% processes 40---50 young fruits.
Again for example: productive target is 20---the rich selenium Greenhouse eggplant of 50 microgram/kilograms, general kind single fruit weight 400-500 gram, the benefit selenium amount of each eggplant is in the 20-50 microgram so, namely begin after bearing fruit to smear, be about about 40 days to gathering, the absorption ratio reference value is 40%, contain selenium fruits and vegetables carpopodium smears with selenium content 0.05% so and smear a circle, the selenium fruits and vegetables carpopodium smears that contains of every gram selenium content 0.05% processes 10---15 young fruits, if with 0.5% contain selenium fruits and vegetables carpopodium smears, every gram contains selenium fruits and vegetables carpopodium smears and processes 100---150 young fruits.
When results, cut off the part that the carpopodium band contains selenium fruits and vegetables carpopodium smears with scissors, then the dress basket transports outside the field, prevents the carpopodium contacting fruit surface with the smears.
Claims (7)
1. contain selenium fruits and vegetables carpopodium smears, it is characterized in that: the material that includes following weight portion:
The refined wool fat double centner;
Purified diet level composite aminophenol powder 6.5---13 kilograms;
Be converted to pure selenium content 0.06---0.6 kilogram selenite;
Water 10---13.5 kilograms;
This contains selenium fruits and vegetables carpopodium smears and prepares by following method:
The first step is selected materials,
Weight ratio according to each raw material takes by weighing raw material;
Second step dissolves purified diet level composite aminophenol powder,
Water is added in the first reactor, adds again purified diet level composite aminophenol powder, be stirred to it and dissolve, be heated to 80 ℃---90 ℃;
The 3rd step, chelating,
In the first reactor, add selenite, stir and maintain the temperature at 89 ℃---91 ℃, the time, making it abundant chelating became chelating attitude amino acid selenium liquid at 6-8 hour;
The 4th step, refined wool fat is mixed with chelating attitude amino acid selenium liquid,
Refined wool fat is packed in the second reactor into heat fused to 80 ℃---90 ℃, and chelating attitude amino acid selenium liquid joined in this second reactor, and stir;
The 5th step, homogeneous in homogenizer
Refined wool fat and chelating attitude amino acid selenium liquid mixture that the 4th step was obtained are cooled to 45 ℃---and 55 ℃, import in the homogenizer, carry out homogeneous;
The 6th step, can
To be cooled to through the mixture behind the homogeneous 40 ℃---45 ℃, become inner wrapping with the paste pouring machine can, naturally cool to after the can below 38 ℃.
2. the selenium fruits and vegetables carpopodium smears that contains according to claim 1 is characterized in that: the material that also comprises following weight portion:
90% gibberellin 1.14---1.26 kilograms, naphthoxyacetic acid 0.26---0.52 kilogram;
90% gibberellin and naphthoxyacetic acid are crushed to the above mixing of 1000 orders with micronizer, then add in the homogenizer in the 5th step, with refined wool fat and chelating attitude amino acid selenium liquid mixture, homogeneous in homogenizer.
3. the selenium fruits and vegetables carpopodium smears that contains according to claim 1, it is characterized in that: described selenite is sodium selenite, weight is 0.13---1.3 kilograms.
4. the selenium fruits and vegetables carpopodium smears that contains according to claim 1, it is characterized in that: described selenite is potassium selenite, weight is 0.16---1.6 kilograms.
5. right to use requires 1 describedly to contain the method that selenium fruits and vegetables carpopodium smears improves the fruits and vegetables Se content, and it is characterized in that: the method comprises the following steps:
The first step: smear
After fruit or vegetables bear fruit, smear a week with coating brush at the carpopodium place of fruit or vegetables, every gram contains the selenium fruits and vegetables carpopodium smears that contains of selenium 0.05% and smears 10---50 carpopodiums;
Second step is plucked
During the fruits and vegetables results, cut off the part of carpopodium band smears with scissors, then frame up.
6. the method for raising fruits and vegetables Se content according to claim 5, it is characterized in that: described fruit is apple, every gram contains the selenium fruits and vegetables carpopodium smears that contains of selenium 0.05% and smears 40---50 carpopodiums.
7. the method for raising fruits and vegetables Se content according to claim 5, it is characterized in that: described vegetables are eggplant, every gram contains the selenium fruits and vegetables carpopodium smears that contains of selenium 0.05% and smears 10-15 carpopodiums.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102992919A (en) * | 2012-12-29 | 2013-03-27 | 广东大众农业科技股份有限公司 | Toothpaste type fertilizer |
| CN103814737B (en) * | 2014-03-10 | 2015-09-09 | 山东省寿光蔬菜产业集团有限公司 | A kind of implantation methods of rich selenium muskmelon |
| CN103814741B (en) * | 2014-03-10 | 2015-10-14 | 山东省寿光蔬菜产业集团有限公司 | The implantation methods of a kind of rich selenium tomato |
| CN103814739B (en) * | 2014-03-10 | 2015-10-28 | 山东省寿光蔬菜产业集团有限公司 | A kind of implantation methods of rich selenium pimento |
| CN103814740B (en) * | 2014-03-10 | 2015-10-14 | 山东省寿光蔬菜产业集团有限公司 | The implantation methods of a kind of rich selenium cucumber |
| CN103798053B (en) * | 2014-03-10 | 2015-09-09 | 山东省寿光蔬菜产业集团有限公司 | A kind of implantation methods of rich selenium eggplant |
| CN104351004A (en) * | 2014-11-25 | 2015-02-18 | 南京农业大学 | Method for simultaneously increasing zinc and selenium contents of pear |
| CN105706712A (en) * | 2016-03-04 | 2016-06-29 | 刘万顺 | Selenium-rich corn production method |
| CN107996131A (en) * | 2017-12-25 | 2018-05-08 | 华侨大学 | A kind of pineapple device for picking |
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| CN1088725A (en) * | 1993-10-30 | 1994-07-06 | 黑龙江省普阳农场 | A kind of method of producing selenium-enriched crop products |
| CN1313034A (en) * | 2001-04-05 | 2001-09-19 | 李春俭 | Plant growth regulator for increasing potassium content in tobacco leaf and its application |
| CN1388094A (en) * | 2001-05-26 | 2003-01-01 | 杨杰民 | Selenium-rich amino acid and its production process |
| CN1608471A (en) * | 2004-07-16 | 2005-04-27 | 杨容甫 | Selenium-enriching agent and its usage and use |
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