CN102038721A - Pinus extract and application thereof - Google Patents

Pinus extract and application thereof Download PDF

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CN102038721A
CN102038721A CN2009101536833A CN200910153683A CN102038721A CN 102038721 A CN102038721 A CN 102038721A CN 2009101536833 A CN2009101536833 A CN 2009101536833A CN 200910153683 A CN200910153683 A CN 200910153683A CN 102038721 A CN102038721 A CN 102038721A
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pinaster
extracting solution
pinus
medicine
application
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CN102038721B (en
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吴江平
秦云飞
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Abstract

The invention provides a pinus extract and application thereof. The pinus extract is prepared by a method comprising the following steps of: burning pinus plant fragments; condensing and recycling exhausted gas to obtain coarse liquid; standing the coarse liquid in a closed container for three to five months; removing an upper layer of oily matter and a lower layer of sedimentation; taking a middle layer of liquid to distill; taking distillate of fractions at 98 DEG C to 103 DEG C; absorbing by active carbon, filtering by filter paper (for filtering more than once); and taking filtrate to obtain the pinus extract. The invention provides the pinus extract with multiple medical effects. The pinus extract has a certain treating effect on various diseases, has good effect particularly on human epidermal injury, has assistant treating functions on 00 AIDS and unexpected infectious diseases, and provides a basis for screening out new medicaments.

Description

A kind of pinaster extracting solution and application thereof
(1) technical field
The present invention relates to a kind of pinaster extracting solution and application thereof, be specially its application in the medicine of preparation treatment epidermis injury of person (comprise scald, burn is burnt, wound, infectious suppuration or comedo etc.) and other diseases.
(2) background technology
Pinaster (Pinus) is the general designation of Pinaceae pine genus plant, evergreen needle arbor, hermaphroditism.The pinaster whole body is precious, and trunk is the extremely wide timber of purposes, also is fine paper making raw material, and the fat liquid of pinaster can be made Colophonium, Oleum Terebinthinae.Folium Pini not only has medical value to be used to prevent and treat hypertension, coronary heart disease, diabetes, apoplexy, senile dementia, and the health care effect arranged, contain rich in amino acid in the Folium Pini, multiple fat-soluble and water soluble vitamins, more than 40 kind of macroelement and various trace elements and crude fibre, can develop multiple enhance immunity, hair growth promoting, blood fat reducing, calm the nerves, classification health food, beverage and drinks such as slow down aging also can be developed skin care item, shampoo product, scouring bath product, article of everyday use such as the pillow of sleeping peacefully.
Kind surplus global pine genus plant has 80.In state-owned 22 kind of 10 mutation, belong to 4 groups of two subgenus, be the five-leaved pine group, comprise Pinus koraiensis, Siberian cedar, siberian dwarf pine, Pinus armandi Franch-P. Komavovii Lavl., pinus fenzeliana var dabeshanensis (P.dabeshanensis), Hainan five-leaved pine (P.fenzeliana), Taiwan five-leaved pine, Himalayan pine (P.griffithii), pinus kwangtungensis (P.kwangtungensis) and wangs pine (P.wangii); The lacebark pine group comprises lacebark pine and Tibet lacebark pine (P.gerardiana); The longleaf pine group comprises Tibet longleaf pine (P.roxbourghii); The Pinus tabuliformis group comprises Pinus densiflora, takahas pinus (P.takahasii), Bashan Mountain pine (P.henryi), Pinus sylvestnis var. mongolica Litv., high illawarra mountain pine, changpai scotch pine, Pinus tabuliformis, Pinus massoniana Lamb, pinus finlaysoniana, Pinus taiwanesis, pinus yunnanensis faranch and Pinus kesiya Royle ex Gordon var. langbianensis (A.Chev) Gaussen (P.kesiyavar.langbianensis) etc.
Pinus koraiensis (Pinus koraiensis Sieb.et Zucc.), another name korean pine, Pinaceae, Pinus is famous and precious rare seeds, be distributed in the Xiaoxinanlin Mountains, Changbai Mountain one band in northeast in China, be distributed in Japan abroad, Korea, Muscovite part, the zone, Pinus koraiensis is evergreen needle arbor, seedling bark ash bronzing, sulci of skin is not dark, and is near level and smooth, the squamous cracking, the shallow colour of camel's hair of endothelium, the crack is bronzing, often branch in big trunk top, heart sapwood is distinguished obviously, the shallow colour of camel's hair band of sapwood HUANGBAI(sic), common epidermis, the heartwood yellowish-brown is little be with flesh-coloured, so the name of Pinus koraiensis is arranged, branch is closely open and flat, tree crown taper shape, the light red brown of hibernaculum, cylindric avette, needle 5 pins are a branch of, long 6~12cm, thick and stiff, 3 of resins, sheath is caducous, the cone cone shape, avette, long 9~14cm, footpath 6~8cm seed is big, and son is edible, the shape of falling ovum triangular shape, June at florescence, cone 9-10 in next year month maturation, this seeds happiness photosensitiveness is strong, in the growth of area, soil ph value 5.5~6.5 hillside, ecological habit is weak positive, likes cool moist climate and acid soil.
Pollen pini thunbergii (Pinus thunbergii Parl.) is called white bud pine, Pinaceae, Pinus, be distributed in China Shandong, Jiangsu, Anhui, Zhejiang, coastal all provinces such as Fujian, aiphyllium, 30 meters of Gao Keda, the bark grey black, 2 needles are grown thickly, firm and thick, sprouting white, various leaves are about 6-15cm, the section semicircle has 3 pitch tubes in the mesophyll, sheath is formed by more than 20 scales, be about 1.2cm, bloom April, spends list, female flower is born in the sprouting top, is purple, and most fruit scale carpels are heavy mutually and line up sphere, each plants base portion, 2 blastocytes of naked life, and male flower is born in the base portion of sprouting, be yellow, the last majority of giving birth to is male, when ripe, most pollen are blown out with the wind, cone became in autumn in next year, and scale splits and the seed that sheds, and seed has thin wing.Happiness light, drought-resistant ridge is thin, not water-fast waterlogging is cold-resistant, suitablely is born in wet dim moistening marine climate zone, the most suitable deep at soil layer, the soil is porous, and contain detritus, the growth of sandy soil place.Because of its anti-sea fog, anti-Caulis Piperis Kadsurae also can be grown seabeach solonchak landlord.Diseases and insect pests resistance is strong, and growth is slow, and the life-span is long.
Japanese black pine (Pinus thubergii), Pinaceae, Pinus, Coastal Area in Eastern China area, broad leaved and deciduous broad leaved forest zone, northern warm temperate zone, warm band broad leaved and deciduous broad leaved forest zone, south, the north subtropical fallen leaves, all there is distribution in evergreen broad-leaved mixed forest district.Height can reach: 30~40 meters, tree crown is extensively avette, dried bark grey black color, hibernaculum canescence.Needle 2 pins 1 bundle, thick and stiff, long 6~12 centimetres, bottle green, normal microbend is given birth in the resin canal.Habit: strong positive, anti-tide wind, the beach of should growing, salt tolerant alkali.Be the warm temperate zone intolerant tree species.Suitable be born in 20 ℃ of year sammings and be not less than~10 ℃ low mountain, hills and footslope, seabeach neutrality less and all can grow on the little alkaline earth below the pH8.0.At ground moistening, fertile and to contain on the sand of humus growth best.
Pinus tabuliformis (Pinus tabulaeformis Carr.), another name Folium Styracis Suberifoliae pine, jack pine, Pinaceae, Pinus have a very wide distribution, ground such as Liaoning, Jilin, the Inner Mongol, Hebei, Henan, Shanxi, Shaanxi, Shandong, Gansu, Ningxia, Qinghai, the north, Sichuan.Also there is distribution in Korea.Arbor highly reaches 25m, and about 1m is surplus for the diameter of a cross-section of a tree trunk 1.3 meters above the ground; Tree crown is turriform or extensively avette the postadolescence, and the geratic period is the plate-like umbrella shape.The bark taupe brown is the flakey cracking, the crack bronzing.Last branch is sturdy, does not have hair, and is isabelline; The hibernaculum circle, the end point, rufous is at other normal verticillate 3~5 lateral buds that have of terminal bud.Leaf 2 pins 1 bundle, rare 3 pins, 1 bundle, long 10~15cm, resin canal 5~8 or more, give birth on the limit; Deposit the sheath place.Male cone is orange-yellow, the green purple of female cone.The fruit scale top of conelet has perversely then, and cone is avette, long 4-9cm.Stockless or extremely short tenon is arranged, but on the Su Cunzhi for the several years; The squama back of the body of fruit scale is plump, and transverse ridge is remarkable, and the squama umbilicus has perverse.Seed is avette, long 6~8mm.Filbert dapple; Wing is about 1cm, and the HUANGBAI(sic) ghost has the brown striped.Cotyledon 8~12.4~May of florescence; Fruit maturation in October next year.Positive seeds, deep-rootedness, happiness light, anti-barren, wind resistance, but in the time of-25 ℃ normal growth still.There is growth at height above sea level 1400 meters in Mount Taishan.Folium Pini, Lignum Pini Nodi are that Chinese medicine " Variorum of Shennong ", " the positive allusion quotation of mongolian medicine " are all on the books.
Pinus sylvestnis var. mongolica Litv. (Pinus sylvestris var.mongolica Litv.) has another name called Hailaer pine (day), Mongolian Pinus densiflora (day), cembra pine, Heihe Pinus densiflora, is the Pinaceae megaphanerophyte.Pinus sylvestnis var. mongolica Litv. is good reproducting tree species, and trunk is perfectly straight, and growth is rapid, and adaptability is strong.Aiphyllium, 15~30 meters of the height of trees, about 1 meter of the diameter of a cross-section of a tree trunk 1.3 meters above the ground.Bark from old tress is thicker lobe, pitchy, and normal flakey cracking: trunk top bark is very thin, and isabelline or faint yellow, thin skin comes off.Wheel branch is obviously whenever taken turns 5~12, mostly is 7~9,20 years before death bough tiltedly go up or be open and flat, annotinous branch is faint yellow, becomes taupe behind the 2-3, the bough base portion is identical with the color of the leather on trunk top.Cylindric ellipse of bud or oval ovum shape do not wait, and be most advanced and sophisticated blunt or sharp, yellowish-brown or pale brown color, and there is resin on the surface.Leaf two pins are a branch of.5~mid-June of florescence belongs to anemophilous flower, and female flower is born in the shoot tip, and male flower is born in the shoot bottom.Living conelet was sagging in 1 year, green, 9~October of next year maturation, cone is long avette, yellow green or lark; The 3rd year spring cone cracking, the squama umbilicus is little, and the excipuliform projection has short thorn, easily comes off, and gives birth to two pieces of seeds on every scale, and seed wing is 3~5 double-lengths of seed, and seed size does not wait, and is avette, pitchy, grey black, black do not wait.Mainly be distributed in the north, Daxing'an Mountainrange (to the north of 50 ° of the north latitude) of China, from More road dagger-axe, Jin He, root river, there is continuously distribution in flakes in east to new woods, to the north of the line of Huma, and there is natural Pinus sylvestnis var. mongolica Litv. woods on the Hulunbeir League grassland.Hebei, the Yulin, the Inner Mongol, all introduce a fine variety on ground such as Xinjiang.
(Picea jezoen s-sCalx.), is a Pinaceae Picea aiphyllium to fish-scale floss, another name fish scale PiceameyeriRehd. Et Wils., kahikatea, long white fish-scale floss, be distributed in Daxing'an Mountainrange, China northeast, the Xiaoxinanlin Mountains, Changbai Mountain, height above sea level 300~2000 meter bands, with the fir Pinus koraiensis, color wood, mixed living trunk such as wood is tall and big satisfactorily perfectly straight, up to 40m, about the thick 1m of the diameter of a cross-section of a tree trunk 1.3 meters above the ground, bough is open and flat, and tip is sagging slightly, on the bottom branch is oblique, be conical tree crown, the bark crineous is taupe when old, the squamous breakaway, the cylindrical or Long Circle of cone, long 4~6cm,, the black seed is avette, long 2.4~3.0cm, the wing ellipse is about the wide 3mm of 9mm, the fruit 9~October of phase, feminine tree, shallow root, it is deep, moistening that soil layer is born in happiness, on the fertile well-drained subacidity forest soil, anti-low humidity, severe cold is that furniture construction is mainly used material.Leaf, bark have the medical value record.Do not see that at present having pinaster to be applied to preparation treatment epidermis injury of person (comprises scald, burn, burn, wound, the infectious suppuration or comedo etc.) report medicine and that end the addiction medicine in the preparation drug rehabilitation, treat vasculitic medicine, use in the medicine of the application in the medicine of the medicine of the medicine of the medicine of the medicine of treatment brain diseases, treatment respiratory tract disease, treatment kidney disease, treatment gastric disease, treatment intestinal tract disease, treatment excretory system disease.
(3) summary of the invention
The object of the invention provides a kind of pinaster extracting solution and application thereof, especially it (comprises scald, burns, burn at preparation treatment epidermis injury of person, wound, the infectious suppuration or comedo etc.) and many-sided application such as the treatment drug rehabilitation ends addiction, treats vasculitic medicine, treatment brain diseases.
The technical solution used in the present invention is:
A kind of pinaster extracting solution is prepared by following method: burning pinaster (Pinus) phytoclasts, and expellant gas reclaims through condensation and obtains thick liquid; Thick liquid left standstill in hermetic container 3 months~5 years, removed upper strata grease and lower sediment, got middle level liquid distillation, get the distillate of 98~103 ℃ of fractions, through activated carbon adsorption, filter paper filtering (more than filtering once), get filtrate, promptly get described pinaster extracting solution.This extracting solution is a water white transparency, deposits long afterwards, or after the sunlight direct projection,, but does not affect the treatment to yellowish-brown for light yellow, has the pungent smoked smell of burning, and extracting solution includes aminoacid, organic acid, alcohols, phenols, bases etc. more than hundred kinds organic chemicals become to be grouped into.
Burning pinaster (Pinus) phytoclasts pinaster (Pinus) phytoclasts that can directly burn is collected flue gas at the QI KOU place, and imports the condensing plant condensation and reclaim, and obtains pinaster Chinese medicine crude extract.
Be further to improve drug effect and extracting solution productive rate, described burning pinaster phytoclasts is meant phytoclasts is placed the airtight container that closes, and burns with the burning things which may cause a fire disaster that adds of container.
Concrete, described method is as follows: the pinaster phytoclasts is placed hermetic container, with outside burning things which may cause a fire disaster hermetic container is heated to carbonization, expellant gas reclaims through condensation and obtains thick liquid, and thick liquid left standstill in hermetic container 3 months~5 years, remove upper strata grease and lower sediment, get middle level liquid distillation, get the distillate of 98~103 ℃ of fractions, through activated carbon adsorption, filter paper filtering, get filtrate, promptly get described pinaster extracting solution.Black remaining in the liquid still-process container of middle level glues shape liquid, and is approaching with described pinaster extracting solution composition, also is applied to the auxiliary treatment of corresponding disease as cream side.
Described burning can adopt special equipment to carry out, and described equipment comprises: the airtight carbonization chamber of calcining pinaster phytoclasts, and the collection chamber of the flue gas that collection pinaster phytoclasts forms when carbonization, described carbonization chamber below is provided with the combustion furnace; The inner chamber of described carbonization chamber communicates with described collection chamber inner chamber by airway, described airway can be provided with a plurality of, be evenly arranged in the described collection chamber inner chamber, common described airway extend into collection chamber height 1/3 place, to prevent that liquid from pouring in down a chimney to carbonization chamber, described collection chamber top is provided with and the airtight lid that is connected of described collection chamber, described lid is the cooling back installation that is provided with cooling water inlet A and coolant outlet A, it is the cooling pan of liquid that the periphery of described collection chamber is provided with the flue gas condensing in the described collection chamber, described cooling pan is provided with cooling water inlet B and coolant outlet B, described collection chamber is arranged in the cooling pan, the bottom of described collection chamber is provided with the sharp mouth shape liquid outlet that thick liquid is discharged, and the bottom that described liquid outlet passes cooling pan communicates with atmosphere.Around the collection chamber and top is provided with cooling device, more helps the condensation of flue gas, and it is divided into two parts, can be convenient to dismounting, clean.Liquid outlet of the present invention is sharp mouth shape, and certain length is arranged, mainly be to guarantee that thick liquid that flue gas condensing becomes can form the liquid sealing of certain altitude at sharp mouth shape liquid outlet place, one side can guarantee collection chamber and atmospheric sealing like this, can make on the other hand to condense into thick liquid and flow out fast.
Recommend described collection chamber to be annular, described liquid outlet can be provided with a plurality of, be evenly arranged in described annular gas-collecting chamber bottom, the bottom center arch of described collection chamber is bell jar shape projection to increase the heat exchange area of described collection chamber and cooling water, accelerates the condensation rate of flue gas.
During concrete operations, to put into carbonization chamber through the pinaster phytoclasts that soaks into earlier, arrange airway, make it to stretch into staving and collection chamber, the snap ring of hold-down mechanism is cooperated with the shelves part, the height of adjusting nut compresses bung and staving, and cooperates lid and collection chamber are airtight, open the cooling water of cooling pan and chiller, light the combustion furnace, the pinaster phytoclasts in the staving carbonization chamber is fired to carbonization, the flue gas that carbonization is produced imports in the collection chamber, under the effect of chiller, flue gas in the collection chamber formation medicinal liquid that is condensed is discharged by liquid outlet, the convenient collection.
Described pinaster phytoclasts is from one of following or wherein two or more mixing: leaves, branch, bark, trunk, tree root, flower, cone.According to the inventive method, when the phytoclasts of getting each different parts was raw material, its extract was formed roughly the same, and just output is slightly had any different, and be that the tree root extraction efficiency is the highest strictly speaking, but the tree root amount very little, therefore generally got full tree burning and got final product.
Pinaster can be taken the common kind of Pinaceae Pinus, and pinaster described in the present invention is preferably one of following or wherein two or more mixing: Pinus koraiensis, fish-scale floss, Pollen pini thunbergii, japanese black pine, Pinus tabuliformis, Pinus sylvestnis var. mongolica Litv..
The application of described pinaster extracting solution in the medicine of preparation treatment epidermis injury of person.Described epidermis injury is for scalding, and burn is burnt, wound (comprise wound, hurt, wound, animal bite etc.), the infectious suppuration or comedo.Described pinaster extracting solution can directly be smeared or with behind the distilled water diluting several times, be applied in people's epidermis affected part, can add also that other are medicinal as adjuvant to, makes the treatment that unguentum, spray are used for human epidermal damage location and other affected part, position.The pinaster extracting solution also can directly or dilute several times pharynx clothes, directly or indirectly acts on focus, plays therapeutical effect.
Described pinaster extracting solution has extremely strong infiltration bactericidal effect, and is remarkable to staphylococcus, escherichia coli, anthrax bacillus, sick frog isolate killing action, and the sterilization effective percentage can be used for preparing antibacterial all more than 99.999%.
Described pinaster extracting solution also has resurrection, repair cell ability, and the nutrition base of blocking virus can be used for preparing the medicine that promotes that cell brings back to life, and has the auxiliary treatment effect for acquired immune deficiency syndrome (AIDS) and sudden infectious disease.Pathogenesis is the succession acquired immunodeficiency syndrome, and immunodeficiency virus infection causes, immunodeficiency companion's opportunistic infection and supervention tumor.On the acquired immune deficiency syndrome (AIDS) pathogenesis, if how to stop HIV to CD 4 +The T cytosis, degree with pinaster extracting solution treatment disease is observed, the pinaster extracting solution has extremely strong infiltration sterilizing ability, can effectively kill or suppress HIV virus, the pinaster extracting solution has extremely strong promotion human body beneficial cell resurrection ability simultaneously, useful cell can improve immunocompetence greatly, and acquired immune deficiency syndrome (AIDS), sudden communicate illness patient are because the accumulation of free radical damages cell.If new extraction method and pinaster extracting solution in conjunction with Chinese medicine share, become a kind of radical scavenger surely at HIV (human immunodeficiency virus) (Human Immunodeficiency Virus), utilize radical scavenger treatment acquired immune deficiency syndrome (AIDS) can receive certain effect.Logical in a few years grope to observe and the combining of five elements balancing theory, progressively grasped the preparation of some effective Therapeutic Method and medicine, pinaster extracting solution advantage not only is effective sterilizing ability, also have resurrection, repair cell ability simultaneously, the nutrition base of blocking virus, this point can tentatively be proved on Fish and plant experimental.
Described pinaster extracting solution also has drug rehabilitation and ends the addiction effect, can be used for the preparation drug rehabilitation and ends the addiction ancillary drug.
Experiment is found, pine extract of the present invention is low to vasculitis, otitis media, esophagitis, esophageal carcinoma, pharyngolaryngitis, gastritis, gastric ulcer, gastric cancer, enteritis, diarrhea, constipation, hemorrhoid, hepatitis B, cirrhotic ascites, hepatocarcinoma, nephritis, renal carcinoma, asthma, hydrothorax, pulmonary carcinoma, diabetes, apoplexy, arteriosclerosis, hypertension, hyperlipidemia, amnesia, senile dementia, prostatitis, alopecia hair growth promoting, immunity function, sub-health population, relieve the effect of alcohol, sober up etc., and certain curative effect is also arranged.
Beneficial effect of the present invention is mainly reflected in: the invention provides a kind of pinaster extracting solution with multiple drug effect, especially epidermis injury of person there is specially good effect, described pinaster extracting solution also has extremely strong infiltration sterilization, antiinflammation, and cell brings back to life function, acquired immune deficiency syndrome (AIDS) and sudden infectious disease had the auxiliary treatment effect, for new medicament screen provides the foundation.
(4) description of drawings
Fig. 1 is condensing unit figure of the present invention;
Fig. 2 is a medicinal liquid extraction element cutaway view of the present invention.
(5) specific embodiment
The present invention is described further below in conjunction with specific embodiment, but protection scope of the present invention is not limited in this:
Embodiment 1: the preparation of pinaster extracting solution
(1) with brick 6 kiln body, kiln body bottom is provided with feeding gate, the top is provided with the gas outlet, put into Pinus koraiensis (Pinus koraiensis Sieb.et Zucc.) respectively, Pollen pini thunbergii (Pinus thunbergii Parl.), japanese black pine (Pinusthubergii), Pinus tabuliformis (Pinus tabulaeformis Carr.), Pinus sylvestnis var. mongolica Litv. (Pinus sylvestris var.mongolica Litv.), fish-scale floss (Picea jezoen, s-sCalx.) full tree, seal up a door, stay gas port, the igniting calcining, after wet gas (wherein major part is a steam) discharge, load onto condensing plant at the QI KOU place and reclaim, obtain crude extract; Described condensing plant is as shown in Figure 1:
Described condensing plant comprises: smoke inlet 13, the surge chamber 10 of flue gas circulation, the collection chamber 2 of the flue gas that collection pinaster phytoclasts forms when carbonization; The inner chamber of described surge chamber communicates with described collection chamber inner chamber by airway 3, described airway is provided with 6, be evenly arranged in the described collection chamber inner chamber, described airway extend into 1/3rd places of collection chamber height, described collection chamber top is provided with and the airtight lid that is connected of described collection chamber, described lid is the cooling back installation 41 that is provided with cooling water inlet 51 and coolant outlet 61, it is the cooling pan 42 of liquid that the periphery of described collection chamber is provided with the flue gas condensing in the described collection chamber, described cooling pan is provided with cooling water inlet 52 and coolant outlet 62, and described collection chamber is arranged in the cooling pan.Described collection chamber is an annular, and the bottom center arch of described collection chamber is bell jar shape projection to increase the heat exchange area of described collection chamber and cooling water, accelerates the condensation rate of flue gas.The bottom of described collection chamber is provided with the sharp mouth shape liquid outlet 21 that thick liquid is discharged, and sharp mouth shape liquid outlet is provided with 4, is evenly distributed on annular collection chamber bottom, and described liquid outlet communicates with atmosphere.
The gap is left in described bell jar shape rising height and described lid bottom.
The part that described lid and collection chamber interlock is down the pot type, and described pot type the bottom of a pan part 411 forms the top cover of described collection chamber 2, and the sidewall 22 of described lid and described collection chamber 2 is tightly connected.Contacted of lid and collection chamber are smooth, use the screw bolt tight on every side, the bell jar shape rising height of described collection chamber is concordant with the height of the coolant outlet 62 of cooling pan, can make flue gas and cooling water in the collection chamber that bigger contact area is arranged like this, makes the flue gas rapid condensation become thick liquid.
Described cooling water inlet 51 is arranged on described lid bottom, described coolant outlet 52 is arranged on described lid top, described cooling water inlet 61 is arranged on described cooling pan bottom, and described coolant outlet 62 is arranged on described cooling pan top.
The gas of being derived by the kiln body enters surge chamber through smoke inlet 13, through the condensing plant condensation, obtains extracting solution by sharp mouth shape liquid outlet 21 collections.
(2) be sub-packed in the pollution-free closed container after crude extract is collected, put into shady place, avoid the sunlight direct projection about 3 months, allow its hydrolysis voluntarily, produce acid, the good liquid of acid is produced in hydrolysis remove upper strata grease, get middle part liquid, discard the precipitation part, stock solution.
(3) stock solution is got the distillate of 98 ℃~103 ℃ of fractions through distillation, and residue black thick liquid is called the extraction waste liquid in the still-process, also has certain therapeutic effect, can retain as adjuvant drug; Distillate was through activated carbon adsorption decolouring about 3 hours, and concussion is with material and impurity such as filter paper filtering active carbons, gained filtrate is described pinaster and extracts medicinal liquid (water white transparency is deposited long afterwards, or after the sunlight direct projection, for light yellow to yellowish-brown, but do not affect the treatment, have the pungent smoked smell of burning, extracting solution includes aminoacid, organic acid, alcohols, phenols, bases etc. more than hundred kinds organic chemicals become to be grouped into).
Embodiment 2: the preparation of pinaster extracting solution
Adopt Fig. 2 device to carry out the preparation of pinaster extracting solution.Described equipment comprises: the airtight carbonization chamber 1 of calcining pinaster phytoclasts, and the collection chamber 2 of the flue gas that collection pinaster phytoclasts forms when carbonization, described carbonization chamber below is provided with the combustion furnace; The inner chamber of described carbonization chamber communicates with described collection chamber inner chamber by airway 3, described airway is provided with 6, be evenly arranged in the described collection chamber inner chamber, described airway extend into 1/3rd places of collection chamber height, described collection chamber top is provided with and the airtight lid that is connected of described collection chamber, described lid is the cooling back installation 41 that is provided with cooling water inlet 51 and coolant outlet 61, it is the cooling pan 42 of liquid that the periphery of described collection chamber is provided with the flue gas condensing in the described collection chamber, described cooling pan is provided with cooling water inlet 52 and coolant outlet 62, and described collection chamber is arranged in the cooling pan.Described collection chamber is an annular, and the bottom center arch of described collection chamber is bell jar shape projection to increase the heat exchange area of described collection chamber and cooling water, accelerates the condensation rate of flue gas.The bottom of described collection chamber is provided with the sharp mouth shape liquid outlet 21 that thick liquid is discharged, and sharp mouth shape liquid outlet is provided with 4, is evenly distributed on annular collection chamber bottom, and described liquid outlet communicates with atmosphere.
The gap is left in described bell jar shape rising height and described lid bottom.
The part that described lid and collection chamber interlock is down the pot type, and described pot type the bottom of a pan part 411 forms the top cover of described collection chamber 2, and the sidewall 22 of described lid and described collection chamber 2 is tightly connected.Contacted of lid and collection chamber are smooth, use the screw bolt tight on every side, the bell jar shape rising height of described collection chamber is concordant with the height of the coolant outlet 62 of cooling pan, can make flue gas and cooling water in the collection chamber that bigger contact area is arranged like this, makes the flue gas rapid condensation become thick liquid.
Described cooling water inlet 51 is arranged on described lid bottom, described coolant outlet 52 is arranged on described lid top, described cooling water inlet 61 is arranged on described cooling pan bottom, and described coolant outlet 62 is arranged on described cooling pan top.
Described carbonization chamber 1 comprises staving 11 and bung 12, and described bung 12 is tightly connected with described staving 11, and described bung 12 tops are provided with the hold-down mechanism that described bung 12 is compressed to described staving 11.
The described hold-down mechanism of described hold-down mechanism is the cross bar 71 that both ends are provided with snap ring 73, but described cross bar is provided with the clamp nut 72 of up-down adjustment, and described staving is provided with the shelves part 74 that cooperates with described snap ring.When being used for bung and staving and compressing, the snap ring of hold-down mechanism is cooperated with a shelves part, and the height by adjusting nut applies a big downward pressure, makes staving and bung seal, evenly arrange a plurality of nuts on the described cross bar, can strengthen the compactness of bung and staving like this.
Thick liquid extracting method: during concrete operations, to put into carbonization chamber 1 through the pinaster phytoclasts that soaks into earlier, arrange airway, make it to stretch into staving (carbonization chamber) and collection chamber 2, the snap ring of hold-down mechanism is cooperated with the shelves part, the height of adjusting nut compresses bung and staving, and cooperates lid and collection chamber are airtight, open the cooling water of cooling pan and chiller, light the combustion furnace, the pinaster phytoclasts in the staving carbonization chamber is fired to carbonization, the flue gas that carbonization is produced imports in the collection chamber, under the effect of chiller, flue gas in the collection chamber formation medicinal liquid that is condensed is discharged by liquid outlet, the convenient collection.Concrete grammar is as follows:
(1) branch of Pinus koraiensis and the Pollen pini thunbergii branch (comprising trunk and leaves) of quality such as put in the carbonization chamber of device shown in Figure 2, seal up a door, stay gas port, the igniting calcining after wet gas discharges, is loaded onto condensing plant to reclaim at the QI KOU place, obtain crude extract;
(2) be sub-packed in the pollution-free closed container after crude extract is collected, put into shady place, avoid the sunlight direct projection about 6 months, allow its hydrolysis voluntarily, produce acid, the good liquid of acid is produced in hydrolysis remove upper strata grease, get middle part liquid, discard the precipitation part, stock solution.
(3) stock solution is got the distillate of 98 ℃~103 ℃ of fractions through distillation, and residue black thick liquid is called the extraction waste liquid in the still-process, also has certain therapeutic effect, can retain as adjuvant drug; Distillate was through activated carbon adsorption decolouring about 4 hours, and material and impurity such as filter paper filtering active carbon are used in concussion, and gained filtrate is described pinaster and extracts medicinal liquid.
Embodiment 3: the preparation of pinaster extracting solution
(1) equipment therefor such as embodiment 1 with brick good kiln body, Pinus koraiensis, Pollen pini thunbergii, japanese black pine, Pinus tabuliformis, the Pinus sylvestnis var. mongolica Litv. of quality, the tree root of fish-scale floss such as put into, seal up a door, stay gas port, the igniting calcining, after the wet gas discharge, load onto condensing plant at the QI KOU place and reclaim, obtain crude extract;
(2) be sub-packed in the pollution-free closed container after crude extract is collected, put into shady place, avoid the sunlight direct projection about 1 year, allow its hydrolysis voluntarily, produce acid, the good liquid of acid is produced in hydrolysis remove upper strata grease, get middle part liquid, discard the precipitation part, stock solution.
(3) stock solution is got the distillate of 98 ℃~103 ℃ of fractions through distillation, and distillate was through activated carbon adsorption decolouring 3 hours, and material and impurity such as filter paper filtering active carbon are used in concussion, and gained filtrate is described pinaster and extracts medicinal liquid.
Embodiment 4: the preparation of pinaster extracting solution
(1) equipment therefor such as embodiment 1 with brick good kiln body, put into 5: 1 Pollen pini thunbergii cone of mass ratio and japanese black pine cone, seal up a door, and stay gas port, and the igniting calcining after the wet gas discharge, is loaded onto condensing plant and reclaimed at the QI KOU place, obtain crude extract;
(2) be sub-packed in the pollution-free closed container after crude extract is collected, put into shady place, avoid sunlight direct projection 3 months, allow its hydrolysis voluntarily, produce acid, the good liquid of acid is produced in hydrolysis remove upper strata grease, get middle part liquid, discard the precipitation part, stock solution.
(3) stock solution is got the distillate of 98 ℃~103 ℃ of fractions through distillation, and distillate was through activated carbon adsorption decolouring 3 hours, and material and impurity such as filter paper filtering active carbon are used in concussion, and gained filtrate is described pinaster and extracts medicinal liquid.
Embodiment 5: the preparation of pinaster extracting solution
(1) equipment therefor such as embodiment 1 with brick good kiln body, put into mass ratio 2: 2: 1: the tree root of 1 Pinus koraiensis, Pinus tabuliformis, Pinus sylvestnis var. mongolica Litv., fish-scale floss, seal up a door, stay gas port, the igniting calcining, after the wet gas discharge, load onto condensing plant at the QI KOU place and reclaim, obtain crude extract;
(2) be sub-packed in the pollution-free closed container after crude extract is collected, put into shady place, avoid sunlight direct projection 6 months, allow its hydrolysis voluntarily, produce acid, the good liquid of acid is produced in hydrolysis remove upper strata grease, get middle part liquid, discard the precipitation part, stock solution.
(3) stock solution is got the distillate of 98 ℃~103 ℃ of fractions through distillation, and distillate was through activated carbon adsorption decolouring 3 hours, and material and impurity such as filter paper filtering active carbon are used in concussion, and gained filtrate is described pinaster and extracts medicinal liquid.
Embodiment 6: the preparation of pinaster extracting solution
(1) equipment therefor such as embodiment 1 with brick good kiln body, put into mass ratio 1: 2: 3: the bark of 4: 5 Pinus koraiensis, Pollen pini thunbergii, Pinus tabuliformis, Pinus sylvestnis var. mongolica Litv., fish-scale floss, seal up a door, stay gas port, the igniting calcining, after the wet gas discharge, load onto condensing plant at the QI KOU place and reclaim, obtain crude extract;
(2) be sub-packed in the pollution-free closed container after crude extract is collected, put into shady place, avoid sunlight direct projection 3 months, allow its hydrolysis voluntarily, produce acid, the good liquid of acid is produced in hydrolysis remove upper strata grease, get middle part liquid, discard the precipitation part, stock solution.
(3) stock solution is got the distillate of 98 ℃~103 ℃ of fractions through distillation, and distillate was through activated carbon adsorption decolouring about 3 hours, and material and impurity such as filter paper filtering active carbon are used in concussion, and gained filtrate is described pinaster and extracts medicinal liquid.
Embodiment 7: the preparation of pinaster extracting solution
(1) equipment therefor such as embodiment 1 with brick good kiln body, put into 10: 1 Pinus sylvestnis var. mongolica Litv. branch of mass ratio (comprising trunk and leaves) and fish-scale floss bark, seal up a door, stay gas port, the igniting calcining, after the wet gas discharge, load onto condensing plant at the QI KOU place and reclaim, obtain crude extract;
(2) be sub-packed in the pollution-free closed container after crude extract is collected, put into shady place, avoid sunlight direct projection 3 months, allow its hydrolysis voluntarily, produce acid, the good liquid of acid is produced in hydrolysis remove upper strata grease, get middle part liquid, discard the precipitation part, stock solution.
(3) stock solution is got the distillate of 98 ℃~103 ℃ of fractions through distillation, and distillate was through activated carbon adsorption decolouring 5 hours, and material and impurity such as filter paper filtering active carbon are used in concussion, and gained filtrate is described pinaster and extracts medicinal liquid.
Embodiment 8: the preparation of pinaster extracting solution
(1) equipment therefor such as embodiment 1 with brick good kiln body, the Pinus sylvestnis var. mongolica Litv. of quality, the trunk of fish-scale floss such as put into, and seal up a door, and stay gas port, and the igniting calcining after wet gas discharges, is loaded onto condensing plant to reclaim at the QI KOU place, obtain crude extract;
(2) be sub-packed in the pollution-free closed container after crude extract is collected, put into shady place, avoid sunlight direct projection 3 months, allow its hydrolysis voluntarily, produce acid, the good liquid of acid is produced in hydrolysis remove upper strata grease, get middle part liquid, discard the precipitation part, stock solution.
(3) stock solution is got the distillate of 98 ℃~103 ℃ of fractions through distillation, and distillate was through activated carbon adsorption decolouring 6 hours, and material and impurity such as filter paper filtering active carbon are used in concussion, and gained filtrate is described pinaster and extracts medicinal liquid.
Embodiment 9: the preparation of pinaster extracting solution
(1) equipment therefor such as embodiment 1 with brick good kiln body, put into mass ratio 10: 1: 10: the full tree of 1 Pinus koraiensis, Pollen pini thunbergii, japanese black pine, Pinus tabuliformis, seal up a door, stay gas port, the igniting calcining, after the wet gas discharge, load onto condensing plant at the QI KOU place and reclaim, obtain crude extract;
(2) be sub-packed in the pollution-free closed container after crude extract is collected, put into shady place, avoid sunlight direct projection 3 months, allow its hydrolysis voluntarily, produce acid, the good liquid of acid is produced in hydrolysis remove upper strata grease, get middle part liquid, discard the precipitation part, stock solution.
(3) stock solution is got the distillate of 98 ℃~103 ℃ of fractions through distillation, and distillate was through activated carbon adsorption decolouring 3 hours, and material and impurity such as filter paper filtering active carbon are used in concussion, and gained filtrate is described pinaster and extracts medicinal liquid.
Embodiment 10: sterilization of pinaster extracting solution and cytothesis test, long term toxicity test
(1) 6 kinds of pinaster extracting solution of trial drug: embodiment 1 gained and trobicin (spectinomycin hydrochloride) (Guangzhou big uncle chemical industry company limited);
Animal subject: view and admire each 70 of man-of-war fish in the tropical fish, Pseudorabora parvas;
Test method: man-of-war fish, each 20 of Pseudorabora parvas are put into water temperature (32 ℃) water of heightening and raised four hours, rapid drawdown water temperature to 20 ℃ four hours, after finishing said process, water temperature is transferred in the normal water temperature (26 ℃~28 ℃) again and raise, after 3 days, a bacterium disease appears on one's body in the tested fish class so repeatedly, melasma, fester, do not eat food hypokinetic disease shape etc. simultaneously.
Man-of-war fish and Pseudorabora parva are arbitrarily divided 7 groups (wherein 6 groups is experimental group, and 1 group is matched group) separately, 10 every group, respectively fish are put into water quality, water temperature, the glass container of equal conditions and raise.
6 groups of experimental group fishes with smearing the affected part with 6 kinds of pinaster extracting solution respectively, were bathed bubble 5 minutes with 80 times of dilution Pinus koraiensis liquid, repeat once again after 10 hours at interval.
The matched group fish is smeared with trobicin, bathed bubble 5 minutes, repeat once again after 10 hours at interval with 80 times of diluents.
After ten days, observe 14 groups of situations, as a result the man-of-war fish: 9~10 of each group survivals of experimental group, 3 of matched group survivals; Pseudorabora parva: 8~9 of each group survivals of experimental group, 4 of matched group survivals.The Fish of experimental group survival do not have a bacterium disease, and melasma is festered, and appetite is recovered to move about back and forth freely in the past; Then also there is silk bacterium disease in the fish of matched group, and melasma is not festered but have, and appetite is still few, does not like the symptom etc. of moving about.
(2) trial drug: embodiment 3 gained pinaster extracting solution and trobicins;
Animal subject: the red Carassius auratus of the long-tail in cycle of the same age is 20 in the pet fish;
Test method: long-tail Carassius auratus straight snips left side afterbody one leaf.Arbitrarily fish for identical ten of sizes and dip in Pinus koraiensis liquid with Cotton swab to smear at the place of cutting once for the first group, fish is put into two identical first group fish jars of preprepared, first group fish is raised under 16 ℃~18 ℃ conditions of water temperature with 3000 times of Pinus koraiensis liquid dilutions; After second group fish shears left side afterbody one leaf, directly put into, raise in the second group fish jar that water temperature is 16 ℃~18 ℃ with 3000 times of trobicin dilutions.Intermittence is changed water simultaneously.Observe surplus 2 of first group fish, surplus 3 of second group after 50 days; Cut caudal lobe portion and observe, first group Carassius auratus caudal lobe grows 3mm~8mm and does not wait, and second group Carassius auratus caudal lobe grows about 1mm, and is uneven.
(3) growth regulator that produce in trial drug: embodiment 3 gained pinaster extracting solution and Jiangsu;
Tried plant: willow;
Test method: the branch root of willow more than 2 years is evenly big or small, diameter 10mm~15mm, length 250mm blocks and gets 30.15 of first groups, 15 of second groups are implanted respectively in the tub of equal big or small condition, and earth is taken from same place in the tub, adds certain nutrient, two boxes is put in the room of identical illumination, temperature and humidity.The first group is watered once with 80 times of dilution pinaster extracting solution every day, and the growth regulator that the second group is produced with Jiangsu waters once every day.Observing discovery, the first group all survives, and it is thick that institute goes out blade, and blade is bottle green, and second is formed 11 alive, and remaining blade approaches, and blade is yellow green.After move to outdoor plantation and observed 1 year, the dark bar of first group root is thick, full of leaves as a result, the second group is then opposite.
(4) trial drug: embodiment 3 gained pinaster extracting solution and shao-hsing rice wine;
Animal subject: " coming laying hen " baby chick of same kind;
Test method: get 50 of the chickens of same chicken house birth, divide two groups of first, second, 25 every group, the first group is mixed in the feedstuff with the pinaster extracting solution, and the second group is infiltrated in the feedstuff with shao-hsing rice wine, after 20 days as a result, finds 23 of first group survivals, and the second group is survived 18.After laying eggs etc. two groups of chicken maturations of first, second, respectively stay 3 of healthy hens, 1 of cock, put two cages respectively into, the raising that uses the same method every day, 1 year, two groups of chickens of first, second respectively select 10 pieces of egg hatchings, and two cages exchange cock once, and two groups of chickens of first, second respectively select 10 pieces of egg hatchings.
Reach a conclusion: the chicken that first group egg is gone out obviously is better than the second group, finds phenomenons such as no gene mutation, residual lower limb, and the second group has found that repeatedly residual lower limb chicken occurs.Observed like this substantially in continuous 3 years.
(5) for the examination strain: staphylococcus, escherichia coli, anthrax bacillus, sick frog isolate;
Preparation for examination culture of strains and bacteria suspension:
Antibacterial is adopted 37 ℃ of cultivations of beef-protein medium.Be seeded in staphylococcus aureus, escherichia coli, anthrax bacillus, sick frog isolate on the beef extract-peptone agar culture medium respectively or on the nutrient agar, cultivate 24h for 37 ℃.
A little cultured thalline of picking is in being equipped with physiological saline solution in vitro respectively with inoculating loop, and vibration is evenly made bacteria suspension.Measure its bacterial concentration with the method for plate culture count, and use dilution method, making bacterium liquid contain the bacterium number is 10 4Individual/ml, be for the examination bacteria suspension.
The mensuration of extract bacteriostasis rate:
The size of bacteriostasis rate can reflect the height of extracting solution bacteria resistance function, and 6 kinds of pinaster extracting solution that embodiment 1 method is made respectively add 3ml and mix with the Nutrient agar of about 10ml in plate, make antibacterial flat board.In the test tube that contains the 20ml nutrient broth of the bacterium of going out, each inserts the strain of staphylococcus aureus, escherichia coli, anthrax bacillus, sick frog isolate, in shaking table, cultivate after 4~5 hours for 37 ℃, getting 50ul bacterium liquid with pipettor is applied on the antibacterial flat board, cultivated colony counting 10 hours for 37 ℃ in the calorstat.
Bacteriostasis rate (%)=(contrast culture clump count-sample culturing clump count)/contrast culture clump count * 100%
After measured, 6 kinds of extracting solution all reach more than 99.999% the bacteriostasis rate of staphylococcus aureus, escherichia coli, anthrax bacillus, sick frog isolate.
Embodiment 11: the contusion of skin table, blunt wound, wound, electric welding burn and scald, electric shock are burnt, the treatment of comedo is practise medicine for many years true case in the process of applicant below observing:
Wu, the man, 71 years old, ride electromobile in August, 2009 because handstone slips, two knees are seriously created scratch, wipe more than the about 1mm of the degree of depth, and brothers have silt swollen in various degree, and injured many places require to execute to control.Processing method: embodiment 1 Pinus koraiensis extracting solution is poured in the spray bottle, evenly sprays, with the absorbent cotton place of cleaning a wound for several times, do not have next day find red and swollen, back every day three times, the no suppurative infection phenomenon of observation after three days.Progressive healing, ten days crusts of spray drop, wound healing, the swollen part of becoming silted up disappeared after 30 days, did not have obvious cicatrix and left over, and certain bad skin is arranged.
The week certain, woman, 17 years old, in July, 2009, certain day collides and falls on the threshold of stair sliding door because of catching up with between class hour, one on the other anterior embedded length 13mm diameter 10mm screw of right lower limb diameter bone, extract to the People's Hospital back, executes through hospital and control, and injection of antibiotics and the routine bacterium liquid that disappears is smeared, wrap up after 25 days, all the time do not have and be clearly better, wound has suppuration, the red and swollen infection, and wound is not seen healing.The back is executed to here and is controlled.Processing method: throw off binder, smear with embodiment 1 Pinus tabuliformis extracting solution, reuse point tweezers folder sterilization dry cotton ball dips in the pinaster extracting solution and cleans a wound, the back is gone into the pinaster extracting solution and is sprayed several every day with spray is bottled, found that wound on the 3rd closes up, the incrustation scar, the crust scar drops after 15 days, the hole healing, no other drug is assisted the doctor in executing the process of controlling.
The building, the woman, 49 years old, the careless left index finger of Potato cutting was cut the about 3mm of the long 20mm degree of depth by kitchen knife, bleeding wounds, horse back is gone to here and is executed and control.Processing method is used: embodiment 3 pinaster extracting solution clean a wound, and spray wound healing after more than 20 day as a result every day five times.
Above situation is executed and is controlled effect and all belong to domestic present sterilization, antiinflammatory special effect because unexpected skin lesion is hindered example and is no less than more than 50 case.
Chen, the man, 48 years old, the electric welder, door industry boss has two more than ten years electric welding history, and the left hand elbow is often burnt by electric welding, and leaves many cicatrixes, domestic burn and scald medicine among the people, domestic pharmaceutical factory burn and scald medicine is standing.Once refer to this thing, send one bottle of fish-scale floss extracting solution to give him, later, patient's readme: it is too magical to scald medicine, after the back spray of electric welding burn is spread, scalds the part redness of not suppurating, and healing time is short, and the scald that stays the partly vestige of cicatrix is also lighter.
Shut out certain, the man, 30 years old, professional electrician, once in electric industry operation by the electricity right hand forefinger of burning because of carelessness, the area of burning reaches 20mm * 60mm, pain is gone to here and is required to execute to control unbearably.Processing method: forefinger is put in the vial of putting into embodiment 2 pinaster extracting solution, and pain is stopped after five minutes.Smear recovery from illness after more than 20 day back every day for four times.
Lin, the man, 50 years old, the cook was engaged in the industry 30 years, was often hindered by oil, to scalding medicine certain understanding was arranged.Once, render lard by the Adeps Sus domestica skin splash hinder the chest, the scald place reaches 40mm * 55mm and gets blister, processing method: puncture blister with sterile needle, spray embodiment 1 Pollen pini thunbergii extracting solution, every day four times is after 12 days, heal in the place by scald, and do not have to stay cicatrix the patient's readme of healing back: this medicine is too severe! It is all good to go over any scald medicine of usefulness than me! In agglutination, promptly do not have red and swollen, suppurate, preventing from scar again, this has been my used best good medicine.
The week certain, the man, 48 years old,, go out and drink with friend because of feeling worried, because the many obnubilation of wine, go back home will be placed on water boiled on the stove water from one's body, the result all scald to be bubbled on left shoulder and whole chest, the family members loses no time to deliver to here out of admiration for a famous person and executes and control, because of refusing, be Ta Shizhi.Processing method: gauze is soaked with embodiment 3 pinaster extracting solution, and with the Pork-pieces scald place that is affixed on of tweezers, the brush pen that continual then usefulness disinfects soaks the pinaster extracting solution and smears back and forth, spray the affected part more than 10 time with the bottled medicine of spray every day later on, the 3rd day, red and swollen cancellation, do not have and infect, heal after January.
Cai, the man, 16 years old, Zheng, the woman, 14 years old, the gold certain, Ma waits 30 comedo patients.Processing method: in 50 times of thermal foggers of packing into of embodiment 3 pinaster extracting solution dilution, connect electricity and open the steam spray switch, sprayed on the face 20 minutes the experimenter with steam, reuse is extruded the Xiao Huang point by pin, the back is dipped in the pinaster extracting solution with absorbent cotton and is spread upon the affected part, after continuous three days to seven days, the whole rehabilitations of experimenter.With the oral embodiment 3 pinaster extracting solution of drug matching, observe and can thoroughly root out the disease candle, the Semen Phaseoli bean is no longer recurred.
Embodiment 12: vasculitis, the Nian Buyu case treatment of a specified duration of mashed foot are observed
Yu, the woman, 81 years old, right lower limb festered 43 years because of dog bite, and pain is unbearably, and is inconvenient on foot.The many places of having sought medical advice since four more than ten years, doctor among the people, regular hospital, folk prescription, normal prescriptions of Chinese medicine is executed to control eventually and is had no result, and the neighbour son says that she " mashed always foot " control badly in this lifetime, executes and controls after the people introduces here.Processing method: with 1: 500 dilution Pinus koraiensis extracting solution foot bath two hours, pick up, dry with disinfecting towel, reuse pinaster extracting solution sprays back and forth for several times, sprays pinaster extracting solution twice later every day, and every day, oral pinaster extracting solution 20CC was with two times of eliminating cold for resuscitation water dilutions.After treatment in 6 months, the part of festering healing, it is also normal to walk, and does not have recurrence.
Answer certain, the man, 64 years old, bipod that vasculitis causes and top shank redness, erosion, pain is unbearably, and is inconvenient on foot.Patient's readme, vasculitis reach 14 years, are insteps always, the heel redness of festering, because food accidentally, causes allergic reaction, the bipod inflammation is heavier sometimes.In many ways execute to control and have no result, heart is very painful.Execute to here upon somebody's introduction and control processing method: measure the swollen portion in two places size with gage earlier: left knee below girth is 326mm, and right knee below girth is 331mm, and left foot anklebone top girth is 289mm, and right crus of diaphragm anklebone top girth is 291mm.Add Pollen pini thunbergii extracting solution foot bath one hour with active carbon with salt then, pick up, dry with disinfecting towel, spray back and forth repeatedly with the Pollen pini thunbergii extracting solution, spray the Pollen pini thunbergii extracting solution every morning once then, after treating that liquid is done, the Pollen pini thunbergii of the sticking shape of embodiment 1 black is extracted waste liquid on the repaste, oral dilution Pollen pini thunbergii extracting solution below 5 times, and all press as the method and treat every day, after one month, red and swollen part disappears, and left knee below girth is 279mm, and right knee below girth is 282mm, left foot anklebone top girth is 240mm, and right crus of diaphragm anklebone top girth is 246mm.Pain disappears, and has made things convenient on foot.As the method, treated three months, to use instead and spray secondary every day, every day, oral Pollen pini thunbergii extracting solution 15CC was with two times of eliminating cold for resuscitation water dilutions, fully recovered after 12 months.Knee below, left side girth is 275mm, and right knee below girth is 280mm, and left foot anklebone top girth is 218mm, and right crus of diaphragm anklebone top girth is 221mm.The redness and the black at shank position are partly decorporated, and also do not meet quick reaction after spicy food is eaten.
Chen, the man, 43 years old, vasculitis, shank begins to be swollen with, the swelling of visible shank blood vessel dish knot, the high skin 10mm that rises of maximum swelling, about two lower limb blood vessels, 27 places have and play bag in various degree, the pimple protuberance.The back is executed to here and is controlled, processing method: bathe one's feet in hot water with hot water every day, then smear embodiment 3 pinasters extract in the waste liquid black mucus once, flush away after seven hours is sprayed embodiment 3 pinaster extracting solution, sees curative effect after five days, after three months, basic healing now adheres to taking every day 20CC pinaster extracting solution, and readme is now got better everyday.
Wu, the man, 71 years old is vasculitis through hospital diagnosis; Lu, 39 years old is vasculitis through hospital diagnosis; People more than 20 such as Zhao is diagnosed as vasculitis, executes to control all obtaining good result with above case method.
The land, the woman, 28 years old, two primary minimum lower limb varicosis protuberance, and distending pain is arranged often entered summer and dare not wear skirt, wearing skirt, to expose shank vein protuberance pimple ugly, after look for me to execute controlling.Execute the method for controlling: smear the sticking shape Pollen pini thunbergii of embodiment 1 black before sleeping every day behind the hot water foot bath and extract waste liquid one time to the next morning, clean the sticking shape Pollen pini thunbergii of black with hot clear water and extract waste liquid, use cloth to wipe with and do two limbs, with the spray bottle embodiment 1 Pollen pini thunbergii extracting solution is evenly sprayed the affected part one time, a large amount of dots in red appear in the affected part periphery after 11 days, the decortication phenomenon appears in red some cancellation after five days, skin table, and 68 days posterior vein protuberances disappear and recover normal.
Zhang, the man, 69 years old, vein protuberance penetrated the protuberance pimple with needle tubing and takes out what blood and cause that pair lower limb fester owing to wait for information the locals, after look for me to execute controlling.Execute the method for controlling: smear at rotten position with embodiment 1 Pinus sylvestnis var. mongolica Litv. extracting solution, fester after surplus in the of ten day after the convergence of wound, spray with embodiment 1 Pinus koraiensis extracting solution, every day four times, skin recovers elasticity after 20 days, smear once with the sticking shape mixed extraction waste liquid of embodiment 3 black, clean two limbs with hot water after one hour, towel off dried, spray Pinus koraiensis extracting solution number time with spray bottle, the bimester of adhering to, two limbs thoroughly take a turn for the better, and expansion has fallen in vein, becoming bent disappears, past all decorporates with the pinprick place is black, and skin recovers elasticity, is tending towards normal.
The pinaster extracting solution has extremely strong penetration, and general vasculitis patient is most to infect outer skin owing to blood vessel causes inflammation, and outer skin is produced with extraneous bacterial infection interaction fester, in case the outburst of vascular inflammation is difficult to cure.General bactericide and antibiotic all are difficult to arrive the focus depths, only limit to epidermis, but pinaster extracting solution skin-permeable deep layer, vasoactive, so the pinaster extracting solution can thoroughly be cured vasculitis, the ulcer of phase property of a specified duration.
Embodiment 13: the otitis media treatment is observed
Wu, the man, 45 years old, as a child ear had inflammation always, can draw clot during the earpick dung sometimes, had pus to flow out in ear during inflammation, execute the method for controlling: cotton-ball bar soaks with embodiment 3 pinaster extracting solution, slowly stretch in the ear and clean pus several times, again embodiment 3 pinasters are extracted number of drops and drip, take effect after three days in ear.Children, tens are tried, and method as above all takes effect.
Embodiment 14: esophagitis, esophageal carcinoma, the treatment of pharyngolaryngitis case are observed
History, the man, 47 years old is esophagitis through hospital diagnosis.The main suit: the esophagus dysphagia, burning sensation is arranged, constipation has dull pain during chest, come here to seek medical advice upon somebody's introduction.Execute the method for controlling: 30CC slowly swallows with the Pinus tabuliformis extracting solution, twice sooner or later.Borborygmus in second day are continuous, just go out a large amount of black loose stool, the urine band blood streak, and behind the row, a feel is happy incomparable.The 3rd day, titillation is arranged on the esophagus.After use morning 20CC instead and slowly swallow, 10~15 times of 15CC dilutions in evening are the pharynx clothes slowly, drink in conjunction with the Pinus tabuliformis extracting solution with the prescription decoction back, adheres to that May is surplus, its transference cure, diet is normal.
Money, the man, 54 years old, the esophageal carcinoma patient, the difficult pharynx of diet, chest pain, constipation is fidgety unusual, and with a haggard face, hair is simple and unadorned, and asthenic body is unable, seeks medical advice through the history introduction.Execute the method for controlling: 50CC Pinus koraiensis extracting solution is swallowed liquid to esophagus slowly and is cooperated Chinese medicine soup side to drink, and takes the dilution of herbal medicine immersion Pinus koraiensis extracting solution evening and drinks for 5 times, boiled water is infused bubble relaxing the bowels with lubricant drugs Chinese medicine when tea-drinking usefulness, after ten days, takes effect, feces rushes down greatly, sees that stool has one deck oily to float in the water, after an action of the bowels, hunger sensation is arranged, swallow two with old duck soup and Radix Panacis Quinquefolii buccal tablets, each once now drinks 50CC Pinus koraiensis extracting solution assistant every day with Chinese medicine decoction always sooner or later sooner or later, can swallow hard slightly food by now, the existing life that always continues.
Grandson, man, 37 years old, pharyngolaryngitis patient, cardinal symptom: bottleneck throat redness when meeting pungent irritable food and shot in a war of words quarrel, pruritus, hoarseness.When serious, throat's pronunciation is overcast, companion's hyperpyrexia, and body temperature is up to more than 39 ℃, and disease time reaches 7 years, and hospital uses antibiolics basically, for the moment the inflammation cancellation.After meeting the situation of stating, disease relapse is controlled for a long time and is had no result.After use the fish-scale floss extracting solution instead, swallow clothes 20cc morning slowly, 20 times of drink-service in evening 10cc fish-scale floss extracting solution dilutions took effect after taking medicine one day, adhered to having a surplus January, cured, and did not have recurrence so far after more, pharyngolaryngitis experimenter's light and heavy degree differs, but all effective in cure.
Chen, man, 63 years old, the esophageal carcinoma patient, postoperative is after half a year, the difficulty of eating, chest dull pain unbearably, sweating due to debility is dripping, the food after forcing to swallow advances stomach makes stomach seriously uncomfortable again, the back listens the people to say, executes to here and controls, and I slowly allow it swallow by esophagus with embodiment 1 fish-scale floss extracting solution 20cc for 3 times with the warm water dilution, every day 3~5 times, different according to circumstances and decide, adhere to obeying liquid after 5 days, think that esophagus has the sense of expansion.The spoon meat of can slowly swallowing now adheres to taking always, than before the flatulence situation seldom occur, mental status also takes a turn for the better greatly.
Jiang, the woman, 53 years old, professional teacher, begun just to feel that there is the sense of reptile the throat, after several class taught, the trunnion sounding was hoarse, and is extremely back with regard to aphonia at 3 in afternoon sometimes, and then it is also relatively more difficult to swallow food, esophageal has burning sensation, and when hard food was swallowed, whole esophagus position was as being pulled open, after my father talks about, I initiatively send one bottle of the Pinus koraiensis extracting solution liquid that embodiment 1 method extracts, and advise and drink its every day 3 times, get extracting solution 20cc~15cc for every and dilute 5~10 times and slowly swallow, throat's sounding is normal after three days, swallowing food behind the first quarter moon does not have pain, adheres to obeying liquid January, and now full recovery is normal.
Journey, in season, the age is many more than 60 years old, all is the esophageal carcinoma patient, executes the method for controlling and front and exemplifies equally, has all received obvious effects now.
Journey, Lu, the literary composition certain, Deng seven examples, the age was not waited at 20 years old to 70 years old, esophagitis, pharyngolaryngitis patient, I am executing in the process of controlling for them, look weight person in various degree, oral consumption is used Pinus koraiensis, Pinus sylvestnis var. mongolica Litv. by the history oral methods, Pollen pini thunbergii, the fish-scale floss extracting solution is swallowed oral slowly, all receive good effect, observed result have rehabilitation and just among rehabilitation.
Embodiment 15: gastritis, the treatment of gastric cancer case are observed
Why certain, woman, 56 years old, hospital diagnosis chronic superficial gastritis;
Yu, woman, 47 years old, hospital diagnosis chronic erosive gastritis;
Two patients can not eat raw and cold food usually, and viscous foodstuff, eat the back tripe and expand, and the sense of feeling sick being arranged, and lethargy is depressed, and conscious extremely is felt bad, and do not have positive effect through hospitalize in many ways, and after the drug withdrawal, self-induction in the past.After look for here, processing method: directly slowly swallow stomach with embodiment 6 pinaster extracting solution 15CC, once drink after 10 times of the 15CC dilutions in evening every morning, drink first quarter moon after, above symptom completely without, gradually take a turn for the better, after use 5 times of branches of every 20CC dilution instead and drink for twice sooner or later, adhere to that January is surplus, be tending towards normally through hospital gastroscope perspective symptom, two are not always the case.
Liu, 80 years old, through hospital diagnosis gastric cancer, skelalgia was felt sick, chest and abdomen swelling and pain, gastralgia, that presses promptly ends.Appetite is poor, and often liquid food is swallowed, and still discharges melena.Chest in evening dull pain repeatedly.Processing method: directly pharynx clothes embodiment 9 pinaster extracting solution 50CC once, after continuous seven days, use 30CC instead, evening, 10CC slowly swallowed for 10 times with the dilution of eliminating cold for resuscitation water, and about first quarter moon is surplus, subjective symptoms changes to some extent, can suitably advance normal diet, conscious digestive function increases to some extent, and body weight has also increased by 2 kilograms, now continue to take, feel that gradually pain slows down.
Cao, man 70 years old, gastric cancer, postoperative 1 year, epigastrium seriality dull pain is felt sick, the vomiting, swallow the food difficulty, the time half belch, acid regurgitation, heartburn, dyspepsia, mood is fidgety, and often hits the person, and it is complicated that the whole state state of an illness becomes, enter the vicious cycle stage, the back is executed to here and is controlled, and advises its hospital medicine of living in normally to take, after taking medicine one hour, again embodiment 1 every of Pinus koraiensis extracting solution is got 20cc~30cc and dilute twice, every day three times with warm water, swallow once with embodiment 1 fish-scale floss extracting solution 10cc before sleeping, do not dilute, clothes Pinus koraiensis extracting solution was just received effect in three days, at first, dim gas is heartburn, the acid regurgitation sx, the patient is just more confident now to adhere to taking everyday, got off in two months, fidgety emotion has not had yet, and dull pain is also few, the drink amount was than having increased by one times in the past, and body weight has also increased by 5 kilograms.
Yu, man, 75 years old, superficial gastritis patient,, gastritis becomes thin anemia, weakness, insomnia because causing, palpitation and amnesia, stomach is belch often, acid regurgitation, swallow food after, whole belly swelling mixes with embodiment 2 Pollen pini thunbergiis and Pinus koraiensis extracting solution and to take, and every 15cc directly slowly swallowed 5 days, every day secondary, after use every 15cc instead and dilute twice with warm water, every day three times is after January, above sx, weight increase 7.5kg poliosis has blackening phenomena, now adheres to taking always.
Jiang, the woman, 54 years old, the hospital diagnosis erosive gastritis adopted the Chinese medicinal formulae treatment, all do not have and receive too positive effect, gastroscopy does not have the improvement sign, when drinking prescription the gastropathy sx some, after the drug withdrawal a few days, gastritis, the sense of expanding of belch acid regurgitation reappears and shows, after stop prescription, adopt embodiment 1 fish-scale floss extracting solution pharynx clothes, get extracting solution 15cc for every, with 2 times~10 times of warm water dilutions, decide the bimester of adhering to obeying extracting solution 05 days on my sensation, in the gastroscopy stomach heal substantially in rotten to the corn position, now adheres to taking the fish-scale floss extracting solution.
History, the literary composition certain, the hole, Deng gastritis sufferer from different provinces, age was not waited at 18 years old~65 years old, and twenties patients take the method calculating of ten day course of treatment of pinaster extracting solution, generally in the middle of first course of treatment, just can receive effect, take the situation of all ill healing and improvement after 5 to 10 courses of treatment.
Embodiment 16: enteritis, diarrhea, constipation therapy are observed
Ten thousand certain, man, 52 years old, I and he Dalian of going on business together.Because of go the restaurant eat seafood two per capita enteritis, diarrhea.After midnight, diarrhoea as notes, sweating due to debility is dripping, feels run-down, green around the gills, I drink Pinus koraiensis extracting solution 20cc at once to see this shape, dilute two times.He does not believe and be unwilling to drink, and back tummy saw that my state of an illness alleviated to some extent in one hour unbearably, and he also requires to drink, and method is as above drunk and entered sleep in back one hour.Getting up in second day, sb.'s illness took a favorable turn, do not have diarrhoea pain.
Chen 63 years old, Pueraria lobota 65 years old is waited tens patients, and the age was suffered from constipation at 60~78 years old, showed constipation with dry stool, reached 3 days~do not discharge feces just in 7 days, and tripe expands, and it is bad to sleep, and upsets and drinks since drinking 20 times of empty stomaches of Pinus koraiensis extracting solution 20cc every day dilution.The branch morning and evening, respectively once drinking defecated in back second day discharged, and adheres to drinking every day, is undoubtedly Gospel for the senile constipation person, and now arrange once just morning on time, felt certainly to have slept, and appetite also has increase, and is happy, and face is also ruddy.
Embodiment 3 pinaster extracting solution are all effective at the diarrhoea pain that causes because of diarrhoea that accidentally wedging is stale, the food that carries disease germs causes and pesticide intoxication, and the experimenter reaches more than ten, and healing is all arranged.The orchard worker has fancy effect after the diarrhoea examination that spraying pesticide causes.
Embodiment 17: the hemorrhoid case observation
Lu, the gold certain, 19 outer hemorrhoids patients such as Cui, processing method: after soaking embodiment 4 pinaster extracting solution with aseptic cotton, cotton ball is filled in the hemorrhoid affected part, take out after five minutes with finger, continuous every day five times, do not wait natural law in three days to 16 days, the experimenter all take a favorable turn.Wherein 13 are not had recurrence, and connecing again after the pain appears in all the other six grades use the method, shows substantially all rehabilitations.
Embodiment 18: the treatment of hepatitis B, cirrhotic ascites, hepatocarcinoma case is observed
Xu certain, the man, 63 years old is hepatocarcinoma through hospital diagnosis.Chest and abdomen swelling and pain, history of virus hepatitis 20 years, right rib dull pain, abdominal distention, the colour of skin is sallow, the slight edema of two lower limb, be hard and dry, dry mouth with bitter taste, body fluid is few, photophobia, spirit is poor, and expression in the eyes is stiff, the canthus corners of the mouth is downward, and liver volume increases, and appetite is few, the stomach poor appetite, processing method: morning is Pinus koraiensis extracting solution 50CC on an empty stomach, and evening, the dilution of 15CC Pinus koraiensis extracting solution was three times, swallow on an empty stomach, after so adhering to five days, pharynx clothes dosage is the same after meal, after drinking more than ten day, just see that thin black feces discharges in a large number, feel abdominal distention and alleviate that appetite increases to some extent, the photophobia degree alleviates, and mental status changes to some extent.Later on drink the Pinus koraiensis extracting solution every day and be no less than 50CC, adhere to that 1 year conscious condition of illness takes a turn for the better to some extent, the time and can also do a muscular labor
Cui, the man, 65 years old is later period of hepatocarcinoma after diagnosing.Can not the long time prolong the life that continues according to city's hospital diagnosis, advise its family members to make arrangements for a funeral.After going home, family members are entirely when giving up for lost, send here, advise drink its every day and be no less than 100CC Pollen pini thunbergii extracting solution, after the result drinks, situation has changed at once, stool is pulled out the thin feces that a large amount of black have the blood streak, after drawing, feels that spirit is good for second day, unexpectedly fail to give attention to eat four liang of rice, also drunk one little bowl of egg soup.Behind the first quarter moon, family firewood, arrangement silo do not have to live not to be done.After adhere to drinking this liquid in 4 years, once sheep loses in the man in winter, goes out to go for sheep, goes home to be unable to leave the bed after enduring cold, and is dead after spending four days.
Answer certain, woman, 31 years old, the great three positive patient, since two thousand seven, belly expands, the face edema, exophthalmos, liver function test: globulin, Archon ratio, glutamic oxaloacetic transaminase, GOT, Y-glutamyl transpeptidase four indices are all defective, after the people makes referrals to here, adhere to drinking embodiment 3 pinaster extracting solution 40CC every day, adhered to drinking two months, liver function except that globulin, Archon than defective, other two are tending towards qualified, adhere to taking embodiment 3 pinaster extracting solution again two months, and it is qualified that every liver function index all belongs to.Face is obviously become thin, and belly does not have tympanites yet, and spirit has been worked energetically.Other liver functions deviant, adhere to taking the pinaster extracting solution several months after, can both obviously feel to take a turn for the better, it is normal that liver function index is tending towards.
The gold certain, the man, 48 years old, ascites was expanded, the both sides of the chest twinge, yellow urine is few, is hard and dry xerostomia happiness drink, inappetence, day by day yellow thin, be cirrhotic ascites through hospital diagnosis, here allows it drink embodiment 3 pinaster extracting solution 50CC on an empty stomach once, afternoon 20CC, borborygmus stomachache behind second day medicine day is rushed down the black loose stool, abdominal distention subtracted greatly on 7, yellowish body subtracts, and appetite increases, and pinaster extracting solution decrement is to 50CC every day, adhere to 1 year surplus, not recurrence again, and also be the carpenter everyday, do finishing and earn money.
Xu certain, man, 45 years old, tax cadre, often wine table dinner party, examination in hospital is an alcoholic liver disease, the pathological manifestations waist soreness, neurolysis, there is tenderness in the gallbladder district, after directly look for me to execute controlling, execute every of the method for controlling and get embodiment 1 Pinus koraiensis extracting solution 10cc, do not wait for 2 times~10 times with the cold water dilution, every day, pharynx clothes were three times, do not wait, grasped by patient oneself for 5 times, after drinking, a large amount of black sticking just discharges are always arranged, the defecation first quarter moon, melena disappears, defecating gradually changes khaki by black, and every morning defecation once, observe and have a surplus half a year, defecation is often regular, the thorough cancellation in dull pain position, spirit also become vivaciously, and dejected emotion is cleared off.
Chen, man, 39 years old, result of laboratory test is a small three positive, frequent myasthenia of limbs, dizziness, bitter taste, blurred vision, dizziness and tinnitus, the nearly 3 years serialitys of having a sleepless night are like this, go to see a doctor, and disease gently alleviates to some extent, later, a period of time still recurs, after the here of seeking medical advice out of admiration for a famous person, I advise it to drink embodiment 1 Pinus sylvestnis var. mongolica Litv. extracting solution and the mixing of depressed liver-energy dispersing and QI regulating Chinese medicine extraction liquid is taken, and effect is fairly obvious, and clothes liquid one day after, second day, patient's readme vision is clear, and disease is gone half certainly, after adhering to taking January, above symptom cancellation, in that to adhere to taking January surplus, showed 2 years, the main suit does not have recurrence.
Shao, Lin waits thirties hepatopaths, private prosecution is after having drunk the Pinus koraiensis extracting solution, and stool is tending towards rule, and urine is clear, insomnia deducts, and some flu, fever, cough symptom all take a favorable turn and reduce, and the liver function index inspection can both not be tending towards normal from meeting.Belly tympanites, costa sternales dull pain all have disappearance.Take on an entirely new look to mental attitude from extremity are aching and limp, dispirited.
Embodiment 19: nephritis, the treatment of patients with renal cell carcinoma case are observed
Pueraria lobota, the man, 63 years old, patients with renal cell carcinoma, the right nephrectomy in 2008 has transparent cyst through looking into left kidney, postoperative is taken other medicine and is still felt the waist ache, after take the Pinus koraiensis extracting solution, every day 30CC; Massage at loin with the Pinus koraiensis extracting solution of 10 times of dilutions every day, adheres to that March is surplus, and face's edema disappears, and soreness of waist pain disappears, after the Shanghai examination in hospital finds that left cyst of kidney disappears, realizes that obviously sleep is good, and spirit is also much better.
Wear certain, the man, 43 years old, pale complexion, edema, soreness of waist look tired out, often owing to after flu and the upper respiratory tract infection, more dispirited, usually very hypologia, seeks medical advice in many ways, do not have too positive effect.Adhere to obeying the Pollen pini thunbergii extracting solution every day from December, 2007, in December, 2008, add drug matching again, existing sb.'s illness took a favorable turn, transference cure.Nephritis patient is tried 4 examples, after taking medicine, obtains some improvement and healing substantially.
Enemy, the man, 72 years old, nephritis patient, two limbs are to the following period of the day from 11 a.m. to 1 p.m of edema, waist can not freely be turned and be crooked, stair activity is with freely, the waist of sleeping evening, there is burning sensation at the back, cures and does not have positive effect in many ways, after the people makes referrals to here, get Pinus koraiensis extracting solution 15cc after I advise it regular meal and take for 2 times with the dilution of eliminating cold for resuscitation water, once use the oral 50cc of Chinese medicine carbonization extracting solution that makes by embodiment 2 methods evening every morning, adhere to obeying Pinus koraiensis extracting solution January, therapeutic effect very, the thorough cancellation of two limb edema, existing adhere to taking always 1 year surplus, the main suit is energetic, and the phenomenon of past alopecia has not had yet
Poplar, man 55 years old, patients with renal cell carcinoma, the right nephrectomy, postoperative 2 years, self-induction neurolysis, disease is also concurrent often, especially obviously respiratory tract infection is serious, makes referrals to here one examination through enemy, and I adopt the Pinus koraiensis extracting solution and the Chinese medicine carbonization extracting solution of enemy and use, oral dose increases to some extent, get for every and take after Pinus koraiensis extracting solution 30cc dilutes 2 times with warm water, once take Chinese medicine extraction liquid 80cc evening every morning, after adhering to taking, the situation of existing main suit respiratory tract infection has not had, and self-induction spirit is good, the existing clothes of pharynx always a year, conscious gastrointestinal function takes a turn for the better greatly, appetite increases, free movement of the bowels, and body weight has been increased to 54 kilograms from 51 kilograms in 2006.
Cold certain, man, 48 years old, the worker of law court makes a definite diagnosis nephritis patient through hospital, the face edema, two limb enlargements, usual soreness of waist and ache in legs is when at life's full flowering, but due to illness pain can't operate as normal, and is usually weak and weary through illness sleepy during working, and evening, insomnia was fidgety, in many ways seek medical advice and do not have too positive effect, after look for me, the medicine that I advise its hospital to open is normally taken, and is every and takes after increasing by 10 times of embodiment 1 Pinus sylvestnis var. mongolica Litv. extracting solution 10cc dilutions, self-induction clothes Pinus sylvestnis var. mongolica Litv. extracting solution is after three days, in high spirits, weak and weary through illness sleepy feeling do not had, and evening, sleep was also normally got up, memory function has also turned better, with surplus February as the method clothes pharynx, above symptom completely without, work energy for increasing.
Hao, Liu waits twenties nephritis cases, and several oral doses that exemplify more than I adopt difference are according to circumstances executed and are controlled, and the experimenter can both take effect as a result, and curative effect is very surprising, can cross 90%, and 10% all has improvement in addition.Embodiment 20: asthma, breast hydrops, pulmonary carcinoma case observed result
Permitted certain, the woman, 63 years old be pulmonary carcinoma after diagnosing, and hydrothorax has changed pulmonary carcinoma late period over to, and the uninterrupted dull pain of both sides of the chest is had a haggard face, and constipation is weak all over, neurolysis, sensation of oppression over the chest with shortness of breath, dizzy coughing and do not have expectorant.Come here to seek medical advice, medicinal new extraction method is extracted in reducing phlegm with relieving oedema or abdominal distension through diuresis or purgation, every meal 50CC pharynx clothes, after one hour, take 30CC Pinus koraiensis extracting solution, the morning and evening twice, took 6 days, can see that chest pain slightly disappears, expectorant expectoration smoothly, spirit is also shaken, and expand in the back, take after 10 days and can see the stool discharge, appetite increases to some extent.Now hold on and take readme: each is convenient than taking a turn for the better to some extent in the past
Answer certain, the man, 64 years old, there was asthma history in family, with regard to sensation of oppression over the chest with shortness of breath, coughed and did not have many diseases such as the concurrent vasculitis of expectorant when the sky cyclostrophic is cold, and early hair color is dry simple and unadorned, can not be engaged in work between more than ten years.Seek medical advice, see its pale complexion edema, the both legs edema of festering, voice are unable, and are very painful.Processing method: clearing away heat and cooling blood, the preventing phlegm from forming and stopping coughing medicine that extracts with Chinese medicine calcining flue gas condensing mixes oral with the Pinus koraiensis extracting solution, every morning 50CC, evening is single obeys pinaster extracting solution 15CC and dilutes 5 times, February of taking medicine is surplus, asthma stops, the expectorant of tussiculaing, and can do some matters in home.Adhere to the March of taking medicine, can work, and can carry FCL medicated beer continuously that gas is not breathed heavily with the mediocrity has not yet had difference, seemingly just as having become the individual with descending.Neighbour is surprised for it, and the elder brother who lives its next door also has serious asthma, but the elder brother is sick light more than him in the past, and present situation is different, and he sees younger brother's work of going to the field, and is very stunned, can't help speaking to oneself: the angle is really arranged? can the asthma of heredity also be cured?
The week certain, man, 63 years old, family's asthma history is arranged, and after 2003, asthma is seriously got up, I understand medical skill, adhering to taking 3 years Chinese medicine does not have improvement, and the back exchanges when practising medicine experience with it, and he has said sentence, the words of the difficult self-insurance of doctor, after ask about medical history, might as well make him drink an examination in conjunction with his soup side with the Pinus tabuliformis extracting solution, every morning taking medicine after meal drink 25CC, the medicine of eating soup again after one hour, adhered to so that effect had been come out one month, belly is little, waistline reduces 50mm, face's edema goes down, conscious taking a step easily, and strength is also long.
Embodiment 21: hyperlipidemia, hypertension, arteriosclerosis, apoplexy, diabetes, amnesia, senile dementia case observation
Shut out certain, the man, 63 years old, the retired worker, the first three years retirement endowment of going back home, it is dizzy to tidy up when cleaning the room prominent sense the same day, the right side numb limbs and tense tendons, used at that time adhere to 10 by the massage method surplus day, the state of an illness is alleviated to some extent.After half a year, palpitate quickly suddenly, facial scorching, movable then unfavorable, the right side limbs can't be movable, suddenly sends prescription on individual diagnosis to hospital, through CT examination, and right basal area cerebral infarction, after hospitalize, the state of an illness alleviates to some extent and leaves hospital.After leaving hospital, dull expression gradually, memory falls sharply, and is hypologia, do not like interchange, is disinclined to action, and lips are purple black sometimes, arrhythmia, prominent sense is cold from head to foot, and is invalid through seeking medical advice in many ways.Please I one the examination, see its symptom, open to search the Chinese medicine of wind by network, waking up the patient from unconsciousness by dissipating phlegm, brain healthy, extracting medicinal liquid with Chinese medicine calcining flue gas condensing then, mix oral March with the Pinus koraiensis extracting solution surplus, the state of an illness takes a favorable turn, the back continuation is drunk with 10 times of eliminating cold for resuscitation water dilutions with pinaster extracting solution 30CC every day, now can see its figure in the collective dance hall.
Hyperlipidemia, hypertension, arteriosclerosis, apoplexy, amnesia, diabetes, senile dementia is old commonly encountered diseases, and general according to observations retired worker belonged to the high-incidence season during this period of time at 60~63 years old, and this moment is mood agitation, speaking incoherently sometimes often.Becoming of having chattered, and what have is wordless, and memory goes down greatly, by conscientious careful observation and constantly clinical in 5 or six years, also obtains many experiences, and the patient looks for me to seek medical advice, and I always decline not open, but controls for their examination, but often receives special effect.So far tried thirties of examples, observe thirties examinations and control effect, all effective in cure.
Luo, the woman, 61 years old, diabetics, blood glucose were checked higher, disease sees dryness of the mouth and thirst and think drinking-water, and is scorching from head to foot, skin pruritus, it is hemorrhage that gingiva is often accompanied, the numb limbs and tense tendons twinge, pain in foot can not stair activity, and the doctor trained in Western medicine conventional treatments is used up, and does not have too obviously to change.The back listens the people to say that the pinaster extracting solution is effective in cure to diabetes.Take 2000CC Pinus koraiensis extracting solution to here away, advise it to dilute 5~10 times with eliminating cold for resuscitation water, drink after meal every day sooner or later, drinks 40CC every day, waits to finish off whole liquid, goes examination in hospital blood glucose, glucose in urine to fall at the end, more confident now having drunk.After together drink with drug matching again, effect is more obvious, gingiva does not have hemorrhage, skin does not have scratchiness yet, and the diabetes of seeking medical advice of initiatively calling now have 11 people, take the pinaster extracting solution and all take an evident turn for the better in various degree, the pinaster extracting solution has blood sugar lowering thus, glucose in urine special effect miscellaneous function.
Hu, woman, 65 years old, patient's obesity, blood fat raises, the chronic pathological changes of covering in the B ultrasonic prompting liver, hepatitis virus mark feminine gender in the blood, constipation is defecated once about three days often, just amount is few, the Duo Jia of hospital that seeks medical advice, the conditioning of soup prescription medicine, all do not have positive effect, after use the Pinus koraiensis extracting solution instead after, get 15~20 times of Pinus koraiensis extracting solution 20cc dilutions for every, every day three times, clothes Pinus koraiensis extracting solution a large amount of defecations that afternoon, the black sticky matter is more, and grease is bubbled through the water column, it is light to feel belly immediately in second day, adhere to taking the Pinus koraiensis extracting solution and have a surplus January, it is normal once a day to defecate, and lipid examination has also reduced, body weight subtracts following 6 kilograms, now adheres to taking always.
Lu, the man, 52 years old, the glycosuria patient, it mainly shows hydrouria usually, and the blood sugar concentration height always has hunger sensation, and thirsty need are constantly drunk water, about weight loss 2.5kg, fatigue and weak, lassitude.Execute the method for controlling: every adds in Pollen pini thunbergii extracting solution 3cc~6cc and the water when drinking water and drinks, by observe and can find the patient from every day more than 20 times number of micturitions be reduced to 16~18 times, drink the Pollen pini thunbergii extracting solution through constantly adhering to, the urine number of times gradually reduced in Zhejiang, the bimester of clothes Pollen pini thunbergii extracting solution after, blood sugar concentration reduces, voided volume reduces, and diet is tending towards normally, but after withdrawing the Pollen pini thunbergii extracting solution, diabetic symptom can occur again, so need adhere to taking for a long time.
Hu, the woman, 68 years old, diabetics, face swells, festering appears in whole body skin table, limbs fatigue sprays the affected part with the Pinus koraiensis extracting solution, ulcer spot incrustation as a result, the skin improvement that comes off, in order on method dosage drink, diabetes complicated symptom all has alleviation.
Lin, white horse with a black mane, the Wang, Huang, Cai waits 30 multidigit diabeticss, by on method drink the Pinus koraiensis extracting solution and can both observe above result substantially.
Embodiment 22: the treatment of prostatitis case is observed
Zhao, the man, 72 years old, often owing to just not making crotch always moist only, the back was surplus January with the treatment by Chinese herbs of Pinus koraiensis extracting solution compatibility for frequent micturition, urgent micturition, urine, and sb.'s illness took a favorable turn, do not have recurrence.
Wu, the man, 43 years old, hospital diagnosis was a prostatitis, the urine bifurcated.After take Pinus tabuliformis extracting solution and drug matching, sb.'s illness took a favorable turn, implements this situation case 12 examples, except that an example did not take effect, all the other all obtained curing rehabilitation.
Embodiment 23: alopecia person hair growth promoting treatment function is observed
Answer certain, the man, 64 years old, hair all turned white, after take the Pinus koraiensis extracting solution after 1 year, local hair begins by leucismus black, originally the alopecia phenomenon completely without.
The week certain, man, 64 years old, alopecia is serious, scalp is scratched where it itches, and as the Semen Glycines size, Pinus koraiensis extracting solution spraying and oral is adopted in the back through the long red and swollen pus point of common scalp, after more than ten day, alopecia stops, and falls part originally and restarts growth, and red and swollen pus point also disappears, such embodiment has more than 50, and it is the same substantially to be tried effect.
Embodiment 24: immunologic hypofunction, the observation of sub-health population
Yu, the woman, 26 years old, often flu, heatstroke, appetite is also more normal, does not have the other diseases symptom through examination in hospital, is diagnosed as immunologic hypofunction.Various health product medicines have been eaten to reach and have been had no result for two end of the year, and take for 10 times with Pollen pini thunbergii extracting solution 20cc dilution the back, twice pharynx clothes on an empty stomach sooner or later, adhere to 20 days after, sensory symptoms makes moderate progress, adhere to 1 year after, heatstroke now, flu have also been lacked, energy is also abundant.
Wu, the man 61 years old, reaches cough in 3 years because flu causes, treatment is had no result always, I went home to visit him in 2006, knew that its cough of speaking is continuous, asked its reason, my scheme of controlling of executing is proposed to him, Chinese medicine in original Chinese medicinal formulae is soaked into, adopt embodiment 2 carbonization collecting methods to concoct, mixed 1: 2 with the fish-scale floss extracting solution behind the collected medicinal liquid, get 1 times of mixed liquor 50cc dilution for every, every day three times, the result takes medicine and took effect the same day, and cough with asthma weakens, it is surplus January to adhere to obeying the fish-scale floss extracting solution, cough is thoroughly good, the appetite aspect than before increase, strength has also turned better.
Lin, the man, 60 years old, gold certain, the woman, 26 years old, the long-time cough of the total companion of the each flu of main suit just began to cough and has not had expectorant, continue after cough for a long time again, expectoration expectorant, yellow/dense.Because nose is obstructed always, often causes headache, work energy weakens the here of seeking medical advice greatly.Execute the method for controlling, use fish-scale floss and 1: 1 volume mixture of Pinus koraiensis extracting solution every day, get one times of mixed liquor 30cc dilution for every, every day, secondary was swallowed clothes after meal, behind the first quarter moon, disease goes 2/3rds, after pinaster extracting solution mixed liquor is reduced to every 15cc, take after diluting 5~10 times, adhere to obeying liquid about January, above transference cure.After 2 years, ask its situation, main suit flu is also few, has caught a cold also not and such long-time cough in the past.
Gold certain, Wu, twenties coughs such as Guo etc.s, the asthma history here of seeking medical advice out of admiration for a famous person, after the Pinus koraiensis extracting solution was obeyed in pharynx, the time was different in size, all receives excellent curative.Cure rate reaches 85%, the improver is arranged 13%, does not have obvious person 2%.
Sub-health population generally all is because think of labor is excessive, usual irregular eating, and all multifactor formation that cause such as life anxiety, disease is difficult to make a definite diagnosis, so often occur sudden death sometimes.Though subhealth state does not have the performance of serious symptom mechanism, affect people's life constantly.The pinaster extracting solution has often also played rare curative effect in sub-health population.Thirties bosses such as the manager who is now always drinking, storekeeper, readme: drink after the pinaster extracting solution, energetic, both legs do not have sensation of aching, and thinking is also clear, and diet also increases, and excretory function is also normal or the like, the consistent medicine of pinaster extracting solution for mystery that claim.
Embodiment 25: the Dealcoholic sobering-up function
Jiang, the man, 41 years old, the village head, village of living in and urban district border on, and treat with courtesy morely, be on the drink, after how drinking at every turn, always with in various degree vomiting, the headache phenomenon, the next morning the eyes edema.Once ask I whether have relieve the effect of alcohol, hangover medicine, I think a way for it the back, drink two times of Pollen pini thunbergii extracting solution 15CC of dilution before the wine, drink two times of Pollen pini thunbergii extracting solution 15CC of dilution after drinking, after this, after he uses this method, really efficacious, vomiting disappears, and the headache symptom does not have, eyes did not have the edema phenomenon in second day, and the mental status is better.
Lee, Cai, enemy, male's age is more than 35, person below 56 years old, 30 multidigits, occupation: president general manager, owner.It is excessive that labor is thought in work, treats with courtesy morely usually, and it is frequent to stay up late, and the ethanol intake is many, often feels mental fatigue, myasthenia of limbs.Go examination in hospital all to belong to normally, relief they to get Pollen pini thunbergii extracting solution 15CC dilution twice every day oral, sooner or later twice, take this liquid certainly after ten days, all self-induction appetite increases, legs and feet are strong, and are energetic, whenever symptoms such as the no headaches of drinking also.
Embodiment 26: acquired immune deficiency syndrome (AIDS), drug rehabilitation function are observed
Ma, man, 26 years old, Lee, the man 21 years old, shuts out certain, the man, 19 years old, the Shandong, 20 years old, because of coming in and going out, because of eating the K powder accidentally by mistake through the public place of entertainment, bar of being everlasting, after sucking several times, the addiction trend is arranged, when no K powder is sucked, normal feel feels run-down, rhinorrhea, and mind is dispirited, it is latent to hit suddenly cigarette-detoxifying, and four also have the drug rehabilitation idea, rent a house one, in television set is arranged, can divert oneself, get Pollen pini thunbergii extracting solution 20CC dilution every day and take for 20 times, behind the clothes, feel to have a strength after three days, after so adhering to taking one month, the mechanism phenomenon produced completely without taking drugs, health is done manual work outside and is subsisted so far, and U.S. happy full that the family that marries and gives birth to babies crosses arranged.
Zhao, poplar is waited 11 drug abuse patients, takes the Pinus koraiensis extracting solution, gets the 30cc dilution every day and takes for 10 times~20 times, and the result improves significantly after taking more, and particularly the rhinorrhea phenomenon reduces, and desire is given birth to the dead sense of desire and is disappeared.
Concrete name is not quite clear, 4 HIV sufferers of three men, one woman, the Pinus koraiensis that to extract by embodiment 2 methods by the go-between and Pollen pini thunbergii mixed extract and black thick liquid are taken away, listen the go-between to state, the patient controls for a long time and does not have the incrustation skin owing to concurrent epidermis ulcer, tongue part monilial infection, extremity fungal infection, and I advise it to be contained in the mouth with Pollen pini thunbergii and Pinus koraiensis mixed extract and spued in 3~5 minutes, every day 2~3 times, concrete number of times is grasped by the patient.Be applied in extremity ulcer part after 3~4 hours with the black thick liquid, with the sticking shape liquid of Warm Wash black removal, spray the affected part back and forth repeatedly with Pinus koraiensis and Pollen pini thunbergii mixed extract, the time spend 20 days after, the go-between gets it filled again and requires to use, and the return information curative effect is obvious, the skin of having formed a scab in several affected parts, the microbial point-like thing of tongue beads cancellation half, the patient also requires oral.Because acquired immune deficiency syndrome (AIDS), drug abuse patient privacy are strong, often need the third party to pass on sometimes, observation oral result is also treated after.
Pinaster extracting solution test clinical observation result of the present invention, overall conclusion is as follows:
1. remarkable to staphylococcus, escherichia coli, anthrax bacillus, sick frog isolate killing action, the sterilization effective percentage is all more than 99.999%.
2. the scratch of exocuticle skin, wound, animal sting wound, burn and scald, broken wound, ulcer are caused pyogenic infection, the external effect of curing the back preventing from scar is obvious.Virus to acquired immune deficiency syndrome (AIDS) and sudden communicate illness is killed inhibitory action, repairs useful cell, and the nutrition base of blocking virus strengthens immune function of human body.
3. the therapeutic effect that people's epidermis inflammation, vasculitis is had thorough healing rehabilitation.
4. to hyperlipidemia, hypertension, arteriosclerosis, apoplexy, amnesia, diabetes, senile dementia has the effect of blood sugar lowering, blood pressure, glucose in urine, vessel softening, reparation brain cell slow down aging.
5. drunk, burbulent wine, addicts there are hepatoprotective and transform oxious component in degraded ethanol and the drugs.
6. alopecia, immunologic hypofunction, sub-health population are had granulation promoting, promote the production of body fluid, reparative regeneration plays the effect of keeping fit.
7. esophageal carcinoma, gastric cancer, pulmonary carcinoma, hepatocarcinoma, cirrhotic ascites, renal carcinoma there are the nutrition base of killing or block cancerous cell, recover the function of useful cell regeneration reparation.
8. esophagitis, gastritis, pleuritis, enteritis, asthma, nephritis, hepatitis B are washed virus element clearly, diminish inflammation, play the effect of strengthening body resistance and dispelling evil.
The pinaster extracting solution has excellent curative at multiple disease.Analyze from above case, the pinaster extracting solution has potent infiltration sterilizing power, and porous acts on internal layer and kills.Antibacterial can't be bred, thereby played the effect of antiinflammatory removing the necrotic tissue.The formation of other diseases comes from basically that virus causes.Be that mainly intrinsic virus produces and extraneous virus is invaded.General intrinsic generation comes from the metabolic function disorder, and its nucleus produces great change, forms virus.Because the effect of virus, human body reflects the mechanism symptom at once, mainly shows each organ inflammation, is converted into tumor by inflammation, and tumor worsens and forms cancer.Extraneous virus is converged intrinsic viral results of interaction after invading human body, just shows sudden communicate illness, as Sa Si virus, and first type H2N2 virus.Acquired immune deficiency syndrome (AIDS) is from pathomechanism, and HIV is to CD 4 +The T cytosis, often these viruses have very strong replicability, so how cut off the replicability of virus? the first, kill surface virus and recessive extremely strong virus.Show that according to U.S.'s data after HIV all killed, the some time can be duplicated again and be produced virus.Data shows that HIV conceals in the intestines and stomach mucosa probably, and medicine is difficult to effect enters, and utilizes the pinaster extracting solution, has extremely strong infiltration killing efficiency, thoroughly kills HIV as accessory drugs.The second, to all disease observation of curative effect, may also have the nutrition base of blocking virus from the pinaster extracting solution, in case viral nutrition is cut off, virus just can't be survived and duplicate so.After there was not body in virus, the pinaster extracting solution can be brought into play extremely strong Memorability again and bring back to life function.The recovery of useful cell, physical mechanism gets up with regard to health.This also meets the theory of Chinese medical science heresy and goes just from the beginning reason.

Claims (18)

1. pinaster extracting solution is prepared by following method: burning pinaster (Pinus) phytoclasts, and expellant gas reclaims through condensation and obtains thick liquid; Thick liquid left standstill in hermetic container 3 months~5 years, removed upper strata grease and lower sediment, got middle level liquid distillation, got the distillate of 98~103 ℃ of fractions, purifiedly promptly got described pinaster extracting solution.
2. pinaster extracting solution as claimed in claim 1 is characterized in that the purification in the described preparation process is through activated carbon adsorption, filter paper filtering, gets filtrate.
3. the method for claim 1, it is characterized in that described method is as follows: the pinaster phytoclasts is placed hermetic container, with outside burning things which may cause a fire disaster hermetic container is heated to carbonization, expellant gas reclaims through condensation and obtains thick liquid, and thick liquid left standstill in hermetic container 3 months~5 years, remove upper strata grease and lower sediment, get middle level liquid distillation, get the distillate of 98~103 ℃ of fractions, through activated carbon adsorption, filter paper filtering, get filtrate, promptly get described pinaster extracting solution.
4. pinaster extracting solution as claimed in claim 1 is characterized in that described pinaster phytoclasts is from one of following or wherein two or more mixing: leaves, branch, bark, trunk, tree root, flower, cone.
5. pinaster extracting solution as claimed in claim 1 is characterized in that described pinaster is one of following or wherein two or more mixing: Pinus koraiensis, fish-scale floss, Pollen pini thunbergii, japanese black pine, Pinus tabuliformis, Pinus sylvestnis var. mongolica Litv..
6. the application of pinaster extracting solution as claimed in claim 1 in the medicine of preparation treatment epidermis injury of person.
7. application as claimed in claim 6 is characterized in that described epidermis injury for scalding, and burn is burnt, wound, the infectious suppuration or comedo.
8. pinaster extracting solution as claimed in claim 1 ends application in the addiction medicine in preparation drug rehabilitation.
9. the application of pinaster extracting solution as claimed in claim 1 in the vasculitic medicine of preparation treatment.
10. the application of pinaster extracting solution as claimed in claim 1 in the medicine of preparation treatment brain diseases.
11. the application of pinaster extracting solution as claimed in claim 1 in the medicine of preparation treatment respiratory tract disease.
12. the application of pinaster extracting solution as claimed in claim 1 in the medicine of preparation treatment kidney disease.
13. the application of pinaster extracting solution as claimed in claim 1 in the medicine of preparation treatment gastric disease.
14. the application of pinaster extracting solution as claimed in claim 1 in the medicine of vegetation treatment intestinal tract disease.
15. the application of pinaster extracting solution as claimed in claim 1 in the medicine of preparation treatment excretory system disease.
16. the application of pinaster extracting solution as claimed in claim 1 in the medicine of preparation treatment acquired immune deficiency syndrome (AIDS).
17. the application of pinaster extracting solution as claimed in claim 1 in the medicine of preparation treatment infectious disease.
18. the application of pinaster extracting solution as claimed in claim 1 in the medicine that the preparation treatment is relieved the effect of alcohol, sobered up.
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CN104557836A (en) * 2014-12-23 2015-04-29 内蒙古满洲里森诺生物科技有限公司 Method for extracting alcohol soluble substance from bark of mongolian pine
CN104644695A (en) * 2014-06-12 2015-05-27 唐泽光 Extraction method of Chinese herbal medicine
CN105602808A (en) * 2015-12-22 2016-05-25 内蒙古满洲里森诺生物科技有限公司 Pinus sylvestris bark extract beverage and preparation method thereof
CN107447501A (en) * 2017-07-26 2017-12-08 南通唐盛纺织有限公司 Antibacterial green finishing technique for fabric
CN108456105A (en) * 2018-02-26 2018-08-28 北京三聚绿能科技有限公司 A kind of pine charcoal base microbe soil conditioner and preparation method thereof
CN109893550A (en) * 2019-03-15 2019-06-18 吴江平 A kind of natural herb pine birch compound fluid and its application
CN110923077A (en) * 2019-11-21 2020-03-27 甘肃农业职业技术学院 Preparation method of pine phytoncide process soap
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CN104644695A (en) * 2014-06-12 2015-05-27 唐泽光 Extraction method of Chinese herbal medicine
CN104436981A (en) * 2014-12-10 2015-03-25 安吉莱达生物制品有限公司 Production process of exhaust-gas scrubbing solution
CN104557836A (en) * 2014-12-23 2015-04-29 内蒙古满洲里森诺生物科技有限公司 Method for extracting alcohol soluble substance from bark of mongolian pine
CN105602808A (en) * 2015-12-22 2016-05-25 内蒙古满洲里森诺生物科技有限公司 Pinus sylvestris bark extract beverage and preparation method thereof
CN107447501A (en) * 2017-07-26 2017-12-08 南通唐盛纺织有限公司 Antibacterial green finishing technique for fabric
CN108456105A (en) * 2018-02-26 2018-08-28 北京三聚绿能科技有限公司 A kind of pine charcoal base microbe soil conditioner and preparation method thereof
CN108456105B (en) * 2018-02-26 2021-02-05 北京三聚绿能科技有限公司 Pine charcoal-based microbial soil conditioner and preparation method thereof
CN109893550A (en) * 2019-03-15 2019-06-18 吴江平 A kind of natural herb pine birch compound fluid and its application
CN110923077A (en) * 2019-11-21 2020-03-27 甘肃农业职业技术学院 Preparation method of pine phytoncide process soap
CN111804277A (en) * 2020-07-23 2020-10-23 黄瑞要 Method for preparing charcoal activated carbon combustible gas bio-oil from crop straws

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