CN102062543A - Electromagnetic stirring and vibration combined device for preparing semi-solid slurry of black metal - Google Patents

Electromagnetic stirring and vibration combined device for preparing semi-solid slurry of black metal Download PDF

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Publication number
CN102062543A
CN102062543A CN 201110006232 CN201110006232A CN102062543A CN 102062543 A CN102062543 A CN 102062543A CN 201110006232 CN201110006232 CN 201110006232 CN 201110006232 A CN201110006232 A CN 201110006232A CN 102062543 A CN102062543 A CN 102062543A
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crucible
melting furnace
teeter chamber
thermocouple
stirring
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CN102062543B (en
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赵升吨
陶文琉
张琦
林文捷
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Xian Jiaotong University
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Xian Jiaotong University
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Abstract

The invention relates to an electromagnetic stirring and vibration combined device for preparing semi-solid slurry of a black metal. The device comprises three main sections: a melting furnace, a stirring chamber, and a crystallizer or a rheologic conveyor, wherein the melting furnace is arranged at the upper part of the stirring chamber, and the crystallizer or the rheologic conveyor is arranged at the lower part of the stirring chamber. When molten metal is poured into the melting furnace, a medium-frequency induction heater is used for maintaining temperature and uniformly heating; when the temperature of the molten metal is within the liquidus temperature range, the molten metal is poured into a stirring crucible in a quantitative amount, and a non-dendritic fine equiaxial spherical or nearly spherical microstructure is obtained by electromagnetically stirring and mechanically vibrating the molten metal; and the prepared fine nearly spherical semi-solid slurry is poured into the crystallizer, then cooled and solidified into a blank, or the slurry is poured into the rheologic conveyor and then is rapidly conveyed to a forming mold for rheoforming. The device can be used for preparing semi-solid slurry of a black metal and nonferrous metal, which improves the efficiency and the quality for preparing metal semi-solid slurry and shortens the preparation time. The device is especially suitable for rheoforming.

Description

A kind of electromagnetic agitation of ferrous metal semi-solid pulp preparation and vibration set composite
Technical field
The invention belongs to the metal semi-solid slurry preparing technical field, be specifically related to a kind of electromagnetic agitation and vibration set composite of ferrous metal semi-solid pulp preparation.
Background technology
Semi-solid metal forming is the novel forming technique of a kind of metal, and the advantage that it combines casting and forges only needs a small amount of operation just can be shaped than complicated shape and high performance workpiece.Compare with conventional cast, this technology has that forming temperature is low, die life significant prolongation, can improve the precision and the mechanical property of workpiece simultaneously.And compare with traditional forge hot, semi-solid state forming technique has that plastic force is low, good fluidity, can realize near-net-shape, especially only need a procedure can be shaped than the workpiece of complicated shape.Up to the present, in low melting point non-ferrous metal metal field, this technology has obtained to use widely, especially in industry such as automobile, Aero-Space, electrical equipment.But to the high-melting-point ferrous material, semi-solid-state shaping is also still in conceptual phase.
In the semi-solid-state shaping process, the semi solid slurry preparation is a very crucial technical step, the success or not of decision semi-solid-state shaping, and its purpose is for having obtained the tiny spherical or torulose microstructure of axle that waits of non-dendrite.Up to the present, people have developed the new technology and the new technology of many preparation metal semi-solid slurries, activate (SIMA method), heat treating process, interpolation powder alterant method etc. as electromagnetic stirring method, mechanical mixing method, vibratory drilling method, strain-induced fusing.But, successfully be applied to have only electromagnetic stirring method on the industrial production, and the preparation alloy be mainly non-ferrous metal, as aluminium alloy, magnesium alloy etc.Compare with non-ferrous metal, the research of ferrous material semi-solid state forming technique is less, reason mainly is ferrous metal fusing point height (1300-1500 ℃), doubles with the fusing point (500-700 ℃) of aluminium alloy, brings very big difficulty for ferrous metal semi-solid pulp preparation and semi-solid-state shaping.
Mechanical mixing method is that the metal semi-solid slurry preparation is used the earliest.This method utilizes rotating vane or the stirring rod nascent solid phase in will solidifying to smash, and obtains the semi solid slurry of spherical or nearly spherical nascent solid phase, and its advantage is that equipment is simple, be of value to and form tiny microstructure; But shortcoming is, ferrous metal melt temperature height during pulp preparation, is lacked, easily causes the burn into metal paste to be vulnerable to pollution etc. the service life of rotating vane or stirring rod, therefore prepares this method at metal semi-solid slurry and uses less.
The electromagnetic agitation ratio juris is to utilize rotary electromagnetic field to produce induction field in molten metal, and molten metal produces motion under the effect of Lorentz force, thereby realizes the purpose to the molten metal stirring.The outstanding advantage of this method is contactless paddling process, has effectively overcome the problem that is similar to churned mechanically blade or stirring rod corrosion contamination, has in addition that mixing parametric control is flexible, an easy adjusting etc.At present, in the preparation of non-ferrous metal semi solid slurry, electromagnetic stirring method is most widely used general, is applied on the industrial production.But to ferrous material, this method also is in initial stage, reason is, ferrous metal fusing point height, melt conductance are low, thereby bring very big difficulty to semi solid slurry preparation, power of agitator is big as required, mixing time long and heating, insulation, cooling procedure in need good measure etc.
The advantage of mechanical oscillation semi solid slurry preparation method is simple, the easy realization of equipment, small investment etc.In recent years, the Central China University of Science and Technology adopted low-frequency mechanical vibrations that A390, ZL 101 alloy etc. is carried out the semi solid slurry preparation, had obtained the more tiny non-dendritic structure that waits axle.But during vibration, thermocouple and the control assembly thereof of measuring temperature are subjected to violent exciting force, cause reducing their job stabilitys, the lost of life.
Control degree of superheat cast semi solid slurry preparation method is to prepare semi-solid metal slurry or blank by control alloy pouring temperature and solidification cooling, and this technical method does not generally adopt any stirring, so preparation technology is simple.Its shortcoming is that efficient is low, and structural homogenity is relatively poor, especially ferrous metal fusing point height, be difficult to temperature control, therefore lower, the difficult realization to this method side's efficient of ferrous metal.
Above-mentioned several preparation metal semi-solid slurries are effects separately, and its efficient is lower, power requirement is bigger, and preparation is difficult to obtain good effect to the ferrous material semi solid slurry.In recent years, had the scholar that low melting point non-ferrous metal semi solid slurry is combined above-mentioned both or many persons and obtained better effects, microstructure is tiny, uniformly spherical or closely spherical, preparation time is short, required power is little etc.
On the other hand, in the semi-solid rheological molding technology, quantitatively cast is a crucial step.Conventional method generally adopts the stopper rod formula, and its advantage is that structure is simpler, and when still pouring into a mould, semi solid slurry is by gravity or pressing mode discharging, instability of flow, so quantitative error is bigger, does not still also have good solution at present.
Summary of the invention
In order to overcome the shortcoming of above-mentioned prior art, a kind of electromagnetic agitation and vibration set composite of ferrous metal semi-solid pulp preparation have been the object of the present invention is to provide, can prepare ferrous metal and non-ferrous metal semi solid slurry or rheological molding, improve the efficient and the quality of preparation metal semi-solid slurry, reduced preparation time.
In order to achieve the above object, the technical solution used in the present invention is:
A kind of electromagnetic agitation of ferrous metal semi-solid pulp preparation and vibration set composite, form by melting furnace 1, the II of teeter chamber, crystallizer IIIA or rheology conveyer IIIB three parts, melting furnace I is installed in II top, teeter chamber, the bottom of the fusion crucible substrate 32 of melting furnace I is stretched in the stirring crucible 10 of the II of teeter chamber, and crystallizer IIIA or rheology conveyer IIIB are installed in II bottom, teeter chamber;
Described melting furnace I comprises fusion crucible 7, the outside of fusion crucible 7 is provided with melting furnace heat-insulation layer 8, the outside of melting furnace heat-insulation layer 8 is provided with medium frequency induction heater 1, fusion crucible 7, melting furnace heat-insulation layer 8 and medium frequency induction heater 1 coaxial melting furnace base plate 9 tops that are installed in, the top of fusion crucible 7 and melting furnace heat-insulation layer 8 is provided with bell 5, last stopper rod 6 is positioned on the center line of fusion crucible 7, the centre bore that the one end passes bell 5 stretches out outside the bell 5, the top of the other end and fusion crucible substrate 32 joins, the top of fusing earthenware snail substrate 32 is positioned at the centre bore of fusion crucible 7 bottoms, be provided with second thermocouple 3a and the three thermocouple 3b in the last stopper rod 6, the end of the second thermocouple 3a and three thermocouple 3b stretches out outside the top of stopper rod 6, the other end of the second thermocouple 3a is positioned at the middle part of stopper rod 6, and the other end of three thermocouple 3b is positioned at the middle part of the stirring crucible 10 of the II of teeter chamber, the part side that last stopper rod 6 stretches out bell 5 is provided with the first protection gas import 4, fusion crucible substrate 32 lower ends have the first extraordinary high-temperature seal ring 31, an end that is provided with first thermocouple, 2, the first thermocouples 2 in the fusion crucible 7 stretches out outside the bell 5;
The described II of teeter chamber comprises stirring crucible 10, the outside of stirring crucible 10 is provided with teeter chamber's heat-insulation layer 11 successively, first resistance heater 12, insulation layer 13, first cooling water system 14, magnetic stirrer 27 and shell 28, and coaxial teeter chamber's base plate 16 tops that are installed in, by top board 30 together with the above-mentioned parts chucking, two identical vibrating motors 18 and spring 17 are installed in teeter chamber's base plate 16 bottoms symmetrically, the axle head eccentric block direction of rotation of two vibrating motors 18 is opposite, be provided with stopper rod 21 down in stirring crucible 10 bottoms, the top of following stopper rod 21 is provided with the second extraordinary high-temperature seal ring 26, the inside of following stopper rod 21 is provided with the 4th thermocouple 22, first cooling water system 14 is provided with first cooling water inlet 25 and first coolant outlet 29, is provided with the second protection gas import 15 in shell 28 side bottom;
When being used for thixotropic slurry, crystallizer IIIA is installed in teeter chamber's base plate 16 bottoms, crystallizer IIIA comprises the crystallizer copper pipe 20 and second cooling water system 23, crystallizer copper pipe 20 coaxial stirring crucible 10 bottoms that are installed in, the outside of crystallizer copper pipe 20 is provided with second cooling water system, 23, the second cooling water systems 23 and is provided with second cooling water inlet 24 and second coolant outlet 19;
When being used for rheological slurry, rheology conveyer IIIB is installed in teeter chamber's base plate 16 bottoms, rheology conveyer IIIB comprises carrier pipe 33, carrier pipe 33 sides join with transport tube 34 by short swash plate 36, the outside of transport tube 34 is provided with second resistance heater 35, carrier pipe 33 coaxial stirring crucible 10 bottoms that are installed in.
The assemblage gap that has 10~12mm between described molten melting furnace I and the II of teeter chamber.
The material of described first extraordinary high-temperature seal ring 31, the second extraordinary high-temperature seal ring 26 adopts soft corundum.
The material of described fusion crucible substrate 32 is the soft rock China ink.
Operation principle of the present invention is:
With pouring into fusion crucible 7 after the metal material fusing or directly METAL HEATING PROCESS being arrived molten condition, adopt Medium frequency induction system 1 to be incubated soaking; When the metal bath temperature, by controlling down the position of stopper rod 21 in stirring crucible 10, quantitatively is poured into the metal bath realization in the stirring crucible 10 of preheating promptly during 0~30 ℃ of scope at the material liquidus curve; In the metal bath cooling procedure, arrive semi-solid state, according to technology required power and frequency, to semi solid slurry stirring crucible 10 carry out electromagnetic agitation and mechanical oscillation compound, smash and produce the primary dendrite tissue in the cooling procedure, to obtain the tiny spherical or torulose microstructure of axle that waits of non-dendrite; When being used for thixotropic slurry, go out the crystallizer copper pipe 20 that tiny nearly spherical semi-solid melt slurry pours into crystallizer IIIA with prepared, cool off and be frozen into blank, when being used for rheological slurry, go out the transport tube 34 that tiny nearly spherical semi-solid melt slurry pours into rheology conveyer IIIB with prepared, deliver to shaping dies rapidly, carry out rheological molding.
Advantage of the present invention is:
1, adopts control degree of superheat casting, apply touchless electromagnetic agitation and the compound preparation metal semi-solid slurry of vibration simultaneously, metal bath can not polluted, the stirring that needs or oscillation power is little, the time is short, efficient is high, technological parameter is controlled flexibly, applied widely, comprise the thixotropic slurry and the rheological slurry of various ferrous metal and multiple non-ferrous metal;
2, the melting furnace of device of the present invention, teeter chamber and crystallizer are an integral body, and it has good sealing property, thereby the oxidation, the temperature control that reduce the pulp preparation process are convenient, accurate;
3, the stopper rod formula is quantitatively poured into a mould under the employing, and its simple in structure, quantitative cast is accurate, error is little, control is flexible, is specially adapted to rheological molding;
4, adopt the installation of two identical vibrating motor symmetries, but axle head eccentric block direction of rotation is opposite, the horizontal exciting force that two vibrating motors take place is cancelled out each other, and exciting force stack longitudinally, it is simple in structure, small investment, efficient height;
5, adopt the soft corundum sealing ring of extraordinary high temperature, teeter chamber and melting furnace are separated, during its vibration, have only the teeter chamber to be subjected to exciting force, but melting furnace and parts thereof are not subjected to exciting force, and each thermocouple of melting furnace and stability increase, the life-span of control assembly thereof are prolonged.
Description of drawings
Fig. 1 uses the structural representation of crystallizer IIIA for the present invention.
Fig. 2 uses the structural representation of rheology conveyer IIIB for the present invention.
The specific embodiment
The present invention is described in further detail below in conjunction with accompanying drawing.
As Fig. 1, shown in Figure 2, a kind of electromagnetic agitation of ferrous metal semi-solid pulp preparation and vibration set composite, by melting furnace I, the II of teeter chamber, crystallizer IIIA or rheology conveyer IIIB three parts are formed, melting furnace I is installed in II top, teeter chamber, but both independently separate, when purpose is mechanical oscillation, make and have only the II of teeter chamber to be subjected to exciting force, but melting furnace I is depressed, thereby the parts to melting furnace I improve job stability and life-span prolongation, the bottom of the fusion crucible substrate 32 of melting furnace I is stretched in the stirring crucible 10 of the II of teeter chamber, and when being used for thixotropic slurry, crystallizer IIIA is installed in II bottom, teeter chamber; When being used for rheological slurry, rheology conveyer IIIB is installed in II bottom, teeter chamber;
Described melting furnace I comprises the fusion crucible 7 that holds metal bath, and the outside of fusion crucible 7 is provided with melting furnace heat-insulation layer 8, and the outside of melting furnace heat-insulation layer 8 is provided with medium frequency induction heater 1; Fusion crucible 7, melting furnace heat-insulation layer 8 and medium frequency induction heater 1 coaxial melting furnace base plate 9 tops that are installed in, fusion crucible 7 materials are corundum, the top of fusion crucible 7 and melting furnace heat-insulation layer 8 is provided with bell 5, last stopper rod 6 is positioned on the center line of fusion crucible 7, the centre bore that the one end passes bell 5 stretches out outside the bell 5, the top of the other end and fusion crucible substrate 32 joins, the top of fusion crucible substrate 32 is positioned at the centre bore of fusion crucible 7 bottoms, be provided with second thermocouple 3a and the three thermocouple 3b in the last stopper rod 6, stretch out outside the top of stopper rod 6 termination of the second thermocouple 3a and three thermocouple 3b, the other end of the second thermocouple 3a is positioned at the middle part of stopper rod 6, measure the temperature of molten metal in fusion crucible 7, and the other end of three thermocouple 3b is positioned at the middle part of the stirring crucible 10 of the II of teeter chamber, measure the temperature of semi solid slurry in stirring crucible 10, the part side that last stopper rod 6 stretches out bell 5 is provided with the first protection gas import 4, adopt of the oxidation of protection gas prevention metal bath at melting furnace I and the II of teeter chamber, the material of last stopper rod 6 is a corundum, because under hot conditions, corundum is harder, therefore the tightness between fusion crucible 7 and the last stopper rod 6 is relatively poor, reach the tightness that goes up between the stopper rod 6 in order to improve fusion crucible 7, this elects graphite as fusion crucible 7 or last stopper rod 6 materials, under hot conditions, graphite is softer, but it is easy like this to metal bath increase carbide, cause polluting, reduce stock quality, therefore in order to overcome this shortcoming, fusion crucible 7 bottoms are provided with fusion crucible substrate 32, the material of fusion crucible substrate 32 is the soft rock China ink, fusion crucible substrate 32 ends have the first extraordinary high-temperature seal ring 31, be provided with first thermocouple 2 in the fusion crucible 7, one end of first thermocouple 2 stretches out outside the bell 5, the temperature control mode of metal bath in fusion crucible 7 is closed loop, PID control, its thermometric is by first thermocouple 2 and the second thermocouple 3a, because first thermocouple 2 is for a long time at metal bath, destroy easily, shorten its life-span, therefore being provided with this first thermocouple 2 conveniently takes apart, preserve, the frequency of medium frequency induction heater 1 and adjustable power, its frequency are 1000~2500Hz, peak power is 45kW, the heating maximum temperature can reach 1650 ℃;
The described II of teeter chamber comprises the stirring crucible 10 that holds semi solid slurry, the outside of stirring crucible 10 is provided with teeter chamber's heat-insulation layer 11, heat-insulation layer 11 outsides in teeter chamber's are provided with first resistance heater 12, its heating peak power is 7000W, maximum temperature is 1450 ℃, the outside of first resistance heating coil 12 is provided with magnetic stirrer 27, the frequency of magnetic stirrer 27 and adjustable power, its power is 0~10.000W, frequency is 0~500Hz, because the coil of magnetic stirrer 27 can not be subjected to high temperature, generally require below 100 ℃, but being heated maximum temperature, stirring crucible 7 can reach 1450 ℃, and the gap between magnetic stirrer 27 and the stirring crucible 10 can not be too big, influence electromagnetic agitation efficient, therefore need good heat insulation cooling provision between the magnetic stirrer 27 and first resistance heater 12, so be provided with insulation layer 13, the outside of insulation layer 13 is provided with first cooling water system 14, first cooling water system 14 is provided with first cooling water inlet 25 and first coolant outlet 29, the flow of its cooling water can control to adjust, in order to protect the collision of magnetic stirrer 27, be provided with shell 28 in magnetic stirrer 27 outsides, coaxial teeter chamber's base plate 16 tops that are installed in of above-mentioned parts, by top board 30 together with above-mentioned part chucking, two identical vibrating motors 18 are installed in teeter chamber's base plate 16 bottoms with spring 17 symmetries, the axle head eccentric block direction of rotation of two vibrating motors 18 is opposite, when vibrating like this, the horizontal exciting force of generation is cancelled out each other, and the longitudinal force stack, II bottom, teeter chamber is provided with down stopper rod 21, the top of following stopper rod 21 is provided with the second extraordinary high-temperature seal ring 26, the inside of following stopper rod 21 is provided with the 4th thermocouple 22, by controlling down the position of stopper rod 21 in stirring crucible 10, can realize quantitative cast, measure the temperature of metal semi-solid slurry in stirring crucible 10 by three thermocouple 3b and the 4th thermocouple 22, and the 4th thermocouple 22 is gone back the temperature of energy measurement preparation back cooling procedure, first resistance heater, 12 coil methods are molybdenum filament, under hot conditions, the oxidation of molybdenum filament is more serious, therefore in order to protect this molybdenum filament, be provided with the second protection gas import 15 in shell 28 sides;
When being used for thixotropic slurry, crystallizer IIIA is installed in teeter chamber's base plate 16 bottoms, crystallizer IIIA comprises crystallizer copper pipe 20, crystallizer copper pipe 20 outsides are provided with second cooling water system 23, crystallizer copper pipe 20 coaxial stirring crucible 10 bottoms that are installed in, its wall thickness is 6~10mm, internal diameter has 30 '~1 ° little tapering, purpose is that the blank after the cooled and solidified is conveniently taken apart, get material, second cooling water system 23 is provided with second cooling water inlet 24 and second coolant outlet 19, the flow controllable adjustable of second cooling water 23, the flow by controlling second cooling water system 23 and the speed of following stopper rod 21, can control the cooling velocity after semi solid slurry prepares, and this temperature signal measures by the 4th thermocouple 22;
When being used for rheological slurry, rheology conveyer IIIB is installed in teeter chamber's base plate 16 bottoms, rheology conveyer IIIB comprises carrier pipe 33, carrier pipe 33 sides join with transport tube 34 by short swash plate 36, the outside of transport tube 34 is provided with second resistance heater 35, the heating maximum temperature of second resistance heater 35 can reach 800 ℃, carrier pipe 33 coaxial stirring crucible 10 bottoms that are installed in.
The assemblage gap that has 10~12mm between describedization stove I and the II of teeter chamber during vibration, have only the II of teeter chamber to be subjected to violent exciting force, and melting furnace I is depressed, and each thermocouple of raising melting furnace I and control assembly stability, life-span prolong.
The material of described first extraordinary high-temperature seal ring 31, the second extraordinary high-temperature seal ring 26 adopts soft corundum, and this material has good sealing property under hot conditions.
The material of described fusion crucible substrate 32 is the soft rock China ink, under hot conditions, can realize good sealing between fusion crucible substrate 32 and last stopper rod 6 and the fusion crucible 7.
Operation principle of the present invention is:
The deposite metal is poured into pre-warmed fusion crucible 7 or directly METAL HEATING PROCESS arrived molten condition, medium frequency induction heater 1 by adjustable frequency and power is incubated soaking, be incubated equal thermal process and be divided into three phases: tentatively adopt high-power (35~40kW), secondly power (12-15kW) in, last small-power (2-5kW), purpose is for obtaining than the even metal melt; Measure metal bath and pass through first thermocouple 2 and the second thermocouple 3a in the temperature of fusion crucible 7, temperature control mode is closed loop, PID control, equal heat requests: the metal bath temperature is controlled at material liquidus curve (0~30 ℃) scope, and maximum temperature can reach 1650 ℃, accuracy of temperature control ± 2 ℃, equal temperatures ± 5 ℃; In order to reduce the oxidation of metal bath, adopt protection gas by the first protection gas import 4 at fusion crucible 7.
When metal bath reaches required temperature at fusion crucible 7, by controlling down the position of stopper rod 21 in stirring crucible 10, realize quantitatively cast, be specially: following stopper rod 21 up moves on to certain position in stirring crucible 10, form a required space with last stopper rod 6, stirring crucible 10, stop; Go up stopper rod 6 then and up move, metal bath is poured into this space at fusion crucible 7, realize quantitatively cast, go up stopper rod 6 then toward moving down sealing.
Quantitatively after the cast, following stopper rod 21 is toward the coil end position that moves down into magnetic stirrer 27, metal bath is poured into the stirring crucible 10 of preheating, when metal bath in stirring crucible 10 in the cooling procedure, open magnetic stirrer 27 and vibrating motor 18, it is compound to carry out electromagnetic agitation and mechanical oscillation, and purpose is produced the primary dendrite tissue by smashing in the metal bath cooling procedure to semi-solid state, to obtain the tiny spherical or torulose microstructure of axle that waits of non-dendrite; Electromagnetic agitation and time of vibration are 0~360s, and its power and frequency adjustable are specially: electromagnetic agitation power 0~10.000W, frequency 0~600Hz; Power 0~the 10000W of mechanical oscillation, frequency 0~100Hz, amplitude 0~2mm; Stirring crucible 10 preheats mode and adopts first resistance heater 12, and the pre-heating temperature of stirring crucible 10 is less than about 100 ℃ of material liquidus curves, and maximum temperature can reach 1450 ℃.
When being used for thixotropic slurry, crystallizer IIIA is installed in 1I bottom, teeter chamber; Behind the preparation slurry, following stopper rod 21 is toward moving down, and goes out tiny torulose semi solid slurry and pours into crystallizer copper pipe 20 prepared, cools off and is frozen into blank; The flow by controlling second cooling water system 23 and the speed of following stopper rod 21 can be controlled the cooling velocity of metal semi-solid slurry in crystallizer copper pipe 20, and purpose is the semi-solid blank that has obtained good microstructure and mechanical property;
When being used for rheological slurry, rheology conveyer IIIB is installed in II bottom, teeter chamber; Behind the preparation slurry, following stopper rod 21 is delivered to shaping dies rapidly then toward moving down the transport tube 34 that the prepared semi solid slurry that goes out is poured into preheating, carries out rheological molding.
Ferrous metal semi-solid thixotropic slurry that the present invention relates to and rheological slurry preparation, it is applied widely, comprise various high-melting-point ferrous metal and multiple low melting point non-ferrous metal semi solid slurry, outstanding advantage need to be electromagnetic agitation and oscillation power is little, efficient is high, preparation time is short, can prepare tiny semi solid slurry or the blank that waits the spherical or nearly spherical microstructure of axle of non-dendrite, be specially adapted to the metal semi-solid rheological molding.
In the accompanying drawing: I is melting furnace; II is the teeter chamber; IIIA is crystallizer; IIIB is the rheology conveyer; 1 is medium frequency induction heater; 2 is first thermocouple; 3a is second thermocouple; 3b is three thermocouple; 4 is the first protection gas import; 5 is bell; 6 is upper stopper rod; 7 is fusion crucible; 8 is the melting furnace heat-insulation layer; 9 is the melting furnace base plate; 10 is stirring crucible; 11 is teeter chamber's heat-insulation layer; 12 is first resistance heater; 13 is the thermal insulation separation thermosphere; 14 is first cooling system; 15 is the second protection gas import; 16 is teeter chamber's base plate; 17 is spring; 18 is vibrating motor; 19 is second coolant outlet; 20 is crystallizer copper pipe; 21 is lower stopper rod; 22 is the 4th thermocouple; 23 is second cooling water system; 24 is second cooling water inlet; 25 is first cooling water inlet; 26 is the second Special high-temperature sealing ring; 27 is magnetic stirrer; 28 is shell; 29 is first coolant outlet; 30 is top board; 31 is the first Special high-temperature sealing ring; 32 is the fusion crucible substrate; 33 is carrier pipe; 34 is transport tube; 35 is second resistance heater; 36 are short swash plate.

Claims (4)

  1. The electromagnetic agitation of a ferrous metal semi-solid pulp preparation with the vibration set composite, it is characterized in that: form by melting furnace (I), teeter chamber (II), crystallizer (IIIA) or rheology conveyer (IIIB) three parts, melting furnace (I) is installed in top, teeter chamber (II), the bottom of the fusion crucible substrate (32) of melting furnace I is stretched in the stirring crucible (10) of teeter chamber (II), and crystallizer (IIIA) or rheology conveyer (IIIB) are installed in bottom, teeter chamber (II);
    Described melting furnace (I) comprises fusion crucible (7), the outside of fusion crucible (7) is provided with melting furnace heat-insulation layer (8), the outside of melting furnace heat-insulation layer (8) is provided with medium frequency induction heater (1), fusion crucible (7), coaxial melting furnace base plate (9) top that is installed in of melting furnace heat-insulation layer (8) and medium frequency induction heater (1), the top of fusion crucible (7) and melting furnace heat-insulation layer (8) is provided with bell (5), last stopper rod (6) is positioned on the center line of fusion crucible (7), the centre bore that the one end passes bell (5) stretches out outside the bell (5), the top of the other end and fusion crucible substrate (32) joins, the top of fusion crucible substrate (32) is positioned at the centre bore of fusion crucible (7) bottom, be provided with second thermocouple (3a) and three thermocouple (3b) in the last stopper rod (6), one end of second thermocouple (3a) and three thermocouple (3b) stretches out outside the top of stopper rod (6), the other end of second thermocouple (3a) is positioned at the middle part of stopper rod (6), and the other end of three thermocouple (3b) is positioned at the middle part of the stirring crucible (10) of teeter chamber (II), the part side that last stopper rod (6) stretches out bell (5) is provided with the first protection gas import (4), fusion crucible substrate (32) lower end has the first extraordinary high-temperature seal ring (31), be provided with first thermocouple (2) in the fusion crucible (7), an end of first thermocouple (2) stretches out outside the bell (5);
    Described teeter chamber (II) comprises stirring crucible (10), the outside of stirring crucible (10) is provided with teeter chamber's heat-insulation layer (11) successively, first resistance heater (12), insulation layer (13), first cooling water system (14), magnetic stirrer (27) and shell (28), and coaxial teeter chamber's base plate (16) top that is installed in, by top board (30) together with the above-mentioned parts chucking, two identical vibrating motors (18) and spring (17) are installed in teeter chamber's base plate (16) bottom symmetrically, the axle head eccentric block direction of rotation of two vibrating motors (18) is opposite, be provided with stopper rod (21) down in stirring crucible (10) bottom, the top of following stopper rod (21) is provided with the second extraordinary high-temperature seal ring (26), the inside of following stopper rod (21) is provided with the 4th thermocouple (22), first cooling water system (14) is provided with first cooling water inlet (25) and first coolant outlet (29), is provided with the second protection gas import (15) in shell (28) side bottom;
    When being used for thixotropic slurry, crystallizer (IIIA) is installed in teeter chamber's base plate (16) bottom, crystallizer (IIIA) comprises crystallizer copper pipe (20) and second cooling water system (23), coaxial stirring crucible (10) bottom that is installed in of crystallizer copper pipe (20), the outside of crystallizer copper pipe (20) is provided with second cooling water system (23), and second cooling water system (23) is provided with second cooling water inlet (24) and second coolant outlet (19);
    When being used for rheological slurry, rheology conveyer (IIIB) is installed in teeter chamber's base plate (16) bottom, rheology conveyer (IIIB) comprises carrier pipe (33), carrier pipe (33) side joins by short swash plate (36) and transport tube (34), the outside of transport tube (34) is provided with second resistance heater (35), coaxial stirring crucible (10) bottom that is installed in of carrier pipe (33).
  2. 2. the electromagnetic agitation of a kind of ferrous metal semi-solid pulp preparation according to claim 1 and vibration set composite is characterized in that: the assemblage gap that has 10~12mm between described molten melting furnace (I) and teeter chamber (II).
  3. 3. the electromagnetic agitation of a kind of ferrous metal semi-solid pulp preparation according to claim 1 and vibration set composite, it is characterized in that: the material of the described first extraordinary high-temperature seal ring (31), the second extraordinary high-temperature seal ring (26) adopts soft corundum.
  4. 4. the electromagnetic agitation of a kind of ferrous metal semi-solid pulp preparation according to claim 1 and vibration set composite, it is characterized in that: the material of described fusion crucible substrate (32) is the soft rock China ink.
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CN102288028A (en) * 2011-08-03 2011-12-21 马忠臣 Medium frequency induction heating smelting device based on combination of electromagnetic stirring and mechanical vibration
CN102650499A (en) * 2012-05-14 2012-08-29 矽明科技股份有限公司 Material taking device of high temperature reaction furnace
CN103170606A (en) * 2011-12-23 2013-06-26 北京有色金属研究总院 Device for manufacturing metal paste in double forcing and homogenizing mode and machining forming method thereof
CN103341612A (en) * 2013-07-16 2013-10-09 北京科技大学 Swing stirring device for preparing semisolid slurry and rheoforming equipment
CN103411440A (en) * 2013-06-20 2013-11-27 宁波长振铜业有限公司 Method for mashing materials in copper liquid and stirring copper liquid
CN103658565A (en) * 2013-11-13 2014-03-26 慈溪市汇丽机电有限公司 Method and special equipment for manufacturing semi-solid metal slurry in low superheat degree permanent magnet stirring mode
CN103862003A (en) * 2014-02-25 2014-06-18 西安交通大学 Triple screw stirring vibrating device for preparing semi-solid billets
CN104275478A (en) * 2013-07-11 2015-01-14 科卢斯博知识产权有限公司 Manifold collar for disstributing fluid through a cold crucible
CN104561852A (en) * 2014-12-26 2015-04-29 西安交通大学 Process for preparing semi-solid state aluminum alloy scroll plate by radial forging strain induction method
CN107388823A (en) * 2017-07-07 2017-11-24 西安交通大学 A kind of Multipurpose electric magnetic induction smelting apparatus and method
CN107983929A (en) * 2018-01-05 2018-05-04 北京科技大学 A kind of heating furnace cobalt alloy cushion block semi-solid die casting process
CN108356248A (en) * 2018-02-28 2018-08-03 江苏大学 A kind of boron-containing high speed steel roller roller set electromagnetic agitation vibration composite casting method
CN109759555A (en) * 2019-01-28 2019-05-17 深圳市银宝山新压铸科技有限公司 A kind of method that Composite Field prepares semi solid slurry
CN109967716A (en) * 2019-03-13 2019-07-05 西安交通大学 A kind of composite-making process and equipment of semi-solid metal slurry
CN110153387A (en) * 2019-06-20 2019-08-23 西安建筑科技大学 A kind of rotational symmetry vibrating machine agitating device being used to prepare semi-solid blank
CN111195731A (en) * 2020-01-10 2020-05-26 上海电气集团股份有限公司 Bottom hole type crucible induction melting gas atomization powder making device and method
CN111826535A (en) * 2020-06-04 2020-10-27 浙大宁波理工学院 Forming system based on low-melting-point alloy semi-solid melt
CN112361810A (en) * 2020-10-23 2021-02-12 广东顺博铝合金有限公司 Refining tank for aluminum ingot production
CN112404371A (en) * 2020-11-19 2021-02-26 西安交通大学 Aluminum alloy wheel hub semisolid rheoforming slurry preparation and transfer device
CN112404391A (en) * 2020-11-19 2021-02-26 西安交通大学 Device and method for preparing particle reinforced metal matrix composite material by semi-solid rheoforming
CN112404390A (en) * 2020-11-19 2021-02-26 西安交通大学 Device and method for preparing semi-solid rheoforming slurry and quantitatively transferring
CN112605349A (en) * 2020-12-08 2021-04-06 安徽中鑫精密铸造科技有限公司 Semi-solid forming process for water-cooling plate for bearing automobile chip
CN113059144A (en) * 2021-05-10 2021-07-02 江苏海宇机械有限公司 Device and method for preparing metal solid-liquid mixture
CN113069971A (en) * 2021-03-31 2021-07-06 南方科技大学 Preparation device and preparation method of metal semi-solid slurry
CN117259713A (en) * 2023-11-23 2023-12-22 龙口市龙蓬精密铜管有限公司 Semi-solid forming device for copper alloy pipe fitting

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CN102288028A (en) * 2011-08-03 2011-12-21 马忠臣 Medium frequency induction heating smelting device based on combination of electromagnetic stirring and mechanical vibration
CN103170606A (en) * 2011-12-23 2013-06-26 北京有色金属研究总院 Device for manufacturing metal paste in double forcing and homogenizing mode and machining forming method thereof
CN102650499A (en) * 2012-05-14 2012-08-29 矽明科技股份有限公司 Material taking device of high temperature reaction furnace
CN103411440A (en) * 2013-06-20 2013-11-27 宁波长振铜业有限公司 Method for mashing materials in copper liquid and stirring copper liquid
CN104275478A (en) * 2013-07-11 2015-01-14 科卢斯博知识产权有限公司 Manifold collar for disstributing fluid through a cold crucible
CN104275478B (en) * 2013-07-11 2019-05-21 科卢斯博知识产权有限公司 For distributing the manifold lantern ring of fluid by cold crucible
CN110170640A (en) * 2013-07-11 2019-08-27 科卢斯博知识产权有限公司 For distributing the manifold lantern ring of fluid by cold crucible
CN103341612B (en) * 2013-07-16 2015-01-07 北京科技大学 Swing stirring device for preparing semisolid slurry and rheoforming equipment
CN103341612A (en) * 2013-07-16 2013-10-09 北京科技大学 Swing stirring device for preparing semisolid slurry and rheoforming equipment
CN103658565A (en) * 2013-11-13 2014-03-26 慈溪市汇丽机电有限公司 Method and special equipment for manufacturing semi-solid metal slurry in low superheat degree permanent magnet stirring mode
CN103862003A (en) * 2014-02-25 2014-06-18 西安交通大学 Triple screw stirring vibrating device for preparing semi-solid billets
CN103862003B (en) * 2014-02-25 2015-07-08 西安交通大学 Triple screw stirring vibrating device for preparing semi-solid billets
CN104561852A (en) * 2014-12-26 2015-04-29 西安交通大学 Process for preparing semi-solid state aluminum alloy scroll plate by radial forging strain induction method
CN104561852B (en) * 2014-12-26 2016-06-29 西安交通大学 The technique that radial forging strain-induced method prepares semi-solid aluminium alloy scroll plate
CN107388823A (en) * 2017-07-07 2017-11-24 西安交通大学 A kind of Multipurpose electric magnetic induction smelting apparatus and method
CN107983929A (en) * 2018-01-05 2018-05-04 北京科技大学 A kind of heating furnace cobalt alloy cushion block semi-solid die casting process
CN108356248A (en) * 2018-02-28 2018-08-03 江苏大学 A kind of boron-containing high speed steel roller roller set electromagnetic agitation vibration composite casting method
CN109759555A (en) * 2019-01-28 2019-05-17 深圳市银宝山新压铸科技有限公司 A kind of method that Composite Field prepares semi solid slurry
CN109967716A (en) * 2019-03-13 2019-07-05 西安交通大学 A kind of composite-making process and equipment of semi-solid metal slurry
CN110153387A (en) * 2019-06-20 2019-08-23 西安建筑科技大学 A kind of rotational symmetry vibrating machine agitating device being used to prepare semi-solid blank
CN111195731A (en) * 2020-01-10 2020-05-26 上海电气集团股份有限公司 Bottom hole type crucible induction melting gas atomization powder making device and method
CN111826535A (en) * 2020-06-04 2020-10-27 浙大宁波理工学院 Forming system based on low-melting-point alloy semi-solid melt
CN112361810A (en) * 2020-10-23 2021-02-12 广东顺博铝合金有限公司 Refining tank for aluminum ingot production
CN112404371A (en) * 2020-11-19 2021-02-26 西安交通大学 Aluminum alloy wheel hub semisolid rheoforming slurry preparation and transfer device
CN112404391A (en) * 2020-11-19 2021-02-26 西安交通大学 Device and method for preparing particle reinforced metal matrix composite material by semi-solid rheoforming
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CN112605349A (en) * 2020-12-08 2021-04-06 安徽中鑫精密铸造科技有限公司 Semi-solid forming process for water-cooling plate for bearing automobile chip
CN113069971A (en) * 2021-03-31 2021-07-06 南方科技大学 Preparation device and preparation method of metal semi-solid slurry
CN113059144A (en) * 2021-05-10 2021-07-02 江苏海宇机械有限公司 Device and method for preparing metal solid-liquid mixture
CN117259713A (en) * 2023-11-23 2023-12-22 龙口市龙蓬精密铜管有限公司 Semi-solid forming device for copper alloy pipe fitting
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