CN105602808A - Pinus sylvestris bark extract beverage and preparation method thereof - Google Patents
Pinus sylvestris bark extract beverage and preparation method thereof Download PDFInfo
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- CN105602808A CN105602808A CN201510961691.6A CN201510961691A CN105602808A CN 105602808 A CN105602808 A CN 105602808A CN 201510961691 A CN201510961691 A CN 201510961691A CN 105602808 A CN105602808 A CN 105602808A
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- extract
- bark
- mongolica
- pinus sylvestris
- preparation
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
- C12G3/00—Preparation of other alcoholic beverages
- C12G3/04—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
Abstract
The present invention relates to a pinus sylvestris bark extract beverage and a preparation method thereof. Aiming at the characteristics that pinus sylvestris bark extract contains a plurality of active ingredients but has high isolation and purification costs for a single ingredient and astringent taste unsuitable for direct consumption, the present invention provides an innovative beverage product by directly integrated usage of the pinus sylvestris bark extract.
Description
Technical field
The present invention relates to a kind of beverage forming based on pinus sylvestris var. mongolica bark extract and preparation method thereof.
Background technology
Research shows, in the alcohol soluble substance of pinus sylvestris var. mongolica bark with alcohol extract, contain flavones, OPC, polyphenol,The active ingredients such as organic acid, polysaccharide, glycoside, have anti-oxidant, anticancer, reduce cholesterol, protect the effects such as cardiovascular.But at present, pinus sylvestris var. mongolica bark is as important forestry accessory substance, and its resource utilization is lower.
Pinus sylvestris var. mongolica bark extract is new product, with respect to existing raw produce extracts such as () soybean, ginkgo leaves, advantage is to contain plurality of active ingredients simultaneously, inferior position is that the low and cost of purity that separates of the purification of single active ingredient is high.
Up to the present there is following limitation in the purposes of pinus sylvestris var. mongolica bark extract.
First, pinus sylvestris var. mongolica bark extract also, just as the raw material for effective component extracting, does not directly utilize camphor treeThe terminal consumption product of sub-Pine Bark---this to pinus sylvestris var. mongolica bark extract trim the feet to fit the shoes, long with short punchUsage, can not embody the characteristics and advantages of pinus sylvestris var. mongolica bark extract.
Secondly the bark extract, extracting using medium is at present all the meals as tablet form as the final products of raw materialFood supplementary, the beverage products of also directly not making with extract.
The above purposes limitation of pinus sylvestris var. mongolica bark extract is because following reason causes.
1) up to the present bark extract is all the raw material for health product, does not still directly utilize and makes beveragePrecedent.
2) pinus sylvestris var. mongolica bark extract has harsh flavor after mixing with water, thereby is not applied at present directly makeThe application of drink.
3) extraction process of existing pinus sylvestris var. mongolica bark extract is for avoiding active ingredient destroyed, in technical processThere is no the especially process of high-temperature sterilization of sterilizing, still, what food_beverage industry was the most frequently used and feasible is high-temperature sterilization. Meanwhile,Bark, as the plant product in exposed field, is inevitable with mushroom. Thereby, current pinus sylvestris var. mongolica bark extractCan only can not directly form end product as the raw material of further purification processing.
Summary of the invention
For pinus sylvestris var. mongolica bark extract there is plurality of active ingredients but single active ingredient separating-purifying cost is high and mouthfulThe pungent puckery feature that is unsuitable for directly drinking of taste, the present invention proposes a kind of drink of innovation of direct comprehensive utilization pinus sylvestris var. mongolica bark extractMaterial product.
A kind of pinus sylvestris var. mongolica bark extract beverage, is characterized in that, this beverage is mixed liquor, and its composition comprises water, tuneTaste composition and extract the extract obtaining with organic media or inorganic medium from pinus sylvestris var. mongolica bark.
A preparation method for pinus sylvestris var. mongolica bark extract beverage, its step comprises:
1) extract and obtain extract from pinus sylvestris var. mongolica bark with organic media or inorganic medium;
2) this extract and water, flavoring ingredients are mixed to get to mixed liquor, this mixed liquor is described beverage.
Wherein, described flavoring ingredients is suitable for drinking and improves taste. Pinus sylvestris var. mongolica bark extract has unpalatableHarsh flavor, is made beverage in order to be directly used in, and the present invention adds that flavoring ingredients improves taste so that it is suitable for directly thereinConnect and drink.
Wherein, described flavoring ingredients comprises tart flavour or smell of vinegar material. Pinus sylvestris var. mongolica bark extract has unpalatable pungent puckeryTaste, in order more to improve acidity, improvement and outstanding taste, can add tart flavour or smell of vinegar material. For example,, in this mixed liquorAlso can add plant citric acid or apple vinegar improves acidity and improves taste.
Wherein, described flavoring ingredients comprises sweet taste or glucide. Pinus sylvestris var. mongolica bark extract has unpalatable pungent puckeryTaste, in order to improve and outstanding taste, can add sweet taste or glucide. For example, in this mixed liquor, also can add plant sugarAssign to improve acidity and improve taste.
Wherein, this extract or this mixed liquor are through carrying out sterilization treatment.
Wherein, described sterilization treatment refers to high-temperature sterilization. Wherein, the temperature of described high-temperature sterilization is at least 100 DEG COr 110 DEG C or 120 DEG C. For example: in to the leaching process of bark, heat certain time length and extract sterilizing simultaneously, orIn the last filling operation of mixed liquor, carry out high-temperature sterilization.
In existing pinus sylvestris var. mongolica bark extraction and extract aftertreatment technology, all adopt not for preventing that extract is destroyedExceed the heat treated of the temperature of 60 degree, also do not adopt any special sterilization process especially to avoid high-temperature technology simultaneously. ButBe, bark extract is directly used in preparation of drinks by the present invention, and bark inevitably can be mixed with mushroom, thereby, thisBeverage products must adopt sterilizing. In food work beverage processing industry, the most frequently used and feasible sterilization process is high-temperature sterilization, butJust in time contrary with the technological requirement of current extraction bark active material. But our experimental data shows, with at least 100 DEG COr the temperature of 110 DEG C or 120 DEG C is by selecting suitable duration to carry out sterilizing, the overwhelming majority of the bark extract that can leave tree hasEffect composition is not destroyed. Thereby the present invention innovates and has adopted high-temperature sterilizing process to make it directly to use to bark extractProduce in beverage.
Wherein, described sterilization treatment can be also ultraviolet sterilization. For example, described concentrated powder is carried out to ultraviolet sterilization.
Wherein, described extract or mixed liquor also can or be removed PROCESS FOR TREATMENT plumbous or that remove arsenic through removal heavy metal. HaveBark in contain micro-lead and arsenic, can adopt the special technique of removing plumbous and arsenic to process for pursuing high-quality more.
Wherein, described organic media is alcohol or ethanolic solution, and described extract is alcohol soluble substance. Wherein, wineThe concentration of essence or ethanolic solution is 20%-100%.
Wherein, described inorganic medium is carbon dioxide or water, and medium adopts means of supercritical extraction while being carbon dioxide.
Wherein, extract and refer to from pinus sylvestris var. mongolica bark with organic media or inorganic medium: extract with organic media, or withInorganic medium extracts, or adopts organic media and inorganic medium to extract simultaneously.
Wherein, when described extract is concentrated powder, the quality accounting of concentrated powder in mixed liquor is 0.25%-15%,When described extract is concentrate, the quality accounting of concentrate in mixed liquor is 0.5%-30%.
Wherein, describedly from pinus sylvestris var. mongolica bark, extract and obtain extract and refer to organic media or inorganic medium: by camphor treePine bark mixes with medium, and bark active ingredient is dissolved in medium and forms fused liquid (or mixture), from fused liquid (or mixture)Middle removal medium obtains the extract that comprises active ingredient.
Wherein, describedly extract in the process that obtains extract and do not wrap from pinus sylvestris var. mongolica bark with organic media or inorganic mediumDraw together adsorption treatment process.
Wherein, describedly from pinus sylvestris var. mongolica bark, extract with organic media or inorganic medium the process that obtains extract and compriseOr do not comprise the technique of absorption or the technique of macroporous resin adsorption. Wherein, through absorbing process, benefit is main effectively one-tenthPoint purity can improve and part harmful components can be removed, shortcoming is that cost increases, output reduces, part active ingredient quiltLoss. If further improve the purity of indivedual active ingredient (as flavones and OPC), in this product preparation processAlso can adopt the technique of macroporous resin adsorption.
Wherein, describedly from pinus sylvestris var. mongolica bark, extract with organic media or inorganic medium the process that obtains extract and comprisePinus sylvestris var. mongolica bark particle is mixed with medium. Wherein, described pinus sylvestris var. mongolica bark particle can stir after mixing with medium. ItsIn, after mixing with medium, can also heat described pinus sylvestris var. mongolica bark particle. Wherein, described pinus sylvestris var. mongolica bark particle and JieMatter can also be carried out ultrasonic processing after mixing. Wherein, described pinus sylvestris var. mongolica bark particle can be placed and soak 2-24 after mixing with mediumHour, then can filter, filter residue, obtain filtrate. Wherein, described in, be filtered into multistage filtering. Wherein, described inFiltrate can also be carried out adsorption treatment through macroreticular resin, after absorption, becomes more highly purified filtrate again by medium recovery. Wherein,Described filtrate can concentrate and obtain concentrate. Wherein, in described concentration process, described medium by from filtrate remove fromAnd obtain concentrate. Wherein, described simmer down to single-action is concentrated. Wherein, described concentrate also can be dried and obtain concentrated powderEnd. Wherein, described be dried as spraying dry. Wherein, described extract is concentrate or concentrated powder.
Wherein, the described process of extracting the extract obtaining from pinus sylvestris var. mongolica bark can comprise with same media or differenceMore than twice or twice leaching process that medium carries out.
Wherein, described mixed liquor can also mix other family tree bark extract or plant extracts.
Wherein, the beverage that described mixed liquor forms is non-alcoholic drink or pick-me-up.
Brief description of the drawings
Accompanying drawing 1 is the preparation flow figure of embodiment 1
Detailed description of the invention
Embodiment 1
Pinus sylvestris var. mongolica bark is processed into the particle of 20~80 order sizes, it is 40%-80% that described particle is put into concentrationEthanolic solution in, after mixing, stir and be heated to 100 DEG C keep within 30 minutes, then stop above stir and heating, itsIn, can also carry out ultrasonic processing. Then, place and soak 12 hours, filter, filter residue, obtain filtrate. ItsIn, described in be filtered into multistage filtering. Then, described filtrate is carried out to the concentrated ethanol of removing of single-action and obtain concentrate. Then alsoCan spray to be dried to described concentrate and obtain concentrated powder. Finally, concentrate or concentrated powder and pure waterBe mixed to get mixed liquor with flavoring ingredients, this mixed liquor is described beverage, capable of direct drinking after filling.
Wherein, flavoring ingredients comprises tart flavour or smell of vinegar material and sweet taste or glucide simultaneously, forms sour-sweet taste.
Wherein, described filtrate can also be passed through or carry out adsorption treatment without macroreticular resin. Through absorbing process, goodPlace is that the purity of main active ingredient can improve and part harmful components can be removed, shortcoming is that cost increases, output reduces,Part active ingredient is lost.
Wherein, described extract or mixed liquor also can be through removing the PROCESS FOR TREATMENT of plumbous and arsenic. In some barks, contain micro-Lead and the arsenic of amount, can adopt the plumbous technique of special removal to process for pursuing more high-quality.
The product of this example is the sour-sweet flavor beverage without alcohol.
Embodiment 2
Pinus sylvestris var. mongolica bark is processed into the particle of 20~80 order sizes, described particle is thrown and keep 30 in 30 DEG CMore than minute, then adopt ethanolic solution to utilize carbon dioxide to carry out means of supercritical extraction as entrainer and obtain filtrate. Then, rightDescribed filtrate is carried out the concentrated concentrate that obtains of vacuum filtration single-action. Then can also spray to be dried to described concentrate and obtainConcentrated powder. Finally, be mixed to get mixed liquor concentrate or concentrated powder and pure water and flavoring ingredients, shouldMixed liquor is described beverage, capable of direct drinking after more than 100 DEG C high-temperature sterilization is also filling.
Wherein, flavoring ingredients comprises tart flavour or smell of vinegar material and sweet taste or glucide simultaneously, forms sour-sweet taste.
Wherein, described filtrate can also be passed through or carry out adsorption treatment without macroreticular resin. Through absorbing process, goodPlace is that the purity of main active ingredient can improve and part harmful components can be removed, shortcoming is that cost increases, output reduces,Part active ingredient is lost.
Wherein, described extract or mixed liquor also can be through removing the PROCESS FOR TREATMENT of plumbous and arsenic. In some barks, contain micro-Lead and the arsenic of amount, can adopt the plumbous technique of special removal to process for pursuing more high-quality.
Claims (10)
1. a pinus sylvestris var. mongolica bark extract beverage, is characterized in that, this beverage is mixed liquor, and its composition comprises water, flavoring ingredientsWith from pinus sylvestris var. mongolica bark, extract with organic media or inorganic medium the extract obtaining.
2. a preparation method for pinus sylvestris var. mongolica bark extract beverage, its step comprises:
1) extract and obtain extract from pinus sylvestris var. mongolica bark with organic media or inorganic medium;
2) this extract and water, flavoring ingredients are mixed to get to mixed liquor, this mixed liquor is described beverage.
3. beverage according to claim 1 and 2 or its preparation method, is characterized in that, described flavoring ingredients comprise tart flavour orSmell of vinegar material.
4. beverage according to claim 1 and 2 or its preparation method, is characterized in that, described flavoring ingredients comprise sweet taste orGlucide.
5. beverage according to claim 1 and 2 or its preparation method, is characterized in that, this extract or this mixed liquor processCarry out sterilization treatment, described sterilization treatment refers to high-temperature sterilization or ultraviolet sterilization or other sterilization process, wherein, describedThe temperature of high-temperature sterilization is at least 100 DEG C or 110 DEG C or 120 DEG C.
6. beverage according to claim 1 and 2 or its preparation method, is characterized in that, described extract or mixed liquor also canProcess removal heavy metal or the PROCESS FOR TREATMENT of removing lead or removing arsenic.
7. beverage according to claim 1 and 2 or its preparation method, is characterized in that, described organic media is alcohol or secondAlcoholic solution, described extract is alcohol soluble substance; Described inorganic medium is carbon dioxide or water, and medium is carbon dioxideShi Caiyong means of supercritical extraction.
8. beverage according to claim 1 and 2 or its preparation method, is characterized in that, when described extract is concentrated powder,The quality accounting of concentrated powder in mixed liquor is 0.25%-15%, and when described extract is concentrate, concentrate is at mixed liquorIn quality accounting be 0.5%-30%.
9. beverage according to claim 1 and 2 or its preparation method, is characterized in that, described with organic media or inorganic JieMatter is extracted and is obtained extract and refer to from pinus sylvestris var. mongolica bark: pinus sylvestris var. mongolica bark is mixed with medium, and bark active ingredient is dissolved inMedium forms fused liquid (or mixture), removes medium and obtain comprising carrying of active ingredient from fused liquid (or mixture)Get thing.
10. beverage according to claim 1 and 2 or its preparation method, is characterized in that, described with organic media or inorganic JieMatter is extracted technique or the macroporous resin adsorption that the process that obtains extract comprises or do not comprise absorption from pinus sylvestris var. mongolica barkTechnique.
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Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1081844A (en) * | 1992-04-02 | 1994-02-16 | 株式会社林原生物化学研究所 | Improve the method and the ingestible products thereof of pine extract taste preference |
CN102038721A (en) * | 2009-10-23 | 2011-05-04 | 吴江平 | Pinus extract and application thereof |
RU2012131943A (en) * | 2012-07-26 | 2014-02-10 | Общество с ограниченной ответственностью "МТК Айсберг" | SOFT DRINK "LANGWAY" |
CN104432063A (en) * | 2014-12-18 | 2015-03-25 | 北京康比特体育科技股份有限公司 | Composition for alleviating athletic fatigue and preparation method thereof |
-
2015
- 2015-12-22 CN CN201510961691.6A patent/CN105602808A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1081844A (en) * | 1992-04-02 | 1994-02-16 | 株式会社林原生物化学研究所 | Improve the method and the ingestible products thereof of pine extract taste preference |
CN102038721A (en) * | 2009-10-23 | 2011-05-04 | 吴江平 | Pinus extract and application thereof |
RU2012131943A (en) * | 2012-07-26 | 2014-02-10 | Общество с ограниченной ответственностью "МТК Айсберг" | SOFT DRINK "LANGWAY" |
CN104432063A (en) * | 2014-12-18 | 2015-03-25 | 北京康比特体育科技股份有限公司 | Composition for alleviating athletic fatigue and preparation method thereof |
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Application publication date: 20160525 |