CN102138883A - Changbai Mountain ledum palustre bactericidal skin care hand washing lotion and preparation method thereof - Google Patents
Changbai Mountain ledum palustre bactericidal skin care hand washing lotion and preparation method thereof Download PDFInfo
- Publication number
- CN102138883A CN102138883A CN2011100672912A CN201110067291A CN102138883A CN 102138883 A CN102138883 A CN 102138883A CN 2011100672912 A CN2011100672912 A CN 2011100672912A CN 201110067291 A CN201110067291 A CN 201110067291A CN 102138883 A CN102138883 A CN 102138883A
- Authority
- CN
- China
- Prior art keywords
- var
- ledum palustre
- preparation
- stem
- changbai mountain
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 235000001506 Ledum palustre Nutrition 0.000 title claims abstract description 65
- 238000002360 preparation method Methods 0.000 title claims abstract description 29
- 230000000844 anti-bacterial effect Effects 0.000 title abstract description 9
- 241000227142 Rhododendron tomentosum Species 0.000 title abstract 6
- 239000006210 lotion Substances 0.000 title abstract 5
- 238000005406 washing Methods 0.000 title abstract 5
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 27
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 21
- 239000002994 raw material Substances 0.000 claims abstract description 19
- 239000003125 aqueous solvent Substances 0.000 claims abstract description 17
- 238000010992 reflux Methods 0.000 claims abstract description 10
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000001768 carboxy methyl cellulose Substances 0.000 claims abstract description 9
- 239000000843 powder Substances 0.000 claims abstract description 9
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 claims abstract description 9
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 claims abstract description 9
- 238000003756 stirring Methods 0.000 claims abstract description 9
- QXNVGIXVLWOKEQ-UHFFFAOYSA-N Disodium Chemical compound [Na][Na] QXNVGIXVLWOKEQ-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract description 7
- 125000000217 alkyl group Chemical group 0.000 claims abstract description 7
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract description 7
- 244000251855 Ledum palustre Species 0.000 claims description 59
- 230000001954 sterilising effect Effects 0.000 claims description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 20
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 16
- 239000002671 adjuvant Substances 0.000 claims description 15
- 238000009835 boiling Methods 0.000 claims description 15
- 239000004094 surface-active agent Substances 0.000 claims description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
- 239000012153 distilled water Substances 0.000 claims description 12
- 239000007788 liquid Substances 0.000 claims description 8
- 239000011780 sodium chloride Substances 0.000 claims description 8
- ULUAUXLGCMPNKK-UHFFFAOYSA-N Sulfobutanedioic acid Chemical compound OC(=O)CC(C(O)=O)S(O)(=O)=O ULUAUXLGCMPNKK-UHFFFAOYSA-N 0.000 claims description 6
- 150000001408 amides Chemical class 0.000 claims description 6
- 235000019864 coconut oil Nutrition 0.000 claims description 6
- 239000003240 coconut oil Substances 0.000 claims description 6
- 238000005303 weighing Methods 0.000 claims description 6
- 239000008367 deionised water Substances 0.000 claims description 4
- 229910021641 deionized water Inorganic materials 0.000 claims description 4
- 230000001105 regulatory effect Effects 0.000 claims description 4
- 238000001816 cooling Methods 0.000 claims description 2
- 230000008595 infiltration Effects 0.000 claims description 2
- 238000001764 infiltration Methods 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 6
- 239000000284 extract Substances 0.000 abstract description 5
- 230000003385 bacteriostatic effect Effects 0.000 abstract description 4
- 241000411851 herbal medicine Species 0.000 abstract description 4
- 238000004140 cleaning Methods 0.000 abstract 2
- 230000000172 allergic effect Effects 0.000 abstract 1
- 208000010668 atopic eczema Diseases 0.000 abstract 1
- 239000002537 cosmetic Substances 0.000 abstract 1
- 230000001804 emulsifying effect Effects 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 241000196324 Embryophyta Species 0.000 description 2
- 241000588724 Escherichia coli Species 0.000 description 2
- 241000191967 Staphylococcus aureus Species 0.000 description 2
- 229940088710 antibiotic agent Drugs 0.000 description 2
- UAHWPYUMFXYFJY-UHFFFAOYSA-N beta-myrcene Chemical compound CC(C)=CCCC(=C)C=C UAHWPYUMFXYFJY-UHFFFAOYSA-N 0.000 description 2
- WTWBUQJHJGUZCY-UHFFFAOYSA-N cuminaldehyde Chemical compound CC(C)C1=CC=C(C=O)C=C1 WTWBUQJHJGUZCY-UHFFFAOYSA-N 0.000 description 2
- HFPZCAJZSCWRBC-UHFFFAOYSA-N p-cymene Chemical compound CC(C)C1=CC=C(C)C=C1 HFPZCAJZSCWRBC-UHFFFAOYSA-N 0.000 description 2
- 239000000341 volatile oil Substances 0.000 description 2
- WCGUUGGRBIKTOS-GPOJBZKASA-N (3beta)-3-hydroxyurs-12-en-28-oic acid Chemical compound C1C[C@H](O)C(C)(C)[C@@H]2CC[C@@]3(C)[C@]4(C)CC[C@@]5(C(O)=O)CC[C@@H](C)[C@H](C)[C@H]5C4=CC[C@@H]3[C@]21C WCGUUGGRBIKTOS-GPOJBZKASA-N 0.000 description 1
- MIJYXULNPSFWEK-GTOFXWBISA-N 3beta-hydroxyolean-12-en-28-oic acid Chemical compound C1C[C@H](O)C(C)(C)[C@@H]2CC[C@@]3(C)[C@]4(C)CC[C@@]5(C(O)=O)CCC(C)(C)C[C@H]5C4=CC[C@@H]3[C@]21C MIJYXULNPSFWEK-GTOFXWBISA-N 0.000 description 1
- 241000722824 Ardisia crenata Species 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 208000035143 Bacterial infection Diseases 0.000 description 1
- JKLISIRFYWXLQG-UHFFFAOYSA-N Epioleonolsaeure Natural products C1CC(O)C(C)(C)C2CCC3(C)C4(C)CCC5(C(O)=O)CCC(C)(C)CC5C4CCC3C21C JKLISIRFYWXLQG-UHFFFAOYSA-N 0.000 description 1
- 241000208421 Ericaceae Species 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- YBRJHZPWOMJYKQ-UHFFFAOYSA-N Oleanolic acid Natural products CC1(C)CC2C3=CCC4C5(C)CCC(O)C(C)(C)C5CCC4(C)C3(C)CCC2(C1)C(=O)O YBRJHZPWOMJYKQ-UHFFFAOYSA-N 0.000 description 1
- MIJYXULNPSFWEK-UHFFFAOYSA-N Oleanolinsaeure Natural products C1CC(O)C(C)(C)C2CCC3(C)C4(C)CCC5(C(O)=O)CCC(C)(C)CC5C4=CCC3C21C MIJYXULNPSFWEK-UHFFFAOYSA-N 0.000 description 1
- 241000700605 Viruses Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- VYBREYKSZAROCT-UHFFFAOYSA-N alpha-myrcene Natural products CC(=C)CCCC(=C)C=C VYBREYKSZAROCT-UHFFFAOYSA-N 0.000 description 1
- 239000006286 aqueous extract Substances 0.000 description 1
- 208000022362 bacterial infectious disease Diseases 0.000 description 1
- 229930006722 beta-pinene Natural products 0.000 description 1
- 238000005202 decontamination Methods 0.000 description 1
- 230000003588 decontaminative effect Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000003467 diminishing effect Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229940100243 oleanolic acid Drugs 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- HZLWUYJLOIAQFC-UHFFFAOYSA-N prosapogenin PS-A Natural products C12CC(C)(C)CCC2(C(O)=O)CCC(C2(CCC3C4(C)C)C)(C)C1=CCC2C3(C)CCC4OC1OCC(O)C(O)C1O HZLWUYJLOIAQFC-UHFFFAOYSA-N 0.000 description 1
- 230000004223 radioprotective effect Effects 0.000 description 1
- 230000000452 restraining effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 150000003505 terpenes Chemical class 0.000 description 1
- 229940096998 ursolic acid Drugs 0.000 description 1
- PLSAJKYPRJGMHO-UHFFFAOYSA-N ursolic acid Natural products CC1CCC2(CCC3(C)C(C=CC4C5(C)CCC(O)C(C)(C)C5CCC34C)C2C1C)C(=O)O PLSAJKYPRJGMHO-UHFFFAOYSA-N 0.000 description 1
- WTARULDDTDQWMU-UHFFFAOYSA-N β-pinene Chemical compound C1C2C(C)(C)C1CCC2=C WTARULDDTDQWMU-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Cosmetics (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The invention discloses a Changbai Mountain ledum palustre bactericidal skin care hand washing lotion and a preparation method thereof, which belong to the technical field of cleaning and skin care cosmetics. Stem leaf extract of ledum palustre, namely a Chinese herbal medicine of Changbai Mountain, is added into a hand washing lotion, so that the hand washing lotion containing the stem leaf extract of ledum palustre has mild property, is nonirritant and non-allergic to skin and has bacteriostatic and skin care effects. The product is prepared from raw materials comprising disodium cocoyl monoethanolamide sulfosuccina, alkyl polyglucoside, glycerol, polyethylene glycol, citric acid, sodium carboxymethyl cellulose, an aqueous solvent, steam leaf extract of ledum palustre and the like according to a certain proportion. The preparation method of the product comprises the following steps of: refluxing stem powder and leaf powder of the ledum palustre through vapor; collecting vapor reflux in 2 to 3 hours; adding various raw materials; and dissolving, stirring, heating, emulsifying, standing and the like to obtain the product. The hand washing lotion disclosed by the invention can be used for cleaning and has the bacteriostatic and skin care effects.
Description
Technical field
The present invention relates to Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. sterilizing skin-protective hand cleanser and preparation method thereof
Background technology
Hands be directly contact at most with the external world in the body part, the easiest contaminated part, also be person to person, extraneous and self virus, very important media of bacterial infection, with healthy closely bound up.At present, social civilization progressively promotes, and the idea of " duty is washed one's hands, sterilized more " has been goed deep in the ordinary populace life, as seen, and antibacterial sterilization type handwashing liquid extensive market.Yet the market grows existing bacteriostatic hand sanitizer and mostly is chemosynthesis class antibacterial at present, and skin is had bigger stimulation.
Ledum Palustre L.var.dilatatum Wahl. is that Angiospermae Ericaceae Ledum Palustre L.var.dilatatum Wahl. belongs to evergreen shrubs, and Chinese Chinese medicine material also is important spice berry, mainly is distributed in Changbai Mountain, Daxinganling District in China.Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. stem and leaf aqueous extract contains the Ledum Palustre L.var.dilatatum Wahl. volatile oil component based on cumal, myrcene, nopinene, paracymene etc., have effects such as inhibiting bacteria and diminishing inflammation, radioprotective, promotion Transdermal absorption, especially the growth to antibacterials such as common staphylococcus aureus, escherichia coli has the good restraining effect; And the performance gentleness, non-stimulated not irritated to skin.
Therefore, develop Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. sterilizing skin-protective hand cleanser, not only can satisfy the demand of the modern civilization life of taste, health, also can satisfy the modern and recover one's original simplicity, return natural life idea, have huge social, economic benefit.
Summary of the invention
One of the object of the invention for overcoming the defective of prior art, provides a kind of natural Chinese medicinal herb skin protection bacteriostatic hand sanitizer, adds to have Changbai Mountain Chinese herbal medicine Ledum Palustre L.var.dilatatum Wahl. stem and leaf extract antibacterial, the skin Caring effect, reach can decontamination again can be antibacterial, the effect of skin protection.Changbai Mountain Chinese herbal medicine Ledum Palustre L.var.dilatatum Wahl. extract performance gentleness, non-stimulated not irritated to skin.
Two of purpose of the present invention, the application of expansion China Chinese herbal medicine promotes the exploitation of Changbai Mountain wild plant resource, promotes the northeast China's economic development.
Handwashing liquid technical formula of the present invention is (every 100ml): surfactant 20ml～40ml, Ledum Palustre L.var.dilatatum Wahl. stem and leaf extracting solution 35ml～50ml, adjuvant 3g～10g, aqueous solvent 15ml～30ml.
Described Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. stem and leaf extracting solution preparation: alembic, condensing tube, adapter are assembled into distilling apparatus, take by weighing exsiccant Ledum Palustre L.var.dilatatum Wahl. stem, leaf powder 10.0g, put into round-bottomed flask, add 300～500ml distilled water, be heated to boiling, little fire keeps boiling, refluxes 2～3 hours, collects Ledum Palustre L.var.dilatatum Wahl. stem, leaf steam backflow.
Described surfactant is by volume prepared by following raw materials according: 40% coconut oil single ethanol amide sulfosuccinic acid monoesters disodium, 10ml～20ml; 40% alkyl polyglucoside, 5ml～20ml;
Described adjuvant is prepared by quality by following raw materials according: NaCl, 1g～2g; Glycerol, 0.5ml～2ml; Polyethylene Glycol, 1g～2g; Citric acid, 0.5g～1g; Sodium carboxymethyl cellulose, 2～4g.
Described aqueous solvent raw material: in deionized water, pure water, infiltration water, the distilled water any one.
Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. sterilizing skin-protective hand cleanser, its preparation method is as follows:
(1) Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. stem and leaf extracting solution preparation: get exsiccant Ledum Palustre L.var.dilatatum Wahl. stem, leaf powder 10.0g, put into round-bottomed flask, add 300～500ml distilled water, be heated to boiling, little fire keeps boiling, refluxes 2～3 hours, collect Ledum Palustre L.var.dilatatum Wahl. stem, leaf steam backflow, it is standby to put 4 ℃ of refrigerators.
(2) get required aqueous solvent, be heated to 50～55 ℃, add surfactant, adjuvant while stirring,, add remaining aqueous solvent, stir cooling until dissolving fully.
(3) treat temperature to 15～20 ℃, add Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. stem and leaf extracting solution, stir.
(4) citric acid is regulated PH to 6.0～7.0, and sodium carboxymethyl cellulose, sodium chloride are regulated denseness, stirs pack or bottling.
Product of the present invention Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. sterilizing skin-protective hand cleanser characteristics: with Changbai Mountain wild plant resource Ledum Palustre L.var.dilatatum Wahl. volatile oil is main component, be rich in terpenoid active substances such as cumal, paracymene, ursolic acid, oleanolic acid, suitably be equipped with surfactant, adjuvant, has effect antibacterial, skin protection, cheap, it is convenient to be suitable for.
Product of the present invention Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. sterilizing skin-protective hand cleanser stable storage: sample is placed color-comparison tube, in (40 ± 1) ℃ constant incubator and (4 ± 2) ℃ refrigerator, place 48h respectively, returning to room temperature observes, there are not any precipitation and metachromatism, inhibited to antibacterials such as escherichia coli, staphylococcus aureuses.
The specific embodiment
Example 1: Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. sterilizing skin-protective hand cleanser and preparation method thereof, technical formula is as follows:
Handwashing liquid technical formula of the present invention is (every 100ml): surfactant 40ml, Ledum Palustre L.var.dilatatum Wahl. stem and leaf extracting solution 35ml, adjuvant 7g, aqueous solvent 24.5ml.
The preparation of described Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. stem and leaf extracting solution: alembic, condensing tube, adapter are assembled into distilling apparatus, take by weighing exsiccant Ledum Palustre L.var.dilatatum Wahl. stem, leaf powder 10.0g, put into round-bottomed flask, add the 300ml distilled water, be heated to boiling, little fire keeps boiling, refluxes 2.5 hours, collect Ledum Palustre L.var.dilatatum Wahl. stem and leaf steam backflow, it is standby to get 35ml.
Described surfactant is by volume prepared by following raw materials according: 40% coconut oil single ethanol amide sulfosuccinic acid monoesters disodium, 20ml; 40% alkyl polyglucoside, 20ml;
Described adjuvant is prepared by weight by following raw materials according: NaCl, 2g; Glycerol, 0.5ml; Polyethylene Glycol, 2g; Citric acid, 1g; Sodium carboxymethyl cellulose, 2g.
Described aqueous solvent raw material is a deionized water.
Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. sterilizing skin-protective hand cleanser preparation method see claim book 6.
Example 2: Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. sterilizing skin-protective hand cleanser and preparation method thereof, technical formula is as follows:
Handwashing liquid technical formula of the present invention is (every 100ml): surfactant 30ml, Ledum Palustre L.var.dilatatum Wahl. stem and leaf extracting solution 30ml, adjuvant 8g, aqueous solvent 29.5ml.
The preparation of described Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. stem and leaf extracting solution: alembic, condensing tube, adapter are assembled into distilling apparatus, take by weighing exsiccant Ledum Palustre L.var.dilatatum Wahl. stem, leaf powder 10.0g, put into round-bottomed flask, add the 350ml distilled water, be heated to boiling, little fire keeps boiling, refluxes 3 hours, collect Ledum Palustre L.var.dilatatum Wahl. stem and leaf steam backflow, it is standby to get 40ml.
Described surfactant is by volume prepared by following raw materials according: 40% coconut oil single ethanol amide sulfosuccinic acid monoesters disodium, 10ml; 40% alkyl polyglucoside, 20ml;
Described adjuvant is prepared by weight by following raw materials according: NaCl, 1g; Glycerol, 0.5ml; Polyethylene Glycol, 2g; Citric acid, 1g; Sodium carboxymethyl cellulose, 4g.
Described aqueous solvent raw material is a distilled water.
Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. sterilizing skin-protective hand cleanser preparation method see claim book 6.
Example 3: Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. sterilizing skin-protective hand cleanser and preparation method thereof, technical formula is as follows:
Handwashing liquid technical formula of the present invention is (every 100ml): surfactant 20ml, Ledum Palustre L.var.dilatatum Wahl. stem and leaf extracting solution 50ml, adjuvant 7g, aqueous solvent 29ml.
The preparation of described Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. stem and leaf extracting solution: alembic, condensing tube, adapter are assembled into distilling apparatus, take by weighing exsiccant Ledum Palustre L.var.dilatatum Wahl. stem, leaf powder 10.0g, put into round-bottomed flask, add the 300ml distilled water, be heated to boiling, little fire keeps boiling, refluxes 3 hours, collect Ledum Palustre L.var.dilatatum Wahl. stem and leaf steam backflow, it is standby to get 50ml.
Described surfactant is by volume prepared by following raw materials according: 40% coconut oil single ethanol amide sulfosuccinic acid monoesters disodium, 10ml; 40% alkyl polyglucoside, 10ml;
Described adjuvant is prepared by weight by following raw materials according: NaCl, 1g; Glycerol, 1ml; Polyethylene Glycol, 1g; Citric acid, 0.5g; Sodium carboxymethyl cellulose, 4g.
Described aqueous solvent raw material is a deionized water.
Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. sterilizing skin-protective hand cleanser preparation method see claim book 6.
Example 4: Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. sterilizing skin-protective hand cleanser and preparation method thereof, technical formula is as follows:
Handwashing liquid technical formula of the present invention is (every 100ml): surfactant 25ml, Ledum Palustre L.var.dilatatum Wahl. stem and leaf extracting solution 40ml, adjuvant 5g, aqueous solvent 18ml.
The preparation of described Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. stem and leaf extracting solution: alembic, condensing tube, adapter are assembled into distilling apparatus, take by weighing exsiccant Ledum Palustre L.var.dilatatum Wahl. stem, leaf powder 10.0g, put into round-bottomed flask, add the 400ml distilled water, be heated to boiling, little fire keeps boiling, refluxes 2 hours, collect Ledum Palustre L.var.dilatatum Wahl. stem and leaf steam backflow, it is standby to get 45ml.
Described surfactant is by volume prepared by following raw materials according: 40% coconut oil single ethanol amide sulfosuccinic acid monoesters disodium, 20ml; 40% alkyl polyglucoside, 5ml.
Described adjuvant is prepared by weight by following raw materials according: NaCl, 1g; Glycerol, 2ml; Polyethylene Glycol, 1g; Citric acid, 1g; Sodium carboxymethyl cellulose, 2g.
Described aqueous solvent raw material is a distilled water.
Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. sterilizing skin-protective hand cleanser preparation method see claim book 6.
Claims (6)
1. Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. sterilizing skin-protective hand cleanser and preparation method thereof, it is characterized in that handwashing liquid technical formula of the present invention is (every 100ml): surfactant 20ml～40ml, Ledum Palustre L.var.dilatatum Wahl. stem and leaf extracting solution 35ml～50ml, adjuvant 3g～10g, aqueous solvent 15ml～30ml.
2. according to claims 1 described Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. sterilizing skin-protective hand cleanser and preparation method thereof, it is characterized in that Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. stem and leaf extracting solution preparation method is that alembic, condensing tube, adapter are assembled into distilling apparatus, take by weighing exsiccant Ledum Palustre L.var.dilatatum Wahl. stem, leaf 10.0g, pulverize, put into round-bottomed flask, add 300～500ml distilled water, be heated to boiling, little fire refluxes, and keeps 2～3 hours, collects Ledum Palustre L.var.dilatatum Wahl. stem and leaf steam backflow.
3. according to the described Changbai Mountain of claims 1-2 Ledum Palustre L.var.dilatatum Wahl. sterilizing skin-protective hand cleanser and preparation method thereof, it is characterized in that, described surfactant is by volume prepared by following raw materials according: 40% coconut oil single ethanol amide sulfosuccinic acid monoesters disodium, 10ml～20ml; 40% alkyl polyglucoside, 5ml～20ml.
4. according to the described Changbai Mountain of claims 1-3 Ledum Palustre L.var.dilatatum Wahl. sterilizing skin-protective hand cleanser and preparation method thereof, it is characterized in that described adjuvant is prepared by quality by following raw materials according: NaCl, 1g～2g; Glycerol, 0.5ml～2ml; Polyethylene Glycol, 1g～2g; Citric acid, 0.5g～1g; Sodium carboxymethyl cellulose, 2～4g.
5. according to the described Changbai Mountain of claims 1-4 Ledum Palustre L.var.dilatatum Wahl. sterilizing skin-protective hand cleanser and preparation method thereof, it is characterized in that, described aqueous solvent be in deionized water, pure water, infiltration water, the distilled water any one.
6. according to the described Changbai Mountain of claims 1-5 Ledum Palustre L.var.dilatatum Wahl. sterilizing skin-protective hand cleanser and preparation method thereof, it is characterized in that the handwashing liquid preparation method is as follows:
(1) Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. stem and leaf extracting solution preparation: get exsiccant Ledum Palustre L.var.dilatatum Wahl. stem, leaf powder 10.0g, put into round-bottomed flask, add 300～500ml distilled water, be heated to boiling, little fire keeps boiling, refluxes 2～3 hours, collect Ledum Palustre L.var.dilatatum Wahl. stem, leaf steam backflow, it is standby to put 4 ℃ of refrigerators;
(2) get required aqueous solvent, be heated to 50～55 ℃, add surfactant, adjuvant while stirring,, add remaining aqueous solvent, stir cooling until dissolving fully;
(3) treat temperature to 15～20 ℃, add Changbai Mountain Ledum Palustre L.var.dilatatum Wahl. stem and leaf extracting solution, stir;
(4) citric acid is regulated PH to 6.0～7.0, and sodium carboxymethyl cellulose, sodium chloride are regulated denseness, stirs pack or bottling.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011100672912A CN102138883B (en) | 2011-03-21 | 2011-03-21 | Changbai Mountain ledum palustre bactericidal skin care hand washing lotion |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011100672912A CN102138883B (en) | 2011-03-21 | 2011-03-21 | Changbai Mountain ledum palustre bactericidal skin care hand washing lotion |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102138883A true CN102138883A (en) | 2011-08-03 |
| CN102138883B CN102138883B (en) | 2013-03-13 |
Family
ID=44406829
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2011100672912A Expired - Fee Related CN102138883B (en) | 2011-03-21 | 2011-03-21 | Changbai Mountain ledum palustre bactericidal skin care hand washing lotion |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102138883B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102631295A (en) * | 2012-03-30 | 2012-08-15 | 中国日用化学工业研究院 | Multifunctional foam liquid soap containing glucoside and derivatives of glucoside, and preparation method thereof |
| CN113136267A (en) * | 2021-05-03 | 2021-07-20 | 芭而蒂洗涤科技(天津)有限公司 | A cleaning product containing Ledum Palustre L extract and its preparation method |
| CN115322837A (en) * | 2022-08-17 | 2022-11-11 | 东北林业大学 | Refined ledum essential oil refining process and antibacterial application thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1709398A (en) * | 2005-06-06 | 2005-12-21 | 沈阳药科大学 | Filtering-degerming Chinese medicine or animal-plant volatile oil or fat emulsion and preparing method |
-
2011
- 2011-03-21 CN CN2011100672912A patent/CN102138883B/en not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1709398A (en) * | 2005-06-06 | 2005-12-21 | 沈阳药科大学 | Filtering-degerming Chinese medicine or animal-plant volatile oil or fat emulsion and preparing method |
Non-Patent Citations (4)
| Title |
|---|
| 《中国洗涤用品工业》 20090331 杨亚莉 功能性洗手液及其配方设计 第66-69页 1-6 , 第3期 * |
| 《高师理科学刊》 20051130 胡秀华 植物杜香祛斑霜的研制 第44-45页 1-6 第25卷, 第4期 * |
| 《高师理科学刊》 20071130 刘庆华，范慧颖 复方杜香消炎洗液的配制及应用 第53-55页 1-6 第27卷, 第6期 * |
| 《齐齐哈尔大学学报》 20061130 刘庆华 杜香油精保湿润肤霜的研制 第21-23页 1-6 第22卷, 第6期 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102631295A (en) * | 2012-03-30 | 2012-08-15 | 中国日用化学工业研究院 | Multifunctional foam liquid soap containing glucoside and derivatives of glucoside, and preparation method thereof |
| CN102631295B (en) * | 2012-03-30 | 2013-07-03 | 中国日用化学工业研究院 | Multifunctional foam liquid soap containing glucoside and derivatives of glucoside, and preparation method thereof |
| CN113136267A (en) * | 2021-05-03 | 2021-07-20 | 芭而蒂洗涤科技(天津)有限公司 | A cleaning product containing Ledum Palustre L extract and its preparation method |
| CN115322837A (en) * | 2022-08-17 | 2022-11-11 | 东北林业大学 | Refined ledum essential oil refining process and antibacterial application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102138883B (en) | 2013-03-13 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103230354B (en) | Sweating suppression deodorant composition | |
| CN104336078A (en) | Chlorine-containing Chinese herbal medicine air disinfectant, and preparation method and application thereof | |
| CN106265147A (en) | A kind of floral water containing natural plant essential oils and preparation method thereof | |
| CN100402094C (en) | Liquid Tibetan incense and its prepn. method | |
| CN102973973B (en) | Air-freshening bacteriostatic agent and preparation method thereof | |
| CN102973972A (en) | Rosemary leaf mosquito-repelling air freshener and preparation method | |
| CN102989025A (en) | Camphor tree leaf mosquito repellent air fresher and preparation method | |
| CN111714543A (en) | Herbal essential oil with sterilization effect and preparation method and application thereof | |
| CN106234439A (en) | A kind of superbacteria antibiosis and sterilization agent and its production and use | |
| CN103637944A (en) | Natural anti-bacterial shower gel | |
| CN110215532A (en) | A kind of plants essential oil water solvent combinations object and preparation method thereof | |
| CN109303729A (en) | A kind of preparation method of Chinese medicine agalloch eaglewood shampoo | |
| CN105475370A (en) | Air disinfectant | |
| CN102138883B (en) | Changbai Mountain ledum palustre bactericidal skin care hand washing lotion | |
| CN104367529A (en) | Mosquito repellent floral water for purifying air and preparation method of mosquito repellent floral water | |
| CN109055047A (en) | A kind of mosquito-proof children laundry detergent | |
| CN105708763B (en) | A kind of floral water containing Folium Artemisiae Argyi extract and preparation method thereof | |
| CN111789780A (en) | A hand-washing-free disinfectant containing Chinese medicinal volatile oil, and its preparation method | |
| CN104758322A (en) | Composition capable of expelling insects, killing bacteria, sterilizing, and relieving nerve, and applications thereof | |
| CN104322570A (en) | Chinese mugwort air sterilization spray and preparation method thereof | |
| CN105456180B (en) | A kind of anti-rash liquid of the sterilization of baby wipes and preparation method thereof | |
| CN103494749B (en) | Natural mosquito repellent | |
| CN104815096A (en) | Nano composite skin disinfection emulsion and preparation method of same | |
| CN107343865B (en) | Compound volatile oil and preparation method and application thereof | |
| CN103462853B (en) | A kind of mosquito-repellent water |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20130313 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |